CN105347772A - Preparation method of gypsum bedrock cotton fiber insulation board - Google Patents

Preparation method of gypsum bedrock cotton fiber insulation board Download PDF

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Publication number
CN105347772A
CN105347772A CN201510877249.5A CN201510877249A CN105347772A CN 105347772 A CN105347772 A CN 105347772A CN 201510877249 A CN201510877249 A CN 201510877249A CN 105347772 A CN105347772 A CN 105347772A
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rock wool
gypsum
rotating speed
melt
stirring
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CN201510877249.5A
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CN105347772B (en
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梅庆波
林大伟
王志慧
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Guangzhou Yuen Peng Heat Insulation Material Co ltd
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Abstract

The invention discloses a preparation method of a gypsum bedrock cotton fiber insulation board, and belongs to the field of insulation boards. The preparation method comprises the following steps: a rock wool material, a gypsum cement mixture and a modified hybrid adhesive are mixed and stirred, and then the mixture is injected into a stainless steel die to be molded and dried, so as to obtain the gypsum bedrock cotton fiber insulation board. According to the preparation method of the gypsum bedrock cotton fiber insulation board, provided by the invention, rock wool, gypsum and cement which are adopted as the main raw materials, and are inorganic materials, thereby being non-toxic and pollution-free, so that the prepared inorganic and non-combustible thermal insulation material can replace the conventional flammable organic thermal insulation material in the market, the problem that the building exterior wall external insulation system is difficult to prevent fire is solved, and great significance on the city safety is further achieved.

Description

A kind of preparation method of gypsum base rock wool fibers warming plate
Technical field
The invention discloses a kind of preparation method of gypsum base rock wool fibers warming plate, belong to warming plate field.
Background technology
Rock wool is a kind of high-quality and efficient lagging material, it has good heat insulating, sound insulation and sound absorbing capabilities, compared with traditional lagging material, have that density is little, thermal conductivity is low, do not burn, nontoxic, applied widely, the outstanding advantages such as stable chemical performance, life cycle are long of preventing fires, be the desirable lagging material of generally acknowledging both at home and abroad.Abroad, especially employ asbestos product in a large number in European construction market, consumption is at more than 20kg per capita in Northern Europe, and the U.S. per capita consumption is that 510kg is due to fire safety problem, in the U.S., rock mineral wool accounts for 70%, and the architectural exterior insulation high more than 22m in Germany almost all adopts rock wool heat-preservation material.But in China, rock wool is also lower as the rate of utilization of building thermal insulation material, be mainly used in the aspects such as the thermal insulation of the light plate of energy petrochemical complex, shipping industry and building, fire prevention, sound insulation, and apply seldom in covil construction, particularly the application of external wall outer insulation is domestic is still blank.Along with organic wall heat insulation material be widely used in public with covil construction since, in rapid succession, the fire resistance of lagging material causes the great attention of various circles of society to Fire Accidents for Buildings.Rock wool has the outstanding advantages such as density is little, thermal conductivity is low, do not burn, and is desirable inorganic heat insulation material.
Organic insulation material (PS, PU) in the market, fire-protection rating is lower.Such as, polystyrene foamed plastics (EPS) burning-point is 346, spontaneous ignition temperature is that 490 external heat sources pass the thick polymkeric substance plastering mortar of 35mm or titanium zinc alloy plate reaches 490, only need several minutes just can cause the chain burning of porous plastics spontaneous combustion EPS energy, very fast melting after the burning of flame retardant grade porous plastics, droplet temperature is far above 490, molten drop drips to part, cause again porous plastics spontaneous combustion, form chain burning, this chain burning is the most fearful part of porous plastics.And the maximum operation (service) temperature of rock wool is more than 650 DEG C, its fusing point is more than 1000 DEG C, and when running into fire, rock-wool heat insulation plate can not cause smog or cause Mars, also can not drip, cause fire spreading.Even if also can not discharge at high operating temperatures environment and the unfavorable or harmful gas of human body.Therefore, rock wool is as the lagging material of external wall, and its fire resistance is also very superior.
Summary of the invention
The technical problem that the present invention mainly solves: for current organic insulation material (PS, PU), fire-protection rating is lower, external heat source reaches burning-point through flame-retardant polymer plastering mortar, only need several minutes just can cause porous plastics spontaneous combustion and cause chain burning, and organic insulation material in the fabrication process, likely there is chemical leakage and make
Become poisoning, fire, the harm of blast, provide a kind of preparation method of gypsum base rock wool fibers warming plate, the present invention's rock wool material, gypsam cement and modification composite adhesive mix and blend, inject shaping and dry the gypsum base rock wool fibers warming plate of stainless steel mould, the rock wool that the present invention adopts, gypsum, cement is main raw material, it is all inorganic materials, nontoxic, pollution-free, obtained inorganic non-combustible lagging material substitutes existing flammable organic insulation material on market, the problem that the fire prevention of external wall external insulation system is difficult can be solved, urban safety is significant.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
1.(1) meter takes 70 ~ 80 parts of basalt by weight, 15 ~ 20 parts of shale, 10 ~ 15 parts of blast furnace slags load stone crusher together and pulverize, building stones mixture after pulverizing is sent into the melting end of tank furnace with feeding machine, the high temperature of 1400 ~ 1600 DEG C that the atomization oil combustion sprayed into by nozzle produces, obtains melt by melting sources;
2.(2) the first roller melt obtained above being flowed into four roller whizzers disperses, carry out centrifugal with the rotating speed of 4000 ~ 5000r/min, got rid of by melt under the influence of centrifugal force and make fiber, remaining melt gets rid of and continues to manufacture fiber to the second roller, until melt system is completely fine;
3.(3) by the fiber collecting that throws away on the collection web of cotton collecting machine, and utilize pendulum bob machine formation multilayer to loosen rock wool layer through pressure cotton machine to form closely knit rock wool body after the compacting of the pressure of 6000 ~ 7000N, obtained rock wool body is put into curing oven, be cured with the temperature of 150 ~ 200 DEG C, obtain rock wool material;
4.(4) 2 ~ 3kg terra alba is taken and 1 ~ 2kg cement is poured in mortar mixer, with the rotating speed stirring at low speed 10 ~ 20min of 50 ~ 60r/min, until mix, for subsequent use;
5.(5) get 30 ~ 50g Xylo-Mucine and put into 2L beaker, add 1000 ~ 1500mL distilled water inwards, be placed on magnetic stirrer, after stirring 10 ~ 20min with the rotating speed of 300 ~ 400r/min, 200 ~ 300mL water glass is added again in beaker, improve rotating speed to 500 ~ 600r/min, continue stirring 30 ~ 40min, obtained modification composite adhesive;
6.(6) by above-mentioned obtained rock wool material, gypsam cement and modification composite adhesive in mass ratio for 3:40:100 mix after pour in pulp blender, with the rotating speed Stirring of 20 ~ 30r/min, the mass concentration adding mixture cumulative volume 2 ~ 5% in whipping process is inwards the sodium hydroxide solution of 30%, continues to stir;
7.(7) after being with stirring to complete, material is injected rapidly the stainless steel mould of 50 × 50 × 10cm, again mould is moved in pressing machine, after carrying out compacting dehydration with the pressure of 4000 ~ 6000N, mould is put into baking oven, after being dried to constant weight with 105 ~ 110 DEG C of temperature, form removal, obtains a kind of gypsum base rock wool fibers warming plate.
Application method of the present invention: first ensure before use that construction base course wall should be solid smooth, surface drying, cracking must not be had, hollowing, loosen or the accumulation of salt in the surface soil, the warming plate lower end first the present invention obtained and basic unit paste, warming plate should laterally be laid from bottom to top in the horizontal direction, and it is solid that limit should be taked to spread side anchor, plate seam should be close to naturally, between plate, gap is≤2mm, during as stitched wide 2mm, filled thermal insulation materials process should be had, adjacent panels face should be concordant, Gao Cha≤1.5mm between plate, the pipeline through walls of warming plate and component, waterproof sealing process is carried out after its outlet position application same material tamps, warming plate is pasted complete, surface treatment is carried out in the face of plastering of reply plate, with stainless steel spatula, finishing mucilage (thickness 1 ~ 1.4mm) is scraped to the painting of whole surface, and be pressed in the surface fibre of warming plate, air-dry.
The invention has the beneficial effects as follows:
(1) the present invention's rock wool material, gypsam cement and modification composite adhesive mix and blend, inject shaping and dry the gypsum base rock wool fibers warming plate of stainless steel mould, the rock wool that the present invention adopts, gypsum, cement are main raw material, are all inorganic materials, nontoxic, pollution-free;
(2) the inorganic non-combustible lagging material that the present invention obtains substitutes existing flammable organic insulation material on market, can solve the problem that the fire prevention of external wall external insulation system is difficult, be significant to urban safety.
Embodiment
First by weight meter takes 70 ~ 80 parts of basalt, 15 ~ 20 parts of shale, 10 ~ 15 parts of blast furnace slags load stone crusher together and pulverize, building stones mixture after pulverizing is sent into the melting end of tank furnace with feeding machine, the high temperature of 1400 ~ 1600 DEG C that the atomization oil combustion sprayed into by nozzle produces, obtains melt by melting sources; The first roller melt obtained being flowed into four roller whizzers disperses, carry out centrifugal with the rotating speed of 4000 ~ 5000r/min, got rid of by melt under the influence of centrifugal force and make fiber, remaining melt gets rid of and continues to manufacture fiber to the second roller, until melt system is completely fine; By the fiber collecting that throws away on the collection web of cotton collecting machine, and utilize pendulum bob machine formation multilayer to loosen rock wool layer through pressure cotton machine to form closely knit rock wool body after the compacting of the pressure of 6000 ~ 7000N, obtained rock wool body is put into curing oven, is cured with the temperature of 150 ~ 200 DEG C, obtain rock wool material; Take 2 ~ 3kg terra alba and 1 ~ 2kg cement is poured in mortar mixer, with the rotating speed stirring at low speed 10 ~ 20min of 50 ~ 60r/min, until mix, for subsequent use; Get 30 ~ 50g Xylo-Mucine and put into 2L beaker, add 1000 ~ 1500mL distilled water inwards, be placed on magnetic stirrer, after stirring 10 ~ 20min with the rotating speed of 300 ~ 400r/min, 200 ~ 300mL water glass is added again in beaker, improve rotating speed to 500 ~ 600r/min, continue stirring 30 ~ 40min, obtained modification composite adhesive; By obtained rock wool material, gypsam cement and modification composite adhesive in mass ratio for 3:40:100 mix after pour in pulp blender, with the rotating speed Stirring of 20 ~ 30r/min, the mass concentration adding mixture cumulative volume 2 ~ 5% in whipping process is inwards the sodium hydroxide solution of 30%, continues to stir;
After band stirring completes, material is injected rapidly the stainless steel mould of 50 × 50 × 10cm, again mould is moved in pressing machine, after carrying out compacting dehydration with the pressure of 4000 ~ 6000N, mould is put into baking oven, after being dried to constant weight with 105 ~ 110 DEG C of temperature, form removal, obtains a kind of gypsum base rock wool fibers warming plate.
Example 1
10.first by weight meter takes 70 parts of basalt, 15 parts of shale, 15 parts of blast furnace slags load stone crusher together and pulverize, building stones mixture after pulverizing is sent into the melting end of tank furnace with feeding machine, the high temperature of 1400 DEG C that the atomization oil combustion sprayed into by nozzle produces, obtains melt by melting sources; The first roller melt obtained being flowed into four roller whizzers disperses, carries out centrifugal, got rid of by melt under the influence of centrifugal force and make fiber with the rotating speed of 4000r/min, remaining melt gets rid of and continues to manufacture fiber to the second roller, until melt system is completely fine; By the fiber collecting that throws away on the collection web of cotton collecting machine, and utilize pendulum bob machine formation multilayer to loosen rock wool layer through pressure cotton machine to form closely knit rock wool body after the compacting of the pressure of 6000N, obtained rock wool body is put into curing oven, is cured with the temperature of 150 DEG C, obtain rock wool material; Take 2kg terra alba and 1kg cement is poured in mortar mixer, with the rotating speed stirring at low speed 10min of 50r/min, until mix, for subsequent use; Get 30g Xylo-Mucine and put into 2L beaker, add 1000mL distilled water inwards, be placed on magnetic stirrer, after stirring 10min with the rotating speed of 300r/min, then add 200mL water glass in beaker, improve rotating speed to 500r/min, continue to stir 30min, obtained modification composite adhesive; By obtained rock wool material, gypsam cement and modification composite adhesive in mass ratio for 3:40:100 mix after pour in pulp blender, with the rotating speed Stirring of 20r/min, the mass concentration adding mixture cumulative volume 2% in whipping process is inwards the sodium hydroxide solution of 30%, continues to stir; After band stirring completes, material is injected rapidly the stainless steel mould of 50 × 50 × 10cm, then mould is moved in pressing machine, after carrying out compacting dehydration with the pressure of 4000N, mould is put into baking oven, after being dried to constant weight with 105 DEG C of temperature, form removal, obtains a kind of gypsum base rock wool fibers warming plate.
First ensure before using that construction base course wall should be solid smooth, surface drying, cracking must not be had, hollowing, loosen or the accumulation of salt in the surface soil, the warming plate lower end first the present invention obtained and basic unit paste, warming plate should laterally be laid from bottom to top in the horizontal direction, and it is solid that limit should be taked to spread side anchor, plate seam should be close to naturally, between plate, gap is 1.3mm, during as stitched wide 2mm, filled thermal insulation materials process should be had, adjacent panels face should be concordant, discrepancy in elevation 1.0mm between plate, the pipeline through walls of warming plate and component, waterproof sealing process is carried out after its outlet position application same material tamps, warming plate is pasted complete, surface treatment is carried out in the face of plastering of reply plate, with stainless steel spatula, finishing mucilage (thickness 1mm) is scraped to the painting of whole surface, and be pressed in the surface fibre of warming plate, air-dry.
Example 2
11.first by weight meter takes 75 parts of basalt, 17 parts of shale, 13 parts of blast furnace slags load stone crusher together and pulverize, building stones mixture after pulverizing is sent into the melting end of tank furnace with feeding machine, the high temperature of 1500 DEG C that the atomization oil combustion sprayed into by nozzle produces, obtains melt by melting sources; The first roller melt obtained being flowed into four roller whizzers disperses, carries out centrifugal, got rid of by melt under the influence of centrifugal force and make fiber with the rotating speed of 4500r/min, remaining melt gets rid of and continues to manufacture fiber to the second roller, until melt system is completely fine; By the fiber collecting that throws away on the collection web of cotton collecting machine, and utilize pendulum bob machine formation multilayer to loosen rock wool layer through pressure cotton machine to form closely knit rock wool body after the compacting of the pressure of 6500N, obtained rock wool body is put into curing oven, is cured with the temperature of 175 DEG C, obtain rock wool material; Take 2.5kg terra alba and 1.5kg cement is poured in mortar mixer, with the rotating speed stirring at low speed 15min of 55r/min, until mix, for subsequent use; Get 40g Xylo-Mucine and put into 2L beaker, add 1250mL distilled water inwards, be placed on magnetic stirrer, after stirring 15min with the rotating speed of 350r/min, then add 250mL water glass in beaker, improve rotating speed to 550r/min, continue to stir 35min, obtained modification composite adhesive; By obtained rock wool material, gypsam cement and modification composite adhesive in mass ratio for 3:40:100 mix after pour in pulp blender, with the rotating speed Stirring of 25r/min, the mass concentration adding mixture cumulative volume 4% in whipping process is inwards the sodium hydroxide solution of 30%, continues to stir; After band stirring completes, material is injected rapidly the stainless steel mould of 50 × 50 × 10cm, then mould is moved in pressing machine, after carrying out compacting dehydration with the pressure of 5000N, mould is put into baking oven, after being dried to constant weight with 108 DEG C of temperature, form removal, obtains a kind of gypsum base rock wool fibers warming plate.
First ensure before using that construction base course wall should be solid smooth, surface drying, cracking must not be had, hollowing, loosen or the accumulation of salt in the surface soil, the warming plate lower end first the present invention obtained and basic unit paste, warming plate should laterally be laid from bottom to top in the horizontal direction, and it is solid that limit should be taked to spread side anchor, plate seam should be close to naturally, between plate, gap is 1.5mm, during as stitched wide 2mm, filled thermal insulation materials process should be had, adjacent panels face should be concordant, discrepancy in elevation 1.3mm between plate, the pipeline through walls of warming plate and component, waterproof sealing process is carried out after its outlet position application same material tamps, warming plate is pasted complete, surface treatment is carried out in the face of plastering of reply plate, with stainless steel spatula, finishing mucilage (thickness 1.2mm) is scraped to the painting of whole surface, and be pressed in the surface fibre of warming plate, air-dry.
Example 3
13.first by weight meter takes 73 parts of basalt, 16 parts of shale, 11 parts of blast furnace slags load stone crusher together and pulverize, building stones mixture after pulverizing is sent into the melting end of tank furnace with feeding machine, the high temperature of 1600 DEG C that the atomization oil combustion sprayed into by nozzle produces, obtains melt by melting sources; The first roller melt obtained being flowed into four roller whizzers disperses, carries out centrifugal, got rid of by melt under the influence of centrifugal force and make fiber with the rotating speed of 5000r/min, remaining melt gets rid of and continues to manufacture fiber to the second roller, until melt system is completely fine; By the fiber collecting that throws away on the collection web of cotton collecting machine, and utilize pendulum bob machine formation multilayer to loosen rock wool layer through pressure cotton machine to form closely knit rock wool body after the compacting of the pressure of 7000N, obtained rock wool body is put into curing oven, is cured with the temperature of 200 DEG C, obtain rock wool material; Take 3kg terra alba and 2kg cement is poured in mortar mixer, with the rotating speed stirring at low speed 20min of 60r/min, until mix, for subsequent use; Get 50g Xylo-Mucine and put into 2L beaker, add 1500mL distilled water inwards, be placed on magnetic stirrer, after stirring 20min with the rotating speed of 400r/min, then add 300mL water glass in beaker, improve rotating speed to 600r/min, continue to stir 40min, obtained modification composite adhesive; By obtained rock wool material, gypsam cement and modification composite adhesive in mass ratio for 3:40:100 mix after pour in pulp blender, with the rotating speed Stirring of 30r/min, the mass concentration adding mixture cumulative volume 5% in whipping process is inwards the sodium hydroxide solution of 30%, continues to stir; After band stirring completes, material is injected rapidly the stainless steel mould of 50 × 50 × 10cm, then mould is moved in pressing machine, after carrying out compacting dehydration with the pressure of 6000N, mould is put into baking oven, after being dried to constant weight with 110 DEG C of temperature, form removal, obtains a kind of gypsum base rock wool fibers warming plate.
First ensure before using that construction base course wall should be solid smooth, surface drying, cracking must not be had, hollowing, loosen or the accumulation of salt in the surface soil, the warming plate lower end first the present invention obtained and basic unit paste, warming plate should laterally be laid from bottom to top in the horizontal direction, and it is solid that limit should be taked to spread side anchor, plate seam should be close to naturally, between plate, gap is 1.8mm, during as stitched wide 2mm, filled thermal insulation materials process should be had, adjacent panels face should be concordant, discrepancy in elevation 1.5mm between plate, the pipeline through walls of warming plate and component, waterproof sealing process is carried out after its outlet position application same material tamps, warming plate is pasted complete, surface treatment is carried out in the face of plastering of reply plate, with stainless steel spatula, finishing mucilage (thickness 1.4mm) is scraped to the painting of whole surface, and be pressed in the surface fibre of warming plate, air-dry.

Claims (1)

1. a preparation method for gypsum base rock wool fibers warming plate, is characterized in that concrete preparation process is:
(1) meter takes 70 ~ 80 parts of basalt by weight, 15 ~ 20 parts of shale, 10 ~ 15 parts of blast furnace slags load stone crusher together and pulverize, building stones mixture after pulverizing is sent into the melting end of tank furnace with feeding machine, the high temperature of 1400 ~ 1600 DEG C that the atomization oil combustion sprayed into by nozzle produces, obtains melt by melting sources;
(2) the first roller melt obtained above being flowed into four roller whizzers disperses, carry out centrifugal with the rotating speed of 4000 ~ 5000r/min, got rid of by melt under the influence of centrifugal force and make fiber, remaining melt gets rid of and continues to manufacture fiber to the second roller, until melt system is completely fine;
(3) by the fiber collecting that throws away on the collection web of cotton collecting machine, and utilize pendulum bob machine formation multilayer to loosen rock wool layer through pressure cotton machine to form closely knit rock wool body after the compacting of the pressure of 6000 ~ 7000N, obtained rock wool body is put into curing oven, be cured with the temperature of 150 ~ 200 DEG C, obtain rock wool material;
(4) 2 ~ 3kg terra alba is taken and 1 ~ 2kg cement is poured in mortar mixer, with the rotating speed stirring at low speed 10 ~ 20min of 50 ~ 60r/min, until mix, for subsequent use;
(5) get 30 ~ 50g Xylo-Mucine and put into 2L beaker, add 1000 ~ 1500mL distilled water inwards, be placed on magnetic stirrer, after stirring 10 ~ 20min with the rotating speed of 300 ~ 400r/min, 200 ~ 300mL water glass is added again in beaker, improve rotating speed to 500 ~ 600r/min, continue stirring 30 ~ 40min, obtained modification composite adhesive;
(6) by above-mentioned obtained rock wool material, gypsam cement and modification composite adhesive in mass ratio for 3:40:100 mix after pour in pulp blender, with the rotating speed Stirring of 20 ~ 30r/min, the mass concentration adding mixture cumulative volume 2 ~ 5% in whipping process is inwards the sodium hydroxide solution of 30%, continues to stir;
(7) after being with stirring to complete, material is injected rapidly the stainless steel mould of 50 × 50 × 10cm, again mould is moved in pressing machine, after carrying out compacting dehydration with the pressure of 4000 ~ 6000N, mould is put into baking oven, after being dried to constant weight with 105 ~ 110 DEG C of temperature, form removal, obtains the insulation of a kind of gypsum base rock wool fibers.
CN201510877249.5A 2015-12-03 2015-12-03 A kind of preparation method of gypsum base rock wool fibers warming plate Expired - Fee Related CN105347772B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106437064A (en) * 2016-08-28 2017-02-22 山东地平线建筑节能科技有限公司 Film coated rock wool board for building curtain wall and preparing method thereof
CN108909066A (en) * 2018-07-11 2018-11-30 苏州福高保温科技有限公司 A kind of preparation method of the high fire line coagulation soil matrix foam heat-insulating board of high-strength light

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101538122A (en) * 2009-04-27 2009-09-23 鞠加会 Hollow-core rock wool and preparation method and applications thereof
CN103086661A (en) * 2011-10-27 2013-05-08 深圳市爱思宝科技发展有限公司 Thermal insulation and heat preservation slurry composition and thermal insulation and heat preservation plate containing the same
CN104496277A (en) * 2014-12-15 2015-04-08 广德施可达岩棉制造有限公司 Novel rock wool material
CN104529175A (en) * 2014-12-15 2015-04-22 广德施可达岩棉制造有限公司 Iron ore-based novel rock wool material

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101538122A (en) * 2009-04-27 2009-09-23 鞠加会 Hollow-core rock wool and preparation method and applications thereof
CN103086661A (en) * 2011-10-27 2013-05-08 深圳市爱思宝科技发展有限公司 Thermal insulation and heat preservation slurry composition and thermal insulation and heat preservation plate containing the same
CN104496277A (en) * 2014-12-15 2015-04-08 广德施可达岩棉制造有限公司 Novel rock wool material
CN104529175A (en) * 2014-12-15 2015-04-22 广德施可达岩棉制造有限公司 Iron ore-based novel rock wool material

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106437064A (en) * 2016-08-28 2017-02-22 山东地平线建筑节能科技有限公司 Film coated rock wool board for building curtain wall and preparing method thereof
CN106437064B (en) * 2016-08-28 2018-10-09 山东地平线建筑节能科技有限公司 A kind of building curtain wall overlay film rock cotton board and preparation method thereof
CN108909066A (en) * 2018-07-11 2018-11-30 苏州福高保温科技有限公司 A kind of preparation method of the high fire line coagulation soil matrix foam heat-insulating board of high-strength light

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