CN105399313A - Preparation method of quartz glass lens tube - Google Patents

Preparation method of quartz glass lens tube Download PDF

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Publication number
CN105399313A
CN105399313A CN201510848279.3A CN201510848279A CN105399313A CN 105399313 A CN105399313 A CN 105399313A CN 201510848279 A CN201510848279 A CN 201510848279A CN 105399313 A CN105399313 A CN 105399313A
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CN
China
Prior art keywords
preparation
shaping
tube
feed liquid
quartz
Prior art date
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Pending
Application number
CN201510848279.3A
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Chinese (zh)
Inventor
刘丽华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DONGHAI HUAYA LIGHTING EQUIPMENT CO LTD
Original Assignee
DONGHAI HUAYA LIGHTING EQUIPMENT CO LTD
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DONGHAI HUAYA LIGHTING EQUIPMENT CO LTD filed Critical DONGHAI HUAYA LIGHTING EQUIPMENT CO LTD
Priority to CN201510848279.3A priority Critical patent/CN105399313A/en
Publication of CN105399313A publication Critical patent/CN105399313A/en
Pending legal-status Critical Current

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Abstract

The invention provides a preparation method of a quartz glass lens tube. The preparation method includes the following steps that 1, a high-purity quartz raw material ranging from 60 to120 meshes in particle size is placed into a tungsten crucible of a continuous smelting furnace, wherein sio2 is larger than or equal to 99.999%; electrically-molten quartz material liquid is subjected to warm and heat sediment in the tungsten crucible at the temperature of 2200-250 DEG C, and after gas impurities and liquid impurities are discharged through an exhaust vent, the material liquid is formed; 3, a formed quartz tube is cut according to the required dimension of a pipe lens, and the quartz tube for the pipe lens is formed. The preparation method has the advantages that the high-voltage-resistant quartz tube is directly produced through a continuous smelting method, the raw material of the quartz raw material with the sio<2> being larger than or equal to 99.999% is adopted, the transparency of a produced product is improved, the high-voltage-resistance and high-temperature resistance of the product are enhanced, and the high-voltage resistance can be larger than or equal to 20.0 Mpa and 20 times that of ordinary glass; the continuous smelting method is adopted for one-step forming, and the preparation is convenient and easy to implement.

Description

A kind of preparation method of silica glass detector tube
Technical field
The present invention relates to illuminating product technical field, be specifically related to a kind of preparation method of silica glass detector tube.
Background technology
Current oil, chemical industry, chemical fibre, pharmacy, the industrial glass pipe visor of sewage disposal are the main accessories on industrial pipeline device.By glass visor, can observe the response situation of the flow medias such as liquid in pipeline, gas, steam at any time, supervision and supervision are produced, and avoid in process of production security incident occurring.Current pipeline viewing mirror mostly applied thickness is the simple glass pipe between 1-3mm, Φ 50-100mm, as pipeline viewing mirror window glass.But this kind of glass is high pressure resistant lower, hot sudden turn of events temperature < 60 DEG C, easily break and damage, reducing service efficiency, range of application is very limited simultaneously.
Summary of the invention
For solving the problems of the technologies described above, the present invention does further to improve to the method for producing above-mentioned Glass tubing and the steps include:
1) the high-purity quartz raw material (sio2 >=99.999%) of 60-120 order number is dropped in the crucible of continuous induction melting furnace depressed place;
2) through being energized the quartzy feed liquid of melting in the crucible of depressed place through the warm precipitation of 2200 DEG C, after venting hole Exhaust Gas impurity and liquid impurity, feed liquid is carried out shaping;
3) according to the requirement size of pipeline viewing mirror, the silica tube after shaping is cut, forms pipeline viewing mirror silica tube.
Be that the former that feed liquid flows through in continuous induction melting furnace carries out shaping by method shaping for feed liquid in described step (2).
Be that silica tube is pulled down through the tractor of variable frequency control the type of making by method shaping for silica tube in described step (2).
Be 380mm by the diameter of the former core bar in continuous induction melting furnace shaping for feed liquid in described step (2), the diameter of former material platform is 420mm.
Advantage: with the high pressure resistant silica tube of continuous smelting method direct production, be characterized in the starting material selecting quartz raw material sio2 >=99.999%, the product of production is not only enhanced the transparency, and enhances the high pressure resistant of product and resistance to elevated temperatures, high pressure resistant >=20.0Mpa is 20 times of simple glass; Continuous smelting method is one-step moulding, convenient and simple.
Embodiment
1) the high-purity quartz raw material (sio2 >=99.999%) of 60-120 order number is dropped in the crucible of continuous induction melting furnace depressed place;
2) through being energized the quartzy feed liquid of melting in the crucible of depressed place through the warm precipitation of 2200 DEG C, after venting hole Exhaust Gas impurity and liquid impurity, feed liquid is carried out shaping.
3) according to the requirement size of pipeline viewing mirror, the silica tube after shaping is cut, forms pipeline viewing mirror silica tube.
Embodiment:
Silica tube below in conjunction with production Φ 80mm is that example is described as follows:
1, the high-purity quartz raw material (sio2 >=99.999%) of 60-120 order number is dropped in the crucible of continuous induction melting furnace depressed place;
2, through being energized the quartzy feed liquid of melting in tungsten crucible through the warm precipitation of 2200 DEG C, after venting hole Exhaust Gas impurity and liquid impurity, feed liquid flows through former and carries out shaping, and the diameter of the former core bar in described continuous induction melting furnace is 380mm, and the diameter of former material platform is 420mm;
3, quartzy feed liquid directly through the shaping Φ 80mm of former, thickness be the silica tube of 8mm;
4, silica tube pulls down through the tractor of variable frequency control the type of making, and obtains the heavy caliber silica tube that Φ is 80mm;
5, according to the requirement size of pipeline viewing mirror, to the silica tube cutting between Ф 80mm, pipeline viewing mirror silica tube is formed.
Certainly, the foregoing is only the preferred embodiment of the present invention, protection scope of the present invention is not limited in above-mentioned embodiment, and every technical scheme belonging to the principle of the invention all belongs to protection scope of the present invention.For a person skilled in the art, some improvements and modifications of carrying out under the prerequisite not departing from principle of the present invention, these improvements and modifications also should be considered as protection scope of the present invention.

Claims (4)

1. a preparation method for silica glass detector tube, is characterized in that: its manufacturing step is as follows:
1) the high-purity quartz raw material (sio2 >=99.999%) of 60-120 order number is dropped in the crucible of continuous induction melting furnace depressed place;
2) through being energized the quartzy feed liquid of melting in the crucible of depressed place through the warm precipitation of 2200 DEG C of ∽ 2500 DEG C, after venting hole Exhaust Gas impurity and liquid impurity, feed liquid is carried out shaping;
3) according to the requirement size of pipeline viewing mirror, the silica tube after shaping is cut, forms pipeline viewing mirror silica tube.
2. the preparation method of silica glass detector tube according to claim 1, is characterized in that: be that the former that feed liquid flows through in continuous induction melting furnace carries out shaping by method shaping for feed liquid in its manufacturing step (2).
3. the preparation method of silica glass detector tube according to claim 1, is characterized in that: be that silica tube is pulled down through the tractor of variable frequency control the type of making by method shaping for silica tube in its manufacturing step (2).
4. the preparation method of silica glass detector tube according to claim 1, it is characterized in that: be 380mm ∽ 400mm by the diameter of the former core bar in continuous induction melting furnace shaping for feed liquid in its manufacturing step (2), the diameter of former material platform is 420 ∽ 435mm.
CN201510848279.3A 2015-11-26 2015-11-26 Preparation method of quartz glass lens tube Pending CN105399313A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510848279.3A CN105399313A (en) 2015-11-26 2015-11-26 Preparation method of quartz glass lens tube

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510848279.3A CN105399313A (en) 2015-11-26 2015-11-26 Preparation method of quartz glass lens tube

Publications (1)

Publication Number Publication Date
CN105399313A true CN105399313A (en) 2016-03-16

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510848279.3A Pending CN105399313A (en) 2015-11-26 2015-11-26 Preparation method of quartz glass lens tube

Country Status (1)

Country Link
CN (1) CN105399313A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112551532A (en) * 2020-12-03 2021-03-26 东海县奥兰石英科技有限公司 Process for removing impurities in quartz powder by continuous melting high-temperature thermal state method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112551532A (en) * 2020-12-03 2021-03-26 东海县奥兰石英科技有限公司 Process for removing impurities in quartz powder by continuous melting high-temperature thermal state method
CN112551532B (en) * 2020-12-03 2022-03-08 东海县奥兰石英科技有限公司 Process for removing impurities in quartz powder by continuous melting high-temperature thermal state method

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Application publication date: 20160316