CN104560351A - Low-foam descaling type water-based cutting fluid and preparation method thereof - Google Patents
Low-foam descaling type water-based cutting fluid and preparation method thereof Download PDFInfo
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- CN104560351A CN104560351A CN201410840334.XA CN201410840334A CN104560351A CN 104560351 A CN104560351 A CN 104560351A CN 201410840334 A CN201410840334 A CN 201410840334A CN 104560351 A CN104560351 A CN 104560351A
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Abstract
The invention discloses low-foam descaling type water-based cutting fluid which is characterized by comprising raw materials in parts by weight as follows: 3-5 parts of zinc dihydrogen phosphate, 2-3 parts of urotropin, 0.4-0.7 parts of cuprous oxide, 4-6 parts of polyoxyethylene alkyl amine, 6-8 parts of chlorinated paraffin, 8-12 parts of stearic acid, 3-5 parts of carnauba wax, 2-3 parts of sodium alkyl polyoxyethylene ether sulfate, 1-2 parts of benzotriazole, 0.6-0.8 parts of water glass, 5-7 parts of auxiliaries and 150-180 parts of water. The dispersion, lubricity and film forming property of the cutting fluid are reinforced through the added auxiliaries; the water glass can improve the problem of large foam of the water-based cutting fluid, can emulsify and suspend dirt and clean the dirt in the cutting fluid, and further has the characteristics of good cooling, cleaning, rust preventing and the like; and the cutting fluid has very good lubricity, cooling, low foam, descaling, rust preventing and cleaning effects.
Description
Technical field
The present invention relates to cutting fluid field, particularly a kind of low bubble descaling type water-base cutting fluid and preparation method thereof.
Background technology
Cutting fluid is that one is used in metal cutting, the mill course of processing, be used for the industrial type fluid of Cooling and Lubricator cutter and workpiece, cutting fluid is formed through science compound compatibility by multiple super strong functional auxiliary agent, possesses good cooling performance, lubricity, rustless property, oil removing cleaning function, anti-corrosion function, easily dilutable feature simultaneously.Overcome the easily difficult dilution in smelly, winter in summer of traditional soap base emulsion, rust-proof effect difference defect, lathe paint is also had no adverse effects, be applicable to ferrous metal cutting and mill processing, belong to leading current abrasive product.But the foam that general cutting fluid operationally produces is large, and easy long-living dirt, the easy performance affecting workpiece, and cleaning process is consuming time, for the trouble that people's arrival is very large, the sodium silicate that the present invention is directed to cutting fluid interpolation prepared by this situation can reduce the large problem of water-base cutting fluid foam, and can emulsification, soil suspension, dirt in easy removing cutting fluid, it also has good cooling, cleaning, the feature such as antirust, also possess simultaneously nontoxic, tasteless, non-corrosive to human body, to equipment not burn into features such as environment do not pollute.
Summary of the invention
The object of this invention is to provide a kind of low bubble descaling type water-base cutting fluid and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of low bubble descaling type water-base cutting fluid, is made up of the raw material of following weight part: primary zinc phosphate 3-5, urotropine 2-3, Red copper oxide 0.4-0.7, polyoxyethylene alkyl amine 4-6, clorafin 6-8, stearic acid 8-12, carnauba wax 3-5, pareth sulfate 2-3, benzotriazole 1-2, sodium silicate 0.6-0.8, auxiliary agent 5-7, water 150-180;
Described auxiliary agent is made up of the raw material of following weight part: rosin 3-5, cyanuric acid zinc 1-2, organosilicon crylic acid latex 2-3.5, isothiazolinone 1-2, calglucon 1-2, natrosol 1-2, glycol ether 5-7, castor-oil plant acid amides 2-3, polyoxyethylene glycol 2-4, vinylcarbinol 4-6, Fatty alcohol polyoxyethylene polyoxypropylene ether 1-2, defoamer 0.2-0.4, water 40-50; Preparation method is that natrosol, polyoxyethylene glycol, organosilicon crylic acid latex, Fatty alcohol polyoxyethylene polyoxypropylene ether are added in water by (1), is heated to 40-50 ° of C, and it is for subsequent use to add defoamer after stirring; (2) rosin, glycol ether, vinylcarbinol, castor-oil plant acid amides are mixed and heated to 50-60 ° of C, after stirring, the product in step (1) is slowly added, stir with the rotating speed of 300-400 rev/min, the reinforced post-heating that terminates is to 70-80 ° of C, and at 1800-2000 rev/min of lower high-speed stirring 10-15 minute, then add all the other surplus materialss continuation stirring 5-10 minute.
One of the present invention low bubble descaling type water-base cutting fluid, be made up of following concrete steps:
(1) clorafin, stearic acid, carnauba wax and pareth sulfate are mixed, be heated to 50-60 ° of C, after stirring reaction 20-40 minute, obtain mixture A;
(2) 50-70 ° of C will be cooled to rapidly after water boil, then add sodium silicate and polyoxyethylene alkyl amine stirs, add auxiliary agent after stirring with 800-900 rev/min of lower stirring reaction 40-60 minute, obtain mixture B;
(3) mixture B is added in mixture A while stirring slowly, temperature is controlled, at 40-55 ° of C, after stirring, add all the other remaining components, filtered after 1400-1600 rev/min of lower high-speed stirring 20-30 minute.
Advantage of the present invention is: the auxiliary agent that the present invention adds, enhance the dispersion of cutting fluid, lubrication, film forming properties, the sodium silicate of adding can reduce the large problem of water-base cutting fluid foam, and can emulsification, soil suspension, remove the dirt in cutting fluid, it also has good cooling, cleaning, the feature such as antirust, and cutting fluid of the present invention has good lubrication, cooling, low bubble, scale removal, antirust and cleaning performance.
Embodiment
Below by specific examples, the present invention is described in detail.
A kind of low bubble descaling type water-base cutting fluid, is made up of the raw material of following weight part (kilogram): primary zinc phosphate 4, urotropine 3, Red copper oxide 0.6, polyoxyethylene alkyl amine 5, clorafin 7, stearic acid 11, carnauba wax 4, pareth sulfate 2, benzotriazole 1, sodium silicate 0.8, auxiliary agent 6, water 180;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): rosin 4, cyanuric acid zinc 1, organosilicon crylic acid latex 3, isothiazolinone 1, calglucon 2, natrosol 2, glycol ether 6, castor-oil plant acid amides 3, polyoxyethylene glycol 2, vinylcarbinol 5, Fatty alcohol polyoxyethylene polyoxypropylene ether 1, defoamer 0.3, water 45; Preparation method is that natrosol, polyoxyethylene glycol, organosilicon crylic acid latex, Fatty alcohol polyoxyethylene polyoxypropylene ether are added in water by (1), is heated to 40-50 ° of C, and it is for subsequent use to add defoamer after stirring; (2) rosin, glycol ether, vinylcarbinol, castor-oil plant acid amides are mixed and heated to 50-60 ° of C, after stirring, the product in step (1) is slowly added, stir with the rotating speed of 300-400 rev/min, the reinforced post-heating that terminates is to 70-80 ° of C, and at 1800-2000 rev/min of lower high-speed stirring 10-15 minute, then add all the other surplus materialss continuation stirring 5-10 minute.
One of the present invention low bubble descaling type water-base cutting fluid, be made up of following concrete steps:
(1) clorafin, stearic acid, carnauba wax and pareth sulfate are mixed, be heated to 50-60 ° of C, after stirring reaction 20-40 minute, obtain mixture A;
(2) 50-70 ° of C will be cooled to rapidly after water boil, then add sodium silicate and polyoxyethylene alkyl amine stirs, add auxiliary agent after stirring with 800-900 rev/min of lower stirring reaction 40-60 minute, obtain mixture B;
(3) mixture B is added in mixture A while stirring slowly, temperature is controlled, at 40-55 ° of C, after stirring, add all the other remaining components, filtered after 1400-1600 rev/min of lower high-speed stirring 20-30 minute.
Cutting fluid performance index of the present invention: emulsion stability experiment (15-30 ° C, 24h) of 5%: do not analyse oil, not graining; Rust-preventing characteristic experiment (35 ± 2 ° of C, iron and steel monolithic 24h) >=48h, without rust staining; Rust-preventing characteristic experiment (35 ± 2 ° of C, iron and steel lamination 8h) >=12h, without rust staining; Corrosion experiment (55 ± 2 ° of C, cast iron 24h) >=48h; Corrosion experiment (55 ± 2 ° of C, red copper 8h) >=12h; To lathe paint compatibility test: non-foaming, do not ftracture, be not clamminess.
Claims (2)
1. one kind low bubble descaling type water-base cutting fluid, it is characterized in that, be made up of the raw material of following weight part: primary zinc phosphate 3-5, urotropine 2-3, Red copper oxide 0.4-0.7, polyoxyethylene alkyl amine 4-6, clorafin 6-8, stearic acid 8-12, carnauba wax 3-5, pareth sulfate 2-3, benzotriazole 1-2, sodium silicate 0.6-0.8, auxiliary agent 5-7, water 150-180;
Described auxiliary agent is made up of the raw material of following weight part: rosin 3-5, cyanuric acid zinc 1-2, organosilicon crylic acid latex 2-3.5, isothiazolinone 1-2, calglucon 1-2, natrosol 1-2, glycol ether 5-7, castor-oil plant acid amides 2-3, polyoxyethylene glycol 2-4, vinylcarbinol 4-6, Fatty alcohol polyoxyethylene polyoxypropylene ether 1-2, defoamer 0.2-0.4, water 40-50; Preparation method is that natrosol, polyoxyethylene glycol, organosilicon crylic acid latex, Fatty alcohol polyoxyethylene polyoxypropylene ether are added in water by (1), is heated to 40-50 ° of C, and it is for subsequent use to add defoamer after stirring; (2) rosin, glycol ether, vinylcarbinol, castor-oil plant acid amides are mixed and heated to 50-60 ° of C, after stirring, the product in step (1) is slowly added, stir with the rotating speed of 300-400 rev/min, the reinforced post-heating that terminates is to 70-80 ° of C, and at 1800-2000 rev/min of lower high-speed stirring 10-15 minute, then add all the other surplus materialss continuation stirring 5-10 minute.
2. a kind of low bubble descaling type water-base cutting fluid according to claim 1, is characterized in that, be made up of following concrete steps:
(1) clorafin, stearic acid, carnauba wax and pareth sulfate are mixed, be heated to 50-60 ° of C, after stirring reaction 20-40 minute, obtain mixture A;
(2) 50-70 ° of C will be cooled to rapidly after water boil, then add sodium silicate and polyoxyethylene alkyl amine stirs, add auxiliary agent after stirring with 800-900 rev/min of lower stirring reaction 40-60 minute, obtain mixture B;
(3) mixture B is added in mixture A while stirring slowly, temperature is controlled, at 40-55 ° of C, after stirring, add all the other remaining components, filtered after 1400-1600 rev/min of lower high-speed stirring 20-30 minute.
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| CN201410840334.XA CN104560351A (en) | 2014-12-30 | 2014-12-30 | Low-foam descaling type water-based cutting fluid and preparation method thereof |
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| CN201410840334.XA CN104560351A (en) | 2014-12-30 | 2014-12-30 | Low-foam descaling type water-based cutting fluid and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114507527A (en) * | 2021-12-13 | 2022-05-17 | 福建中安高新材料研究院有限公司 | ITO etching solution and preparation method and application method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103666734A (en) * | 2013-12-05 | 2014-03-26 | 马鞍山市恒毅机械制造有限公司 | Water-base microscale lubricating-system cutting fluid and producing method thereof |
| CN103710120A (en) * | 2013-12-05 | 2014-04-09 | 马鞍山市恒毅机械制造有限公司 | Water-based antirust semisynthesis cutting fluid and preparation method therefor |
| CN103725401A (en) * | 2013-12-06 | 2014-04-16 | 当涂县金龙机械厂 | Water-soluble lubricating antirust cutting fluid and preparation method thereof |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103666734A (en) * | 2013-12-05 | 2014-03-26 | 马鞍山市恒毅机械制造有限公司 | Water-base microscale lubricating-system cutting fluid and producing method thereof |
| CN103710120A (en) * | 2013-12-05 | 2014-04-09 | 马鞍山市恒毅机械制造有限公司 | Water-based antirust semisynthesis cutting fluid and preparation method therefor |
| CN103725401A (en) * | 2013-12-06 | 2014-04-16 | 当涂县金龙机械厂 | Water-soluble lubricating antirust cutting fluid and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114507527A (en) * | 2021-12-13 | 2022-05-17 | 福建中安高新材料研究院有限公司 | ITO etching solution and preparation method and application method thereof |
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Application publication date: 20150429 |