CN105353067B - 一种用于测定茶叶中农药残留量的方法 - Google Patents
一种用于测定茶叶中农药残留量的方法 Download PDFInfo
- Publication number
- CN105353067B CN105353067B CN201510824933.7A CN201510824933A CN105353067B CN 105353067 B CN105353067 B CN 105353067B CN 201510824933 A CN201510824933 A CN 201510824933A CN 105353067 B CN105353067 B CN 105353067B
- Authority
- CN
- China
- Prior art keywords
- stirring rod
- cellulose
- ene coatings
- triazole
- polymer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
编号 | 农药种类 | 保留时间/min | 定性离子 |
1 | 多效唑 | 6.78 | 236 |
2 | 抑芽唑 | 6.98 | 206 |
3 | 己唑醇 | 7.80 | 214 |
4 | 烯效唑 | 8.93 | 236 |
5 | 腈菌唑 | 14.05 | 179 |
6 | 氟硅唑 | 15.99 | 233 |
7 | 丙环唑 | 17.68 | 259 |
8 | 三唑酮 | 18.04 | 208 |
9 | 戊唑醇 | 21.61 | 250 |
10 | 糠菌唑 | 23.99 | 173 |
11 | 苯醚甲环唑 | 26.23 | 323 |
12 | 烯唑醇 | 27.01 | 268 |
13 | 硅氟唑 | 27.89 | 276 |
14 | 卞氯三唑醇 | 31.41 | 292 |
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510824933.7A CN105353067B (zh) | 2015-11-23 | 2015-11-23 | 一种用于测定茶叶中农药残留量的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510824933.7A CN105353067B (zh) | 2015-11-23 | 2015-11-23 | 一种用于测定茶叶中农药残留量的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105353067A CN105353067A (zh) | 2016-02-24 |
CN105353067B true CN105353067B (zh) | 2017-05-03 |
Family
ID=55329071
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510824933.7A Active CN105353067B (zh) | 2015-11-23 | 2015-11-23 | 一种用于测定茶叶中农药残留量的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN105353067B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113075317A (zh) * | 2021-03-24 | 2021-07-06 | 日照市市场监管检验检测中心 | 一种茶叶中赤霉素含量的检测方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4268269A (en) * | 1979-09-04 | 1981-05-19 | The Sherwin-Williams Company | Field test method for estimation of concentration of organic materials in water |
JP2006242825A (ja) * | 2005-03-04 | 2006-09-14 | Nippon Meat Packers Inc | 残留農薬の抽出方法及び抽出キット |
CN102735784A (zh) * | 2011-04-11 | 2012-10-17 | 中国科学院长春应用化学研究所 | 一种超高效液相色谱-串联四级杆质谱同时测定中药中100种农药残留的方法 |
CN104897805A (zh) * | 2015-05-14 | 2015-09-09 | 成都中医药大学 | 一种快速检测植物中药材中多效唑残留量的方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AP2013007168A0 (en) * | 2011-03-15 | 2013-10-31 | Peerless Worldwide Llc | Facile synthesis of graphene, graphene derivativesand abrasive nanoparticles and their various uses , including as tribolofically-beneficial lubricantadditives |
-
2015
- 2015-11-23 CN CN201510824933.7A patent/CN105353067B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4268269A (en) * | 1979-09-04 | 1981-05-19 | The Sherwin-Williams Company | Field test method for estimation of concentration of organic materials in water |
JP2006242825A (ja) * | 2005-03-04 | 2006-09-14 | Nippon Meat Packers Inc | 残留農薬の抽出方法及び抽出キット |
CN101166965A (zh) * | 2005-03-04 | 2008-04-23 | 日本肉类批发商株式会社 | 残留农药的萃取方法和萃取试剂盒 |
CN102735784A (zh) * | 2011-04-11 | 2012-10-17 | 中国科学院长春应用化学研究所 | 一种超高效液相色谱-串联四级杆质谱同时测定中药中100种农药残留的方法 |
CN104897805A (zh) * | 2015-05-14 | 2015-09-09 | 成都中医药大学 | 一种快速检测植物中药材中多效唑残留量的方法 |
Non-Patent Citations (5)
Title |
---|
Preparation of Cellulose/Graphene Composite and Its Applications for Triazine Pesticides Adsorption from Water;Che Zhang等;《ACS Sustainable Chemistry & Engineering》;20150130;第3卷(第3期);396-405 * |
Residues of trifloxystrobin and tebuconazole in/on tomato(Lycopersicon esculantum Mill.) and soil;Thomas George 等;《Pesticide Research Journal》;20130630;第25卷(第1期);18-23 * |
崔淑华 等.大葱及草莓中49种杀菌剂残留量的气相色谱-质谱法测定.《分析测试学报》.2012,第31卷(第12期),24-28. * |
李家威.分子印迹搅拌棒的研制及其在农药残留分析中的应用.《万方学位论文数据库》.2010,15,21,36-37,61-91. * |
苏建峰 等.气相色谱 - 质谱法与气相色谱法测定茶叶及茶叶加工品中 295 种农药多残留.《分析测试学报》.2015,第34卷(第6期),625-638. * |
Also Published As
Publication number | Publication date |
---|---|
CN105353067A (zh) | 2016-02-24 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Caldas et al. | A vortex-assisted MSPD method for the extraction of pesticide residues from fish liver and crab hepatopancreas with determination by GC–MS | |
Lu et al. | Simultaneous determination of pyrethrins residues in teas by ultra-performance liquid chromatography/tandem mass spectrometry | |
CN103323547B (zh) | 分析烟草及烟草制品中有机氯、菊酯类和二硝基苯胺类农药残留的gc-ms/ms方法 | |
CN105277640B (zh) | 一种用于测定茶叶中农药残留量的方法 | |
CN105241981B (zh) | 一种用于测定茶叶中农药残留量的方法 | |
CN101166965A (zh) | 残留农药的萃取方法和萃取试剂盒 | |
Nan et al. | Novel and rapid method for determination of organophosphorus pesticide residues in edible fungus using direct gas purge microsyringe extraction coupled on-line with gas chromatography–mass spectrometry | |
Chatzimitakos et al. | Magnetic graphene oxide as a convenient nanosorbent to streamline matrix solid-phase dispersion towards the extraction of pesticides from vegetables and their determination by GC–MS | |
Chen et al. | Determination and dissipation of afidopyropen and its metabolite in wheat and soil using QuEChERS–UHPLC–MS/MS | |
Baba et al. | Chromatographic separation of arsenic species with pentafluorophenyl column and application to rice | |
Zhao et al. | Rapid determination of organonitrogen, organophosphorus and carbamate pesticides in tea by ultrahigh-performance liquid chromatography–tandem mass spectrometry (UPLC-MS/MS) | |
CN105334277A (zh) | 用于葡萄酒农残分析的快速前处理方法及检测方法 | |
Prestes et al. | Comparison of several extraction procedures for the determination of biopesticides in soil samples by ultrahigh pressure LC‐MS/MS | |
Luo et al. | Determination, residue and risk assessment of trifloxystrobin, trifloxystrobin acid and tebuconazole in Chinese rice consumption | |
CN107664670A (zh) | 玉米中种菌唑残留的超高效液相色谱‑串联质谱检测方法 | |
CN105353067B (zh) | 一种用于测定茶叶中农药残留量的方法 | |
Chen et al. | Simultaneous analysis of multiple pesticide residues in tobacco by magnetic carbon composite-based QuEChERS method and liquid chromatography coupled to quadrupole time-of-flight mass spectrometry | |
Sun et al. | Residual level of dimethachlon in rice‐paddy field system and cooked rice determined by gas chromatography with electron capture detector | |
Yu et al. | Residue behavior and safety evaluation of pymetrozine in tea | |
Amaral et al. | Evaluation of sample preparation procedures and krypton as an interference standard probe for arsenic speciation by HPLC-ICP-QMS | |
Doran et al. | Simultaneous determination of niclosamide and its degradates in water by LC-MS/MS | |
CN107687966A (zh) | 盐酸吗啉胍纯度标准物质及其制备方法与应用 | |
CN105277645B (zh) | 一种用于测定茶叶中农药残留量的方法 | |
Shi et al. | Dissipation of oxaziclomefone residues from rice, soil, and paddy field water using carbon nanotube-based QuEChERS and HPLC-MS analysis | |
CN102353740A (zh) | 一种同步测定三唑类手性农药对映体含量的方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
CB03 | Change of inventor or designer information |
Inventor after: He Yusong Inventor before: Yuan Xiaolin |
|
CB03 | Change of inventor or designer information | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20170329 Address after: 523000 Dongcheng District City, Dongguan province old cattle Wai Wai Village Industrial Zone Applicant after: He Yusong Address before: 523000 Dongcheng District City, Dongguan province old cattle Wai Wai Village Industrial Zone Applicant before: Yuan Xiaolin |
|
TA01 | Transfer of patent application right | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20181219 Address after: 437300 Fifteen Company of Chibi Yanglou Dong Teahouse, Xianning City, Hubei Province Patentee after: HUBEI CHIBI ZHAO LIQIAO TEA INDUSTRY CO., LTD. Address before: 523000 Industrial Zone of Niushan Laowui Village, Dongcheng District, Dongguan City, Guangdong Province Patentee before: He Yusong |
|
TR01 | Transfer of patent right |