CN105286134A - Method for preparing photocatalytic mouth mask - Google Patents
Method for preparing photocatalytic mouth mask Download PDFInfo
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- CN105286134A CN105286134A CN201510880301.2A CN201510880301A CN105286134A CN 105286134 A CN105286134 A CN 105286134A CN 201510880301 A CN201510880301 A CN 201510880301A CN 105286134 A CN105286134 A CN 105286134A
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Abstract
The invention discloses a method for preparing a mouth mask and particularly relates to a method for preparing a photocatalytic mouth mask. The method for preparing the photocatalytic mouth mask includes the steps that cloth is placed in traditional Chinese medicine liquid and soaked for 30-45 min, taken out, cleaned in clean water at the temperature of 25-35 DEG C, placed into a drying box and dried, and a mouth mask inner layer and a preprocessed mouth mask surface layer are obtained for use; 2-4 mass parts of silver-loading nano titanium dioxide powder, 1-2 mass parts of nano selenium powder and 1 mass part of nano silicon dioxide powder are obtained and mixed evenly, 8 mass parts of deionized water and 10 mass parts of anhydrous ethanol are added and evenly mixed, and a photocatalyst solution is obtained for use; the preprocessed mouth mask surface layer is placed in the photocatalyst solution, soaked and taken out after being soaked for 8-12 hours and dried in the shade keeping out of the sun, and the mouth mask surface layer is manufactured; the mouth mask surface layer and the mouth mask inner layer are sewn into the mouth mask. The mouth mask prepared through the method can be repeatedly used, does not contain adhesives, and is high in degrading speed and good in effect.
Description
Technical field
The present invention relates to a kind of preparation method of mouth mask, particularly relate to a kind of preparation method of photocatalysis mouth mask, it belongs to consumer goods industries.
Background technology
Mouth mask generally refers to and is worn over nose and mouth for filtering the air of turnover mouth and nose, to reach the apparatus of the gas of blocking harmful, smell, spittle turnover wearer mouth and nose.Current mouth mask is prepared from mainly with the material such as cloth or paper, is divided into disposable mask and can two kinds, reusable mouth mask.Wherein disposable breathing mask is high due to use cost, there is the problem of energy waste, and can reusable mouth mask, because use cost is low, and has the feature of energy-conserving and environment-protective, and is widely used.
Mouth mask mainly deter to as if particle, by covering the mouth of people, nose and chin portion, forming the space of and face sealing, forcing contaminated air through filtration by people's air-breathing, reach the object of filtering contaminants.Along with the fast development of industry, thing followed problem of environmental pollution is also on the rise, especially the health of haze to the mankind causes great threat, the main component aerosol of haze is particle, the specifically diameter fine particle that is less than 2.5 microns, it directly can enter human lung, is to threaten very harmful pollutant to human health at present.Usual mask body adopts the filtering material of anti-particle to make, and this mouth mask only has filtering function cannot filter this fine particle.
In order to solve the problems of the technologies described above, some photocatalytic breathing masks are developed, because photocatalyst material can produce similar photosynthetic catalytic reaction under the irradiation of sunshine or fluorescent lamp, organic pollutant degradation in air can be become carbon dioxide and water, thus reach the effect of being degraded by particulates, well solve the injury of material harmful in air to human body.
But still there is following technical problem in existing photocatalytic breathing mask, the adhesive adding bonding is all needed in preparation process, this still to have certain influence to human body, and the degradation speed of existing photocatalytic breathing mask is slower, cause still having part molecule be not degraded and enter human body, degradation effect needs to be improved further.
Summary of the invention
The present invention is exactly the preparation method of a kind of photocatalysis mouth mask provided to solve the problems of the technologies described above, and it can be reused, use cost is low, and it is not containing adhesive, more healthy, and its degradation speed is fast, good degrading effect.
In order to solve the problems of the technologies described above, the present invention is achieved through the following technical solutions:
A preparation method for photocatalysis mouth mask, its method is as follows:
Get 1-2 mass parts dried peppermint leaf, after 1-2 mass parts tarragon, 2-4 mass parts balloonflower root, 1-2 mass parts Radix Glycyrrhizae, 0.5-1.5 mass parts honeysuckle, 1-2 mass parts dandelion mix, add the water of 20-25 mass parts, be heated to 100 DEG C, at 100 DEG C, insulation decocts 30-45 minute, filters herb liquid is for subsequent use; Cloth is put into herb liquid and soaks 30-45 minute, take out after cleaning up in the clear water of 25-35 DEG C and put into drying box inner drying, obtain mouth mask internal layer and pretreatment mouth mask surface layer is for subsequent use; Get 2-4 mass parts Ag-carried nanometer titanium dioxide powder, the nanometer selenium powder of 1-2 mass parts, the nano grade silica particles of 1 mass parts mix, and the absolute ethyl alcohol of the deionized water and 10 mass parts that add 8 mass parts mixes, and obtains photocatalyst solution, for subsequent use; Pretreatment mouth mask surface layer is put into photocatalyst solution soak, soak after 8-12 hour, take out, dry in the shade at lucifuge, shady and cool place, obtained mouth mask surface layer; Mouth mask surface layer and mouth mask internal layer are stitched into mouth mask.
Above-mentioned dried peppermint leaf is 1.5 mass parts, and tarragon is 1.5 mass parts, and balloonflower root is 3 mass parts, and Radix Glycyrrhizae is 1.5 mass parts, honeysuckle is 1 mass parts, and dandelion is 1.5 mass parts.
Above-mentioned Ag-carried nanometer titanium dioxide powder is 3 mass parts, nanometer selenium powder 1.5 mass parts, nano grade silica particles 1 mass parts.
Above-mentioned decocting time is 40 minutes.
Above-mentioned soak time is 10 hours.
Owing to adopting technique scheme, the tool of the present invention being has the following advantages and effect:
The cloth making mouth mask first processes by the present invention in Chinese medicine, serve sterilization, sterilization and prophylactic effect, through verification experimental verification, it has good effect to the attachment of photocatalyst, photocatalyst solution adopts raw material of the present invention and consumption, and after acting synergistically with Chinese medicine, can reach the effect of better sterilizing, haze, anti-formaldehyde, anti-dimethylbenzene, the present invention can fast degradation organic pollution, good degrading effect.The mouth mask adopting preparation method of the present invention to obtain can be reused, use cost is low, and it is not containing adhesive, more healthy, and its degradation speed is fast, good degrading effect.
Detailed description of the invention
Face is explained in further detail the present invention with test data in conjunction with the embodiments.Following examples are only specific embodiments of the invention, but design concept of the present invention is not limited thereto, and all changes utilizing this design the present invention to be carried out to unsubstantiality, all should belong to the behavior of invading scope.
Method in following embodiment, if no special instructions, is conventional method.
embodiment 1
Get 1.5 mass parts dried peppermint leaves, after 1.5 mass parts tarragons, 3 mass parts balloonflower roots, 1.5 mass parts Radix Glycyrrhizaes, 1 mass parts honeysuckle, 1.5 mass parts dandelions mix, add the water of 22 mass parts, be heated to 100 DEG C, at 100 DEG C, be incubated decoction 40 minutes, filter herb liquid is for subsequent use; Cloth is put into herb liquid to soak 40 minutes, take out, after cleaning up in the clear water of 30 DEG C, put into drying box inner drying, obtain mouth mask internal layer and pretreatment mouth mask surface layer is for subsequent use; Get 3 mass parts Ag-carried nanometer titanium dioxide powder, the nanometer selenium powder of 1.5 mass parts, the nano grade silica particles of 1 mass parts mix, and the absolute ethyl alcohol of the deionized water and 10 mass parts that add 8 mass parts mixes, and obtains photocatalyst solution, for subsequent use; Pretreatment mouth mask surface layer being put into photocatalyst solution soaks after 10 hours, takes out, dries in the shade at lucifuge, shady and cool place, obtained mouth mask surface layer; Mouth mask surface layer and mouth mask internal layer are stitched into mouth mask.
embodiment 2
Get 1 mass parts dried peppermint leaf, after 2 mass parts tarragons, 4 mass parts balloonflower roots, 2 mass parts Radix Glycyrrhizaes, 1.5 mass parts honeysuckles, 2 mass parts dandelions mix, add the water of 20 mass parts, be heated to 100 DEG C, at 100 DEG C, be incubated decoction 30 minutes, filter herb liquid is for subsequent use; Cloth is put into herb liquid to soak 30 minutes, take out, after cleaning up in the clear water of 25 DEG C, put into drying box inner drying, obtain mouth mask internal layer and pretreatment mouth mask surface layer is for subsequent use; Get 2 mass parts Ag-carried nanometer titanium dioxide powder, the nanometer selenium powder of 2 mass parts, the nano grade silica particles of 1 mass parts mix, and the absolute ethyl alcohol of the deionized water and 10 mass parts that add 8 mass parts mixes, and obtains photocatalyst solution, for subsequent use; Pretreatment mouth mask surface layer is put into photocatalyst solution soak, soak after 8 hours, take out, dry in the shade at lucifuge, shady and cool place, obtained mouth mask surface layer; Mouth mask surface layer and mouth mask internal layer are stitched into mouth mask.
embodiment 3
Get 2 mass parts dried peppermint leaves, after 1 mass parts tarragon, 2 mass parts balloonflower roots, 1 mass parts Radix Glycyrrhizae, 0.5 mass parts honeysuckle, 1 mass parts dandelion mix, add the water of 25 mass parts, be heated to 100 DEG C, at 100 DEG C, be incubated decoction 45 minutes, filter herb liquid is for subsequent use; Cloth is put into herb liquid and soaks 30-45 minute, take out, after cleaning up in the clear water of 35 DEG C, put into drying box inner drying, obtain mouth mask internal layer and pretreatment mouth mask surface layer is for subsequent use; Get 4 mass parts Ag-carried nanometer titanium dioxide powder, the nanometer selenium powder of 1 mass parts, the nano grade silica particles of 1 mass parts mix, and the absolute ethyl alcohol of the deionized water and 10 mass parts that add 8 mass parts mixes, and obtains photocatalyst solution, for subsequent use; Pretreatment mouth mask surface layer is put into photocatalyst solution soak, soak after 12 hours, take out, dry in the shade at lucifuge, shady and cool place, obtained mouth mask surface layer; Mouth mask surface layer and mouth mask internal layer are stitched into mouth mask.
embodiment 4
Get 1.3 mass parts dried peppermint leaves, after 1.7 mass parts tarragons, 2.7 mass parts balloonflower roots, 1.3 mass parts Radix Glycyrrhizaes, 1.2 mass parts honeysuckles, 1.7 mass parts dandelions mix, add the water of 22 mass parts, be heated to 100 DEG C, at 100 DEG C, be incubated decoction 35 minutes, filter herb liquid is for subsequent use; Cloth is put into herb liquid to soak 35 minutes, take out, after cleaning up in the clear water of 28 DEG C, put into drying box inner drying, obtain mouth mask internal layer and pretreatment mouth mask surface layer is for subsequent use; Get 2.6 mass parts Ag-carried nanometer titanium dioxide powder, the nanometer selenium powder of 1.7 mass parts, the nano grade silica particles of 1 mass parts mix, and the absolute ethyl alcohol of the deionized water and 10 mass parts that add 8 mass parts mixes, and obtains photocatalyst solution, for subsequent use; Pretreatment mouth mask surface layer is put into photocatalyst solution soak, soak after 9 hours, take out, dry in the shade at lucifuge, shady and cool place, obtained mouth mask surface layer; Mouth mask surface layer and mouth mask internal layer are stitched into mouth mask.
embodiment 5
Get 1.7 mass parts dried peppermint leaves, after 1.3 mass parts tarragons, 3.5 mass parts balloonflower roots, 1.7 mass parts Radix Glycyrrhizaes, 0.8 mass parts honeysuckle, 1.4 mass parts dandelions mix, add the water of 24 mass parts, be heated to 100 DEG C, at 100 DEG C, be incubated decoction 42 minutes, filter herb liquid is for subsequent use; Cloth is put into herb liquid to soak 42 minutes, take out, after cleaning up in the clear water of 32 DEG C, put into drying box inner drying, obtain mouth mask internal layer and pretreatment mouth mask surface layer is for subsequent use; Get 3.5 mass parts Ag-carried nanometer titanium dioxide powder, the nanometer selenium powder of 1.3 mass parts, the nano grade silica particles of 1 mass parts mix, and the absolute ethyl alcohol of the deionized water and 10 mass parts that add 8 mass parts mixes, and obtains photocatalyst solution, for subsequent use; Pretreatment mouth mask surface layer is put into photocatalyst solution soak, soak after 11 hours, take out, dry in the shade at lucifuge, shady and cool place, obtained mouth mask surface layer; Mouth mask surface layer and mouth mask internal layer are stitched into mouth mask.
Prepare straw decomposing inoculant by embodiment 1-5 method and a kind of bacterial classification of independent inoculation, result of the test is as follows:
Mouth mask in use, detect by this area conventional method, can by close to the organic pollutant degradation in 2 centimetres, mouth mask within 0.5-1 second, wherein embodiment 1 best results was 0.5 second, and after using after 150 times repeatedly cleaning, use, effect still can reach the organic pollutant degradation in 0.7-1.3 time second 2 centimetres.
Claims (5)
1. the preparation method of a photocatalysis mouth mask, it is characterized in that method is as follows: get 1-2 mass parts dried peppermint leaf, after 1-2 mass parts tarragon, 2-4 mass parts balloonflower root, 1-2 mass parts Radix Glycyrrhizae, 0.5-1.5 mass parts honeysuckle, 1-2 mass parts dandelion mix, add the water of 20-25 mass parts, be heated to 100 DEG C, at 100 DEG C, insulation decocts 30-45 minute, filters herb liquid is for subsequent use; Cloth is put into herb liquid and soaks 30-45 minute, take out after cleaning up in the clear water of 25-35 DEG C and put into drying box inner drying, obtain mouth mask internal layer and pretreatment mouth mask surface layer is for subsequent use; Get 2-4 mass parts Ag-carried nanometer titanium dioxide powder, the nanometer selenium powder of 1-2 mass parts, the nano grade silica particles of 1 mass parts mix, and the absolute ethyl alcohol of the deionized water and 10 mass parts that add 8 mass parts mixes, and obtains photocatalyst solution, for subsequent use; Pretreatment mouth mask surface layer is put into photocatalyst solution soak, soak after 8-12 hour, take out, dry in the shade at lucifuge, shady and cool place, obtained mouth mask surface layer; Mouth mask surface layer and mouth mask internal layer are stitched into mouth mask.
2. the preparation method of a kind of photocatalysis mouth mask according to claim 1, it is characterized in that described dried peppermint leaf is 1.5 mass parts, tarragon is 1.5 mass parts, and balloonflower root is 3 mass parts, Radix Glycyrrhizae is 1.5 mass parts, honeysuckle is 1 mass parts, and dandelion is 1.5 mass parts.
3. the preparation method of a kind of photocatalysis mouth mask according to claim 1, is characterized in that described Ag-carried nanometer titanium dioxide powder is 3 mass parts, nanometer selenium powder 1.5 mass parts, nano grade silica particles 1 mass parts.
4. the preparation method of a kind of photocatalysis mouth mask according to claim 1, is characterized in that described decocting time is 40 minutes.
5. the preparation method of a kind of photocatalysis mouth mask according to claim 1, is characterized in that described soak time is 10 hours.
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| CN201510880301.2A CN105286134A (en) | 2015-12-07 | 2015-12-07 | Method for preparing photocatalytic mouth mask |
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| CN201510880301.2A CN105286134A (en) | 2015-12-07 | 2015-12-07 | Method for preparing photocatalytic mouth mask |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107114835A (en) * | 2017-04-10 | 2017-09-01 | 浙江工业大学 | A kind of anti-mercury mouth mask |
| CN107715589A (en) * | 2016-03-22 | 2018-02-23 | 蒋志超 | A kind of anti-haze spray |
| CN108208966A (en) * | 2016-12-12 | 2018-06-29 | 刘婷婷 | A kind of production method of antibacterial mask |
| CN114468416A (en) * | 2020-10-23 | 2022-05-13 | 亿利新材料有限公司 | Prevent antibacterial cool type gauze mask of haze |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107715589A (en) * | 2016-03-22 | 2018-02-23 | 蒋志超 | A kind of anti-haze spray |
| CN108208966A (en) * | 2016-12-12 | 2018-06-29 | 刘婷婷 | A kind of production method of antibacterial mask |
| CN107114835A (en) * | 2017-04-10 | 2017-09-01 | 浙江工业大学 | A kind of anti-mercury mouth mask |
| CN114468416A (en) * | 2020-10-23 | 2022-05-13 | 亿利新材料有限公司 | Prevent antibacterial cool type gauze mask of haze |
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Application publication date: 20160203 |
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