CN105350093B - A kind of negative pressure array centrifuges pneumoelectric device for spinning - Google Patents
A kind of negative pressure array centrifuges pneumoelectric device for spinning Download PDFInfo
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- CN105350093B CN105350093B CN201510778785.XA CN201510778785A CN105350093B CN 105350093 B CN105350093 B CN 105350093B CN 201510778785 A CN201510778785 A CN 201510778785A CN 105350093 B CN105350093 B CN 105350093B
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- negative pressure
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Abstract
The invention discloses a kind of negative pressure array to centrifuge pneumoelectric device for spinning, including high-voltage alternating generator, feeder, babinet, centrifugal energy nozzle, centrifuge driving mechanism and negative pressure reception device, there is liquid storage cylinder inside centrifugal energy nozzle, centrifugal energy nozzle is equipped with wire vent pore, negative pressure reception device includes collector, negative tube and negative pressure generator, negative tube forms the negative pressure mouth of pipe in the bottom of babinet, collector is nested in the negative pressure mouth of pipe, negative pressure reception device sets multiple, and annular array is arranged in centered on centrifugal energy nozzle, high-voltage alternating generator, which is formed, to be used to produce electric field, feeder forms the air-flow sprayed by wire vent pore.The polymer that air-flow, electric field, negative pressure and centrifugal force make to eject forms nanofiber, nanofiber deposits in negative pressure reception device becomes three-dimensional structure, improve the thickness of fiber deposition, it is more preferable to the compatibility of biomaterial, the material of technique is applied widely, and the supporting structure of acquisition is more advantageous to the cell growth in organizational project.
Description
Technical field
The present invention is used for nano fiber scaffold technical field, more particularly to a kind of negative pressure array centrifugation pneumoelectric spinning dress
Put.
Background technology
Electrospinning is to prepare the effective ways of nanofiber.Fibre diameter generally between tens nanometer between a few micrometers, with
The adjoining dimensions of the fibrous framework such as collagen in extracellular matrix.Using natural polymer or synthesis macromolecule electrospinning fibre structure group
Weaver's engineering support, can with the structure or even biological function of bionic extracellular matrix, sticking, break up and breeding beneficial to cell,
The regeneration and reparation of tissue are guided, becomes the research hotspot of tissue engineering bracket.Numerous studies report display, electro spinning nano fiber
Stent can provide preferable cell adhesion, propagation and differentiation microenvironment.
But Traditional DC electrospinning process still has certain technology bottle for efficiently preparing controllable three-dimensional structure
Neck.
Electrostatic spinning, which prepares fibrous framework, has following limitation：
1st, traditional electrostatic spinning be spinning solution or melt under the orientation of direct current field force, formed taylor cone,
The final surface tension that breaks through forms jet stream.Jet stream is drawn into nanofiber under the action of Coulomb force, and fiber is connect layer by layer
Ground collecting board attracts accumulation, forms the stent of film or approximate three-dimensional.But the fiber of stent is to carry out heap by charge attraction
Product, arrangement is close, the gap between fiber is too small, makes cell be difficult to grow into, can not construct gratifying three-dimensional tissue.Separately
On the one hand, traditional direct current electrospinning, electric field force direction is constant, when the viscosity of spinning solution or melt is larger, what jet stream needed
It is high to start voltage.
2nd, with the increase of film frame thickness, the electric field between nozzle and collecting board will gradually weaken, and cause film frame
Surface charges constantly accumulate, and because of band like charges, the fiber first deposited has an impact electric field distribution, and for subsequently penetrating
Miscarriage is raw to be repelled, so as to influence the duration of formation and the spinning of taylor cone, is reduced spinning efficiency, is ultimately resulted in electrospinning mistake
Journey terminates, and limits the thickness that can obtain stent（Usually micron order thickness）, manufacture the electrospinning of the real meaning of big thickness
Three-dimensional structure is still more difficult.
3rd, when using the collector of given shape, fiber is toward the larger place deposition of electric field strength such as at tip, it is difficult to
Form three-dimensional structure.
4th, traditional sprinkler heads formula electrospinning inefficiency, single nozzle electrospinning yield usually only have 0.1-1g/h, it is difficult to realize big rule
Mould, efficient three-dimensional rack are manufactured.
High-speed air-blowing polymer solution carries out the extensive technology for preparing nanofiber（High-speed flow spinning technology）, can be with
The more original electrostatic spinning speed of the preparation speed of fiber is set to improve more than 10 times, still, traditional gas is spun to be connect using closed more
Device or drum receiver are received, under action of high-speed airflow, recoil air-flow is easily produced, how influences the orientated deposition of fiber
Using the standby nano fiber scaffold with three-dimensional fluff structure of high speed gas spinning, the technique for still lacking stable versatility.And
And the fibre diameter of rotor spinning is larger（Micron order）, diameter has a very wide distribution, prepares nanofiber and still suffer from technical bottleneck.
Laboratory research at present and the mainly electrostatic spinning of industrialized production and application（High direct voltage electrospinning）, high voltage power supply
Generally use direct current（DC）Power supply is as high voltage power supply；Ac high-voltage electrospinning（AC electrospinning）Early in electrostatic spinning
The technology early stage of development has had researcher to use, but is not still furtherd investigate and developed so far.Exchange electrospinning
Production efficiency is of a relatively high.Moreover, exchange electrospinning need not be grounded or connect the collector of negative voltage, the flexibility ratio of collection mode
Higher.But directional collecting has given shape, the fibrous framework of structure more difficult, moreover, production efficiency also needs into one
Step improves.
CN1849418A is in charged electrode and in the space between electrode, being applied using air stream to nanofiber and being made
With promotion nanofiber is opened from charged electrode drift, is laid on the equipment for storage nano fiber before charged electrode.
A kind of nanofiber low pressure electric spinning equipment with auxiliary electrode described in CN102965743A, is arranged on collecting board using wind turbine
Side, makes fiber be deposited on collecting board by air-extraction function.CN103952780A collects side in electrostatic spinning and is provided with negative pressure suction
Air port, the micro nanometer fiber that the air-flow absorption produced using inlet scoop is ejected from spinneret needle end, makes it pinpoint or determine area
Domain is attached in the mesh base fabric before inlet scoop, by control the relative movement orbit of mesh base fabric and spinneret syringe needle and speed,
Form equally distributed web.Above-mentioned patent collects side by electrostatic spinning and introduces negative-pressure air-flow in favor of electrostatic spinning micro-nano
The collection of rice fiber, for improving fibre net homogeneity.But collect exchange pneumoelectric spinning nano fibre using negative pressure and prepare three-dimensional branch
There is not been reported for the scheme of frame.
In conclusion preparing, material ranges are extensive, fibre diameter is minimum, string diameter is evenly distributed, structure is fluffy, thickness pole
Greatly, the nanofiber three-dimensional rack of excellent in mechanical performance is still without general solution.
The content of the invention
To solve the above problems, the present invention provides a kind of negative pressure array centrifugation pneumoelectric device for spinning.Apparatus structure is simple, material
Expect wide adaptability, production efficiency is high, and obtainable three-dimensional rack thickness is big, and density is low, and porosity is high, is expected to realize mass production.
The three-dimensional fiber branch of different mechanical strengths, biocompatibility and degradation property can directly be prepared using different spinning materials
Frame.
The technical solution adopted by the present invention to solve the technical problems is：A kind of negative pressure array centrifuges pneumoelectric device for spinning,
Turn including high-voltage alternating generator, feeder, babinet, the centrifugal energy nozzle being located in the babinet, the driving centrifugal energy nozzle
Dynamic centrifugation driving mechanism and the negative pressure reception device positioned at the bottom of box, the centrifugal energy nozzle inside have liquid storage
Chamber, centrifugal energy nozzle spray the wire vent to form jet stream equipped with the spinning solution or melt made when centrifugal energy nozzle rotates in liquid storage cylinder
Pore, the negative pressure reception device include collector, negative tube and the negative pressure generator that negative pressure can be produced in negative tube, institute
State negative tube and the negative pressure mouth of pipe is formed in the bottom of babinet, the collector has loose structure and is nested in the negative pressure mouth of pipe
Interior, the negative pressure reception device setting is multiple, and multiple negative pressure reception devices are arranged in centered on the centrifugal energy nozzle
Annular array, high-voltage alternating generator are connected with the centrifugal energy nozzle and can form use between centrifugal energy nozzle and negative pressure reception device
In the electric field for producing solution jet or melt jet stream, feeder is connected with the centrifugal energy nozzle and can be formed to be sprayed by wire vent pore
The air-flow gone out.
The improvement of technical solution of the present invention is further used as, the top of the babinet is set above each negative pressure reception device
There is air-blast device, the air-blast device can be produced blows to negative pressure reception dress by solution fiber or melt fiber that wire vent pore sprays
The secondary air put.
The improvement of technical solution of the present invention is further used as, the centrifugal energy nozzle is cylindrical, the outer cylinder of centrifugal energy nozzle
Some wire vent pores are opened up on wall, the top of the centrifugal energy nozzle is equipped with head cover, feed inlet and air inlet is opened up in the middle part of head cover,
The air inlet is connected by gas-guide tube with feeder, further includes liquid feed device, and the liquid feed device is accessed by catheter
The feed inlet.
The improvement of technical solution of the present invention is further used as, the centrifugation driving mechanism includes being located at the centrifugal energy nozzle bottom
The rotation axis in portion and pass through shaft coupling with rotation axis connection speed adjustable direct current motor.
The improvement of technical solution of the present invention is further used as, further includes and covers on outside the insulation at the top of the centrifugation driving mechanism
Shell, the insulation crust are hollow cylindrical shape, and the top of insulation crust is equipped with circular hole, and the rotation axis is through circular hole with centrifuging
Nozzle is connected.
The improvement of technical solution of the present invention is further used as, the top of the insulation crust is equipped with and centrifugal energy nozzle can be heated
Heating unit.
The improvement of technical solution of the present invention is further used as, the collector is the metal gate in cubic or cylindrical shape
Net.
The improvement of technical solution of the present invention is further used as, the collector is cylindrical perforated nonwoven fabrics product.
Be further used as the improvement of technical solution of the present invention, the negative pressure generator be located at it is true on the negative tube
Sky pump.
The improvement of technical solution of the present invention is further used as, high-voltage alternating generator includes function signal generator and high pressure
Amplifier.
Disclosed negative pressure array centrifugation pneumoelectric device for spinning, by rationally setting centrifugal energy nozzle, centrifugation to drive
Mechanism, and negative pressure reception device is set centered on the centrifugal energy nozzle and is circularized so that centrifugal energy nozzle is in centrifugation driving machine
When rotating under the driving of structure, the polymer jet stream ejected from centrifugal energy nozzle addition of centrifugal force, while be filled in supply
Under the airflow thrust put and the vacuum suction effect of negative pressure reception device, air flow path is controllable, and fiber is determined toward negative pressure collecting device
To deposition, meanwhile, air-flow passes through the porous fluffy structure of collector, is exported from the lower section of collector and side, and auxiliary fiber
Continuous deposition on the collector, becomes the three dimensional scaffold structure of porous fluffy.
Apparatus structure of the present invention is simple, can promote the nanofiber biological support of three-dimensional structure during spinning
Directly formed.Cost is relatively low, strong suitable for preparing different mechanics with different spinning materials suitable for solution electrospinning and melting electrospinning
The Three Dimensional Fiber Scaffolds of degree, biocompatibility and degradation property, and a large amount of nanofibers can be directly prepared by this method
Biological support；
The present invention innovatively uses negative pressure collecting device, the neutral nanofiber for exchanging pneumoelectric spinning acquisition is carried out three-dimensional
Collect, under the injection of centrifugal energy nozzle high-speed flow and the vacuum suction of negative pressure collecting device effect, air flow path controllability is significantly
Enhancing, compared to classic flat-plate collector or closed collector, can effectively make high-speed flow by so as to avoid producing anti-
Qi of chong channel ascending adversely stream, influences fiber deposition.On the contrary, high-speed flow is by aided nano fiber, orientated deposition becomes with spy on the collector
Shape shape, structure three-dimensional supporting structure, and it is difficult to solve the problems, such as that exchange electrospinning fibre is collected.
Compared with conventional electrostatic spinning prepares biological support, nano fiber scaffold is prepared using the present invention, due to fiber into
Electroneutral, collector is without ground connection or connects negative high voltage, can be easier, effectively deposition forms the big three-dimensional fibrous structure of thickness.
Moreover, charge accumulated will not be caused, do not make significant difference to subsequent fiber deposition, spinning can be carried out for a long time, technique is more stable.
Compared with conventional air spinning prepares biological support, invention introduces high-voltage alternating electric field, jet stream is cut in air-flow
Under power and the collective effect of alternating electric field, further stretching splitting, the three-dimensional rack fibre diameter of acquisition is thinner, and string diameter is distributed more
Uniformly, excellent in mechanical performance, solve rotor spinning prepare biological support fibre diameter it is big, the problem of string diameter skewness.
Compared with commonly exchange electrospinning, the present invention is under the collective effect of alternating electric field and high-speed flow, production efficiency pole
The earth improves, and is 10-20 times of traditional electrospinning.Moreover, under the action of high-speed flow shearing, exacerbate and droplet surface is disturbed
Dynamic, the startup alternating voltage for forming nanofiber is greatly lowered, while solves the problems, such as that nozzle is susceptible to plugging.Moreover, at a high speed
The lower jet stream stretching splitting of air-flow auxiliary, the nanofiber diameter of formation are substantially reduced.
Traditional electrostatic spinning is under the action of electric field, successively attracts accumulation, branch by electrically opposite ground connection collecting board
The fiber alignment of frame is close, the gap between fiber is too small, makes cell be difficult to grow into, can not construct gratifying three-dimensional group
Knit.When using the collector of given shape, fiber is toward the larger place deposition of electric field strength such as at tip, it is difficult to is formed three-dimensional
Structure.And use the present invention, alternating electric field, high-speed flow, receiver negative pressure collective effect under, jet stream stretching splitting, penetrate
Galvanic electricity alternately changes, and the nanofiber of formation is in electroneutral, and is oriented under the auxiliary of controllable air flow on negative pressure receiver
Three-dimensional structure is deposited into, very big, loose, low-density the stent of thickness can be obtained, be more advantageous to cell growth.
The insulation of babinet surfaces externally and internally, the insulation of the present invention, top is closed, the earthing of casing.Device for spinning and collector are placed in
In babinet.The influence that external environment deposits spinning process and fiber can be reduced, while improves security, prevents ac high-voltage from making
Into unexpected injury.
The present invention by using the spining technology based on negative pressure receiver, can prepare material ranges extensively, fibre diameter pole
Small, string diameter is evenly distributed, structure is fluffy, thickness is very big, the nanofiber three-dimensional rack of excellent in mechanical performance, technique versatility
It is good, it can be widely applied to field of tissue engineering technology.
Brief description of the drawings
The invention will be further described below in conjunction with the accompanying drawings：
Fig. 1 is spinning theory structure schematic diagram of the present invention；
Fig. 2 is centrifugal energy nozzle, centrifugation driving mechanism, insulation crust and schematic diagram of heating device of the present invention；
Fig. 3 is centrifugal energy nozzle jet current principle schematic diagram of the present invention；
Fig. 4 is negative pressure reception device arrangement architecture schematic diagram of the present invention.
Embodiment
Referring to figs. 1 to Fig. 4, that show the concrete structure of the preferred embodiments of the invention.It will be detailed below this
Invent the design feature of each element, and during if being described to direction (upper and lower, left and right, before and after), it is with shown in Fig. 1
Structure is that reference describes, but the actual use direction of the present invention is not limited thereto.
The present invention provides a kind of negative pressure array to centrifuge pneumoelectric device for spinning, including high-voltage alternating generator 1, feeder
2nd, the centrifugation driving mechanism and position that babinet 3, the centrifugal energy nozzle 4 being located in the babinet 3, the driving centrifugal energy nozzle 4 rotate
Negative pressure reception device 5 in 3 bottom of babinet, the inside of centrifugal energy nozzle 4 have liquid storage cylinder, and centrifugal energy nozzle 4 is equipped with
The spinning solution in liquid storage cylinder or melt is set to spray the wire vent pore 41 to form jet stream during the rotation of centrifugal energy nozzle 4, the negative pressure connects
Receiving apparatus 5 includes collector 51, negative tube 52 and the negative pressure generator 53 that negative pressure can be produced in negative tube 52, described to do something in a fit of pique
Pressure generator 53 is preferably the vacuum pump being located on the negative tube 52.The negative tube 52 forms negative pressure in the bottom of babinet 3
The mouth of pipe, the collector 51 have loose structure and are nested in the negative pressure mouth of pipe, and it is in cube that the collector 51, which uses,
The metal grid mesh of shape or cylindrical shape, or cylindrical perforated nonwoven fabrics product.The negative pressure reception device 5 set it is multiple,
And multiple negative pressure reception devices 5 are arranged in annular array centered on the centrifugal energy nozzle 4, high-voltage alternating generator 1 with
The centrifugal energy nozzle 4 is connected and can be formed between centrifugal energy nozzle 4 and negative pressure reception device 5 and is used to produce solution jet or melt is penetrated
The electric field of stream, feeder 2 is connected with the centrifugal energy nozzle 4 and can form the air-flow sprayed by wire vent pore 41, wherein supplying
Device 2 can provide the multiple gases including compressed air, nitrogen, carbon dioxide, there is provided variety classes, temperature, wet
Degree, the air-flow of air pressure, air-flow aid in taylor cone into stretching, deposit with fiber.The top of the babinet 3 receives in each negative pressure and fills
The top for putting 5 is equipped with air-blast device 6, and the air-blast device 6 can produce the solution fiber for spraying wire vent pore 41 or melt is fine
Dimension blows to the secondary air of negative pressure reception device 5.
The centrifugal energy nozzle 4 is cylindrical, opens up some wire vent pores 41 in the outer cylindrical wall of centrifugal energy nozzle 4, it is described from
The top of heart nozzle 4 is equipped with head cover, and feed inlet and air inlet are opened up in the middle part of head cover, and the air inlet passes through gas-guide tube and supply
Device 2 connects, and further includes liquid feed device 7, and the liquid feed device 7 accesses the feed inlet by catheter.The centrifugation driving
Mechanism includes being located at the rotation axis 81 of 4 bottom of centrifugal energy nozzle and straight by the adjustable speed that shaft coupling 82 is connected with rotation axis 81
Galvanic electricity machine 83.The rotating speed of centrifugal energy nozzle 4 can be adjusted by adjusting the rotating speed of speed adjustable direct current motor 83, so as to adjust jet stream
Rotary speed, with the diameter and the uniformity of control fiber.
The insulation crust 9 covered at the top of the centrifugation driving mechanism is further included, the insulation crust 9 is hollow cylinder
Shape, the top of insulation crust 9 are equipped with circular hole, and the rotation axis 81 is connected through circular hole with centrifugal energy nozzle 4, the insulation crust 9
Top be equipped with can to centrifugal energy nozzle 4 heat heating unit 91, centrifugal energy nozzle 4 can be heated, with realize centrifugation spray
Spinning melt is directly obtained in first 4.
High-voltage alternating generator 1 includes function signal generator and high-voltage amplifier, and the ac high voltage generator 1 can carry
For random waveform, frequency, amplitude voltage.
Disclosed negative pressure array centrifugation pneumoelectric device for spinning, by rationally setting centrifugal energy nozzle 4, centrifugation to drive
Mechanism, and negative pressure reception device 5 is set centered on the centrifugal energy nozzle 4 and is circularized so that centrifugal energy nozzle 4 drives in centrifugation
When rotating under the driving of mechanism, the polymer jet stream ejected from centrifugal energy nozzle 4 addition of centrifugal force, while supply
The airflow thrust of device, electric field force, the vacuum suction of negative pressure reception device 5 and air-blast device 6 air-flow guiding function under, air-flow
Path is controllable, fiber toward 5 orientated deposition of negative pressure collecting device, meanwhile, air-flow pass through collector 51 porous fluffy structure, from receipts
The lower section of storage and side export, and auxiliary fiber continuous deposition on the collector, become the three dimensional scaffold structure of porous fluffy.
Following examples can be respectively referred to for spinning solution and melt：
Embodiment 1：
Disclosed negative pressure array centrifugation pneumoelectric device for spinning, in use, spinning solution preparation is being carried out first,
Weigh 1800 milligrams of PLLA（The dalton of molecular weight=200,000）, it is dissolved in 30 ml（9:1, CH2Cl2/DMF,v/v）In solvent, 6% is made
PLLA solution, is sealed with sealed membrane, stand-by when magnetic agitation 3 is small.
Load PLLA solution in liquid feed device 7, open liquid feed device 7, flow 1mL/min, opens feeder 2, adjusts
Solar term pressure is 0.75MPa, opens negative pressure reception device 5, then opens the switch of speed adjustable direct current motor 83, and rotary rpm is
5000rpm, makes the PLLA solution at wire vent pore 41 form solid jet under the action of centrifugal force and air-flow, jet stream is through meticulous
Change, evaporation process, under the air-flow guiding function of electric field force, the vacuum suction of negative pressure reception device 5 and air-blast device 6, in negative pressure
A large amount of three-dimensional manometer PLLA fibrous frameworks are collected into reception device 5.
Embodiment 2：
Disclosed negative pressure array centrifugation pneumoelectric device for spinning, it is poly- by 20 grams using polylactic acid as raw material during use
Lactic acid is added in feed inlet, is then opened heating unit 91 and is switched, polylactic acid is heated to molten condition in centrifugal energy nozzle 4,
Negative pressure reception device 5 to be opened, opens feeder 2, adjusting air pressure is 0.8MPa, opens the switch of speed adjustable direct current motor 83,
Rotary rpm is 6000rpm, makes the polylactic acid melt centrifugal force at wire vent pore 41, forms solid jet under the action of air-flow,
Jet stream is by refinement, evaporation process, the air-flow guiding function of electric field force, the vacuum suction of negative pressure reception device 5 and air-blast device 6
Under, a large amount of three-dimensional manometer PLLA fibrous frameworks are collected into negative pressure reception device 5.
The disclosed centrifugal spinning device for preparing three-dimensional manometer fiber, simple in structure, easy to operate, control letter
List, technological process are short.
Certainly, the invention is not limited to the above embodiment, and those skilled in the art are without prejudice to originally
Equivalent variations or replacement can be also made on the premise of spirit, these equivalent modifications or replacement are all contained in the application right
It is required that in limited range.
Claims (10)
1. a kind of negative pressure array centrifuges pneumoelectric device for spinning, it is characterised in that：Including high-voltage alternating generator, feeder, case
Centrifugation driving mechanism that body, the centrifugal energy nozzle being located in the babinet, the driving centrifugal energy nozzle rotate and positioned at the case
The negative pressure reception device of body bottom, the centrifugal energy nozzle inside have liquid storage cylinder, and centrifugal energy nozzle is equipped with to be rotated in centrifugal energy nozzle
When spinning solution in liquid storage cylinder or melt is sprayed the wire vent pore to form jet stream, the negative pressure reception device includes collecting
Device, negative tube and the negative pressure generator that negative pressure can be produced in negative tube, the negative tube form negative pressure in the bottom of babinet
The mouth of pipe, the collector have loose structure and are nested in the negative pressure mouth of pipe, and the negative pressure reception device setting is multiple, and
Multiple negative pressure reception devices are arranged in annular array centered on the centrifugal energy nozzle, high-voltage alternating generator with it is described from
Heart nozzle is connected and can be formed between centrifugal energy nozzle and negative pressure reception device for producing the electric field of solution jet or melt jet stream,
Feeder is connected and can be formed the air-flow sprayed by wire vent pore with the centrifugal energy nozzle.
2. negative pressure array according to claim 1 centrifuges pneumoelectric device for spinning, it is characterised in that：The top of the babinet exists
The top of each negative pressure reception device is equipped with air-blast device, the air-blast device can produce the solution fiber that sprays wire vent pore or
Melt fiber blows to the secondary air of negative pressure reception device.
3. negative pressure array according to claim 2 centrifuges pneumoelectric device for spinning, it is characterised in that：The centrifugal energy nozzle is in circle
Tubular, opens up some wire vent pores in the outer cylindrical wall of centrifugal energy nozzle, and the top of the centrifugal energy nozzle is equipped with head cover, in head cover
Portion opens up feed inlet and air inlet, and the air inlet is connected by gas-guide tube with feeder, further includes liquid feed device, the confession
Liquid device accesses the feed inlet by catheter.
4. negative pressure array according to claim 1 centrifuges pneumoelectric device for spinning, it is characterised in that：The centrifugation driving mechanism
Including being located at the rotation axis of the centrifugal energy nozzle bottom and by shaft coupling and the speed adjustable direct current motor of rotation axis connection.
5. negative pressure array according to claim 4 centrifuges pneumoelectric device for spinning, it is characterised in that：Further include cover on it is described from
Insulation crust at the top of heart driving mechanism, the insulation crust are hollow cylindrical shape, and the top of insulation crust is equipped with circular hole, institute
Rotation axis is stated through circular hole with centrifugal energy nozzle to be connected.
6. negative pressure array according to claim 5 centrifuges pneumoelectric device for spinning, it is characterised in that：The top of the insulation crust
Portion is equipped with the heating unit that can be heated to centrifugal energy nozzle.
7. negative pressure array according to claim 1 centrifuges pneumoelectric device for spinning, it is characterised in that：The collector is in vertical
The metal grid mesh of cube shape or cylindrical shape.
8. negative pressure array according to claim 1 centrifuges pneumoelectric device for spinning, it is characterised in that：The collector is in circle
The perforated nonwoven fabrics product of tubular.
9. negative pressure array according to claim 1 centrifuges pneumoelectric device for spinning, it is characterised in that：The negative pressure generator
For the vacuum pump being located on the negative tube.
10. negative pressure array according to claim 1 centrifuges pneumoelectric device for spinning, it is characterised in that：High-voltage alternating generator
Including function signal generator and high-voltage amplifier.
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| CN201510778785.XA CN105350093B (en) | 2015-11-13 | 2015-11-13 | A kind of negative pressure array centrifuges pneumoelectric device for spinning |
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| CN201510778785.XA CN105350093B (en) | 2015-11-13 | 2015-11-13 | A kind of negative pressure array centrifuges pneumoelectric device for spinning |
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| CN105350093B true CN105350093B (en) | 2018-04-17 |
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Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105951195B (en) * | 2016-06-24 | 2018-02-02 | 武汉纺织大学 | A kind of microgravity suspension centrifugal spinning method |
| CN106917147A (en) * | 2017-01-22 | 2017-07-04 | 广东工业大学 | A kind of electrostatic spinning apparatus |
| CN109097849B (en) * | 2018-09-28 | 2021-05-04 | 上海云同新材料科技有限公司 | Nanofiber generating device |
| CN110219060B (en) * | 2019-06-26 | 2021-01-26 | 广东工业大学 | Centrifugal electrostatic spinning device |
| CN110714230B (en) * | 2019-09-29 | 2021-03-23 | 亿茂环境科技股份有限公司 | Negative pressure traction device for centrifugal spinning |
| CN111155178B (en) * | 2020-01-08 | 2021-03-16 | 盐城工学院 | Novel centrifugal spinning device |
| CN113622082B (en) * | 2020-05-06 | 2022-09-23 | 深圳陶陶科技有限公司 | Preparation method and application of centrifugal spinning non-woven fabric |
| CN111926459B (en) * | 2020-08-14 | 2021-07-30 | 青岛华仕达机器股份有限公司 | Continuous melt-blown fabric production line |
| CN113584615B (en) * | 2021-09-01 | 2022-05-03 | 福建永荣锦江股份有限公司 | Coaxial driving centrifugal spinning winding device |
| CN114351354B (en) * | 2021-12-03 | 2023-03-28 | 东华大学 | Super-elastic electrostatic spinning thermal insulation flocculus with waveform structure and preparation method thereof |
| CN114808164B (en) * | 2022-05-06 | 2023-08-04 | 武汉纺织大学 | Collecting device for centrifugal spinning and using method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US6189804B1 (en) * | 1998-03-27 | 2001-02-20 | Behr Systems, Inc. | Rotary atomizer for particulate paints |
| US7134857B2 (en) * | 2004-04-08 | 2006-11-14 | Research Triangle Institute | Electrospinning of fibers using a rotatable spray head |
| KR100780346B1 (en) * | 2006-09-19 | 2007-11-30 | 주식회사 아모메디 | An electro-centrifugal spinning apparatus and a method for mass production of nano-fibers using the same |
| WO2009055413A1 (en) * | 2007-10-23 | 2009-04-30 | Ppg Industries Ohio, Inc. | Fiber formation by electrical-mechanical spinning |
| US8597552B2 (en) * | 2009-03-16 | 2013-12-03 | Evan Koslow | Apparatus, systems and methods for producing particles using rotating capillaries |
| CN102703998B (en) * | 2012-06-21 | 2014-09-03 | 中原工学院 | Jet yarn spinning device for electrostatic spun nano fiber and preparing method |
| CN103628149B (en) * | 2013-11-25 | 2015-10-14 | 北京化工大学 | A kind of high pressure draught auxiliary nozzle spinning electrostatic spinning apparatus |
| CN204097612U (en) * | 2014-10-31 | 2015-01-14 | 苏州大学 | A kind ofly be applied to the air-flow rotating disk device for spinning preparing nanofiber |
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