CN105419410A - Environment-friendly wallpaper coating composition and preparation method thereof - Google Patents
Environment-friendly wallpaper coating composition and preparation method thereof Download PDFInfo
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Abstract
The invention discloses an environment-friendly wallpaper coating composition. The environment-friendly wallpaper coating composition comprises, by mass parts, 0.4-0.6 part of methyl cellulose ether, 1.6-2.0 part of tapioca starch, 0.7-0.9 part of industrial salt, 61-72 part of calcium carbonate powder, 0.07-0.15 part of thixotropic lubricant, 9-12 part of talcum powder, 0.12-0.25 part of polyacrylamide, 0.1-5.5 part of dispersing agent, 0.5-1.5 part of antifoaming agent, 0.1-5.5 part of wetting agent, 0.3-0.6 part of preservative, 0.5-2.2 part of thickening agent, 5.3-7.5 part of titanium dioxide, 0.3-1.2 part of mildew preventive, 13-20 part of calcium phosphate, 10-13 part of deionized water and 0.5-1.2 part of PH modifier. A preparation method for preparing the environment-friendly wallpaper coating composition comprises the steps of adding deionized water into a reaction kettle first and adding the raw materials into the reaction kettle to heat, stir and grind the raw materials to obtain the wallpaper coating composition. The environment-friendly wallpaper coating composition has the advantages of being high in decorative performance, good in scrub resistance, good in water-proof performance, good in alkali resistance, high in contamination resistance and stain resistance and high in cohesion, antibacterial, antifungal, good in flame resistance and long in practical life, resistant to yellowing and convenient to construct and stable in storage. The environment-friendly wallpaper coating composition is simple in preparation technology and low in manufacturing cost.
Description
Technical field
The present invention relates to a kind of Environment-friendlywallpaper wallpaper coating composition and preparation method thereof.
Background technology
Along with improving constantly of living standards of the people, the class of apparatus for building, dress sulphur requires also more and more higher, and the use of wallpaper coating also increases thereupon, and formaldehyde is exactly wherein most important objectionable impurities.
The impact of formaldehyde on human body is mainly manifested in the aspects such as allotriosmia, stimulation, allergy, abnormal pulmonary function, dysfunction of liver and immunologic dysfunction, strong impulse effect is had to human body skin and mucous membrane, the protein coagulating sex change in cell can be made, suppress all cell functions, the low metering formaldehyde of Long Term Contact can cause chronic respiratory tract disease, causes nasopharyngeal carcinoma, colorectal carcinoma, the cancer of the brain, nuclear transgenation etc.Through WHO confirm, hang up one's hat formaldehyde 0.5ppm pollute reach half a year more than, easily suffer from the disease of leukemia, nasopharyngeal carcinoma and respiratory system, when the concentration of formaldehyde reaches 0.06 ~ 0.07 milligram/cubic metre in every cubic metres of air, will there is slight asthma in children.
Summary of the invention
The object of the invention is the technical scheme providing a kind of Environment-friendlywallpaper wallpaper coating composition and preparation method thereof for the deficiency existing for prior art, there is ornamental strong, good scrub resistance, water-fast with alkali resistance, high dirt resistance and spot-resistant, cohesive force is strong, antibacterial and mouldproof, good flame resistivity, there is practical life length, color inhibition simultaneously, easy construction, the advantages such as stable storing.
In order to solve the problems of the technologies described above, the present invention adopts following technical scheme:
A kind of Environment-friendlywallpaper wallpaper coating composition, is characterized in that comprising following mass parts: methyl cellulose ether 0.4 ~ 0.6, tapioca (flour) 1.6 ~ 2.0, Industrial Salt 0.7 ~ 0.9, dry powder 61 ~ 72, thixotropic lubricant 0.07 ~ 0.15, talcum powder 9 ~ 12, polyacrylamide 0.12 ~ 0.25, dispersion agent 0.1 ~ 5.5, defoamer 0.5 ~ 1.5, wetting agent 0.1 ~ 5.5, sanitas 0.3 ~ 0.6, thickening material 0.5 ~ 2.2, titanium dioxide 5.3 ~ 7.5, mould inhibitor 0.3 ~ 1.2, calcium phosphate 13 ~ 20, deionized water 10 ~ 13, PH conditioning agent 0.5 ~ 1.2.
Preferably, dispersion agent is poly-hydroxy acid sodium salt or poly-hydroxy acid ammonium salt, has larger impact to the package stability of wallpaper coating, improves the stability of composition.
Preferably, defoamer is the mixture of organosilicon and mineral oil.
Preferably, wetting agent is polyoxyethylene nonylphenol ether or alkylphenol polyoxyethylene.
Preferably, thickening material is one or more mixtures in Natvosol, PU thickening material or alkali swelling type thickening material, adding Natvosol, PU thickening material or alkali swelling type thickening material can make the usage quantity of other auxiliary agents in coating reduce, thus the cost of auxiliary agent in coating is reduced, and the cost reduced is used for polyacrylamide to improve the performance of coating, obtain the environment-friendly type wallpaper coating that water-dilutable can be stablized, flow leveling is good and film is smooth to the touch, contribute to the suspension of coating and prevent coating from occurring sagging phenomenon when brushing.
Preferably, mould inhibitor is one or more mixtures in dichlofluanid, Kathon, Top Form Wormer, and mould inhibitor effectively can improve the moisture protection of wallpaper coating, extends the work-ing life of wallpaper coating.
Preferably, Industrial Salt is sodium hydroxide.
Prepare the method for a kind of Environment-friendlywallpaper wallpaper coating composition described above, it is characterized in that comprising the steps:
(1) first deionized water is added in reactor, then methyl cellulose ether is added successively, Natvosol, tapioca (flour), defoamer, wetting agent and dispersion agent, stir with stirrer, control rotating speed and stir 3 ~ 5min under 350 ~ 550r/min condition, be uniformly mixed post-heating to 80 ~ 95 DEG C, the reacting by heating time is 5 ~ 8min, add Industrial Salt again, polyacrylamide and titanium dioxide, after adding, the rotating speed of stirrer is adjusted to 1250 ~ 1900r/min, churning time is 10 ~ 15min, carry out dispersion grinding to fineness with sand mill again and be less than 50 μm, mixing solutions is obtained after filtration,
(2) mixing solutions obtained above is stirred under rotating speed 300 ~ 500r/min condition, add dry powder, talcum powder and PH conditioning agent gradually, the pH value (this pH value scope is more conducive to the storage of coating) in 8.5 ± 0.5 scopes of adjustment mixing solutions, the viscosity of mixing solutions is adjusted to (25 ± 2) mPas (25 DEG C) with thickening material, sieve and add calcium phosphate in the backward solution obtained and stir, obtain slurry compound;
(3) in slurry compound obtained above, finally add thixotropic lubricant and calcium phosphate dispersed with stirring is even, then be less than 45 μm through shredder development fineness, then add after sanitas and mould inhibitor stir and obtain target wall paper coating composition.
The present invention, owing to have employed technique scheme, has following beneficial effect:
1, during construction to body of wall without dry wet requirement, odorlessness, pollution-free to indoor environment, to no skin irritation, cohesive strength is high, resistance to percussion, and manufacture craft is simple, dependable performance;
2, moisture resistancely to go mouldy lastingly, or not do not peel off, and not easily aging, good permeability, make VOC drop to Schwellenwert, make room have good indoor-outdoor air quality, for people's lives provide required a home from home;
3, easy to use, acid and alkali-resistance, durable in use, saving of labor, save time, fast drying, constantly can neutralize degraded with the obnoxious flavour in room air, reduce indoor formaldehyde content, reach the object purified air;
4, there is high dirt resistance and spot-resistant, good flame resistivity, also there is the characteristic of long service life, color inhibition simultaneously.
5, as functional type indoor wall wallpaper coating, there is the advantages such as device effect is good, easy construction.
Embodiment
A kind of Environment-friendlywallpaper wallpaper coating composition of the present invention, comprises following mass parts:
Methyl cellulose ether 0.4 ~ 0.6, tapioca (flour) 1.6 ~ 2.0, Industrial Salt 0.7 ~ 0.9, preferably, Industrial Salt is sodium hydroxide, dry powder 61 ~ 72, thixotropic lubricant 0.07 ~ 0.15, talcum powder 9 ~ 12, polyacrylamide 0.12 ~ 0.25, dispersion agent 0.1 ~ 5.5, preferably, dispersion agent is poly-hydroxy acid sodium salt or poly-hydroxy acid ammonium salt, larger impact is had on the package stability of wallpaper coating, improve the stability of composition, defoamer 0.5 ~ 1.5, preferably, defoamer is the mixture of organosilicon and mineral oil, wetting agent 0.1 ~ 5.5, preferably, wetting agent is polyoxyethylene nonylphenol ether or alkylphenol polyoxyethylene, sanitas 0.3 ~ 0.6, thickening material 0.5 ~ 2.2, preferably, thickening material is Natvosol, one or more mixtures in PU thickening material or alkali swelling type thickening material, add Natvosol, PU thickening material or alkali swelling type thickening material can make the usage quantity of other auxiliary agents in coating reduce, thus the cost of auxiliary agent in coating is reduced, and the cost reduced is used for polyacrylamide to improve the performance of coating, obtain water-dilutable can stablize, the environment-friendly type wallpaper coating that the good and film of flow leveling is smooth to the touch, contribute to the suspension of coating and prevent coating from occurring sagging phenomenon when brushing, titanium dioxide 5.3 ~ 7.5, mould inhibitor 0.3 ~ 1.2, preferably, mould inhibitor is dichlofluanid, Kathon, one or more mixtures in Top Form Wormer, mould inhibitor effectively can improve the moisture protection of wallpaper coating, extend the work-ing life of wallpaper coating, calcium phosphate 13 ~ 20, deionized water 10 ~ 13, PH conditioning agent 0.5 ~ 1.2.
Prepare the method for a kind of Environment-friendlywallpaper wallpaper coating composition described above, comprise the steps:
(1) first deionized water is added in reactor, then methyl cellulose ether is added successively, Natvosol, tapioca (flour), defoamer, wetting agent and dispersion agent, stir with stirrer, control rotating speed and stir 3 ~ 5min under 350 ~ 550r/min condition, be uniformly mixed post-heating to 80 ~ 95 DEG C, the reacting by heating time is 5 ~ 8min, add Industrial Salt again, polyacrylamide and titanium dioxide, after adding, the rotating speed of stirrer is adjusted to 1250 ~ 1900r/min, churning time is 10 ~ 15min, carry out dispersion grinding to fineness with sand mill again and be less than 50 μm, mixing solutions is obtained after filtration,
(2) mixing solutions obtained above is stirred under rotating speed 300 ~ 500r/min condition, add dry powder, talcum powder and PH conditioning agent gradually, the pH value (this pH value scope is more conducive to the storage of coating) in 8.5 ± 0.5 scopes of adjustment mixing solutions, the viscosity of mixing solutions is adjusted to (25 ± 2) mPas (25 DEG C) with thickening material, sieve and add calcium phosphate in the backward solution obtained and stir, obtain slurry compound;
(3) finally in slurry compound obtained above, thixotropic lubricant is added and calcium phosphate dispersed with stirring is even, 45 μm are less than again through shredder development fineness, then add after sanitas and mould inhibitor stir and obtain target wall paper coating composition, the performance of wallpaper paint composition is as shown in table 1.
The performance of table 1 wallpaper coating
Embodiment 1
A kind of Environment-friendlywallpaper wallpaper coating composition, comprise following mass parts: methyl cellulose ether 0.4, tapioca (flour) 1.6, Industrial Salt 0.7, preferably, Industrial Salt is sodium hydroxide, dry powder 61, thixotropic lubricant 0.07, talcum powder 9, polyacrylamide 0.12, dispersion agent 0.1, preferably, dispersion agent is poly-hydroxy acid sodium salt, larger impact is had on the package stability of wallpaper coating, improve the stability of composition, defoamer 0.5, preferably, defoamer is the mixture of organosilicon and mineral oil, wetting agent 0.1, preferably, wetting agent is polyoxyethylene nonylphenol ether, sanitas 0.3, thickening material 0.5, preferably, thickening material is Natvosol and PU thickening material, add Natvosol and PU thickening material can make the usage quantity of other auxiliary agents in coating reduce, thus the cost of auxiliary agent in coating is reduced, and the cost reduced is used for polyacrylamide to improve the performance of coating, obtain water-dilutable can stablize, the environment-friendly type wallpaper coating that the good and film of flow leveling is smooth to the touch, contribute to the suspension of coating and prevent coating from occurring sagging phenomenon when brushing, titanium dioxide 5.3, mould inhibitor 0.3, preferably, mould inhibitor is dichlofluanid, mould inhibitor effectively can improve the moisture protection of wallpaper coating, extend the work-ing life of wallpaper coating, calcium phosphate 13, deionized water 10, PH conditioning agent 0.5.
Prepare the method for a kind of Environment-friendlywallpaper wallpaper coating composition described above, comprise the steps:
(1) first deionized water is added in reactor, then methyl cellulose ether, Natvosol, tapioca (flour), defoamer, wetting agent and dispersion agent is added successively, stir with stirrer, control rotating speed and stir 3min under 350r/min condition, be uniformly mixed post-heating to 80 DEG C, the reacting by heating time is 5min, add Industrial Salt, polyacrylamide and titanium dioxide again, after adding, the rotating speed of stirrer is adjusted to 1250r/min, churning time is 10min, carry out dispersion grinding to fineness with sand mill again and be less than 50 μm, after filtration, obtain mixing solutions;
(2) mixing solutions obtained above is stirred under rotating speed 300r/min condition, add dry powder, talcum powder and PH conditioning agent gradually, the pH value of adjustment mixing solutions is in 8 (this pH value scope is more conducive to the storage of coating), the viscosity of mixing solutions is adjusted to (25 ± 2) mPas (25 DEG C) with thickening material, sieve and add calcium phosphate in the backward solution obtained and stir, obtain slurry compound;
(3) in slurry compound obtained above, finally add thixotropic lubricant and calcium phosphate dispersed with stirring is even, then be less than 45 μm through shredder development fineness, then add after sanitas and mould inhibitor stir and obtain target wall paper coating composition.
Embodiment 2
A kind of Environment-friendlywallpaper wallpaper coating composition, comprise following mass parts: methyl cellulose ether 0.6, tapioca (flour) 2.0, Industrial Salt 0.9, preferably, Industrial Salt is sodium hydroxide, dry powder 72, thixotropic lubricant 0.15, talcum powder 12, polyacrylamide 0.25, dispersion agent 5.5, preferably, dispersion agent is poly-hydroxy acid ammonium salt, larger impact is had on the package stability of wallpaper coating, improve the stability of composition, defoamer 1.5, preferably, defoamer is the mixture of organosilicon and mineral oil, wetting agent 5.5, preferably, wetting agent is alkylphenol polyoxyethylene, sanitas 0.6, thickening material 2.2, preferably, thickening material is Natvosol and alkali swelling type thickening material, add Natvosol and alkali swelling type thickening material can make the usage quantity of other auxiliary agents in coating reduce, thus the cost of auxiliary agent in coating is reduced, and the cost reduced is used for polyacrylamide to improve the performance of coating, obtain water-dilutable can stablize, the environment-friendly type wallpaper coating that the good and film of flow leveling is smooth to the touch, contribute to the suspension of coating and prevent coating from occurring sagging phenomenon when brushing, titanium dioxide 7.5, mould inhibitor 1.2, preferably, mould inhibitor is Kathon, mould inhibitor effectively can improve the moisture protection of wallpaper coating, extend the work-ing life of wallpaper coating, calcium phosphate 20, deionized water 13, PH conditioning agent 1.2.
Prepare the method for a kind of Environment-friendlywallpaper wallpaper coating composition described above, comprise the steps:
(1) first deionized water is added in reactor, then methyl cellulose ether, Natvosol, tapioca (flour), defoamer, wetting agent and dispersion agent is added successively, stir with stirrer, control rotating speed and stir 5min under 550r/min condition, be uniformly mixed post-heating to 95 DEG C, the reacting by heating time is 8min, add Industrial Salt, polyacrylamide and titanium dioxide again, after adding, the rotating speed of stirrer is adjusted to 1900r/min, churning time is 15min, carry out dispersion grinding to fineness with sand mill again and be less than 50 μm, after filtration, obtain mixing solutions;
(2) mixing solutions obtained above is stirred under rotating speed 500r/min condition, add dry powder, talcum powder and PH conditioning agent gradually, the pH value of adjustment mixing solutions is in 9 (this pH value scope is more conducive to the storage of coating), the viscosity of mixing solutions is adjusted to (25 ± 2) mPas (25 DEG C) with thickening material, sieve and add calcium phosphate in the backward solution obtained and stir, obtain slurry compound;
(3) in slurry compound obtained above, finally add thixotropic lubricant and calcium phosphate dispersed with stirring is even, then be less than 45 μm through shredder development fineness, then add after sanitas and mould inhibitor stir and obtain target wall paper coating composition.
Embodiment 3
A kind of Environment-friendlywallpaper wallpaper coating composition, comprise following mass parts: methyl cellulose ether 0.5, tapioca (flour) 1.8, Industrial Salt 0.8, preferably, Industrial Salt is sodium hydroxide, dry powder 67, thixotropic lubricant 0.1, talcum powder 10.5, polyacrylamide 0.19, dispersion agent 3.1, preferably, dispersion agent is poly-hydroxy acid sodium salt, larger impact is had on the package stability of wallpaper coating, improve the stability of composition, defoamer 1.0, preferably, defoamer is the mixture of organosilicon and mineral oil, wetting agent 3.1, preferably, wetting agent is polyoxyethylene nonylphenol ether, sanitas 0.45, thickening material 1.15, preferably, thickening material is PU thickening material and alkali swelling type thickening material, add PU thickening material and alkali swelling type thickening material can make the usage quantity of other auxiliary agents in coating reduce, thus the cost of auxiliary agent in coating is reduced, and the cost reduced is used for polyacrylamide to improve the performance of coating, obtain water-dilutable can stablize, the environment-friendly type wallpaper coating that the good and film of flow leveling is smooth to the touch, contribute to the suspension of coating and prevent coating from occurring sagging phenomenon when brushing, titanium dioxide 6.5, mould inhibitor 7.5, preferably, mould inhibitor is Top Form Wormer, mould inhibitor effectively can improve the moisture protection of wallpaper coating, extend the work-ing life of wallpaper coating, calcium phosphate 17, deionized water 12, PH conditioning agent 0.9.
Prepare the method for a kind of Environment-friendlywallpaper wallpaper coating composition described above, comprise the steps:
(1) first deionized water is added in reactor, then methyl cellulose ether, Natvosol, tapioca (flour), defoamer, wetting agent and dispersion agent is added successively, stir with stirrer, control rotating speed and stir 4min under 450r/min condition, be uniformly mixed post-heating to 90 DEG C, the reacting by heating time is 7min, add Industrial Salt, polyacrylamide and titanium dioxide again, after adding, the rotating speed of stirrer is adjusted to 1550r/min, churning time is 13min, carry out dispersion grinding to fineness with sand mill again and be less than 50 μm, after filtration, obtain mixing solutions;
(2) mixing solutions obtained above is stirred under rotating speed 400r/min condition, add dry powder, talcum powder and PH conditioning agent gradually, the pH value (this pH value scope is more conducive to the storage of coating) in 8 scopes of adjustment mixing solutions, the viscosity of mixing solutions is adjusted to (25 ± 2) mPas (25 DEG C) with thickening material, sieve and add calcium phosphate in the backward solution obtained and stir, obtain slurry compound;
(3) in slurry compound obtained above, finally add thixotropic lubricant and calcium phosphate dispersed with stirring is even, then be less than 45 μm through shredder development fineness, then add after sanitas and mould inhibitor stir and obtain target wall paper coating composition.
These are only specific embodiments of the invention, but technical characteristic of the present invention is not limited thereto.Any based on the present invention, for realizing substantially identical technique effect, done ground simple change, equivalent replacement or modification etc., be all covered by among protection scope of the present invention.
Claims (8)
1. an Environment-friendlywallpaper wallpaper coating composition, is characterized in that comprising following mass parts: methyl cellulose ether 0.4 ~ 0.6, tapioca (flour) 1.6 ~ 2.0, Industrial Salt 0.7 ~ 0.9, dry powder 61 ~ 72, thixotropic lubricant 0.07 ~ 0.15, talcum powder 9 ~ 12, polyacrylamide 0.12 ~ 0.25, dispersion agent 0.1 ~ 5.5, defoamer 0.5 ~ 1.5, wetting agent 0.1 ~ 5.5, sanitas 0.3 ~ 0.6, thickening material 0.5 ~ 2.2, titanium dioxide 5.3 ~ 7.5, mould inhibitor 0.3 ~ 1.2, calcium phosphate 13 ~ 20, deionized water 10 ~ 13, PH conditioning agent 0.5 ~ 1.2.
2. a kind of Environment-friendlywallpaper wallpaper coating composition according to claim 1, is characterized in that: described dispersion agent is poly-hydroxy acid sodium salt or poly-hydroxy acid ammonium salt.
3. a kind of Environment-friendlywallpaper wallpaper coating composition according to claim 1, is characterized in that: described defoamer is the mixture of organosilicon and mineral oil.
4. a kind of Environment-friendlywallpaper wallpaper coating composition according to claim 1, is characterized in that: described wetting agent is polyoxyethylene nonylphenol ether or alkylphenol polyoxyethylene.
5. a kind of Environment-friendlywallpaper wallpaper coating composition according to claim 1, is characterized in that: described thickening material is one or more mixtures in Natvosol, PU thickening material or alkali swelling type thickening material.
6. a kind of Environment-friendlywallpaper wallpaper coating composition according to claim 1, is characterized in that: described mould inhibitor is one or more mixtures in dichlofluanid, Kathon, Top Form Wormer.
7. a kind of Environment-friendlywallpaper wallpaper coating composition according to claim 1, is characterized in that: described Industrial Salt is sodium hydroxide.
8. prepare the method for a kind of Environment-friendlywallpaper wallpaper coating composition as claimed in claim 1, it is characterized in that comprising the steps:
(1) first described deionized water is added in reactor, then described methyl cellulose ether is added successively, described Natvosol, described tapioca (flour), described defoamer, described wetting agent and described dispersion agent, stir with stirrer, control rotating speed and stir 3 ~ 5min under 350 ~ 550r/min condition, be uniformly mixed post-heating to 80 ~ 95 DEG C, the reacting by heating time is 5 ~ 8min, add described Industrial Salt again, described polyacrylamide and described titanium dioxide, after adding, the rotating speed of stirrer is adjusted to 1250 ~ 1900r/min, churning time is 10 ~ 15min, carry out dispersion grinding to fineness with sand mill again and be less than 50 μm, mixing solutions is obtained after filtration,
(2) mixing solutions obtained above is stirred under rotating speed 300 ~ 500r/min condition, add described dry powder, described talcum powder and described PH conditioning agent gradually, adjust the pH value of described mixing solutions in 8.5 ± 0.5 scopes, the viscosity of described mixing solutions is adjusted to (25 ± 2) mPas (25 DEG C) with described thickening material, sieve and add described calcium phosphate in the backward solution obtained and stir, obtain slurry compound;
(3) finally in slurry compound obtained above, described thixotropic lubricant is added and described calcium phosphate dispersed with stirring is even, be less than 45 μm through shredder development fineness again, then add after described sanitas and described mould inhibitor stir and obtain target wall paper coating composition.
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