CN105315570B - A kind of ancient painted pottery mud and preparation method thereof - Google Patents
A kind of ancient painted pottery mud and preparation method thereof Download PDFInfo
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- CN105315570B CN105315570B CN201410277489.7A CN201410277489A CN105315570B CN 105315570 B CN105315570 B CN 105315570B CN 201410277489 A CN201410277489 A CN 201410277489A CN 105315570 B CN105315570 B CN 105315570B
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Abstract
The invention provides a kind of ancient painted pottery mud and preparation method thereof, the ancient painted pottery mud is made up of plasticizer, PVC paste resin, inorganic fillings, lubricant, colouring agent, color fixing agent, based on its percentage by weight, plasticizer 25 35%, PVC paste resin 5 15%, inorganic fillings 50% 60%, lubricant 8% 15%, colouring agent 0.1% 3%, color fixing agent 0.02% 3%.The soft plasticity of ancient painted pottery mud prepared by the present invention is good, is 2.5 times of plasticine, with can through steaming, boiling, toast, the heating mode formation ancient painted pottery product such as microwave the characteristics of, simple production process of the present invention is with low cost, easy to use, is conducive to promoting the use of.
Description
Technical field
The present invention relates to a kind of ancient painted pottery field, more particularly to a kind of ancient painted pottery mud and preparation method thereof
Background technology
Ancient painted pottery is a kind of polymerism clay, and this material color enriches, and pliability is good, is a kind of collection clay, paper clay, carving
The features such as moulding greasy filth, plasticine creates material for the handicraft of the whole body.Material audient is wide, manually sculpture, intention system
, can be as color is beautiful, pattern is ever-changing, hard such as the exquisite ornaments and handicraft of pottery after high-temperature heating after being molded.
It is also relatively stricter to heating tool and condition requirement but current ancient painted pottery mud plasticity is not good, it is unfavorable for product promotion
Use.Therefore develop that a kind of plasticity is good, color is beautiful persistently, can pass through using the ancient painted pottery raw material resources of China's abundant
The ancient painted pottery mud of the mode hot briquetting such as boiling, baking, microwave, with very important production practices meaning.
The content of the invention
The purpose of the present invention be overcome in the prior art weak point there is provided a kind of ancient painted pottery mud and preparation method thereof.
In order to solve the above technical problems, the present invention proposes following technical scheme:
A kind of ancient painted pottery mud, by plasticizer, PVC paste resin, inorganic fillings, lubricant, colouring agent, color fixing agent structure
Into, based on its percentage by weight, plasticizer 25-35%, PVC paste resin 5-15%, inorganic fillings 50%-60%, profit
Lubrication prescription 8%-15%, colouring agent 0.1%-3%, color fixing agent 0.02%-3%.
It is preferred that, above-mentioned ancient painted pottery mud, plasticizer is by trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil structure
Into by its weight ratio meter, trioctyl lemon acid:Tri-n-butyl citrate:Epoxidized soybean oil ratio is respectively 0.9~1.1:0.9
~1.1:0.2~0.3.
It is preferred that, above-mentioned ancient painted pottery mud, inorganic fillings is in diatomite, calcium carbonate, zinc sulfate and mixture of calcium sulfate
Any one is combined.
It is preferred that, above-mentioned ancient painted pottery mud, lubricant is any one in acceptable mineral oil, silicone oil in ceramics industry.
It is preferred that, above-mentioned ancient painted pottery mud, color fixing agent is acrylic resin modified.
It is preferred that, above-mentioned ancient painted pottery mud, colouring agent is inorganic pigment.
It is preferred that, above-mentioned ancient painted pottery mud, based on its percentage by weight, trioctyl lemon acid 11.3%, tri-n-butyl citrate
11.4%, epoxidized soybean oil 2.3%, PVC paste resin 15%, diatomite 50%, acceptable mineral oil in ceramics industry
8%, iron oxide red 1%, acrylic resin modified 1%.
It is preferred that, ancient painted pottery mud preparation technology is comprised the following steps that:
(1) plasticizer being made up of trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is well mixed, obtained
Mixture A.
(2) mixture A, Corvic, inorganic fillings are mixed evenly in proportion, stirred 40 minutes, it is cold
But place, obtain mixture B.
(3) lubricant is put into mixture B in proportion, instilled dropwise while stirring, stirred 30 minutes, taking-up treats cold
But, mixture C is obtained.
(4) mixture C is put into mixer or hand is rubbed 20 minutes, taken out to be cooled, obtain mixture D.
(5) toner is mixed into mixture D in proportion and stirred, it is to be cooled, obtain mixture E.
(6) color fixing agent is injected to mixture E in proportion and stirred, is kneaded 40 minutes, must mixed with hand or mixer
Thing F.
(7) with extruder extruding mixture F repeatedly, cut out and standard ancient painted pottery mud is made, thickness about 0.5-1cm ancient painted pottery is made
Mud.
The beneficial effects of the invention are as follows:
Compared with prior art, the present invention is by improving ancient painted pottery mud formula and preparation method, and its plasticity is common plasticine
2.5 times of product, color is true to nature persistently, both can also pass through the high-temperature heating sides such as boiling by oven cooking cycle, microwave heating
Formula achieve it is hard reach the effect placed for a long time as made pottery, not because of time, water, fire and modification.
Embodiment
Technical scheme of the present invention is further described with reference to specific embodiment.
Embodiment 1
1st, raw material are mixed
(1) trioctyl lemon acid 11.3kg, tri-n-butyl citrate 11.4kg, epoxidized soybean oil 2.3kg, polyvinyl chloride are taken
Resin 15kg, diatomite 50kg are pasted, acceptable mineral oil 8kg in ceramics industry, iron oxide red 1kg are acrylic resin modified
1kg。
(2) by trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is sufficiently mixed uniformly in proportion, must be mixed
Thing A.
(3) mixture A, PVC paste resin, diatomite are sufficiently mixed, stirred 40 minutes, cooling is placed, and must be mixed
Thing B.
(3) mineral oil is added in mixture B, feed postition is:While stirring plus mineral oil, stir about 25 minutes is cold
But it is positioned to mixture C.
(4) mixture C is put into mixer stirring or hand is rubbed, about 20 minutes, taken out cooling, obtain mixture D.
(5) iron oxide red is put into mixture D, stirred, taken out cooling, obtain mixture E.
(6) by acrylic resin modified instillation mixture E, stir, kneaded 40 minutes with hand or mixer, obtain mixed
Compound F.2nd, it is compressing
Mixture E is extruded repeatedly with extruder, cuts out and standard ancient painted pottery mud is made, thickness about 0.8cm.
Above-mentioned ancient painted pottery mud is made after ancient painted pottery ornaments according to art shapes, inserts in steamer and steams, after 45 minutes, you can
The ancient painted pottery ornaments of a set of color light tone.
Embodiment 2
1st, raw material are mixed
(1) trioctyl lemon acid 15.2kg, tri-n-butyl citrate 15.2kg, epoxidized soybean oil 4.6kg, polyvinyl chloride are taken
Resin 5kg, calcium carbonate 51kg are pasted, acceptable mineral oil 8kg in ceramics industry, carbon black 0.5kg are acrylic resin modified
0.5kg。
(2) by trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is sufficiently mixed uniformly in proportion, must be mixed
Thing A.
(3) mixture A, PVC paste resin, diatomite are sufficiently mixed, stirred 40 minutes, cooling is placed, and must be mixed
Thing B.
(3) mineral oil is added in mixture B, feed postition is:While stirring plus mineral oil, stir about 25 minutes is cold
But it is positioned to mixture C.
(4) mixture C is put into mixer stirring or hand is rubbed, about 20 minutes, taken out cooling, obtain mixture D.
(5) carbon black is put into mixture D, stirred, taken out cooling, obtain mixture E.
(6) by acrylic resin modified instillation mixture E, stir, kneaded 40 minutes with hand or mixer, obtain mixed
Compound F.
2nd, it is compressing
Extruded repeatedly with extruder, cut out and standard ancient painted pottery is made, thickness about 0.9cm.
Above-mentioned ancient painted pottery mud is made after ancient painted pottery ornaments according to art shapes, after being wrapped with preservative film, inserted in 15% salt solution
Cook, after boiling rear constant temperature cooking about 50 minutes, you can obtain the ancient painted pottery ornaments of a set of color light tone.
Embodiment 3
1st, raw material are mixed
(1) trioctyl lemon acid 11.3kg, tri-n-butyl citrate 11.4kg, epoxidized soybean oil 2.3kg, polyvinyl chloride are taken
Paste resin 5kg, calcium carbonate 60kg, acceptable silicone oil 9kg in ceramics industry, cadmium yellow 0.8kg, acrylic resin modified 0.2kg.
(2) by trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is sufficiently mixed uniformly in proportion, must be mixed
Thing A.
(3) mixture A, PVC paste resin, diatomite are sufficiently mixed, stirred 40 minutes, cooling is placed, and must be mixed
Thing B.
(3) mineral oil is added in mixture B, feed postition is:While stirring plus mineral oil, stir about 25 minutes is cold
But it is positioned to mixture C.
(4) mixture C is put into mixer stirring or hand is rubbed, about 20 minutes, taken out cooling, obtain mixture D.
(5) cadmium yellow is put into mixture D, stirred, taken out cooling, obtain mixture E.
(6) by acrylic resin modified instillation mixture E, stir, kneaded 40 minutes with hand or mixer, obtain mixed
Compound F.
2nd, it is compressing
Extruded repeatedly with extruder, cut out and standard ancient painted pottery soil is made, thickness about 1cm.
Above-mentioned ancient painted pottery mud is made after ancient painted pottery ornaments according to art shapes, inserts in steamer and steams, after 45 minutes, you can
The ancient painted pottery ornaments of a set of color light tone.
Embodiment 4
1st, raw material are mixed
(1) trioctyl lemon acid 11.1kg, tri-n-butyl citrate 11.1kg, epoxidized soybean oil 2.8kg, polyvinyl chloride are taken
Resin 5kg, calcium carbonate 50kg are pasted, acceptable silicone oil 15kg in ceramics industry, iron oxide yellow 2kg are acrylic resin modified
3kg。
(2) by trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is sufficiently mixed uniformly in proportion, must be mixed
Thing A.
(3) mixture A, PVC paste resin, diatomite are sufficiently mixed, stirred 40 minutes, cooling is placed, and must be mixed
Thing B.
(3) mineral oil is added in mixture B, feed postition is:While stirring plus mineral oil, stir about 25 minutes is cold
But it is positioned to mixture C.
(4) mixture C is put into mixer stirring or hand is rubbed, about 20 minutes, taken out cooling, obtain mixture D.
(5) iron oxide yellow is put into mixture D, stirred, taken out cooling, obtain mixture E.
(6) by acrylic resin modified instillation mixture E, stir, kneaded 40 minutes with hand or mixer, obtain mixed
Compound F.
2nd, it is compressing
Extruded repeatedly with extruder, cut out and standard ancient painted pottery mud is made, thickness about 0.8cm.
Above-mentioned ancient painted pottery mud is made after ancient painted pottery handicraft according to art shapes, inserts in micro-wave oven and to be heated with moderate heat, 10 points
Zhong Hou, you can obtain the ancient painted pottery handicraft of a set of color light tone.
Embodiment 5
1st, raw material are mixed
(1) trioctyl lemon acid 11.6kg, tri-n-butyl citrate 11.7kg, epoxidized soybean oil 3.5kg, polyvinyl chloride are taken
Paste resin 10kg, zinc sulfate and barium sulfate 53kg, acceptable silicone oil 10kg, laterite 0.1kg, modified acroleic acid in ceramics industry
Resin 0.1kg.
(2) by trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is sufficiently mixed uniformly in proportion, must be mixed
Thing A.
(3) mixture A, PVC paste resin, diatomite are sufficiently mixed, stirred 40 minutes, cooling is placed, and must be mixed
Thing B.
(3) mineral oil is added in mixture B, feed postition is:While stirring plus mineral oil, stir about 25 minutes is cold
But it is positioned to mixture C.
(4) mixture C is put into mixer stirring or hand is rubbed, about 20 minutes, taken out cooling, obtain mixture D.
(5) laterite is put into mixture D, stirred, taken out cooling, obtain mixture E.
(6) by acrylic resin modified instillation mixture E, stir, kneaded 40 minutes with hand or mixer, obtain mixed
Compound F.
2nd, it is compressing
Extruded repeatedly with extruder, cut out and standard ancient painted pottery mud is made, thickness about 0.8cm.
Above-mentioned ancient painted pottery mud is made after ancient painted pottery ornaments according to art shapes, inserts in steamer and steams, after 45 minutes, you can
The ancient painted pottery ornaments of a set of color light tone.
Embodiment 6
1st, raw material are mixed
(1) trioctyl lemon acid 13.7kg, tri-n-butyl citrate 13.6kg, epoxidized soybean oil 2.7kg, polyvinyl chloride are taken
Resin 8kg, diatomite 50kg are pasted, acceptable mineral oil 11kg in ceramics industry, cinnabar 0.98kg are acrylic resin modified
0.02kg。
(2) by trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is sufficiently mixed uniformly in proportion, must be mixed
Thing A.
(3) mixture A, PVC paste resin, diatomite are sufficiently mixed, stirred 40 minutes, cooling is placed, and must be mixed
Thing B.
(3) mineral oil is added in mixture B, feed postition is:While stirring plus mineral oil, stir about 25 minutes is cold
But it is positioned to mixture C.
(4) mixture C is put into mixer stirring or hand is rubbed, about 20 minutes, taken out cooling, obtain mixture D.
(5) cinnabar is put into mixture D, stirred, taken out cooling, obtain mixture E.
(6) by acrylic resin modified instillation mixture E, stir, kneaded 40 minutes with hand or mixer, obtain mixed
Compound F.
2nd, it is compressing
Extruded repeatedly with extruder, cut out and standard ancient painted pottery mud is made, thickness about 0.7cm.
Above-mentioned ancient painted pottery mud is made after ancient painted pottery ornaments according to art shapes, inserts in baking oven and toasts, after 30 minutes, you can
The ancient painted pottery ornaments of a set of color light tone.
Embodiment 7
1st, raw material are mixed
(1) trioctyl lemon acid 5.8kg, tri-n-butyl citrate 5.8kg, epoxidized soybean oil 1.2kg, Welvic are taken
Resin 2.5kg, diatomite 27.5kg, acceptable mineral oil 6kg in ceramics industry, barba hispanica 0.5kg are acrylic resin modified
0.5kg。
(2) by trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is sufficiently mixed uniformly in proportion, must be mixed
Thing A.
(3) mixture A, PVC paste resin, diatomite are sufficiently mixed, stirred 40 minutes, cooling is placed, and must be mixed
Thing B.
(3) mineral oil is added in mixture B, feed postition is:While stirring plus mineral oil, stir about 25 minutes is cold
But it is positioned to mixture C.
(4) mixture C is put into mixer stirring or hand is rubbed, about 20 minutes, taken out cooling, obtain mixture D.
(5) barba hispanica is put into mixture D, stirred, taken out cooling, obtain mixture E.
(6) by acrylic resin modified instillation mixture E, stir, kneaded 40 minutes with hand or mixer, obtain mixed
Compound F.
2nd, it is compressing
Extruded repeatedly with extruder, cut out and standard ancient painted pottery mud is made, thickness about 0.7cm.
Above-mentioned ancient painted pottery mud is made after ancient painted pottery ornaments according to art shapes, inserts in baking oven and toasts, after 30 minutes, you can
The ancient painted pottery ornaments of a set of color light tone.
Application test example
Experiment one:Ancient painted pottery mud in embodiment 1 and plasticine are subjected to plasticity contrast test:
1st, experimental instrument and equipment
Precision 0.01mm compression plastometers.
2nd, experimental condition
A. environment temperature:(25±2)℃
B. envionmental humidity:(55-75) %
C. specimen size:The cylinders of Φ 28 × 38
D. displacement range:0-25mm, displacement accuracy≤1%
E. pressure range:0-500N, pressure precision≤1%
3 test methods and procedures
It is prepared by 3.1 samples
White oil is coated on upper and lower pressing plate, good anti-adhesion performance is made it have.The height being kneaded into by hand is more than
40mm, upper and lower surface are smooth, length and width be all higher than 40mm sample blocks put on stainless steel, firmly mould is vertically depressed, make
Pug is completely filled with mould, then prescinds unnecessary pug with cutting mud device, with doctor blade, is finally slightly less than mould with a diameter
Has the plastic cylinder of internal diameter.
It will gently release, put on stainless steel in sample from mould.
Sample is carefully moved to and avoids deforming in lower platen center, moving process.
3.2 determination step
Sample is measured with precision 0.01mm compression plastometers and compresses the pressure F10 and F50 born when 10% and 50%,
And plasticity is obtained according to formula below calculating.
R is plasticity, and instrument can be calculated and be shown automatically
A is the constant for the cylindrical specimens of Φ 28 × 38, and this value is 1.80.
Same sample must carry out 6 parallel tests, and each plasticity index measured value relative deviation not should be greater than 15%, if
There is a measured value for being more than 15% to leave out, test result takes its average value, calculating is accurate to 2 significant digits number.If having
The relative deviation of two measured values is then resurveyed more than 15%.After being completed, the detritus on instrument is removed, absolute oil mark is wiped.
4th, experimental result
The ancient painted pottery mud of table one, plasticine plasticity experimental result
Unit:kg.cm
Project | 1 | 2 | 3 | 4 | 5 | Average |
Ancient painted pottery mud | 2.12 | 2.02 | 2.16 | 2.10 | 2.04 | 2.088 |
Plasticine | 0.82 | 0.83 | 0.81 | 0.82 | 0.81 | 0.820 |
Test result indicates that, ancient painted pottery mud plasticity is better than plasticine in embodiment 1, and is 2.5 times of commercially available plasticine.
Experiment two:The ancient painted pottery mud that ancient painted pottery mud in embodiment 1 and two kinds of different formulations are made carries out plasticity contrast test:
1st, experiment material
Contrast ancient painted pottery mud 1 is formulated:Take trioctyl lemon acid 18.5kg, epoxidized soybean oil 9.5kg, PVC paste resin
15kg, diatomite 50kg, acceptable mineral oil 8kg in ceramics industry, iron oxide red 1kg, acrylic resin modified 1kg.
Contrast ancient painted pottery mud 2 is formulated:Take tri-n-butyl citrate 17.1kg, trioctyl lemon acid 7.9kg, Welvic tree
Fat 15kg, diatomite 50kg, acceptable mineral oil 8kg in ceramics industry, iron oxide red 1kg, acrylic resin modified 1kg.
Manufacture method in both preparation method be the same as Examples 1.
2nd, test method is with " experiment one, 3 "
3rd, experimental result
The different formulations ancient painted pottery mud plasticity experimental result of table two
Unit:kg.cm
Project | 1 | 2 | 3 | 4 | 5 | Average |
Ancient painted pottery mud | 2.12 | 2.02 | 2.16 | 2.10 | 2.04 | 2.088 |
Ancient painted pottery mud 1 | 1.91 | 1.84 | 1.89 | 1.92 | 1.99 | 1.910 |
Ancient painted pottery mud 2 | 1.12 | 1.15 | 1.20 | 1.18 | 1.23 | 1.176 |
Test result indicates that, ancient painted pottery mud plasticity is better than two kinds of ancient painted pottery mud of contrast in embodiment 1.
The above-mentioned detailed description carried out to a kind of ancient painted pottery mud and preparation method thereof with reference to embodiment, be it is illustrative without
It is limited, several embodiments can be included according to limited scope, therefore in the case where not departing from present general inventive concept
Change and modifications, should belong within protection scope of the present invention.
Claims (8)
1. a kind of ancient painted pottery mud, it is characterised in that:By plasticizer, PVC paste resin, inorganic fillings, lubricant, colouring agent,
Color fixing agent is constituted, based on its percentage by weight, plasticizer 25-35%, PVC paste resin 5-15%, inorganic fillings
50%-60%, lubricant 8%-15%, colouring agent 0.1%-3%, color fixing agent 0.02%-3%;Plasticizer is by citric acid three
Monooctyl ester, tri-n-butyl citrate, epoxidized soybean oil are constituted, by its weight ratio meter, trioctyl lemon acid:Tri-n-butyl citrate:
Epoxidized soybean oil ratio is respectively
2. ancient painted pottery mud as claimed in claim 1, it is characterised in that:Inorganic fillings are diatomite, calcium carbonate, zinc sulfate and sulphur
Any one in sour calcium compound or any combination.
3. according to the ancient painted pottery mud as described in claim 1, it is characterised in that:Lubricant be ceramics industry in acceptable mineral oil,
Any one in silicone oil.
4. ancient painted pottery mud as claimed in claim 1, it is characterised in that:Color fixing agent is acrylic resin modified.
5. ancient painted pottery mud as claimed in claim 1, it is characterised in that:Colouring agent is inorganic pigment.
6. ancient painted pottery mud as claimed in claim 1, it is characterised in that:Based on its percentage by weight, trioctyl lemon acid 11.3%,
Tri-n-butyl citrate 11.4%, epoxidized soybean oil 2.3%, PVC paste resin 15%, diatomite 50%, in ceramics industry
Acceptable mineral oil 8%, iron oxide red 1%, acrylic resin modified 1%.
7. ancient painted pottery mud as claimed in claim 1, it is characterised in that:Obtained by following methods:
(1) plasticizer being made up of trioctyl lemon acid, tri-n-butyl citrate, epoxidized soybean oil is well mixed, must mixed
Thing A;
(2) mixture A, Corvic, inorganic fillings are mixed evenly in proportion, stirred 40 minutes, cooling is put
Put, obtain mixture B;
(3) lubricant is put into mixture B in proportion, instilled dropwise while stirring, stirred 30 minutes, taken out to be cooled, obtain
Mixture C;
(4) mixture C is put into mixer or hand is rubbed 20 minutes, taken out to be cooled, obtain mixture D;
(5) toner is mixed into mixture D in proportion and stirred, it is to be cooled, obtain mixture E;
(6) color fixing agent is injected to mixture E in proportion and stirred, is kneaded 40 minutes with hand or mixer, obtains mixture F;
(7) with extruder extruding mixture F repeatedly, cut out and standard ancient painted pottery mud is made, thick 0.5-1cm ancient painted pottery mud is made.
8. the ancient painted pottery mud as described in claim 1 or 7, it is characterised in that:Its plasticity is 2.5 times of plasticine.
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CN106751143A (en) * | 2016-11-29 | 2017-05-31 | 金华博科彩泥技术研发有限公司 | Make clay of erasing rubber and preparation method thereof by oneself |
CN107828153A (en) * | 2017-11-23 | 2018-03-23 | 珠海库摩饰品有限公司 | A kind of soft ceramic mud and its manufacture craft |
CN108102243A (en) * | 2017-11-27 | 2018-06-01 | 广德粤华塑业制品有限公司 | A kind of PVC environmental protection color |
CN108976821A (en) * | 2018-06-19 | 2018-12-11 | 润亚科技(深圳)有限公司 | A kind of macromolecule ebonite mud |
CN109053030A (en) * | 2018-10-16 | 2018-12-21 | 得时宝(广州)科技有限公司 | A kind of pottery mud and preparation method thereof |
CN111423209A (en) * | 2020-05-14 | 2020-07-17 | 界首市卢氏刻花彩陶有限公司 | Preparation method of painted pottery pug |
CN111777827A (en) * | 2020-06-16 | 2020-10-16 | 佛山市顺德区怡德塑料制品有限公司 | Modified PVC material and preparation method thereof |
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CN1778839A (en) * | 2004-11-24 | 2006-05-31 | 于淼 | Formula of plastic rubber |
CN101186736A (en) * | 2007-12-18 | 2008-05-28 | 东莞市汇欣工贸有限公司 | Soft ceramic mud and preparation method thereof |
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CN1778839A (en) * | 2004-11-24 | 2006-05-31 | 于淼 | Formula of plastic rubber |
CN101186736A (en) * | 2007-12-18 | 2008-05-28 | 东莞市汇欣工贸有限公司 | Soft ceramic mud and preparation method thereof |
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