CN105273617A - Preparation method for high temperature-resistant organosilicon coating - Google Patents
Preparation method for high temperature-resistant organosilicon coating Download PDFInfo
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- CN105273617A CN105273617A CN201410325173.0A CN201410325173A CN105273617A CN 105273617 A CN105273617 A CN 105273617A CN 201410325173 A CN201410325173 A CN 201410325173A CN 105273617 A CN105273617 A CN 105273617A
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Abstract
The invention discloses a preparation method for a high temperature-resistant organosilicon coating. The preparation method comprises the following steps: weighing, by mass, 45 to 60% of grafted organosilicon resin and 2 to 4% of an auxiliary agent, adding the grafted organosilicon resin and the auxiliary agent into a dispersion cylinder and carrying out stirring at a speed of 400 to 500 r/min for 8 to 12 min so as to prepare a uniform premix; and weighing, by mass, 35 to 45% of a heatproof pigment aluminum powder, adding the heatproof pigment aluminum powder into the prepared premix under stirring, adjusting a rotating speed to be 400 to 600 r/min, carrying out stirring for 25 to 50 min and controlling the temperature of the dispersion cylinder to be no more than 45 DEG C, detection viscosity of no less than 95 s and solid content of no less than 75% so as to prepare the organosilicon coating. The organosilicon coating prepared in the invention can be constructed by spraying, brushing and roller coating and withstand a high temperature of 800 DEG C and has strong corrosion resistance.
Description
Technical field
The invention belongs to paint field, be specifically related to a kind of preparation method of high-temperature resistant silicone coating.
Background technology
Face the future the development trend of " low-carbon (LC) ", and high temperature organosilicon paint industry early has preparation in fact.In recent years, coating industry is devoted to exploitation low stain, high solid or solvent-free (comprising powder, photocuring) coating, water-borne coatings (organosilicon heat-resistant lacquer) always; The anti-soil technology of exploitation low environment risk and antifouling paint; The rust-stabilising pigment of exploitation non-lead, chromium and substitute develop the process for cleanly preparing of titanium dioxide, iron oxide pigment; Positive formulation coating industry process for cleanly preparing judgement criterias etc., to promote the development of coating industry novel process, novel material and new technology.In addition, the new coatings such as the glass energy-saving coating developed in recent years, heat loss through radiation High tailored coating, sunshade thermal insulation coating, high temperature resistant sealing paint, efficient resistance to stained solar heat absorbing coating, also on " low-carbon (LC) " road, new opportunity to develop is brought for coating industry, but in high-temperature resistant coating for comparatively high temps as 600 degree with the weathering resistance of coating, especially erosion resistance, still Shortcomings.
Summary of the invention
The invention provides a kind of preparation method of resistant to elevated temperatures organosilicon coating, the corrosion resistant performance that its obtained coating has still had when 800 degree of temperature.
A preparation method for high-temperature resistant silicone coating, comprises the following steps:
(1) get grafted-organosilicon resin 45-60% by mass parts, auxiliary agent 2%-4% puts in dispersion cylinder and stirs, and stirring velocity is that 400-500 turns/min, stirs 8-12 minute obtained uniform pre-composition;
(2) get heat resistant pigment aluminium powder 35-45% by mass parts adds in the obtained pre-composition of step (1) under whipped state, adjusting rotary speed is that 400-600 turns/min, churning time is 25-50 minute, control dispersion cylinder temperature≤45 DEG C, inspection viscosimetric≤95s, Gu Han Liang≤75%, obtained organosilicon coating.
Wherein said grafted-organosilicon resin is for containing moisture curing organic resin.
The organosilicon coating that the preparation method of high-temperature resistant silicone coating obtains, containing grafted-organosilicon resin 45-58%(weight part), heat resistant pigment aluminium powder 35-45%(weight part), auxiliary agent 2%-4%(weight part).
The preparation method of high-temperature resistant silicone coating of the present invention prepares on production line at existing coating and just can realize, do not need to increase new facility investment, and obtained high-temperature resistant silicone coating can adopt spraying coating process, brush, roll coating process is constructed, 800 degree of high temperature can be stood for a long time, and there is corrosion resistant performance.
Embodiment
Below by way of specific embodiment, the specific embodiment of the present invention is described further.
Embodiment one:
First grafted-organosilicon resin 45% is got; Heat resistant pigment 35%; Auxiliary agent 4%, by mass percentage.By silicone resin, auxiliary agent, put in dispersion cylinder, turn on agitator slowly stirs, and stirring velocity is 400 turns/min, stirs after 10 minutes, estimate its evenly after, to be added under whipped state by aluminium powder, adjusting rotary speed is 400 turns/min again, and churning time is 50 minutes, control dispersion cylinder temperature≤45 DEG C (jacketed type device can be adopted if desired), inspection viscosimetric≤95s, Gu containing amount≤75%, obtain finished product.
Result of use: above-mentioned formula making sheet is made 5 pieces of test plate (panel)s respectively, wherein one piece is done measuring mechanical property, and all the other do chemical property test, thickness 60 microns, and after paint film maintains 10 days, to the test of its Progressive symmetric erythrokeratodermia energy limit, result is as follows:
The performance data of the organic silicon coating of a kind of 700 degree of high temperature obtained by table 1 embodiment 1
Embodiment two:
First grafted-organosilicon resin silicone resin 60% is got; Heat resistant pigment 35%; Auxiliary agent 2%, by mass percentage.
By silicone resin, auxiliary agent, put in dispersion cylinder, turn on agitator slowly stirs, and stirring velocity is 500 turns/min, stirs after 8 minutes, estimate its evenly after, to be added under whipped state by aluminium powder, adjusting rotary speed is 600 turns/min again, and churning time is 25 minutes, control dispersion cylinder temperature≤45 DEG C (jacketed type device can be adopted if desired), inspection viscosimetric≤95s, Gu containing amount≤75%, obtain finished product.
Result of use: above-mentioned formula making sheet is made 5 pieces of test plate (panel)s respectively, wherein one piece is done measuring mechanical property, and all the other do chemical property test, thickness 80 microns, and after paint film maintains 7 days, carry out performance test to it, result is as follows:
Embodiment three:
First grafted-organosilicon resin 58% is got; Heat resistant pigment 45%; Auxiliary agent 4%, by mass percentage.
By silicone resin, auxiliary agent, put in dispersion cylinder, turn on agitator slowly stirs, and stirring velocity is 400 turns/min, stirs after 12 minutes, estimate its evenly after, to be added under whipped state by aluminium powder, adjusting rotary speed is 480 turns/min again, and churning time is 45 minutes, control dispersion cylinder temperature≤45 DEG C (jacketed type device can be adopted if desired), inspection viscosimetric≤95s, Gu containing amount≤75%, obtain finished product.
Result of use: above-mentioned formula making sheet is made 5 pieces of test plate (panel)s respectively, wherein one piece is done measuring mechanical property, and all the other do chemical property test, thickness 80 microns, and after paint film maintains 7 days, carry out performance test to it, result is as follows:
The coating test data obtained by above-mentioned three embodiments can find out to have good chemical property performance, and a kind of 800 degree of resistant to elevated temperatures organosilyl utilizations of the present invention, can make original function greatly strengthen, reduce corrosive problem that Yin Gaowen brings.
The invention is not restricted to previous embodiment, those of ordinary skill in the art can do other various corresponding change and distortion according to the technical conceive of technical solution of the present invention.But all these change the protection domain that all should belong to the application's claim with distortion.
Claims (3)
1. a preparation method for high-temperature resistant silicone coating, is characterized in that comprising the following steps:
(1) get grafted-organosilicon resin 45-60% by mass parts, auxiliary agent 2%-4% puts in dispersion cylinder and stirs, and stirring velocity is that 400-500 turns/min, stirs 8-12 minute obtained uniform pre-composition;
(2) get heat resistant pigment aluminium powder 35-45% by mass parts adds in the obtained pre-composition of step (1) under whipped state, adjusting rotary speed is that 400-600 turns/min, churning time is 25-50 minute, control dispersion cylinder temperature≤45 DEG C, inspection viscosimetric≤95s, Gu Han Liang≤75%, obtained organosilicon coating.
2. the preparation method of high-temperature resistant silicone coating as claimed in claim 1, is characterized in that described grafted-organosilicon resin is for containing moisture curing organic resin.
3. the organosilicon coating obtained by the preparation method of high-temperature resistant silicone coating described in claim 1, it is characterized in that, described coating contains grafted-organosilicon resin 45-58%(weight part), heat resistant pigment aluminium powder 35-45%(weight part), auxiliary agent 2%-4%(weight part).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410325173.0A CN105273617A (en) | 2014-07-09 | 2014-07-09 | Preparation method for high temperature-resistant organosilicon coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410325173.0A CN105273617A (en) | 2014-07-09 | 2014-07-09 | Preparation method for high temperature-resistant organosilicon coating |
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| Publication Number | Publication Date |
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| CN105273617A true CN105273617A (en) | 2016-01-27 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410325173.0A Pending CN105273617A (en) | 2014-07-09 | 2014-07-09 | Preparation method for high temperature-resistant organosilicon coating |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105949988A (en) * | 2016-05-31 | 2016-09-21 | 无锡伊佩克科技有限公司 | Boron modified polyurethane composite coating and preparation method thereof |
| CN107541142A (en) * | 2017-10-17 | 2018-01-05 | 江苏欣安新材料技术有限公司 | A kind of high temperature organosilicon paint and its production method |
-
2014
- 2014-07-09 CN CN201410325173.0A patent/CN105273617A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105949988A (en) * | 2016-05-31 | 2016-09-21 | 无锡伊佩克科技有限公司 | Boron modified polyurethane composite coating and preparation method thereof |
| CN107541142A (en) * | 2017-10-17 | 2018-01-05 | 江苏欣安新材料技术有限公司 | A kind of high temperature organosilicon paint and its production method |
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Application publication date: 20160127 |
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| WD01 | Invention patent application deemed withdrawn after publication |