CN105419985A - Cleaning agent and preparing method thereof - Google Patents
Cleaning agent and preparing method thereof Download PDFInfo
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- CN105419985A CN105419985A CN201511025876.2A CN201511025876A CN105419985A CN 105419985 A CN105419985 A CN 105419985A CN 201511025876 A CN201511025876 A CN 201511025876A CN 105419985 A CN105419985 A CN 105419985A
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- clean
- out system
- salt
- oyster shell
- shell whiting
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/46—Animal products
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/268—Carbohydrates or derivatives thereof
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Molecular Biology (AREA)
- Zoology (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Storage Of Fruits Or Vegetables (AREA)
Abstract
The invention provides a cleaning agent and a preparing method thereof. The cleaning agent is prepared from, by weight, 10-60 parts of salt, 10-70 parts of shell powder and 5-20 parts of a multifunctional auxiliary. The preparing method comprises the following steps that the multifunctional auxiliary is sprayed to the surface of the shell powder to be mixed after being dissolved with alcohol, then the salt is added into the shell powder to be mixed again, and after drying is carried out, the cleaning agent is obtained. According to the cleaning agent, raw material components are composed of natural substances, in the using process, pollution to the environment is avoided, and residues after washing do not harm the human body; moreover, in the aspect of the cleaning effect, the cleaning agent has a sterilizing effect, further has effects of removing pesticide residues, clearing dirt and retaining freshness, and the effect of the cleaning agent is further enriched and promoted.
Description
Technical field
The present invention relates to detergent applications, in particular to a kind of clean-out system and preparation method thereof.
Background technology
Along with the raising of industrialization degree, the fertile indiscriminate use of pesticide of various agriculture, the abuse of edible additive, cause the continuous outburst of bacterium on the food such as fruit, vegetables, Pesticide Residue, the orthobiosis of serious puzzlement human consumer, washes out safety, eating health, is the target of human consumer's unremitting pursue.
The main component of cleaning product existing on current market is tensio-active agent, although it can wash-out fruit, vegetable surface impurity, owing to being be made by chemical products, environmental pollution is comparatively large, and residue is also unfavorable to the health of people.In catering industry, it is more obvious that a large amount of above-mentioned harm using these surfactant wash products to bring shows.
In view of this, special proposition the present invention.
Summary of the invention
The first object of the present invention is to provide a kind of clean-out system.This clean-out system is prepared from by crude substance, and solve the environmental pollution that existing cleaning product in use causes comparatively large, residue is to the disadvantageous problem of HUMAN HEALTH.And, in clean-out system provided by the invention, by salt, oyster shell whiting and a certain amount of multifunctional assistant being combined, obtained clean-out system has sterilization, removes pesticide residue, removes dirt and fresh-keeping effect, enriches and improve effect of clean-out system further.
The second object of the present invention is to provide a kind of making method of described clean-out system, and the method is easy and simple to handle, salt, oyster shell whiting and multifunctional assistant fully can be mixed.
In order to realize above-mentioned purpose of the present invention, spy by the following technical solutions:
A kind of clean-out system, with parts by weight, the material component of described clean-out system comprises: salt 10-60 part, oyster shell whiting 10-70 part and multifunctional assistant 5-20 part.
In clean-out system provided by the invention, material component forms by crude substance, when being used for washing fruit, vegetables by this clean-out system, not only can not cause any pollution to environment, and the residue after washing also can not damage human body.
In clean-out system provided by the invention, salt in material component occupies indispensable status in daily life, not only edible, simultaneously can be a large amount of using in daily life, particularly can be used for washing fruit, vegetables, the even wound of people, there is good germicidal action, in all age for consumers in general widely use, but its effect is comparatively single.For this problem, the present invention is by being combined together salt and oyster shell whiting and a certain amount of multifunctional assistant, obtained clean-out system not only has the effect of sterilization, but also has removal pesticide residue, removing dirt and fresh-keeping effect, enriches and improve effect of clean-out system further.
Clean-out system provided by the invention not only may be used for the cleaning of fruit, vegetables, sterilization can be reached, go to remain, decontamination, fresh-keeping effect, also can be used for the cleaning of the food such as seafood, fresh meat, curing salted meat, the effect of sterilization, decontamination, elimination peculiar smell can be reached.
The consumption of each material component also has impact to the effect of clean-out system of the present invention, and in order to ensure effect of clean-out system, the Optimum (all with parts by weight) of each material component is salt 10-60 part, oyster shell whiting 10-70 part and multifunctional assistant 5-20 part.Preferably, the consumption of each material component is salt 20-40 part, oyster shell whiting 30-50 part and multifunctional assistant 15-20 part.
Preferably, the granularity of described oyster shell whiting is less than 5 μm.
In clean-out system provided by the invention, oyster shell whiting as one of main active component, its effect have two: one be oyster shell whiting as a kind of alkaline matter, the cellularstructure of harmful levels of pathogens can be destroyed, play effect of sterilization.Meanwhile, oyster shell whiting has larger surface-area, has larger adsorption, can also adsorb pesticide residue, the organic pollutent on the surface such as fruit, vegetables.Can play effect fully in order to ensure oyster shell whiting, in clean-out system provided by the invention, the granularity of oyster shell whiting used is defined as and is less than 5 μm.The oyster shell whiting of this globule size and salt and multifunctional assistant combine rear obtained clean-out system, in use, not only can be dissolved in the water rapidly, all kinds of residue and the dirt on the surfaces such as fruit, vegetables, seafood, meat product can also be adsorbed simultaneously significantly, play sterilization better, go effect that is residual and decontamination.
Preferably, the making method of described oyster shell whiting comprises the steps:
Shell is carried out weathering, high-temperature calcination process, hyperfine abrasive process, obtain oyster shell whiting.
Shell can remove the organic composition in shell after weathering, is conducive to follow-up obtained shell powder and forms unique sack cavity structure; The impurity in shell can be removed further by high-temperature calcination process, most importantly, by calcining in hot environment, the molecular structure framework of curable shell; After shell after high-temperature calcination is carried out hyperfine abrasive process, obtain granularity and meet all satisfactory oyster shell whiting with structure.
Further preferably, described shell is scallop or Octopus.
Adopt the oyster shell whiting that scallop or Octopus obtain as raw material, its pH can reach more than 13, as a kind of strong alkaline substance, has good clean effect.The more important thing is, easily form unique blister cavities molecular sieve three-dimensional arrangement, thus there is better adsorption effect, in use also more dissolving easily in water or in other solvent to all kinds of residual and dirt simultaneously.Wherein, the effect of the oyster shell whiting adopting the shell of Octopus to obtain is better than the oyster shell whiting adopting scallop obtained.
Further preferably, in described high-temperature calcination treatment step, the temperature of calcining is 1100-1300 DEG C.
By being calcined in 1100-1300 DEG C of hot environment by oyster shell whiting, the impurity of in shell more than 99.9% can be removed, and, after shell is calcined at 1100-1300 DEG C, unique blister cavities molecular sieve structure can be formed.
Can fully remove in order to ensure the organic composition in shell, preferably, the time of described weathering is 2-3.
Preferably, described multifunctional assistant comprises trehalose and D-wood sugar, and both mass ratioes are (3-4): (1-2).
Multifunctional assistant used in the present invention is that trehalose and D-wood sugar form according to specified proportion, with salt and oyster shell whiting combine rear obtained clean-out system not only can sterilization, remove pesticide residue, remove dirt, also there is fresh-keeping effect.
Preferably, described salt is that the sodium chloride content that non-sea salt obtains after decolouring mineral removal treatment is greater than 99%, and not containing the refined edible salt of iodine.
A making method for clean-out system provided by the invention, comprises the steps:
After being dissolved by multifunctional assistant alcohol, spray mixes to oyster shell whiting surface, after salt be added in oyster shell whiting again mix, namely obtain clean-out system after oven dry.
Making method provided by the invention is easy and simple to handle, salt, oyster shell whiting and multifunctional assistant fully can be mixed.
Compared with prior art, beneficial effect of the present invention is:
(1) material component of clean-out system provided by the invention forms by crude substance, when being used for washing fruit, vegetables by this clean-out system, not only can not cause any pollution to environment, and the residue after washing also can not damage human body.
(2) the present invention is by being combined together salt and oyster shell whiting and a certain amount of multifunctional assistant, obtained clean-out system not only has the effect of sterilization, but also there is removal pesticide residue, removing dirt and fresh-keeping effect, enrich and improve effect of clean-out system further, not only may be used for the cleaning of fruit, vegetables, also can be used for the cleaning of the food such as seafood, fresh meat, curing salted meat, purposes is more extensive.
(3) in clean-out system provided by the invention, 5 μm are less than by the granularity of oyster shell whiting being defined as, the oyster shell whiting of this globule size and salt and multifunctional assistant combine rear obtained clean-out system, in use, not only can be dissolved in the water rapidly, all kinds of residue and the dirt on the surfaces such as fruit, vegetables, seafood, meat product can also be adsorbed simultaneously significantly.
(4) in clean-out system provided by the invention, shell can remove the organic composition in shell after weathering, is conducive to follow-up obtained shell powder and forms unique sack cavity structure; The impurity in shell can be removed further by high-temperature calcination process, most importantly, by calcining in hot environment, the molecular structure framework of curable shell; After shell after high-temperature calcination is carried out hyperfine abrasive process, obtain granularity and meet all satisfactory oyster shell whiting with structure.
(5) the present invention is by adopting scallop or Octopus as the obtained oyster shell whiting of raw material, its pH can reach more than 13, as a kind of strong alkaline substance, there is good clean effect, and easily form unique blister cavities molecular sieve three-dimensional arrangement, thus there is better adsorption effect, in use also more dissolving easily in water or in other solvent to all kinds of residual and dirt simultaneously.
(6) the present invention is by calcining oyster shell whiting in 1100-1300 DEG C of hot environment, can remove the impurity of in shell more than 99.9%, and, after shell is calcined at 1100-1300 DEG C, unique blister cavities molecular sieve structure can be formed.
(7) multifunctional assistant that form according to specified proportion by adopting trehalose and D-wood sugar of the present invention, with salt and oyster shell whiting combine rear obtained clean-out system not only can sterilization, remove pesticide residue, removing dirt, also has fresh-keeping effect.
Embodiment
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but it will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting the scope of the invention.Unreceipted actual conditions person in embodiment, the condition of conveniently conditioned disjunction manufacturers suggestion is carried out.Agents useful for same or the unreceipted production firm person of instrument, be and can buy by commercially available the conventional products obtained.
Embodiment 1
Take food salt 1kg, oyster shell whiting 1kg, trehalose 0.25kg, D-wood sugar 0.25kg.
By take obtain salt, oyster shell whiting, trehalose and D-wood sugar mixing after, obtain powder cleaning salt.
Embodiment 2
Take food salt 2kg, oyster shell whiting 3kg, trehalose 1kg, D-wood sugar 1kg.
Preparation method is with embodiment 1.
Embodiment 3
Take food salt 6kg, oyster shell whiting 7kg, trehalose 1.5kg, D-wood sugar 0.5kg.
Wherein, the granularity of oyster shell whiting is less than 5 μm.
Making method comprises the steps:
By trehalose, D-wood sugar with 2kg raw spirit dissolve after spray to oyster shell whiting surface, after again salt is mixed with oyster shell whiting, namely obtain powder cleaning salt after oven dry.
Embodiment 4
Take food salt 4kg, oyster shell whiting 5kg, trehalose 0.9kg, D-wood sugar 0.6kg.
Wherein, the granularity of oyster shell whiting is less than 5 μm, and salt used is that the sodium chloride content that non-sea salt obtains after decolouring mineral removal treatment is greater than 99%, and not containing the refined edible salt of iodine.
Making method comprises the steps:
Get scallop shell, weathering carried out high-temperature calcination process after 3 years at 1100 DEG C, and the shell after high-temperature calcination is carried out hyperfine abrasive process, obtained the oyster shell whiting that granularity is less than 5 μm;
By trehalose, D-wood sugar with 1.5kg raw spirit dissolve after spray to oyster shell whiting surface, after again salt is mixed with oyster shell whiting, namely obtain powder cleaning salt after oven dry.
Embodiment 5
Take food salt 4kg, oyster shell whiting 3kg, trehalose 1.6kg, D-wood sugar 0.4kg.
Wherein, the granularity of oyster shell whiting is less than 5 μm, and salt used is that the sodium chloride content that non-sea salt obtains after decolouring mineral removal treatment is greater than 99%, and not containing the refined edible salt of iodine.
Making method comprises the steps:
Get Octopus shell, weathering carried out high-temperature calcination process after 2 years at 1300 DEG C, and the shell after high-temperature calcination is carried out hyperfine abrasive process, obtained the oyster shell whiting that granularity is less than 5 μm;
By trehalose, D-wood sugar with 2kg raw spirit dissolve after spray to oyster shell whiting surface, after again salt is mixed with oyster shell whiting, namely obtain powder cleaning salt after oven dry.
Embodiment 6
Get refining without iodine edible salt 5.5kg, oyster shell whiting 4kg, trehalose 0.4kg, D-wood sugar 0.1kg.Wherein, the granularity of oyster shell whiting is less than 5 μm, and salt used is that the sodium chloride content that non-sea salt obtains after decolouring mineral removal treatment is greater than 99%, and not containing the refined edible salt of iodine.
Making method comprises the steps:
Get Octopus shell, weathering carried out high-temperature calcination process after 2 years at 1300 DEG C, and the shell after high-temperature calcination is carried out hyperfine abrasive process, obtained the oyster shell whiting that granularity is less than 5 μm;
The deionized water adding 0.5kg after trehalose, the mixing of D-wood sugar is made slurry one, making slurry two by adding 1kg deionized water in oyster shell whiting, carrying out intimate mixing with edible salt again after slurry one and slurry two being mixed and making cleaning cream.
Use clean-out system provided by the invention carry out fruit, vegetables, seafood, fresh meat or butcher's meat cleaning time, using method is as follows: get clean-out system 0.1-0.5 part provided by the invention, add in 20 parts of clear water and stir, article to be cleaned are soaked in water completely, gently rub 2-3 time, article to be cleaned can be taken out after 5-10 minute, sterilization can be reached, remove pesticide residue, remove dirt and fresh-keeping effect.
Experimental example
In order to verify the result of use of clean-out system provided by the invention, the result of use of the result of use of clean-out system and following several comparative example also contrasts by the present invention.
Comparative example 1
The clean-out system of the one-component be only made up of salt.In use, get 0.5 part of this clean-out system and be dissolved in 20 parts of clear water, stir, article to be cleaned are soaked in water completely, gently rub 2-3 time, after 5-10 minute, article to be cleaned can be taken out.
Comparative example 2
The clean-out system of the one-component be only made up of oyster shell whiting.Using method is with comparative example 1.
Comparative example 3
The clean-out system be made up of salt 3kg and oyster shell whiting 4kg.Using method is with comparative example 1.
Comparative example 4
The clean-out system be made up of clear water.During use, article to be cleaned are soaked in water completely, gently rub 2-3 time, after 5-10 minute, article to be cleaned can be taken out.
In comparative example 2 and comparative example 3, the commercially available prod on market all bought by oyster shell whiting used.
Test 1
Before test, spray certain density bacterium liquid in advance respectively on green vegetables surface, in bacterium liquid, the content of various bacterium is in table 1.
Table 1 cleans the content of the various bacterium of front sample surfaces
Green vegetables sample is divided into 10 parts, adopts the clean-out system provided in embodiment 1-embodiment 6 and comparative example 1-comparative example 4 to clean respectively.Detect the content of the surperficial bacterial classification after every part of green vegetables sample clean after cleaning more respectively, its result is as shown in table 2.
Table 2 cleans the content of the various bacterium of rear sample surfaces
As can be seen from the comparing result of table 2, the clean-out system adopting the present invention to prepare effectively can remove the malignant bacteria on surface, and its Be very effective is better than comparative example.
And, because cleaning products of the present invention forms by crude substance, to environment and the equal fanout free region of human body, be the first-selection of health diet.
Test 2
Get the Chinese cabbage that market is bought, detect the content of wherein Cypermethrin, its detected result is as shown in table 3.
Table 3 cleans the content of Cypermethrin in front Chinese cabbage
| Cypermethrin content/ppb | |
| Initial value | 2800 |
| After 2 days | 1800 |
| After 4 days | 800 |
Cabbages leaves is divided into 10 parts, cleans with the clean-out system provided in embodiment 1-embodiment 6 and comparative example 1-comparative example 4 respectively.Detect the content of the Cypermethrin after every part of cabbages leaves cleaning after cleaning more respectively, its result such as table 4 shows.
Table 4 cleans the content of rear sample surfaces Cypermethrin
As can be seen from table 4 comparing result, the clean-out system adopting the present invention to prepare effectively can remove the pesticide residue on surface, and it is significantly better than comparative example.
Test 3
The fresh meat that market is bought or fishes and shrimps have certain bad smell, in order to verify the cleaning performance of clean-out system provided by the invention, by embodiment 1-embodiment 6 and comparative example 1-comparative example 4 respectively in order to clean fresh pork, detect its deodorizing effect respectively.Its Detection results is as shown in table 5.
Examination criteria:
Excellent: without any bad smell;
Good: without any obvious bad smell;
Difference: obvious bad smell can be smelt.
Table 5 deodorizing effect comparing result
| Deodorizing effect | |
| Embodiment 1 | Good |
| Embodiment 2 | Good |
| Embodiment 3 | Excellent |
| Embodiment 4 | Excellent |
| Embodiment 5 | Excellent |
| Embodiment 6 | Excellent |
| Comparative example 1 | Difference |
| Comparative example 2 | Difference |
| Comparative example 3 | Good |
| Comparative example 4 | Difference |
As can be seen from the detected result of table 5, the clean-out system adopting the present invention to prepare has good deodorizing effect, and it is significantly better than comparative example.
Although illustrate and describe the present invention with specific embodiment, however it will be appreciated that can to make when not deviating from the spirit and scope of the present invention many other change and amendment.Therefore, this means to comprise all such changes and modifications belonged in the scope of the invention in the following claims.
Claims (10)
1. a clean-out system, is characterized in that, with parts by weight, the material component of described clean-out system comprises:
Salt 10-60 part, oyster shell whiting 10-70 part and multifunctional assistant 5-20 part.
2. clean-out system according to claim 1, it is characterized in that, with parts by weight, the material component of described clean-out system comprises:
Salt 20-40 part, oyster shell whiting 30-50 part and multifunctional assistant 15-20 part.
3. clean-out system according to claim 1, it is characterized in that, the granularity of described oyster shell whiting is less than 5 μm.
4. clean-out system according to claim 3, it is characterized in that, the making method of described oyster shell whiting comprises the steps:
Shell is carried out weathering, high-temperature calcination process, hyperfine abrasive process, obtain oyster shell whiting.
5. clean-out system according to claim 4, it is characterized in that, described shell is scallop or Octopus.
6. clean-out system according to claim 5, it is characterized in that, in described high-temperature calcination treatment step, the temperature of calcining is 1100-1300 DEG C.
7. clean-out system according to claim 5, it is characterized in that, the time of described weathering is 2-3.
8. clean-out system according to claim 1, it is characterized in that, described multifunctional assistant comprises trehalose and D-wood sugar, and both mass ratioes are (3-4): (1-2).
9. clean-out system according to claim 1, is characterized in that, described salt is that the sodium chloride content that non-sea salt obtains after decolouring mineral removal treatment is greater than 99%, and not containing the refined edible salt of iodine.
10. the making method of clean-out system described in any one of claim 1-9, is characterized in that, comprise the steps:
After being dissolved by multifunctional assistant alcohol, spray mixes to oyster shell whiting surface, after salt be added in oyster shell whiting again mix, namely obtain clean-out system after oven dry.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511025876.2A CN105419985A (en) | 2015-12-30 | 2015-12-30 | Cleaning agent and preparing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511025876.2A CN105419985A (en) | 2015-12-30 | 2015-12-30 | Cleaning agent and preparing method thereof |
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| CN105419985A true CN105419985A (en) | 2016-03-23 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201511025876.2A Pending CN105419985A (en) | 2015-12-30 | 2015-12-30 | Cleaning agent and preparing method thereof |
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| CN (1) | CN105419985A (en) |
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| CN106085614A (en) * | 2016-06-20 | 2016-11-09 | 安徽强旺生物工程有限公司 | Fruit-vegetable clear desalinization of soil by flooding or leaching and preparation method thereof |
| CN107245382A (en) * | 2017-06-16 | 2017-10-13 | 中原工学院 | A kind of fruits and vegetables washing salt based on the potent removal residues of pesticides of the de- function double-unit system of suction |
| CN110205207A (en) * | 2019-05-09 | 2019-09-06 | 五邑大学 | A kind of fruits and vegetables cleaning agent based on shell and its preparation method and application method |
| CN115404132A (en) * | 2022-09-06 | 2022-11-29 | 洁美来(山东)生态科技有限公司 | Ecological detergent powder production method and ecological detergent powder |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106085614A (en) * | 2016-06-20 | 2016-11-09 | 安徽强旺生物工程有限公司 | Fruit-vegetable clear desalinization of soil by flooding or leaching and preparation method thereof |
| CN107245382A (en) * | 2017-06-16 | 2017-10-13 | 中原工学院 | A kind of fruits and vegetables washing salt based on the potent removal residues of pesticides of the de- function double-unit system of suction |
| CN110205207A (en) * | 2019-05-09 | 2019-09-06 | 五邑大学 | A kind of fruits and vegetables cleaning agent based on shell and its preparation method and application method |
| CN115404132A (en) * | 2022-09-06 | 2022-11-29 | 洁美来(山东)生态科技有限公司 | Ecological detergent powder production method and ecological detergent powder |
| CN115404132B (en) * | 2022-09-06 | 2023-07-21 | 洁美来(山东)生态科技有限公司 | Ecological cleaning powder raw material crushing device |
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