CN105343915B - A kind of natural air cleaning agent and preparation method thereof - Google Patents
A kind of natural air cleaning agent and preparation method thereof Download PDFInfo
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- CN105343915B CN105343915B CN201510777708.2A CN201510777708A CN105343915B CN 105343915 B CN105343915 B CN 105343915B CN 201510777708 A CN201510777708 A CN 201510777708A CN 105343915 B CN105343915 B CN 105343915B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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Abstract
The invention discloses a kind of natural air cleaning agent to be made up of compound essential oil, cosolvent, ethanol, distilled water, and each component is according to compound essential oil：Cosolvent：Ethanol：Distilled water=0.2 1:1‑2:5:15 volume ratio allotment is formed, and the compound essential oil is made up of the component of following parts by weight：10 55 parts of folium artemisiae argyi, 40 100 parts of myrtillin folium, 20 65 parts of tea free, 10 40 parts of lemon peel, 15 60 parts of lavandulae flos.The present invention is for mycotic spore because of the stronger feature of the resistance such as heat-resisting, resistance to drying, a fairly large number of problem in atmosphere be present, based on the extraction and constituent analysis to natural plant essential oils, with reference to the bacteria resistance function analysis to mould, good smell is developed and with air purification function, air freshener that is nontoxic, not adding preservative according to smelling score value, it is significant to improving air ambient, raising people's quality of life.
Description
Technical field
The invention belongs to cleaning agent technical field, and in particular to a kind of natural air cleaning agent and preparation method thereof.
Background technology
With the rapid development of growth and the industry of urban population, motor vehicles surge, pollutant emission and air suspension
Thing rolls up, and the country haze weather occurs again and again, and haze problem is constantly accumulated in China's fast industrialization, urbanization process
Environmental problem concentrated reflection, troubling is the air quality around us, and haze is micro- to virus, bacterium, mould etc.
Biology provides the condition survived in more air, causes because the ill number of air quality problems increases year by year.
Plants essential oil（Essential oils）It is a kind of pure natural botanical extract mixture, chemical composition is more multiple
It is miscellaneous, generally with functional characteristics such as medical value, aromatic odor and antibacterial anti-corrosions.As fruit of a cubeb litsea tree volatile oil can be used for article and residence
Room is mould proof, and volatile argyi leaf oil has certain inhibitory action to Respiratory Syncytial Virus(RSV).The antibacterial action report of plants essential oil is very
It is more, such as tea tree ethereal oil, red bayberry leaf essential oil, lemon, oil of Cymbopogon winterianus, Herba Origani Vulgaris quintessence oil, Artemisia stelleriana essential oil, its antibacterial main matter
Including Multiple components such as 1,8- cineoles, Thymol, cedrol, nerol, neral, citral, citronellols, main suppression
Bacterium and its viruses such as Escherichia coli processed, staphylococcus aureus, beading reaping hook germ, Curvularia mould.Plants essential oil because
Its volatility and bacteriostatic activity, gradually it is developed applied to purification air, such as fruit of a cubeb litsea tree fruit oil with leaf oil as mould inhibitor, to more
Number fungi has inhibitory action and antifungi vigor is stronger, has strong fragrance.The characteristics of using plants essential oil fragrance, sterilization, only
Change air, improve IAQ.The complicated component of plants essential oil, but the composition of most plants essential oil is mainly terpenes
Compound and aromatic compound etc. form, and these compounds have strong fragrance.The spies such as the fragrant, medicinal of essential oil, antibacterial
Property makes it more incorporate among our life.Deposited mostly by the air freshener that main component is developed of plants essential oil at present
When in use, it is necessary to which spraying substantial amounts of air freshener can be only achieved certain effect, due in Modern Family, using wood mostly
Matter furniture, wood floors, spraying substantial amounts of air freshener has certain destruction to this kind of wood furniture, can not be real
Realize the purpose for improving air ambient, improving people's quality of life.
The content of the invention
For problems of the prior art, present invention aims at providing a kind of natural air cleaning agent and its system
Preparation Method.
The present invention is realized by the following technical programs：
A kind of described natural air cleaning agent, it is characterised in that it is made up of compound essential oil, cosolvent, ethanol, distilled water,
Each component is according to compound essential oil：Cosolvent：Ethanol：Distilled water=0.2-1:1-2:5:15 volume ratio allotment forms, the compound
Essential oil is made up of the component of following parts by weight：Folium artemisiae argyi 10-55 parts, myrtillin folium 40-100 parts, tea free 20-65 parts, lemon
Skin 10-40 parts, lavandulae flos 15-60 parts.
A kind of described natural air cleaning agent, it is characterised in that the compound essential oil：Cosolvent：Ethanol：Distilled water
Volume ratio is 0.5:1.5:5:15.
A kind of described natural air cleaning agent, it is characterised in that the compound essential oil by following parts by weight component group
Into：Folium artemisiae argyi 10-55 parts, myrtillin folium 60-100 parts, tea free 20-50 parts, lemon peel 20-40 parts, lavandulae flos 45-60 parts.
A kind of described natural air cleaning agent, it is characterised in that the compound essential oil by following parts by weight component group
Into：55 parts of folium artemisiae argyi, 100 parts of myrtillin folium, 20 parts of tea free, 40 parts of lemon peel, 60 parts of lavandulae flos.
Described a kind of natural air cleaning agent, it is characterised in that the cosolvent is rilanit special PEG-40.
Described a kind of natural air cleaning agent, it is characterised in that the ethanol is full gear ethanol.
The preparation method of described a kind of natural air cleaning agent, it is characterised in that follow these steps to carry out：
1）Formula ratio folium artemisiae argyi 10-55 parts, myrtillin folium 40-100 parts, tea free 20-65 parts, lemon peel 10-40 are taken respectively
Crushed after part, lavandulae flos 15-60 parts are well mixed, be crushed to 100-200 mesh, obtain mixture；
2）By mixture and water in mass ratio：Mixture：Water=1:6 ratio mixing, using steam distillation in 160-
Under the conditions of 170 DEG C of oil baths, distillation extraction 6-8h, compound essential oil is made；
3）By step 2）Obtained compound essential oil is with cosolvent, ethanol, distilled water according to compound essential oil：Cosolvent：Ethanol：
Distilled water=0.2-1:1-2:5:15 volume ratio is allocated, and air freshener is made.
A kind of preparation method of described natural air cleaning agent, it is characterised in that the step 3）Middle compound essential oil：Help
Solvent：Ethanol：Volume ratio=0.5 of distilled water:1.5:5:15.
The present invention for mycotic spore because of the stronger feature of the resistance such as heat-resisting, resistance to drying, exist in atmosphere quantity compared with
The problem of more, based on the extraction and constituent analysis to natural plant essential oils, with reference to the bacteria resistance function analysis to mould, according to smelling
Score value develops good smell and with air purification function, air freshener that is nontoxic, not adding preservative, to improving air ring
Border, raising people's quality of life are significant.
Brief description of the drawings
Fig. 1 is the purification of air result of the test of the air freshener of embodiment 1；
Fig. 2 is the purification of air result of the test of the air freshener of embodiment 2；
Fig. 3 is the purification of air result of the test of the air freshener of embodiment 3；
Fig. 4 is control group result of the test.
Embodiment
By specific examples below, the invention will be further described.
Embodiment 1
A kind of natural air cleaning agent, is made up of compound essential oil, cosolvent, ethanol, distilled water, and each component is according to compound essence
Oil：Cosolvent：Ethanol：Distilled water=0.5:1.5:5:15 volume ratio allotment forms, and wherein compound essential oil is by following parts by weight
Component composition：55 parts of folium artemisiae argyi, 100 parts of myrtillin folium, 20 parts of tea free, 40 parts of lemon peel, 60 parts of lavandulae flos.Cosolvent selects
With rilanit special PEG-40, ethanol is full gear ethanol, and its preparation method is each raw material for weighing above-mentioned formula ratio respectively, will
100-200 mesh is crushed to after raw material mixing, obtains mixture, by mixture and water according to solid-liquid ratio 1：6 ratio mixing, using water
Steam distillation method under the conditions of 160-170 DEG C of oil bath, distillation extraction 6-8h, be made compound essential oil, by obtained compound essential oil with
Rilanit special PEG-40, full gear ethanol, distilled water are according to volume ratio 0.5:1.5:5:15 are allocated, and air cleaner is made
Agent.
Embodiment 2
A kind of natural air cleaning agent, is made up of compound essential oil, cosolvent, ethanol, distilled water, and each component is according to compound essence
Oil：Cosolvent：Ethanol：Distilled water=0.2:2:5:15 volume ratio allotment forms, and wherein compound essential oil is by following parts by weight
Component forms：10 parts of folium artemisiae argyi, 60 parts of myrtillin folium, 50 parts of tea free, 40 parts of lemon peel, 45 parts of lavandulae flos.Cosolvent is selected
Rilanit special PEG-40, ethanol are full gear ethanol, and its preparation method is each raw material for weighing above-mentioned formula ratio respectively, by original
100-200 mesh is crushed to after material mixing, obtains mixture, by mixture and water according to solid-liquid ratio 1：6 ratio mixing, is steamed using water
Under the conditions of 160-170 DEG C of oil bath distillation extraction 6-8h, compound essential oil is made, by obtained compound essential oil and hydrogen in steam distillation method
Change castor oil PEG-40, full gear ethanol, distilled water according to volume ratio 0.2:2:5:15 are allocated, and air freshener is made.
Embodiment 3
A kind of natural air cleaning agent, is made up of compound essential oil, cosolvent, ethanol, distilled water, and each component is according to compound essence
Oil：Cosolvent：Ethanol：Distilled water=1:1:5:15 volume ratio allotment form, wherein compound essential oil by following parts by weight group
It is grouped into：40 parts of folium artemisiae argyi, 100 parts of myrtillin folium, 50 parts of tea free, 20 parts of lemon peel, 15 parts of lavandulae flos.Cosolvent selects hydrogen
Change castor oil PEG-40, ethanol is full gear ethanol, and its preparation method is each raw material for weighing above-mentioned formula ratio respectively, by raw material
100-200 mesh is crushed to after mixing, obtains mixture, by mixture and water according to solid-liquid ratio 1：6 ratio mixing, using vapor
Under the conditions of 160-170 DEG C of oil bath distillation extraction 6-8h, compound essential oil is made, by obtained compound essential oil and hydrogenation in the way of distillation
Castor oil PEG-40, full gear ethanol, distilled water are according to volume ratio:1:1:5:15 are allocated, and air freshener is made.
Experimental example
Crush, myrtillin folium, lavandulae flos, lemon peel, folium artemisiae argyi, tea tree leaf raw material respectively with material-water ratio 1：6 mixing,
160-170 DEG C of oil bath distillation extraction 6-8h, receives essential oil respectively.Essential oil made from each component is passed through after dchloromethane
GC-MS is analyzed, qualitative to volatile ingredient progress using the databases of U.S. NIST ' 98, identifies hill gooseberry, lavender, lemon respectively
The derived essential oils such as lemon, folium artemisiae argyi, tea tree are respectively 32,30,53,113 and 44 kind.Hill gooseberry's essential oil main component be citral and
(E)-citral, both account for 82.8%, and Lavender mainly contains linalyl formate, linalool and camphor, accounts for essential oil total amount
74%, lemon mainly contains limonene, terpinenes, left-handed-beta- firpenes and terpinol, accounts for more than the 90% of essential oil total amount, tea
It is caproic acid, dipentene, trans -2- hexenoic acids, benzylalcohol to set essential oil main component, accounts for more than the 30% of essential oil total amount, P-Cymene
Include binapacryl, eudesmol, 4- isopropenyl toluenes, caryophyllene oxide, diisobutylene methyl carbitol and 3,3,6- front threes
Base-Isosorbide-5-Nitrae-heptadiene -6- alcohol, accounts for the 60% of essential oil total amount.
The bacteriostatic experiment of folk prescription essential oil
1 μ L points are taken to be connected to mould medium the aspergillus niger bacterium solution of activation, per 3 points of ware, by 100 μ L various concentrations essential oils
It is added among culture dish lid, is inverted culture 24h, measures mold colony diameter, is not added with the dimethyl sulfoxide of essential oil as control.By following
Formula calculates bacteriostasis rate
Half-inhibition concentration（EC50）After the bacteriostasis rate matched curve of various concentrations, to try to achieve mould according to every kind of essential oil
50% be suppressed when theoretical essential oil concentration.The fungistatic effect of different essential oils is with half-inhibition concentration（EC50）Evaluated.It is real
Result discovery is tested, different essential oils are lemon to the inhibitory action order of aspergillus niger（0.28%）>Hill gooseberry's essential oil（0.34%）>
Tea tree ethereal oil（0.53%）>P-Cymene（1.22%）>Lavender（1.58%）, it is EC50 values that its bracket is interior；Wherein essential oil
In the compound such as citral, geraniol, limonene, eudesmol and linalool there is bacteriostatic activity effect, lemon, peach
Golden ma's essential oil, tea tree ethereal oil, P-Cymene and Lavender are respectively provided with preferably to Escherichia coli and staphylococcus aureus
Inhibitory action.
The bacteriostatic experiment of compound essential oil
According to lemon, hill gooseberry's essential oil, tea tree ethereal oil, P-Cymene and lavender essence in folk prescription essential oil bacteriostatic test
Oil is to aspergillus niger half-inhibition concentration EC50 measure, with reference to the extraction yield of this several essential oil, is converted into part of raw material respectively
Number, and design orthogonal test L16（4 5）The water-glass of five factor four, be shown in Table 1：
The L16 (4 of table 15) the water-glass of five factor four
Factor level combination in table 1, take respectively the lemon peels of different numbers, myrtillin folium, tea free, folium artemisiae argyi and
Lavandulae flos raw material, crushed after mixing, add material-water ratio（Mass ratio）For 1:6 water, using steam distillation, 160-170
DEG C oil bath distillation extraction 6-8h, the essential oil of acquirement, be diluted to DMSO 1% ratio, with the bacteriostatic experiment side of folk prescription essential oil
Method carries out the antibacterial test of compound essential oil, the results are shown in Table 2.
The mixing compounding orthogonal test of table 2 L16 (45) to mould inhibitory action result
As can be known from Table 2, the obtained essential oil of proportioning combination extraction of different material, it is formulated after air freshener to mould
The inhibitory action of bacterium is widely different, and bacteriostasis rate changes between 30-100% respectively, according to range analysis, wherein to bacteriostasis
The raw material from big to small of influenceing be folium artemisiae argyi（D）>Myrtillin folium（C）>Tea free（A）>Lemon peel（B）>Lavandulae flos（E）, suppression
Bacterium rate has three group of formula more than 90%, is respectively formulated one：D4C4A1B4E4, i.e., when 55 parts of folium artemisiae argyi, 100 parts of myrtillin folium,
20 parts of tea free, 40 parts of lemon peel, 60 parts of lavandulae flos, in the formulated bacteriostasis rate of essential oil that this condition is also extracted up to 100%.Match somebody with somebody
Side two：D1C2A3B4E3, i.e., when 10 parts of folium artemisiae argyi, 60 parts of myrtillin folium, 50 parts of tea free, 40 parts of lemon peel, 45 parts of lavandulae flos,
In the formulated bacteriostasis rate of essential oil that this condition is also extracted up to 98%.Formula three：D3C4A3B2E1, i.e., when 40 parts of folium artemisiae argyi, myrtillin folium
100 parts, 50 parts of tea free, 20 parts of lemon peel, 15 parts of lavandulae flos, reached in the formulated bacteriostasis rate of essential oil that this condition is also extracted
90%。
16 groups of compound essential oils are matched according to orthogonal test, it is sprayed on respectively and heard on fragrant paper, it is random to invite more than 100
Passerby carries out smelling and given a mark by ten point system, evaluates the fragrance preference degree of compound essential oil.2 are the results are shown in Table, as seen from the table, 16 groups
Essential oil is preferably evaluated, and between 8.9-9.3, three assemble the wherein preferable three group of formula preference degree of fungistatic effect
Side is respectively provided with the aromatic odor for gaining universal acceptance, being liked.
The preparation of air freshener and air purification effect
The allotment of air freshener
The good formulas obtained according to orthogonal test in table 2, the i.e. D4C4A1B4E4 of formula one of embodiment 1, embodiment 2
Two D3C4A3B2E1 and the D1C2A3B4E3 of formula three of embodiment 3 are formulated, with essential oil：Cosolvent：Ethanol：Distilled water=0.2-1:
1-2:5:15 ratio allotment, obtains clear, the natural air cleaning agent of good smell.Wherein cosolvent is hydrogenated castor
Oil（PEG-40）, ethanol is full gear ethanol.
Air bells laid method is to Assessment of cleaning efficiency
With reference to the public place air microbe method of inspection（GB/T 182041-2000）, and according to acquisition time and place
Difference improved, establish be adapted to this experiment air bells laid method.By the air freshener of each group allotment respectively according to above-mentioned
The air bells laid method of determination, selects progress in identical (m of 5.0 m × 3.0 × 3.0 m) the students' dormitory room of volume, during experiment
Environment temperature is room temperature, and door and window is closed.Before the spraying of compound essential oil air freshener, first place micro- in culture medium collection air
Biology, acquisition time 2h, as control.After collection sprays compound essential oil air freshener about 5mL, 30min respectively after terminating, open
Culture dish lid gathers microorganism.Every group of experiment is carried out three an equal amount of students' dormitorys, and each dormitory sets 5 samplings
Point.Sampling terminates flat board putting 37 DEG C of insulating box culture 48h, calculates and compares each group colony count, judges compound essential oil air
The power of cleaning agent fungistatic effect, as a result as Figure 1-4.It can be seen that the air cleaner that i.e. embodiment 1 is formulated of formula one
Clean-up effect is best, and mould clearance rate is 89% in air, is secondly the air cleaner purification effect of the i.e. Example formulations of formula two
Fruit, mould clearance rate is 80% in air, is finally the air cleaner clean-up effects that i.e. embodiment 3 is formulated of formula three, mould in air
Bacterium clearance rate is 75%.
Claims (5)
1. a kind of natural air cleaning agent, it is characterised in that be made up of compound essential oil, cosolvent, ethanol, distilled water, each component is pressed
According to compound essential oil：Cosolvent：Ethanol：Distilled water=0.2-1:1-2:5:15 volume ratio allotment form, the compound essential oil by with
The component composition of lower parts by weight：Folium artemisiae argyi 10-55 parts, myrtillin folium 40-100 parts, tea free 20-65 parts, lemon peel 10-40
Part, lavandulae flos 15-60 parts；The cosolvent is rilanit special PEG-40；
Above-mentioned natural air cleaning agent, follows these steps to prepare：
1）Formula ratio folium artemisiae argyi 10-55 parts, myrtillin folium 40-100 parts are taken respectively, tea free 20-65 parts, lemon peel 10-40 parts, are smoked
Crushed after clothing showy flowers of herbaceous plants 15-60 parts are well mixed, be crushed to 100-200 mesh, obtain mixture；
2）By mixture and water in mass ratio：Mixture：Water=1:6 ratio mixing, using steam distillation in 160-170
Under the conditions of DEG C oil bath, distillation extraction 6-8h, compound essential oil is made；
3）By step 2）Obtained compound essential oil is with cosolvent, ethanol, distilled water according to compound essential oil：Cosolvent：Ethanol：Distillation
Water=0.2-1:1-2:5:15 volume ratio is allocated, and air freshener is made.
A kind of 2. natural air cleaning agent according to claim 1, it is characterised in that the compound essential oil：Cosolvent：Second
Alcohol：The volume ratio of distilled water is 0.5:1.5:5:15.
3. a kind of natural air cleaning agent according to claim 1 or 2, it is characterised in that the compound essential oil is by following heavy
Measure the component composition of number：Folium artemisiae argyi 10-55 parts, myrtillin folium 60-100 parts, tea free 20-50 parts, lemon peel 20-40 parts, smoke
Clothing showy flowers of herbaceous plants 45-60 parts.
4. a kind of natural air cleaning agent according to claim 1 or 2, it is characterised in that the compound essential oil is by following heavy
Measure the component composition of number：55 parts of folium artemisiae argyi, 100 parts of myrtillin folium, 20 parts of tea free, 40 parts of lemon peel, 60 parts of lavandulae flos.
5. a kind of natural air cleaning agent according to claim 1 or 2, it is characterised in that the ethanol is full gear ethanol.
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| CN106212462B (en) * | 2016-07-20 | 2018-09-04 | 深圳神农特医食品有限公司 | Herbal mixture air sanitizer and preparation method thereof and application method |
| CN107096367A (en) * | 2017-05-04 | 2017-08-29 | 吴金龙 | Plants essential oil scavenging solution and preparation method thereof |
| CN107158915A (en) * | 2017-06-02 | 2017-09-15 | 叶春枝 | The indoor air purification agent of pure plant extracts |
| CN108371191A (en) * | 2018-04-24 | 2018-08-07 | 纯美生物医药科技（上海）有限公司 | A kind of air antiseptic and its preparation method and application |
| CN109276970A (en) * | 2018-09-30 | 2019-01-29 | 浙江维康日用品有限公司 | A kind of car removes the production of aldehyde lemon charcoal bag |
| CN112107984A (en) * | 2020-09-04 | 2020-12-22 | 中国人民解放军海军特色医学中心 | Plant type sterilization deodorant and preparation method thereof |
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| CN102986526A (en) * | 2011-11-02 | 2013-03-27 | 福建省亚热带植物研究所 | Open-type plant tissue culture method |
| CN102641512B (en) * | 2012-05-04 | 2014-11-12 | 柳州华力家庭品业股份有限公司 | Chinese herbal medicinal formaldehyde and foreign smell removing agent and preparation method thereof |
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