CN105384535B - One special fertilizer for fruit trees formula and its production method - Google Patents

One special fertilizer for fruit trees formula and its production method Download PDF

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Publication number
CN105384535B
CN105384535B CN201510935124.3A CN201510935124A CN105384535B CN 105384535 B CN105384535 B CN 105384535B CN 201510935124 A CN201510935124 A CN 201510935124A CN 105384535 B CN105384535 B CN 105384535B
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fertilizer
parts
nitrate
chelated
weight
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CN105384535A (en
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赵鸿
赵鸿一
常瑞青
夏峰
王永旭
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Chifeng Herun Facility Vegetable Productivity Promotion Center Co Ltd
Chifeng Mengding Biotechnology Co Ltd
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Chifeng Herun Facility Vegetable Productivity Promotion Center Co Ltd
Chifeng Mengding Biotechnology Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

The present invention relates to a special fertilizer for fruit trees, including following components:Inorganic chemical fertilizer, crude oil humic acid, yellow potassium humate, amino acid primary liquid, rare earth, secondary nutrients, chelated microelements, fungicide, degeneration-resistant siliceous fertilizer.Fruit tree fertilizer provided by the invention can ensure that inorganic microelement is not lost in, and effectively sterilization contributes to plant growth.

Description

One special fertilizer for fruit trees formula and its production method
Technical field
The present invention relates to agriculture fields, more specifically, it relates to a special fertilizer for fruit trees formula and its production method.
Background technology
Fertilizer is to provide nutrient necessary to one or more kinds of plants, improves soil property, increases soil fertility A horizontal substance.One of material base of agricultural production.
To adapt to the needs of agricultural modernization development, chemical fertilizer produces in addition to continuing growing yield, just towards efficiently multiple Combination, and the fertile pipeline of fertilizer machinery, fortune, liquid manure sprinkling irrigation instrumentation direction is combined to develop.Liquefied ammonia, ammonium polyphosphate, polyphosphoric acid Potassium etc. becomes the main fertilizer variety greatly developed because having many advantages, such as that nutrient density is high or accessory ingredient is few.Many chemical fertilizer It also tends to that fluid fertilizer is made, and mixes trace-element fertilizer and pesticide wherein, become multi-effect compound fertilizer material, be convenient for The combination of pipeline transportation and fertilizer irrigation (sprinkling irrigation, trickle irrigation) has the advantages that saving of labor, water-saving and saves fertilizer.As industrialized agriculture is (as moulded Expect greenhouse etc.) development, vegetables, melon and fruit will gradually increase the demand of carbon dioxide fertilizer.But it applies in large quantities for a long time Chemical fertilizer often results in environmental pollution.In order to keep Agro-ecology to balance, organic fertilizer should be advocated and be used cooperatively with chemical fertilizer, so as to Meeting crop to avoiding soil property deterioration and environmental pollution while nutrient requirement.
The specific aim of fertilizer at this stage is not strong, the larger area of especially day and night temperature, applicability in middle highlands It is not strong.
Invention content
The purpose of the present invention:Be to provide a kind of preferable fruit-specific fertilizer material formula of the resistance for adverse circumstances and Its production method.
It is this that there is enhancing tree vigo(u)r, flower and fruit protecting, the novel humic acid water-soluble fertilizer for improving biennial bearing of fruits multi-efficiency, It is former containing middle and trace elements such as crude oil humic acid, yellow potassium humate, amino acid, rare earth and zinc, copper, iron, boron, calcium, magnesium etc. Material is by mass ratio as follows:
As preferred:The inorganic chemical fertilizer be urea, monoammonium phosphate, several mixtures of potassium nitrate, it is total according to fertilizer The component of the parts by weight of weight is configured to:
100~120 parts of urea;
80~100 parts of monoammonium phosphate;
50~80 parts of potassium nitrate.
As preferred:The secondary nutrients are the mixtures of calcium nitrate and magnesium nitrate, according to the weight of fertilizer total weight The component of amount part is configured to:
2~10 parts of calcium nitrate;
3~10 parts of magnesium nitrate.
As preferred:Chelated microelements are configured to according to the component of parts by weight:
The chelated microelements are chelated zinc (EDTA-Zn), chelating boron (EDTA-B), chelated iron (EDTA-Fe), chela One or more of molybdenum (EDTA-Mo), chelated copper (EDTA-Cu), Chelated Manganese (EDTA-Mn) mixture is closed, it is total according to fertilizer The component of the parts by weight of weight is configured to:
Preferably, plant growth regulator can be added, such as amine fresh fat pulvis (DA-6), butyric acid potassium pulvis, paclobutrazol One or more kinds of mixtures in pulvis, gibberellin pulvis.
As preferred:The degeneration-resistant siliceous fertilizer is the ammonium hydroxide for the ethyl orthosilicate that diatomite absorbs.
Preferably, degeneration-resistant nutrient growth particle can be added, such as brassin lactones pulvis.
The fungicide is
The production method of one special fertilizer for fruit trees,
(1) inorganic chemical fertilizer mixture is prepared
By urea, monoammonium phosphate, potassium nitrate co-grinding in proportion, inorganic chemical fertilizer mixing is made after stirring evenly Object, it is spare;
(2) preparation of degeneration-resistant siliceous fertilizer:By weight, diatom is added by the molten addition to ammonium hydroxide of ethyl orthosilicate first Stone absorbs the ammonia spirit of ethyl orthosilicate, spare.
(3) by inorganic chemical fertilizer, fungicide, chelated microelements, degeneration-resistant siliceous fertilizer, rare earth, secondary nutrients, ammonia Base acid stoste, yellow potassium humate, crude oil humic acid are through crushing plus water mixes thoroughly dissolving, barrelling, and the special Water soluble fertilizer of fruit tree is made Material.
After being added to inorganic fertilizer, chelated microelements are in addition also added, this is just due in inorganic fertilizer In, the nutriment for providing plant growth mainly exists with ionic forms, but plant is not easy to absorb this part ion state Trace element, meanwhile, under rainwater or natural conditions, the trace element in inorganic fertilizer is also easier to be lost in, stability Difference.By the way that chelate trace element is added, plant itself is relatively strong to the absorbability of chelate, also, chelate is because of it Nutriment needed for plant is locked to intramolecular by characteristic by chemical bond, and which reduces the losses of nutrient.
Present agricultural rare-earth element is based on lanthanum (La), cerium (Ce) the two elements, including a small amount of praseodymium (Pr), neodymium (Nd), A kind of inorganic salts or organic salt of light rare earth, usually nitrate [R (NO3)2] mixture.Its effect is being capable of rare earth energy Leaf growth is effectively facilitated, Ye Chong, leaf area and leaf thickness obviously increase, and can significantly improve chlorophyll content in leaf blades, and enhancing is photosynthetic Make, also there is preferable promotion growth simultaneously for plant root, and heavy metal in soil content can be reduced, especially There is effect outstanding on for plant stress-resistance effect.Output of the fruit tree is improved, pollution suddenly is reduced.
Electedly, it is used degeneration-resistant, brassin lactones can be selected, preferable degeneration-resistant effect can be played, improve product Matter improves yield, and beautiful in colour, blade is more thick and solid.In addition, degeneration-resistant siliceous fertilizer is also added with, wherein degeneration-resistant siliceous fertilizer is inhaled for diatomite The ammonium hydroxide of the ethyl orthosilicate of receipts, ethyl orthosilicate is a kind of preferable siliceous fertilizer of degeneration-resistant effect, but it is particularly easy to hydrolyze, Under the system of ammonium hydroxide, the generation of its hydrolysis can be reduced, while by diatomaceous absorption, due to diatomite and positive silicic acid The system of ethyl ester is close, contains gap again in diatomite, therefore ethyl orthosilicate can be adsorbed on because of the principle of its similar compatibility In diatomite, after being in application in soil, can slow release when playing the role of long effectively avoid during application Unnecessary loss, needs the later stage to be applied again, the advantages of having reached siliceous fertilizer long action time.
The present invention in crude oil humic acid, yellow potassium humate, rare earth, amino acid and zinc, copper, iron, boron, calcium, magnesium etc., it is micro Element is base-material, and the biological regulator needed for science compound botanical and degeneration-resistant nutrient growth particulate material are closed using chelating technology At.After fruit tree is for applying bar, spreading manuer in holes, rush and apply, fruit tree cortex or root is promoted directly to absorb, rapid conduction enhances photosynthesis, Absorption of the fruit tree to various nutrients is balanced, keeps root system, blade, the growth of strain body vigorous, promotes prematurity, precocity fruiting.It is anti-to early spring The guarantors such as jelly, anti-corrosion, arid flower, fruit retention significant effect repeatedly apply bar, spread manuer in holes, rushs to apply and can expand fruit rapidly, hyperchromic, the nothing of derusting Symptom.Effectively prevent the yellow leaf of fruit tree, leaflet, burn day, the generation and harm of dehiscent fruit, bitter acne, deformity, rot disease, improves fruit tree Biennial bearing improves the fruit ratio of first-grade products, increases production 25%-40% or more.
Feature with the following functions:
1, activity is high, quick permeation, plays quick Healing to fruit-tree grafting wound, enhances photosynthesis, improves fruit tree production The hardness of amount and fruit, storage tolerance.
2, viscosity is moderate, and permanent resistance of rainwater washing against, fertilizer efficiency period are long after smearing.
3, deep to take root, better resistance, enhance growing way, repellent insect pest.
4, top dressing can be replaced, it is at low cost, improve utilization rate of fertilizer.
5, swollen fruit is fast, quality is excellent, increases wax colouring, purification fruit face, and the market competitiveness is strong.
The fertilizer has the characteristics that use easy, efficient simultaneously, and the fertilizer is smearable from fruit tree bud to harvest time, converts 1-3 times of water stirs evenly, and smears 50-80 centimeters of fruit tree height one week, 20-30 days primary.
The invention of the Novel fruit-tree dedicated fertilizer matching method and its production technology, it is efficient for north cold area fruit tree Safety in production provides a kind of novel effective green fertilizer.
Embodiment
Below by embodiment, the invention will be further described.It should be understood that the method for the embodiment of the present invention It is only used for illustrating the present invention, rather than limiting the invention, to preparation side of the invention under the concept thereof of the present invention The simple modifications of method belong to the scope of protection of present invention.All raw materials and solvent used in embodiment are purchased from Sigma Biochemical and Organic Compounds for Research and Diagnostic Clinical Reagents companies, compound of formula H are purchased from Shanghai Yaoming Kangde New Medicine Development Co., Ltd.
Compound of formula I prepares embodiment:
20 milliliters of 0.3 mM of Formula II compound and isopropanol are added in 50 milliliters of round-bottomed flasks, 0.35 mmoles are added That quinazoline isothiocyanates, back flow reaction, TLC tracking reactions place room temperature after reaction, and decompression boils off solvent, column layer Analysis separation (petroleum ether: ethyl acetate=10: 3, volume ratio;Silica gel 200-300 mesh), the compound of formula I of white solid is obtained, is received Rate 85%.
Structural Identification:1HNMR(DMSO-d6):δ (ppm), 11.32 (s, 1H, NH), 10.40 (s, 1H, NH), 9.74 (s, 1H, CH), 9.36 (s, 1H, CH), 8.70 (s, 2H, CH), 7.99 (d, H, CH), 7.90 (d, H, CH), 7.80 (t, 4H, CH), 7.72 (m, 1H, CH), 7.67 (m, 4H, CH)
The activity experiment of compound of formula I:
Activity experiment 1:The PPAR δ activity for the compound of the present invention indicated by Formulas I is confirmed by transfecting detection.In addition, It also tests for the selectivity of PPAR hypotype PPAR α and PPAR γ.Test cell toxicity is detected by MTT, passes through animal Experimental study activity in vivo.
CV-1 cells are used in this detection.By the cell inoculation to containing (non-specific added with 10%FBS, DBS Property cow's serum, through degreasing) and 1% penicillin/streptomycin DMEM 96 orifice plates in, and in 37 DEG C, 5%CO2Incubator in Culture.Experiment is carried out according to inoculation, transfection, sample administration and the step of confirmation.Specifically, by CV-1 cell inoculations to 96 holes Plate (5000 cells/wells), transfects after 24 hours.It can be confirmed by overall length PPAR Plasmid DNA, due to uciferase activity The active reporter dnas of PPAR provide beta galactosidase DNA and transfection reagent in relation to transfection efficiency information for transfecting.It will Sample is dissolved in dimethyl sulfoxide (DMSO), is administered to it in cell with various concentration by medium.It cultivates in the incubator After cell 24 hours, cell cracking is made by using lysis buffer.Uciferase activity is measured using photometer and microplate reader And betagalactosidase activity.Use the value for the luciferase that the value amendment of beta galactosidase obtains.It is drawn using these values Figure, and calculate EC50
Compound hPPARδ hPPARα hPPARγ
I 2.2nM ia ia
It can be seen that the compound of the present invention for PPAR δ have it is highly selective.
Execute the cytotoxicity that MTT detections are the compounds indicated by formula (I) in order to test the present invention.MTT is dissolved in The yellow substance of water, but the insoluble crystalline substance of purple can be become by the dehydrogenase in mitochondria when it is introduced into living cells Body.It can confirm cytotoxicity by measuring OD550 after MTT is dissolved in dimethyl sulfoxide.Experiment is following to be carried out.
By CV-1 cell inoculations in 96 orifice plates (5000 cells/wells).In 37 DEG C, 5%CO2Incubator in cultivate institute It states cell 24 hours, and the sample of various concentration is applied to it.Then, again by the cell culture 24 hours, add thereto Enter MTT reagents.After culture 15 minutes, the purple crystals of generation are dissolved in dimethyl sulfoxide.Optical density is measured using microplate reader, with Confirm cytotoxicity.
As a result, the compound indicated by formula (I) is identified does not have cytotoxicity for PPAR, even if a concentration of at its EC50Value 100 times~1000 times when it is also such.
Activity experiment 2:
Reagent agent:25Kg compound of formula I, 3.8kg fatty alcohol polyoxyethylene ether, 6kg sodium alkyl benzene sulfonates, 6kg isopropyls Alcohol, 4kg dimethylformamides, water complement to 100kg.
Various composition is mixed, shearing to active ingredient grain size is less than 3 μm in cutting kettle.The effect of emulsifier It is when it is dispersed in the surface of dispersate, forming film or electric double layer can make dispersed phase carry charge, can prevent dispersed phase Droplet condense mutually.Isopropanol, dimethylbenzene then must can effectively merge missible oil and water, keep its stability.
For studying object:Apple, kind Fuji apple.
Experimental field:Experiment selection is in Zibo City of the Shandong Province Yiyuan County townshiies Zhong Zhuan, and soil property is yellow soil, and fertilizer and water management is consistent, Apple tree growing way is uniformly neat, the age of tree 12 years, experimental field natural occurrence.
Experimental design:Experiment sets a chemicals treatment district altogether.Handle A:Above-mentioned compound of formula I lotion;Handle B:Clear water blank Control.
It using random alignment between district's groups, is repeated 4 times, amounts to 15 cells, 8 plants of apple tree investigation are taken per cell, it is entire to try Test 120 plants of apple of investigation.
Spraying time, number and method:When the orchard spring tip takes out the hair phase, to apple progress first time spray, dispenser is using storage Battery sprayer constant sprays, and medicine liquid spray is uniformly thoughtful, spouting liquid 20ml/800m2.Interval sprays 1 time for 7 days, applies 3 altogether It is secondary.
Disease investigation method:Investigation takes at random every time, per 10 tips of cell, investigates blade incidence, calculates the state of an illness and refers to Number and preventive effect.
Downy mildew blade stage division:
0 grade:Blade disease-free spot;
1 grade:Blade has 1~2 scab;
3 grades:Blade has 3~5 scabs;
5 grades:Blade has 6~8 scabs;
7 grades:Scab 8 or more, area accounts for 1/2 page or less;
9 grades:The connected area of scab accounts for 1/2 page or more.
Drug effect calculation formula:
Disease index=[∑ (the morbidity numbers at different levels × disease series)/investigation
Sum × highest series] × 100
Relative control effect (%)=(the one treatment region state of an illness of check plot disease index
Index)/check plot disease index × 100
Primary investigation data are after processing, for statistical analysis according to Deng Kenshi difference analysis methods using SAS softwares.
As a result with analysis:
Fertilizer prepares embodiment:
(1) inorganic chemical fertilizer mixture is prepared
According to corresponding parts by weight by urea, monoammonium phosphate, potassium nitrate co-grinding in proportion, nothing is made after stirring evenly Chemical machine fertiliser mixtures, for use;
(2) preparation of degeneration-resistant siliceous fertilizer:By weight, first by the ammonium hydroxide of the molten addition of 100 parts of ethyl orthosilicates to 300 parts In, 200 parts of kieselguhr is being added, the ammonia spirit of ethyl orthosilicate is being absorbed, it is spare.
It (3) will be by inorganic chemical fertilizer, plant growth regulator pulvis, chelated microelements, degeneration-resistant nutrient growth grain Sub, degeneration-resistant siliceous fertilizer, rare earth, amino acid primary liquid, yellow potassium humate, crude oil humic acid are through crushing plus water mixes thoroughly dissolving, dress Bucket, is made fruit tree Water-soluble fertilizer special.
The fertilizer has the characteristics that use easy, efficient simultaneously, and the fertilizer is smearable from fruit tree bud to harvest time, converts 1-3 times of water stirs evenly, and smears 50-80 centimeters of fruit tree height one week, 20-30 days primary.
Composite bio-fertilizer of the present invention is made by the above method.
By taking Fuji apple as an example, apply the fertilizer configured in following embodiments in soil per acre, and planting environment is in Inner Mongol Highlands in Gu, day and night temperature carry out Fuji apple's plantation at 10~15 DEG C, and to it, are compared:
Table 1:Embodiment matches fertilizer components according to parts by weight
Table 2:Comparative example is matched to fertilizer components according to parts by weight and (compound of formula I is not added)
Fertilizer components title Embodiment one Embodiment two Embodiment three
Urea 100 120 110
Monoammonium phosphate 100 90 80
Potassium nitrate 70 50 80
Crude oil humic acid 300 400 500
Yellow potassium humate 300 200 100
Amino acid primary liquid 70 50 100
Lanthanum nitrate 2 2 2
Calcium nitrate 5 8 10
Magnesium nitrate 10 8 5
Chelated Manganese 1 3 5
Chelate boron 4.5 3 1
Chelated iron 0.15 1 2
Chelate molybdenum 0.1 0.08 0.05
Chelated copper 0.08 0.5 0.8
Chelated zinc 0.8 0.5 0.05
Degeneration-resistant siliceous fertilizer 3 3 3
Axial root system length after 7 days 5cm 6cm 6cm
Plant height after 30 days 20cm 25cm 15cm
Plant stem thickness after 30 days 2.0cm 2.0cm 1.0cm
Ripening fruits counterpoise 180g 165g 100g
Apple marssonina leaf spot incidence (%) 48 51 45
It can be obtained by above-mentioned test data, by using the fertilizer of the preparation of the present invention, plant seedlings can be promoted Growth, have simultaneously for process fruit and preferably expand effect, and planted in the case of environment rather harsh, There can be preferable anti-adversity.

Claims (6)

1. a kind of Formulas I compound represented, with following representations:
2. a special fertilizer for fruit trees formula, is configured to according to the component of parts by weight:
The fungicide is compound of formula I described in claim 1:
The wherein described inorganic chemical fertilizer is one or more of urea, monoammonium phosphate, potassium nitrate, according to fertilizer total weight The component of parts by weight is configured to:
100~120 parts of urea;
80~100 parts of monoammonium phosphate;
50~80 parts of potassium nitrate;
The degeneration-resistant siliceous fertilizer is the ammonium hydroxide for the ethyl orthosilicate that diatomite absorbs.
3. fertilizer formula according to claim 2, it is characterised in that the secondary nutrients are calcium nitrate and magnesium nitrate Mixture, be configured to according to the component of the parts by weight of fertilizer total weight:
2~10 parts of calcium nitrate;
3~10 parts of magnesium nitrate.
4. fertilizer formula according to claim 2, it is characterised in that the chelated microelements are chelated zinc, chelating One or more of boron, chelated iron, chelating molybdenum, chelated copper, Chelated Manganese mixture, according to the group of the parts by weight of fertilizer total weight Divide and is configured to:
5. fertilizer formula according to claim 2, it is characterised in that the rare earth is one kind in lanthanum nitrate and cerous nitrate Or it is several.
6. according to the production method of any special fertilizer for fruit trees of claim 2 to 5, it is characterised in that:
(1) inorganic chemical fertilizer mixture is prepared
By urea, monoammonium phosphate, potassium nitrate co-grinding in proportion, inorganic chemical fertilizer mixture is made after stirring evenly, it is standby With;
(2) preparation of degeneration-resistant siliceous fertilizer:By weight, kieselguhr is added by the molten addition to ammonium hydroxide of ethyl orthosilicate first, it is right The ammonia spirit of ethyl orthosilicate is absorbed, spare;
(3) by inorganic chemical fertilizer, fungicide, chelated microelements, degeneration-resistant siliceous fertilizer, rare earth, secondary nutrients, amino acid Stoste, yellow potassium humate, crude oil humic acid are through crushing plus water mixes thoroughly dissolving, barrelling, and fruit tree Water-soluble fertilizer special is made.
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CN1651358A (en) * 2004-02-08 2005-08-10 吴永常 Beneficial trace element enriched multi element leaf surface fertilizer
CN101096326A (en) * 2006-06-28 2008-01-02 吴嫦华 Organic silicon leaf fertilizer and preparation method thereof
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