CN105331192A - Water-based ink preparation and preparation method thereof - Google Patents
Water-based ink preparation and preparation method thereof Download PDFInfo
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- CN105331192A CN105331192A CN201510920424.4A CN201510920424A CN105331192A CN 105331192 A CN105331192 A CN 105331192A CN 201510920424 A CN201510920424 A CN 201510920424A CN 105331192 A CN105331192 A CN 105331192A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/14—Printing inks based on carbohydrates
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention provides a water-based ink preparation and a preparation method thereof. The ink preparation is prepared from acrylic resin, carboxymethyl cellulose, butyl hydroxy anisd, triethanolamine, potassium sorbate, stearamide, pentaerythritol, starch, polyoxyethylene polyoxy propanol amidogen ether, linoleic acid, dye, ethanol and water. The preparation method of the water-based ink preparation comprises the steps of firstly, mixing all components at the normal temperature, stirring the components for 20-30 minutes through a high speed dispersion machine at the rotating speed of 6000-9000 rpm, obtaining dispersed color paste, then pouring the color paste into a sand mill, putting a certain number of glass balls therein at the same time, conducting milling for 5-7 hours, conducting filtration and package, and obtaining the water-based ink preparation. The ink preparation has a good dyeing property, and the defect that ink preparations on the market which take acrylic resin as the base material are poor in drying property can be made up; the heat resistance is good; the ink preparation can be dried quickly; the fineness also reaches the national standard range; the production process is simple, and the ink preparation is suitable for industrialized production.
Description
Technical field
The present invention relates to chemistry painting industry field, be specifically related to a kind of water color ink preparation and preparation method thereof.
Background technology
Along with the development of modern economy society, the development of press also more and more receives publicity, and becomes one of measurement industrialization of the country, modern mark gradually.Meanwhile, solvent type ink has also become larger source of pollution owing to having volatile solvent etc.; On the other hand, along with the rising of material cost, its cost also further increases.In this case, can protection of the environment, the water color ink economized on resources arises at the historic moment, and has become an important directions of nowadays ink industry development.Water color ink also claims water-based inks, is take water as primary solvent, floods a kind of printing-ink processed by the water base binder of aqueous high molecular compound formation and dye well related auxiliaries through composite.Water color ink is owing to taking water as primary solvent, therefore price is well below other ink, and it is hardly containing volatile organic compounds simultaneously, environmentally safe; Also ensure that the health of user.
Summary of the invention
the technical problem solved:the object of this invention is to provide a kind of coloring effect good; Resistance toheat is good; Can rapid drying; Stability is good; Fineness is also up to state standards the water color ink preparation of scope.
technical scheme:a kind of water color ink preparation, comprises with parts by weight: acrylic resin 15-25 part, carboxymethyl cellulose 10-20 part, butylated hydroxy anisole 0.5-1 part, trolamine 5-10 part, potassium sorbate 0.1-0.2 part, stearylamide 0.5-1 part, tetramethylolmethane 0.5-1 part, starch 1-2 part, polyoxyethylene polyoxy propyl alcohol amidogen ether 0.5-1 part, linolic acid 0.1-0.2 part, dyestuff 10-20 part, ethanol 5-15 part, water 15-25 part.
Preferred further, described a kind of water color ink preparation, comprises with parts by weight: acrylic resin 18-23 part, carboxymethyl cellulose 12-28 part, butylated hydroxy anisole 0.7-0.9 part, trolamine 6-8 part, potassium sorbate 0.13-0.18 part, stearylamide 0.6-0.9 part, tetramethylolmethane 0.7-0.9 part, starch 1.3-1.8 part, polyoxyethylene polyoxy propyl alcohol amidogen ether 0.6-0.9 part, linolic acid 0.13-0.18 part, dyestuff 12-18 part, ethanol 8-13 part, water 18-23 part.
The preparation method of above-mentioned water color ink preparation comprises the following steps:
Step 1: mixed at normal temperatures by all components, stirs 20-30 minute by high speed dispersor under rotating speed 6000-9000rpm, obtains the mill base of dispersion;
Step 2: poured into by mill base in sand mill, puts into a certain amount of glass sphere simultaneously, and grinding 5-7 hour, filters and packages and get final product.
Preferred further, step 1 medium speed is 7000-8000rpm, and churning time is 23-28 minute.
Preferred further, in step 2, milling time is 5.5-6.5 hour.
beneficial effect:water color ink preparation of the present invention has good tint permanence, and compensate for a lot on the market take acrylic resin as the defect of the tinting strength difference of the ink formulations of base-material; Heat resisting temperature can reach 180 DEG C, and range of application can increase greatly; First dryness is the highest also reaches 25mm/30s, can rapid drying; Fineness is also up to state standards scope, and the stability of ink is also better.
Embodiment
Embodiment 1
A kind of water color ink preparation, comprises with parts by weight: acrylic resin 15 parts, carboxymethyl cellulose 10 parts, butylated hydroxy anisole 0.5 part, trolamine 5 parts, potassium sorbate 0.1 part, stearylamide 0.5 part, tetramethylolmethane 0.5 part, starch 1 part, polyoxyethylene polyoxy propyl alcohol amidogen ether 0.5 part, linolic acid 0.1 part, dyestuff 10 parts, ethanol 5 parts, 15 parts, water.
The preparation method of above-mentioned water color ink preparation is: first mixed at normal temperatures by all components, stirred 20 minutes for 6000 times at rotating speed by high speed dispersor, the mill base that must disperse, then mill base is poured in sand mill, put into a certain amount of glass sphere simultaneously, grind 5 hours, filter and package and obtain the present invention.
Embodiment 2
A kind of water color ink preparation, comprises with parts by weight: acrylic resin 18 parts, carboxymethyl cellulose 12 parts, butylated hydroxy anisole 0.7 part, trolamine 6 parts, potassium sorbate 0.13 part, stearylamide 0.6 part, tetramethylolmethane 0.7 part, starch 1.3 parts, polyoxyethylene polyoxy propyl alcohol amidogen ether 0.6 part, linolic acid 0.13 part, dyestuff 12 parts, ethanol 8 parts, 18 parts, water.
The preparation method of above-mentioned water color ink preparation is: first mixed at normal temperatures by all components, stirred 23 minutes under rotating speed 7000rpm by high speed dispersor, the mill base that must disperse, then mill base is poured in sand mill, put into a certain amount of glass sphere simultaneously, grind 5.5 hours, filter and package and obtain the present invention.
Embodiment 3
A kind of water color ink preparation, comprises with parts by weight: acrylic resin 20 parts, carboxymethyl cellulose 15 parts, butylated hydroxy anisole 0.7 part, trolamine 7 parts, potassium sorbate 0.15 part, stearylamide 0.8 part, tetramethylolmethane 0.8 part, starch 1.5 parts, polyoxyethylene polyoxy propyl alcohol amidogen ether 0.7 part, linolic acid 0.15 part, dyestuff 15 parts, ethanol 10 parts, 20 parts, water.
The preparation method of above-mentioned water color ink preparation is: first mixed at normal temperatures by all components, stirred 25 minutes under rotating speed 7500rpm by high speed dispersor, the mill base that must disperse, then mill base is poured in sand mill, put into a certain amount of glass sphere simultaneously, grind 6 hours, filter and package and obtain the present invention.
Embodiment 4
A kind of water color ink preparation, comprises with parts by weight: acrylic resin 23 parts, carboxymethyl cellulose 28 parts, butylated hydroxy anisole 0.9 part, trolamine 8 parts, potassium sorbate 0.18 part, stearylamide 0.9 part, tetramethylolmethane 0.9 part, starch 1.8 parts, polyoxyethylene polyoxy propyl alcohol amidogen ether 0.9 part, linolic acid 0.18 part, dyestuff 18 parts, ethanol 13 parts, 23 parts, water.
The preparation method of above-mentioned water color ink preparation is: first mixed at normal temperatures by all components, stirred 28 minutes under rotating speed 8000rpm by high speed dispersor, the mill base that must disperse, then mill base is poured in sand mill, put into a certain amount of glass sphere simultaneously, grind 6.5 hours, filter and package and obtain the present invention.
Embodiment 5
A kind of water color ink preparation, comprises with parts by weight: acrylic resin 25 parts, carboxymethyl cellulose 20 parts, butylated hydroxy anisole 1 part, trolamine 10 parts, potassium sorbate 0.2 part, stearylamide 1 part, tetramethylolmethane 1 part, starch 2 parts, polyoxyethylene polyoxy propyl alcohol amidogen ether 1 part, linolic acid 0.2 part, dyestuff 20 parts, ethanol 15 parts, 25 parts, water.
The preparation method of above-mentioned water color ink preparation is: first mixed at normal temperatures by all components, stirred 30 minutes under rotating speed 9000rpm by high speed dispersor, the mill base that must disperse, then mill base is poured in sand mill, put into a certain amount of glass sphere simultaneously, grind 7 hours, filter and package and obtain the present invention.
Comparative example 1
The difference of the present embodiment and embodiment 5 is not containing stearylamide.Specifically:
A kind of water color ink preparation, comprises with parts by weight: acrylic resin 25 parts, carboxymethyl cellulose 20 parts, butylated hydroxy anisole 1 part, trolamine 10 parts, potassium sorbate 0.2 part, tetramethylolmethane 1 part, starch 2 parts, polyoxyethylene polyoxy propyl alcohol amidogen ether 1 part, linolic acid 0.2 part, dyestuff 20 parts, ethanol 15 parts, 25 parts, water.
The preparation method of above-mentioned water color ink preparation is: first mixed at normal temperatures by all components, stirred 30 minutes under rotating speed 9000rpm by high speed dispersor, the mill base that must disperse, then mill base is poured in sand mill, put into a certain amount of glass sphere simultaneously, grind 7 hours, filter and package and obtain the present invention.
Comparative example 2
The difference of the present embodiment and embodiment 5 is, not containing carboxymethyl cellulose, to replace with acrylic resin.Specifically:
A kind of water color ink preparation, comprises with parts by weight: acrylic resin 45 parts, butylated hydroxy anisole 1 part, trolamine 10 parts, potassium sorbate 0.2 part, stearylamide 1 part, tetramethylolmethane 1 part, starch 2 parts, polyoxyethylene polyoxy propyl alcohol amidogen ether 1 part, linolic acid 0.2 part, dyestuff 20 parts, ethanol 15 parts, 25 parts, water.
The preparation method of above-mentioned water color ink preparation is: first mixed at normal temperatures by all components, stirred 30 minutes under rotating speed 9000rpm by high speed dispersor, the mill base that must disperse, then mill base is poured in sand mill, put into a certain amount of glass sphere simultaneously, grind 7 hours, filter and package and obtain the present invention.
Each embodiment and comparative example are compared, comparing result is as following table 1:
The performance index of table 1 water color ink preparation
| Name of product | Tinting strength (%, standard specimen is 90-110) | Fineness (μm) | Heat resisting temperature (DEG C) | First dryness (mm/30s) |
| Embodiment 1 | 101 | 7 | 173 | 22.5 |
| Embodiment 2 | 101 | 7 | 175 | 23.5 |
| Embodiment 3 | 102 | 7 | 176 | 24 |
| Embodiment 4 | 105 | 7 | 180 | 25 |
| Embodiment 5 | 104 | 7 | 177 | 24.5 |
| Reference examples 1 | 91 | 7 | 177 | 20.5 |
| Reference examples 2 | 84 | 7 | 152 | 24 |
As known from Table 1, the tinting strength of embodiment 1-5 is fine, close with mark product; Heat resisting temperature can reach 180 DEG C, can expand its range of application; First dryness is the highest also reaches 25mm/30s, can rapid drying; Fineness is also up to state standards scope.Compare with comparative example 1, find comparative example 1 tint permanence and first dryness all poor, may be because stearylamide can improve its tinting strength and first dryness as tensio-active agent.Compare with comparative example 2, find that the tinting strength of comparative example 2 and heat resisting temperature are significantly less than embodiment, illustrate that the effect after acrylic resin and carboxymethyl cellulose compound is compared to independent acrylic resin, product better effects if.In addition, the property indices of the ink formulations of embodiment 4 gained is all best, is optimum embodiment of the present invention.
Claims (6)
1. a water color ink preparation, is characterized in that: comprise with parts by weight: acrylic resin 15-25 part, carboxymethyl cellulose 10-20 part, butylated hydroxy anisole 0.5-1 part, trolamine 5-10 part, potassium sorbate 0.1-0.2 part, stearylamide 0.5-1 part, tetramethylolmethane 0.5-1 part, starch 1-2 part, polyoxyethylene polyoxy propyl alcohol amidogen ether 0.5-1 part, linolic acid 0.1-0.2 part, dyestuff 10-20 part, ethanol 5-15 part, water 15-25 part.
2. a kind of water color ink preparation according to claim 1, is characterized in that: comprise with parts by weight: acrylic resin 18-23 part, carboxymethyl cellulose 12-28 part, butylated hydroxy anisole 0.7-0.9 part, trolamine 6-8 part, potassium sorbate 0.13-0.18 part, stearylamide 0.6-0.9 part, tetramethylolmethane 0.7-0.9 part, starch 1.3-1.8 part, polyoxyethylene polyoxy propyl alcohol amidogen ether 0.6-0.9 part, linolic acid 0.13-0.18 part, dyestuff 12-18 part, ethanol 8-13 part, water 18-23 part.
3. a kind of water color ink preparation as claimed in claim 1, is characterized in that: described granules of pigments degree area requirement is at 10-25 μm.
4. the preparation method of a kind of water color ink preparation described in any one of claim 1 to 2, is characterized in that: comprise the following steps:
Step 1: mixed at normal temperatures by all components, stirs 20-30 minute by high speed dispersor under rotating speed 6000-9000rpm, obtains the mill base of dispersion;
Step 2: poured into by mill base in sand mill, puts into a certain amount of glass sphere simultaneously, and grinding 5-7 hour, filters and packages and get final product.
5. the preparation method of a kind of water color ink preparation according to claim 4, it is characterized in that: described step 1 medium speed is 7000-8000rpm, churning time is 23-28 minute.
6. the preparation method of a kind of water color ink preparation according to claim 4, is characterized in that: in described step 2, milling time is 5.5-6.5 hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510920424.4A CN105331192A (en) | 2015-12-14 | 2015-12-14 | Water-based ink preparation and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510920424.4A CN105331192A (en) | 2015-12-14 | 2015-12-14 | Water-based ink preparation and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105331192A true CN105331192A (en) | 2016-02-17 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510920424.4A Pending CN105331192A (en) | 2015-12-14 | 2015-12-14 | Water-based ink preparation and preparation method thereof |
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| CN (1) | CN105331192A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1860193A (en) * | 2003-09-30 | 2006-11-08 | 理想科学工业株式会社 | Aqueous ink for mimeograph printing and method for mimeograph printing |
| CN101024747A (en) * | 2006-02-21 | 2007-08-29 | 东北理光株式会社 | Oil-drip type emulsification ink for silk screen printing |
-
2015
- 2015-12-14 CN CN201510920424.4A patent/CN105331192A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1860193A (en) * | 2003-09-30 | 2006-11-08 | 理想科学工业株式会社 | Aqueous ink for mimeograph printing and method for mimeograph printing |
| CN101024747A (en) * | 2006-02-21 | 2007-08-29 | 东北理光株式会社 | Oil-drip type emulsification ink for silk screen printing |
Non-Patent Citations (1)
| Title |
|---|
| 赵秀萍等: "《现代包装设计与印刷》", 29 February 2004, 化学工业出版社 * |
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Application publication date: 20160217 |
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