CN105296124A - Composite metal machining liquid and preparation method thereof - Google Patents
Composite metal machining liquid and preparation method thereof Download PDFInfo
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- CN105296124A CN105296124A CN201510867822.4A CN201510867822A CN105296124A CN 105296124 A CN105296124 A CN 105296124A CN 201510867822 A CN201510867822 A CN 201510867822A CN 105296124 A CN105296124 A CN 105296124A
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Abstract
The invention relates to composite metal machining liquid and a preparation method thereof. The preparation method comprises the following steps: (1) respectively taking oleic acid, dioctyl sodium sulfosuccinate, propylene glycol alginate, octylphenol polyoxyethylene ether and dodecyl dimethyl benzyl ammonium chloride according to weight parts, and uniformly mixing the components at the temperature of 40 to 50 DEG C, so as to obtain a mixture A; (2) respectively taking 2-diethylaminoethyl methacrylate, lauryl dimethyl amine oxide, cocamidopropyl betaine, glycerinum, 1,3,5-triazine-1,3,5(2H,4H,6H)-triethanol and deionized water according to weight parts, and stirring the components in the step (2) at the temperature of 50 to 60 DEG C for 30 to 50 minutes, so as to obtain a mixture B; (3) pouring the mixture A into the mixture B and stirring, wherein the stirring is performed after the pouring, then cooling, so as to prepare the composite metal machining liquid. The obtained composite metal machining liquid through preparation has the advantages of good lubricating property and excellent overall performance.
Description
Technical field
The invention belongs to machining field, relate to a kind of composition metal cutting fluid and preparation method thereof.
Background technology
Cutting fluid is that one is used in metal cutting, the mill course of processing, is used for Cooling and Lubricator
cutterwith the industrial type fluid of workpiece, cutting fluid is formed through the cooperation of science compound by multiple super strong functional auxiliary agent, possesses good cooling performance, lubricity, rustless property, oil removing cleaning function, anti-corrosion function, easily dilutable feature simultaneously.Overcome traditional soap base
emulsioneasily difficult dilution in smelly, winter in summer, rust-proof effect difference defect, lathe paint is also had no adverse effects, be applicable to ferrous metal cutting and mill processing, belong to leading current abrasive product.
Conventional its lubricity of the cutting fluid for metal is poor, and its stability is not high yet, and the change of character can occur after long-time storage, and its dilution property also decreases.Significantly limit the application of cutting fluid.
Summary of the invention
The technical problem solved: the object of the invention is openly a kind of novel composition metal cutting fluid and preparation method thereof, improves the lubricity of common cutting fluid and package stability thereof, dilution.
Technical scheme: the invention discloses a kind of composition metal cutting fluid, comprise the composition of following weight part:
Oleic acid 16-25 part,
Two fourth sodium dioctyl sulfo 2-6 parts,
Propylene glycol alginate 3-7 part,
Polyoxyethylene octylphenol ether 4-8 part,
Dodecyl benzyl dimethyl ammonium chloride 2-5 part,
Diethylaminoethyl methacrylate 3-6 part,
Lauryl dimethyl amine oxide 3-6 part,
AMONYL 380LC 4-9 part,
Glycerine 2-6 part,
Three red oily 1-4 parts,
Deionized water 300-400 part.
Further, described a kind of composition metal cutting fluid, comprises the composition of following weight part:
Oleic acid 18-22 part,
Two fourth sodium dioctyl sulfo 3-5 parts,
Propylene glycol alginate 4-6 part,
Polyoxyethylene octylphenol ether 5-7 part,
Dodecyl benzyl dimethyl ammonium chloride 3-4 part,
Diethylaminoethyl methacrylate 4-5 part,
Lauryl dimethyl amine oxide 4-5 part,
AMONYL 380LC 5-8 part,
Glycerine 3-5 part,
Three red oily 2-3 parts,
Deionized water 330-370 part.
The preparation method of described a kind of composition metal cutting fluid, comprises the steps:
(1) oleic acid 16-25 part, two fourth sodium dioctyl sulfo 2-6 parts, propylene glycol alginate 3-7 part, polyoxyethylene octylphenol ether 4-8 part, dodecyl benzyl dimethyl ammonium chloride 2-5 part is got by weight respectively, being mixed at temperature is 40-50 DEG C by above-mentioned composition, is compound A;
(2) diethylaminoethyl methacrylate 3-6 part, lauryl dimethyl amine oxide 3-6 part, AMONYL 380LC 4-9 part, glycerine 2-6 part, three red oily 1-4 parts, deionized water 300-400 part is got by weight respectively, composition in step (2) is stirred 30-50min at temperature is 50-60 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 20-40min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
Further, the preparation method of described a kind of composition metal cutting fluid, in described step (1), temperature is 45 DEG C.
Further, the preparation method of described a kind of composition metal cutting fluid, in described step (2), churning time is 40min.
Further, the preparation method of described a kind of composition metal cutting fluid, again stirs 30min after being finished down in described step (3).
Beneficial effect: composition metal cutting fluid prepared by method of the present invention has excellent package stability and dilution effect, in addition, also there is good lubricity and rustless property, composition metal cutting fluid of the present invention is different from conventional metal working fluid, its moiety and common cutting fluid difference larger, and not containing heavy metal, over-all properties is good.
Embodiment
Embodiment 1
(1) oleic acid 25 parts, two fourth sodium dioctyl sulfo 2 parts, propylene glycol alginate 7 parts, polyoxyethylene octylphenol ether 4 parts, dodecyl benzyl dimethyl ammonium chloride 5 parts is got by weight respectively, being mixed at temperature is 50 DEG C by above-mentioned composition, is compound A;
(2) diethylaminoethyl methacrylate 3 parts, lauryl dimethyl amine oxide 3 parts, AMONYL 380LC 9 parts, glycerine 6 parts, three red oil 4 parts, deionized water 400 parts is got by weight respectively, composition in step (2) is stirred 30min at temperature is 60 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 40min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
Embodiment 2
(1) oleic acid 16 parts, two fourth sodium dioctyl sulfo 6 parts, propylene glycol alginate 3 parts, polyoxyethylene octylphenol ether 8 parts, dodecyl benzyl dimethyl ammonium chloride 2 parts is got by weight respectively, being mixed at temperature is 40 DEG C by above-mentioned composition, is compound A;
(2) diethylaminoethyl methacrylate 6 parts, lauryl dimethyl amine oxide 6 parts, AMONYL 380LC 4 parts, glycerine 2 parts, three red oil 1 part, deionized water 300 parts is got by weight respectively, composition in step (2) is stirred 50min at temperature is 50 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 20min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
Embodiment 3
(1) oleic acid 22 parts, two fourth sodium dioctyl sulfo 3 parts, propylene glycol alginate 6 parts, polyoxyethylene octylphenol ether 5 parts, dodecyl benzyl dimethyl ammonium chloride 3 parts is got by weight respectively, being mixed at temperature is 50 DEG C by above-mentioned composition, is compound A;
(2) diethylaminoethyl methacrylate 4 parts, lauryl dimethyl amine oxide 5 parts, AMONYL 380LC 8 parts, glycerine 5 parts, three red oil 2 parts, deionized water 330 parts is got by weight respectively, composition in step (2) is stirred 30min at temperature is 60 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 40min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
Embodiment 4
(1) oleic acid 18 parts, two fourth sodium dioctyl sulfo 5 parts, propylene glycol alginate 4 parts, polyoxyethylene octylphenol ether 7 parts, dodecyl benzyl dimethyl ammonium chloride 4 parts is got by weight respectively, being mixed at temperature is 40 DEG C by above-mentioned composition, is compound A;
(2) diethylaminoethyl methacrylate 5 parts, lauryl dimethyl amine oxide 4 parts, AMONYL 380LC 5 parts, glycerine 3 parts, three red oil 3 parts, deionized water 370 parts is got by weight respectively, composition in step (2) is stirred 50min at temperature is 50 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 20min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
Embodiment 5
(1) oleic acid 20 parts, two fourth sodium dioctyl sulfo 4 parts, propylene glycol alginate 5 parts, polyoxyethylene octylphenol ether 6 parts, dodecyl benzyl dimethyl ammonium chloride 3 parts is got by weight respectively, being mixed at temperature is 45 DEG C by above-mentioned composition, is compound A;
(2) diethylaminoethyl methacrylate 4 parts, lauryl dimethyl amine oxide 4 parts, AMONYL 380LC 7 parts, glycerine 4 parts, three red oil 2 parts, deionized water 350 parts is got by weight respectively, composition in step (2) is stirred 40min at temperature is 50 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 30min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
Comparative example 1
(1) getting oleic acid 25 parts, two fourth sodium dioctyl sulfo 2 parts, dodecyl benzyl dimethyl ammonium chloride 5 parts by weight respectively, mixed by above-mentioned composition at temperature is 50 DEG C, is compound A;
(2) diethylaminoethyl methacrylate 3 parts, lauryl dimethyl amine oxide 3 parts, AMONYL 380LC 9 parts, glycerine 6 parts, three red oil 4 parts, deionized water 400 parts is got by weight respectively, composition in step (2) is stirred 30min at temperature is 60 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 40min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
Comparative example 2
(1) oleic acid 25 parts, two fourth sodium dioctyl sulfo 2 parts, propylene glycol alginate 7 parts, polyoxyethylene octylphenol ether 4 parts, dodecyl benzyl dimethyl ammonium chloride 5 parts is got by weight respectively, being mixed at temperature is 50 DEG C by above-mentioned composition, is compound A;
(2) get AMONYL 380LC 9 parts, glycerine 6 parts, three red oil 4 parts, deionized water 400 parts by weight respectively, the composition in step (2) is stirred 30min at temperature is 60 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 40min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
Comparative example 3
(1) getting oleic acid 25 parts, propylene glycol alginate 7 parts, polyoxyethylene octylphenol ether 4 parts, dodecyl benzyl dimethyl ammonium chloride 5 parts by weight respectively, mixed by above-mentioned composition at temperature is 50 DEG C, is compound A;
(2) get diethylaminoethyl methacrylate 3 parts, lauryl dimethyl amine oxide 3 parts, glycerine 6 parts, three red oil 4 parts, deionized water 400 parts by weight respectively, the composition in step (2) is stirred 30min at temperature is 60 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 40min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
The composition metal cutting fluid of embodiment prepared by the present invention all has very good storage stability, at room temperature stores the phenomenon all not producing layering or flocculation after 1 year.
Rustless property and the lubricity thereof of the composition metal cutting fluid of embodiment 1 to 5 and comparative example 1 to 3 are as follows:
| Rust-preventing characteristic (35 ± 2 DEG C) one-level graphitic cast iron | Last non seizure load PB value | |
| Embodiment 1 | Rustless after monolithic 60h, rustless after lamination 30h | 695 |
| Embodiment 2 | Rustless after monolithic 60h, rustless after lamination 30h | 701 |
| Embodiment 3 | Rustless after monolithic 72h, rustless after lamination 35h | 744 |
| Embodiment 4 | Rustless after monolithic 72h, rustless after lamination 35h | 732 |
| Embodiment 5 | Rustless after monolithic 84h, rustless after lamination 40h | 791 |
Rustless property and the lubricity thereof of comparative example are as follows:
| Rust-preventing characteristic (35 ± 2 DEG C) one-level graphitic cast iron | Last non seizure load PB value | |
| Comparative example 1 | Rustless after monolithic 24h, rustless after lamination 18h | 617 |
| Comparative example 2 | Rustless after monolithic 36h, rustless after lamination 24h | 622 |
| Comparative example 3 | Rustless after monolithic 36h, rustless after lamination 24h | 604 |
Claims (6)
1. a composition metal cutting fluid, is characterized in that, described composition metal cutting fluid comprises the composition of following weight part:
Oleic acid 16-25 part,
Two fourth sodium dioctyl sulfo 2-6 parts,
Propylene glycol alginate 3-7 part,
Polyoxyethylene octylphenol ether 4-8 part,
Dodecyl benzyl dimethyl ammonium chloride 2-5 part,
Diethylaminoethyl methacrylate 3-6 part,
Lauryl dimethyl amine oxide 3-6 part,
AMONYL 380LC 4-9 part,
Glycerine 2-6 part,
Three red oily 1-4 parts,
Deionized water 300-400 part.
2. a kind of composition metal cutting fluid according to claim 1, is characterized in that, described composition metal cutting fluid comprises the composition of following weight part:
Oleic acid 18-22 part,
Two fourth sodium dioctyl sulfo 3-5 parts,
Propylene glycol alginate 4-6 part,
Polyoxyethylene octylphenol ether 5-7 part,
Dodecyl benzyl dimethyl ammonium chloride 3-4 part,
Diethylaminoethyl methacrylate 4-5 part,
Lauryl dimethyl amine oxide 4-5 part,
AMONYL 380LC 5-8 part,
Glycerine 3-5 part,
Three red oily 2-3 parts,
Deionized water 330-370 part.
3. the preparation method of a kind of composition metal cutting fluid according to claim 1, it is characterized in that, described preparation method comprises the steps:
(1) oleic acid 16-25 part, two fourth sodium dioctyl sulfo 2-6 parts, propylene glycol alginate 3-7 part, polyoxyethylene octylphenol ether 4-8 part, dodecyl benzyl dimethyl ammonium chloride 2-5 part is got by weight respectively, being mixed at temperature is 40-50 DEG C by above-mentioned composition, is compound A;
(2) diethylaminoethyl methacrylate 3-6 part, lauryl dimethyl amine oxide 3-6 part, AMONYL 380LC 4-9 part, glycerine 2-6 part, three red oily 1-4 parts, deionized water 300-400 part is got by weight respectively, composition in step (2) is stirred 30-50min at temperature is 50-60 DEG C, is compound B;
(3) being poured into slowly in the compound B of step (2) by the compound A that step (1) is obtained, pour into while stir, stir 20-40min again after being finished down, cooling, is the composition metal cutting fluid of preparation.
4. the preparation method of a kind of composition metal cutting fluid according to claim 3, is characterized in that, in described step (1), temperature is 45 DEG C.
5. the preparation method of a kind of composition metal cutting fluid according to claim 3, is characterized in that, in described step (2), churning time is 40min.
6. the preparation method of a kind of composition metal cutting fluid according to claim 3, is characterized in that, again stirs 30min after being finished down in described step (3).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510867822.4A CN105296124A (en) | 2015-12-02 | 2015-12-02 | Composite metal machining liquid and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510867822.4A CN105296124A (en) | 2015-12-02 | 2015-12-02 | Composite metal machining liquid and preparation method thereof |
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| CN105296124A true CN105296124A (en) | 2016-02-03 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102311860A (en) * | 2011-04-26 | 2012-01-11 | 东莞市安美润滑科技有限公司 | Water-based cutting fluid used for processing neodymium-iron-boron material slices and application method thereof |
| CN102911777A (en) * | 2012-10-18 | 2013-02-06 | 沈阳创达技术交易市场有限公司 | Metal cutting fluid and preparation method thereof |
| CN104164283A (en) * | 2014-08-19 | 2014-11-26 | 清华大学 | Microemulsion metal cutting fluid |
| CN104789339A (en) * | 2015-04-02 | 2015-07-22 | 安徽豪鼎金属制品有限公司 | Alkaline cutting fluid comprising raw silk |
-
2015
- 2015-12-02 CN CN201510867822.4A patent/CN105296124A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102311860A (en) * | 2011-04-26 | 2012-01-11 | 东莞市安美润滑科技有限公司 | Water-based cutting fluid used for processing neodymium-iron-boron material slices and application method thereof |
| CN102911777A (en) * | 2012-10-18 | 2013-02-06 | 沈阳创达技术交易市场有限公司 | Metal cutting fluid and preparation method thereof |
| CN104164283A (en) * | 2014-08-19 | 2014-11-26 | 清华大学 | Microemulsion metal cutting fluid |
| CN104789339A (en) * | 2015-04-02 | 2015-07-22 | 安徽豪鼎金属制品有限公司 | Alkaline cutting fluid comprising raw silk |
Non-Patent Citations (1)
| Title |
|---|
| 侯海云: "《表面活性剂物理化学基础》", 31 August 2014 * |
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Application publication date: 20160203 |