CN105330257A - Ceramic tile manufactured by waste and manufacturing method - Google Patents
Ceramic tile manufactured by waste and manufacturing method Download PDFInfo
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- CN105330257A CN105330257A CN201510884323.6A CN201510884323A CN105330257A CN 105330257 A CN105330257 A CN 105330257A CN 201510884323 A CN201510884323 A CN 201510884323A CN 105330257 A CN105330257 A CN 105330257A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
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Abstract
The invention discloses a ceramic tile manufactured by waste. The ceramic tile is prepared from, by mass, 25-30% of porcelain clay, 15-20% of mountain flour, 14-22% of sodium sand, 5-10% of potassium sand, 10-20% of high alumina sand, 2-3% of talc mud and 5-15% of recycling mud. The recycling mud is formed by smashing and mixing green bricks, edging waste residues, filter cakes of sewage treatment tanks and ditch sludge. The invention further provides a manufacturing method of the ceramic brick. The problem that waste of a ceramic plant is hard to dispose is solved, raw material waste is reduced, the production cost is saved, and the physical and chemical properties of the produced ceramic brick are excellent.
Description
Technical field
The invention belongs to technical field of ceramic production, relate to a kind of pottery and preparation method thereof, relate in particular to a kind of ceramic tile utilizing waste material to prepare and preparation method thereof.
Background technology
Pottery is for main raw material with natural clay and various natural mineral, through pulverizing the various goods of mixing, shaping and that calcining is obtained various materials, the generation of ceramic making skill can trace back to B.C. 4500 to B.C. 2500, along with the development of science and technology in modern age, many ceramic kinds are newly there is again in the last hundred years, in the course that pottery develops rapidly, create some problems gradually, namely ceramic industry waste material is increasing, not only cause immense pressure to environment, also limit the development of urban economy and the Sustainable development of ceramic industry.
Ceramic waste material is mainly from the waste material owing to producing in shaping, dry, glazing, carrying, roasting and storage procedure in Ceramic Production process, the mode of ceramic waste material by simple landfill normally solves by existing processing mode, or be used to landfill gully, roadbed etc., even be poured directly into the places such as roadside, farmland, rivers and canals, because ceramic waste material cannot be degraded, again containing chemical substance in waste material, pollute the physical environment such as soil, air on the contrary.And, ceramic raw material is a kind of non-renewable resource, under nearly more than ten years pottery production capacity significantly expands, storage capacity is close to exhaustion, therefore the scrap feed material produced in Production of Ceramics how is made full use of, economize on resources, cut the waste, from the generation of source abatement pollutent, it is present stage problem demanding prompt solution.
Summary of the invention
For this reason, technical problem to be solved by this invention is in existing Production of Ceramics, produce a large amount of ceramic waste material, directly bury and waste resource contaminate environment again, thus propose a kind ofly reduce the wasting of resources and be beneficial to the ceramic tile utilizing waste material to prepare and the preparation method of Sustainable development.
For solving the problems of the technologies described above, technical scheme of the present invention is:
The invention provides a kind of ceramic tile utilizing waste material to prepare, by percentage to the quality, it is composed of the following components: china clay 25-35%, stone flour 15-20%, sodium sand 14-22%, potassium sand 5-10%, high alumina sand 10-20%, talcum mud 2-3%, reclaims mud 5-15%; Described recovery mud is obtained through being pulverized and mixed by adobe, edging waste residue, treatment tank press cake and ditch mud.
As preferably, by percentage to the quality, described ceramic tile is composed of the following components: china clay 30%, stone flour 18%, sodium sand 18%, potassium sand 6%, high alumina sand 15%, talcum mud 3%, reclaims mud 10%.
As preferably, in described recovery mud, the mass percent of described adobe is 25-60%, the mass percent of described edging waste residue is 15-30%, the mass percent of described treatment tank press cake is 10-50%, and the mass percent of described ditch mud is 5-15%.
As preferably, in described recovery mud, the mass percent of described adobe is 40%, and the mass percent of described edging waste material is 20%, and the mass percent of described treatment tank press cake is 30%, and the mass percent of described ditch mud is 10%.
As preferably, described adobe is the green compact become into klining.
The present invention also provides a kind of method preparing described ceramic tile, comprises the steps:
S1, described recovery mud and described china clay, stone flour, sodium sand, potassium sand, high alumina sand and talcum mud are mixed into preparing material;
S2, described preparing material is added water for ball milling become preparation slurry, described preparation slurry is sieved screening deironing;
S3, the described preparation slurry after deironing in described step S2 is carried out mist projection granulating, obtain preparing powder, make described preparation powder water ratio be 6.8-7.2%; The temperature of mist projection granulating is 620-650 DEG C, and the sands are running out was in 30 seconds;
S4, by old at least 24 hours of described preparation powder;
S5, cloth compression moulding;
S6, glazing stamp;
S7, to burn till, obtain finished product ceramic tile; Firing period 55-60min, firing temperature 1190-1210 DEG C.
As preferably, in described step S2 in mechanical milling process, the mass ratio of described preparing material and ballstone, water is: preparing material: ballstone: water=1:1.5:0.5, Ball-milling Time 12-13h; The fineness of the described preparation slurry obtained after ball milling is 1.8-2.2%, and flow velocity is 30-50m/s, and density is 1.70-1.75g/cm
3.
As preferably, the particle weight in step S3 after mist projection granulating than grating is:
Wherein prepare described in 40 objects and prepare powder sum described in powder and 60 objects and be greater than 80%.
As preferably, the pressure suppressed in described step S5 is 170-190bar; Burn till in described step S7 and carry out under oxidizing atmosphere.
As preferably, add water for ball milling in described step S2 and adopt 60T ball mill; Described double-deck screen shale shaker at the middle and upper levels screen-aperture is 60 orders, and lower floor's screen-aperture is 50 orders; Described deironing adopts 30 10000 Gauss's iron removing sticks to carry out.
Technique scheme of the present invention has the following advantages compared to existing technology: the ceramic tile utilizing waste material to prepare of the present invention, composed of the following components: china clay 25-35%, stone flour 15-20%, sodium sand 14-22%, potassium sand 5-10%, high alumina sand 10-20%, talcum mud 2-3%, reclaim mud 5-15%; Described recovery mud is obtained through being pulverized and mixed by adobe, edging waste residue, treatment tank press cake and ditch mud.The adobe produced in Production of Ceramics process, edging waste residue, treatment tank press cake and ditch biosolid waste are used as the raw materials for production of pottery by the present invention, solve the reluctant problem of pot bank's waste material, decrease wastage of material, save production cost, the ceramic tile goods high specific surface area of producing, can be used for making porcelain Antique Imitation Tiles.
In order to make content of the present invention be more likely to be clearly understood, the present invention is further detailed explanation according to a particular embodiment of the invention below.
Embodiment
Embodiment 1
The present embodiment provides a kind of ceramic tile utilizing waste material to prepare, by percentage to the quality, composed of the following components: china clay 30%, stone flour 18%, sodium sand 18%, potassium sand 6%, high alumina sand 15%, talcum mud 3%, reclaims mud 10%.Wherein, described recovery mud is obtained through being pulverized and mixed by adobe, edging waste residue, treatment tank press cake and ditch mud, be specially: in described recovery mud, the mass percent of described adobe is 40%, the mass percent of described edging waste material is 20%, the mass percent of described treatment tank press cake is 30%, and the mass percent of described ditch mud is 10%, and described adobe is the green compact become into klining.
The present embodiment additionally provides a kind of method preparing described ceramic tile, and it comprises the steps:
S1, described recovery mud and described china clay, stone flour, sodium sand, potassium sand, high alumina sand and talcum mud are mixed into preparing material according to aforementioned proportion;
S2, the ball milling in 60T ball mill that described preparing material to be added water become preparation slurry, in mechanical milling process, the mass ratio of preparing material and ballstone, water is: preparing material: ballstone: water=1:1.5:0.5, Ball-milling Time is 12.5h, the fineness of the preparation slurry obtained after ball milling is 2%, flow velocity is 40m/s, and density is 1.725g/cm
3, then described preparation slurry is crossed double-deck screen shale shaker and deironing, described double-deck screen shale shaker at the middle and upper levels screen-aperture is 60 orders, and lower floor's screen-aperture is 50 orders; Described deironing adopts the iron removing stick of 30 10000 Gausses to carry out;
S3, the described preparation slurry after deironing in described step S2 is carried out mist projection granulating in sponging granulator, obtain the preparation powder that water ratio is 7%; After mist projection granulating, particle weight in the preparation powder obtained
S4, described preparation powder to be put in feed bin old 30 hours;
S5, the preparation powder after old to be distributed in the mould of ceramic press and compression moulding;
S6, according to demand glazing stamp;
S7, in kiln, at 1200 DEG C, burn till 58min, obtain finished product ceramic tile.
Embodiment 2
The present embodiment provides a kind of ceramic tile utilizing waste material to prepare, by percentage to the quality, composed of the following components: china clay 28%, stone flour 20%, sodium sand 14%, potassium sand 10%, high alumina sand 10%, talcum mud 3%, reclaims mud 15%.Wherein, described recovery mud is obtained through being pulverized and mixed by adobe, edging waste residue, treatment tank press cake and ditch mud, be specially: in described recovery mud, the mass percent of described adobe is 25%, the mass percent of described edging waste material is 30%, the mass percent of described treatment tank press cake is 30%, and the mass percent of described ditch mud is 15%, and described adobe is the green compact become into klining.
The present embodiment additionally provides a kind of method preparing described ceramic tile, and it comprises the steps:
S1, described recovery mud and described china clay, stone flour, sodium sand, potassium sand, high alumina sand and talcum mud are mixed into preparing material according to aforementioned proportion;
S2, the ball milling in 60T ball mill that described preparing material to be added water become preparation slurry, in mechanical milling process, the mass ratio of preparing material and ballstone, water is: preparing material: ballstone: water=1:1.5:0.5, Ball-milling Time is 12h, the fineness of the preparation slurry obtained after ball milling is 1.8%, flow velocity is 30m/s, and density is 1.70g/cm
3, then described preparation slurry is crossed double-deck screen shale shaker and deironing, described double-deck screen shale shaker at the middle and upper levels screen-aperture is 60 orders, and lower floor's screen-aperture is 50 orders; Described deironing adopts the iron removing stick of 30 10000 Gausses to carry out;
S3, the described preparation slurry after deironing in described step S2 is carried out mist projection granulating in sponging granulator, obtain the preparation powder that water ratio is 6.8%; After mist projection granulating, particle weight in the preparation powder obtained
S4, described preparation powder to be put in feed bin old 24 hours;
S5, the preparation powder after old to be distributed in the mould of ceramic press and compression moulding;
S6, according to demand glazing stamp;
S7, in kiln, at 1190 DEG C, burn till 55min, obtain finished product ceramic tile.
Embodiment 3
The present embodiment provides a kind of ceramic tile utilizing waste material to prepare, by percentage to the quality, composed of the following components: china clay 35%, stone flour 15%, sodium sand 14%, potassium sand 5%, high alumina sand 20%, talcum mud 2%, reclaims mud 9%.Wherein, described recovery mud is obtained through being pulverized and mixed by adobe, edging waste residue, treatment tank press cake and ditch mud, be specially: in described recovery mud, the mass percent of described adobe is 40%, the mass percent of described edging waste material is 20%, the mass percent of described treatment tank press cake is 30%, and the mass percent of described ditch mud is 10%, and described adobe is the green compact become into klining.
The present embodiment additionally provides a kind of method preparing described ceramic tile, and it comprises the steps:
S1, described recovery mud and described china clay, stone flour, sodium sand, potassium sand, high alumina sand and talcum mud are mixed into preparing material according to aforementioned proportion;
S2, the ball milling in 60T ball mill that described preparing material to be added water become preparation slurry, in mechanical milling process, the mass ratio of preparing material and ballstone, water is: preparing material: ballstone: water=1:1.5:0.5, Ball-milling Time is 13h, the fineness of the preparation slurry obtained after ball milling is 2.2%, flow velocity is 50m/s, and density is 1.75g/cm
3, then described preparation slurry is crossed double-deck screen shale shaker and deironing, described double-deck screen shale shaker at the middle and upper levels screen-aperture is 60 orders, and lower floor's screen-aperture is 50 orders; Described deironing adopts the iron removing stick of 30 10000 Gausses to carry out;
S3, the described preparation slurry after deironing in described step S2 is carried out mist projection granulating in sponging granulator, obtain the preparation powder that water ratio is 7.2%; After mist projection granulating, particle weight in the preparation powder obtained
S4, described preparation powder to be put in feed bin old 48 hours;
S5, the preparation powder after old to be distributed in the mould of ceramic press and compression moulding;
S6, according to demand glazing stamp;
S7, in kiln, at 1210 DEG C, burn till 55min, obtain finished product ceramic tile.
Embodiment 4
The present embodiment provides a kind of ceramic tile utilizing waste material to prepare, by percentage to the quality, composed of the following components: china clay 25%, stone flour 18%, sodium sand 22%, potassium sand 8%, high alumina sand 19%, talcum mud 3%, reclaims mud 5%.Wherein, described recovery mud is obtained through being pulverized and mixed by adobe, edging waste residue, treatment tank press cake and ditch mud, be specially: in described recovery mud, the mass percent of described adobe is 50%, the mass percent of described edging waste material is 18%, the mass percent of described treatment tank press cake is 20%, and the mass percent of described ditch mud is 12%, and described adobe is the green compact become into klining.
The present embodiment additionally provides a kind of method preparing described ceramic tile, and it comprises the steps:
S1, described recovery mud and described china clay, stone flour, sodium sand, potassium sand, high alumina sand and talcum mud are mixed into preparing material according to aforementioned proportion;
S2, the ball milling in 60T ball mill that described preparing material to be added water become preparation slurry, in mechanical milling process, the mass ratio of preparing material and ballstone, water is: preparing material: ballstone: water=1:1.5:0.5, Ball-milling Time is 12.5h, the fineness of the preparation slurry obtained after ball milling is 1.9%, flow velocity is 45m/s, and density is 1.73g/cm
3, then described preparation slurry is crossed double-deck screen shale shaker and deironing, described double-deck screen shale shaker at the middle and upper levels screen-aperture is 60 orders, and lower floor's screen-aperture is 50 orders; Described deironing adopts the iron removing stick of 30 10000 Gausses to carry out;
S3, the described preparation slurry after deironing in described step S2 is carried out mist projection granulating in sponging granulator, obtain the preparation powder that water ratio is 7%; After mist projection granulating, particle weight in the preparation powder obtained
S4, described preparation powder to be put in feed bin old 24 hours;
S5, the preparation powder after old to be distributed in the mould of ceramic press and compression moulding;
S6, according to demand glazing stamp;
S7, in kiln, at 1210 DEG C, burn till 55min, obtain finished product ceramic tile.
Experimental example
Detect the ceramic tile character utilizing waste material to prepare described in embodiment 1-4 according to standard GB/T/T4100-2006, result is as shown in table 1:
Table 1
| Water-intake rate (%) | Strength at break (N) | The modulus of rupture (MPa) | Stain resistance | Angularity (%) |
| 0.39 | 1435 | 36 | 5 grades | ±0.03 |
The above results shows, the ceramic brick surface utilizing waste material to prepare of the present invention is smooth, water-intake rate is low, intensity is high, easy fracture, stain resistance are not good, physico-chemical property is excellent, and the adobe produced in Production of Ceramics process, edging waste residue, treatment tank press cake and ditch biosolid waste are used as the raw materials for production of pottery, solve the reluctant problem of pot bank's waste material, decrease wastage of material, save production cost.
Obviously, above-described embodiment is only for clearly example being described, and the restriction not to embodiment.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here exhaustive without the need to also giving all embodiments.And thus the apparent change of extending out or variation be still among the protection domain of the invention.
Claims (10)
1. the ceramic tile utilizing waste material to prepare, is characterized in that, by percentage to the quality, composed of the following components: china clay 25-35%, stone flour 15-20%, sodium sand 14-22%, potassium sand 5-10%, high alumina sand 10-20%, talcum mud 2-3%, reclaims mud 5-15%; Described recovery mud is obtained through being pulverized and mixed by adobe, edging waste residue, treatment tank press cake and ditch mud.
2. the ceramic tile utilizing waste material to prepare according to claim 1, is characterized in that, by percentage to the quality, composed of the following components: china clay 30%, stone flour 18%, sodium sand 18%, potassium sand 6%, high alumina sand 15%, talcum mud 3%, reclaims mud 10%.
3. the ceramic tile utilizing waste material to prepare according to claim 1 and 2, it is characterized in that, in described recovery mud, the mass percent of described adobe is 25-60%, the mass percent of described edging waste residue is 15-30%, the mass percent of described treatment tank press cake is 10-50%, and the mass percent of described ditch mud is 5-15%.
4. the ceramic tile utilizing waste material to prepare according to claim 3, it is characterized in that, in described recovery mud, the mass percent of described adobe is 40%, the mass percent of described edging waste material is 20%, the mass percent of described treatment tank press cake is 30%, and the mass percent of described ditch mud is 10%.
5. the ceramic tile utilizing waste material to prepare according to claim 4, is characterized in that, described adobe is the green compact become into klining.
6. prepare a method for the ceramic tile described in any one of claim 1-5, it is characterized in that, comprise the steps:
S1, described recovery mud and described china clay, stone flour, sodium sand, potassium sand, high alumina sand and talcum mud are mixed into preparing material;
S2, described preparing material is added water for ball milling become preparation slurry, described preparation slurry is sieved screening deironing;
S3, the described preparation slurry after deironing in described step S2 is carried out mist projection granulating, obtain preparing powder; Described preparation powder water ratio is made to be 6.8-7.2%; The temperature of mist projection granulating is 620-650 DEG C, and the sands are running out was in 30 seconds;
S4, by old at least 24 hours of described preparation powder;
S5, cloth compression moulding;
S6, glazing stamp;
S7, to burn till, obtain finished product ceramic tile; Firing period 55-60min, firing temperature 1190-1210 DEG C.
7. the preparation method of ceramic tile according to claim 6, is characterized in that, in described step S2 in mechanical milling process, the mass ratio of described preparing material and ballstone, water is: preparing material: ballstone: water=1:1.5:0.5, Ball-milling Time 12-13h; The fineness of the described preparation slurry obtained after ball milling is 1.8-2.2%, and flow velocity is 30-50m/s, and density is 1.70-1.75g/cm
3.
8. the preparation method of ceramic tile according to claim 7, is characterized in that, the particle weight in step S3 after mist projection granulating than grating is:
Wherein prepare described in 40 objects and prepare powder sum described in powder and 60 objects and be greater than 80%.
9. the preparation method of ceramic tile according to claim 8, is characterized in that, the pressure suppressed in described step S5 is 170-190bar; Burn till in step S7 and carry out under oxidizing atmosphere.
10. the preparation method of the ceramic tile according to any one of claim 6-9, is characterized in that: add water for ball milling in described step S2 and adopt 60T ballstone machine; The described employing double-deck screen shale shaker that sieves, wherein upper strata screen-aperture is 60 orders, and lower floor's screen-aperture is 50 orders; Described deironing adopts 30 10000 Gauss's iron removing sticks to carry out.
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| CN110950638A (en) * | 2019-12-31 | 2020-04-03 | 淄博金卡陶瓷有限公司 | Process for producing porcelain archaized brick from red mud |
| CN111777404A (en) * | 2020-06-16 | 2020-10-16 | 日昌升建筑新材料设计研究院有限公司 | Filter cake brick making process |
| CN111763072A (en) * | 2020-07-17 | 2020-10-13 | 佛山市品为先陶瓷有限公司 | Metallic ceramic tile and preparation method thereof |
| CN112430065A (en) * | 2020-12-01 | 2021-03-02 | 湖南宏康陶瓷有限公司 | Ceramic tile edge grinding slurry material and waste leftover material recycling production process |
| CN115504766A (en) * | 2022-08-05 | 2022-12-23 | 醴陵陶润实业发展有限公司 | Formula of recyclable ceramic and manufacturing method thereof |
| CN116425511A (en) * | 2023-06-07 | 2023-07-14 | 新明珠集团股份有限公司 | Composition for preparing ceramic green body, skin glazed ceramic tile and preparation method of ceramic green body |
| CN116425511B (en) * | 2023-06-07 | 2023-08-29 | 新明珠集团股份有限公司 | Composition for preparing ceramic green body, skin glazed ceramic tile and preparation method of ceramic green body |
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