CN105267088A - Lotus seed core honeysuckle nectar moisturizing skin lotion and preparation method thereof - Google Patents
Lotus seed core honeysuckle nectar moisturizing skin lotion and preparation method thereof Download PDFInfo
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- CN105267088A CN105267088A CN201510651156.0A CN201510651156A CN105267088A CN 105267088 A CN105267088 A CN 105267088A CN 201510651156 A CN201510651156 A CN 201510651156A CN 105267088 A CN105267088 A CN 105267088A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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Abstract
The invention discloses a lotus seed core honeysuckle nectar moisturizing skin lotion and a preparation method thereof. The lotus seed core honeysuckle nectar moisturizing skin lotion provided by the invention comprises the following components by weight: 0.1-1 part of a surfactant, 1-10 parts of glycerin, 0.1-2 parts of vitamin E, 0.1-2 parts of amino acids, 0.1-2 parts of beet extracted liquid, 0.1-2 parts of aloe extracted liquid, 0.1-5 parts of lotus seed core extracted liquid, 0.1-5 parts of honeysuckle extracted liquid, 0.1-0.5 part of Germall plus, 0.1-1 part of allantoin, 0.1-0.5 part of honeysuckle essential oil, 0.1-0.5 part of lotus seed core essential oil, and 68.5-97.9 part of active water. The lotus seed core honeysuckle nectar moisturizing skin lotion provided by the invention has the advantages of simple making process, short making period, safety and no toxic or side effect.
Description
Technical field
The present invention relates to technical field of skin care.More particularly, the present invention relates to a kind of embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid and preparation method thereof.
Background technology
Along with the development of society and the raising of living standard, people more and more pay attention to beauty treatment and make up.Liking to be beautiful is the nature of people, and skin care, slow down aging, to keep the youth here be the dream that numerous women pursues, so all kinds of cosmetics and skincare product has just become one of approach of realizing their dream.Water preparation class skin care item are the important a member in skin-care cosmetics, but for a long time, formula is simple, and component is single, and makees base material with a large amount of pure water, and this is the common defects of traditional water preparation class skin care item; Some by amount of grease dispersion water preparation class skin care item wherein then due to cost, the restriction of the factors such as stability, effect level of skin protection water preparation significantly can not be promoted, even some water preparations still rest on the conceptual phase of falling short of the reality, and can not play larger effect in beauty and skin care process.
Calcium in Semen Nelumbinis, phosphorus and potassium content are very abundant, containing 81.3 grams, protein in per kilogram Semen Nelumbinis, and 9.8 grams, fat, sugar 304 milligrams, calcium 436 milligrams, 1.397 milligrams, phosphorus, ferrum 31.4 milligrams, also containing materials such as other multivitamins, trace element, nuciferine, Herba Melicae Scabrosae glycosides, except can forming the composition of skeleton and tooth, promote blood coagulation in addition, make some enzyme activation, maintain nerve conductivity, calm neural, maintain the effect such as the retractility of muscle and the rhythm and pace of moving things of heart beating.Abundant phosphorus or the key component of Nuclear extract, help body to carry out protein, fat, carbohydate metabolism, and maintain acid-base balance, also play an important role to the formation of sperm.Semen Nelumbinis have the sedate effect that nourishes heart.Middle-aged and elderly people particularly brain worker often eats, can brain-strengthening, and memory reinforcing, increases work efficiency, and can prevent the generation of senile dementia.The core that Semen Nelumbinis central authorities are green, claim embryo nelumbinis, containing the multiple alkaloid such as liensinine, isoliensinine, taste is extremely bitter, has the function of clearing away heat-fire, also has significant cardiotonic, can expand peripheral blood vessel, reduce blood pressure.Can aphtha of the mouth and tongue be treated, and conduce to sleep.
Flos Lonicerae to various pathogens as staphylococcus aureus, Hemolytic streptococcus, escherichia coli, dysentery bacterium, vibrio cholera, Bacillus typhi, Salmonella paratyphi etc. all have certain inhibitory action.Flos Lonicerae sweet in the mouth, cold in nature, there is the effect of heat-clearing and toxic substances removing, dispelling wind and heat pathogens.Flos Lonicerae has heat-clearing and toxic substances removing, dredges the effect of throat, relieving restlessness of relieving summer heat.The effect of Flos Lonicerae is except medicinal, and its beauty treatment, fat-reducing and the effect of health care are more magical, and the huge protection play health and repair are very significant.Effect of Flos Lonicerae has expelling summer-heat, relieving alcoholic intoxication, cephalocathartic, quenches one's thirst, noxious substance in purged body, the effectiveness of blood fat reducing, fat-reducing, skin cleaning and beauty, in advance anti-aging, life lengthening.
Radix Betae sweet in the mouth, property is put down micro-cool, the effects such as energy invigorating the stomach and promoting digestion, relieving cough and resolving phlegm, pleasant diuresis, heat reliving and toxin-eliminating, liver detoxification.Mineral compound contained by it and plant compound are that Radix Betae is distinctive, these compound energy infection, increase cell oxygen content, improve skin water activity, promote that skin water balance increases elasticity of skin, make skin more soft and smooth, more healthy, improve the self regulation level of skin.
Summary of the invention
An object of the present invention is to solve at least the problems referred to above and defect, and the advantage will illustrated after providing.
A further object of the invention is to provide a kind of embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid, chemical products is relied on to improve the problem of skin quality for existing beauty and skin care product, utilize Radix Betae, the innate efficacy of embryo nelumbinis and Flos Lonicerae extractive solution nourishes skin, in outward appearance, Radix Betae extracting solution is aubergine, last finished product is claret, there is great identification, achieve unique aesthetic feeling that this embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid outward appearance is beautiful, due to people use time, good replenishing water and preserving moisture can not only be reached, tender white beautiful skin, moisten smooth, effect, good psychological cosmetic result can also be reached.
A further object of the invention is by the mixed proportion of embryo nelumbinis extracting solution and Flos Lonicerae extractive solution is adjusted to optimal proportion, make the effective ingredient optimization from described two kinds of medical materials, detect described extract component in acne-removing inflammation-diminishing, the effect recovering impaired skin barrier function, and on the basis of described testing result, provide the compositions of a kind of acne-removing inflammation-diminishing and the differentiation of induced skin keratinocyte.
A further object of the invention is irradiated Radix Betae by the long wave ultraviolet of proper strength, far infrared and X-ray, coerce the betanin accumulated in beet cell matter to be secreted, and the cell wall of Radix Betae is destroyed, the nitrate in Radix Betae, folic acid and the vitamin B12 with nature redness at utmost discharge.
A further object of the invention is by carrying out low-frequency vibration process before obtained finished product, and the hydrogen bond angle of liquid will broaden significantly, combines to manufacture stronger molecule.This can reduce acidity and the basicity of water effectively, and its pH pH-value reached between 6.9-7.2 is balanced.By the change of hydrogen bond, water can reassemble into the frequency of similar human body cell in order to absorption of human body, effectively can increase the water content of skin.
To achieve these goals, the invention provides a kind of embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid, be made up of the component of following weight proportion: surfactant 0.1-1 weight portion, glycerol 1-10 weight portion, vitamin E 0.1-2 weight portion, aminoacid 0.1-2 weight portion, Radix Betae extracting solution 0.1-2 weight portion, Aloe extraction solution 0.1-2 weight portion, embryo nelumbinis extracting solution 0.1-5 weight portion, Flos Lonicerae extractive solution 0.1-5 weight portion, germall 0.1-0.5 weight portion, allantoin 0.1-1 weight portion, Flos Lonicerae quintessence oil 0.1-0.5 weight portion, embryo nelumbinis quintessence oil 0.1-0.5 weight portion and activated water 68.5-97.9 weight portion.
Preferably, described surfactant is one or more in polyacrylic acid, C13-14 isoparaffin and tridecyl alcohol.
Preferably, described aminoacid is one or more in lact albumin hydrolysate and Herba bromi japonici aminoacid.
A preparation method for embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid, comprises the following steps:
Step one, get 8/10 of described activated water by weight and pour emulsifying pot into, again surfactant and glycerol are added in emulsifying pot successively, stir with the speed of 900 revs/min and insulation after being warming up to 70-75 DEG C, stir and within 15 minutes, obtain A material, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: surfactant 0.1-1 weight portion, glycerol 1-10 weight portion;
Step 2, the emulsifying pot in step one is evacuated to-0.06 ~-0.04Mpa, suction vitamin E and aminoacid after temperature is down to 60 DEG C, insulated and stirred obtains B material for 10 minutes, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: vitamin E 0.1-2 weight portion, aminoacid 0.1-2 weight portion; And
Step 3, it is in 1/10 of described magnetic water that germall and allantoin are dissolved in weight portion respectively, temperature in pot to be emulsified is down to 45 DEG C, by germall, allantoin, Radix Betae extracting solution, Aloe extraction solution, embryo nelumbinis extracting solution and Flos Lonicerae extractive solution are once fed in emulsifying pot, stir 30 minutes under the pressure of-0.08 ~-0.06Mpa, get product through 100 order single layer filter cloth impurity screenings, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: Radix Betae extracting solution 0.1-2 weight portion, Aloe extraction solution 0.1-2 weight portion, embryo nelumbinis extracting solution 0.1-5 weight portion, Flos Lonicerae extractive solution 0.1-5 weight portion, germall 0.1-0.5 weight portion, allantoin 0.1-1 weight portion, Flos Lonicerae quintessence oil 0.1-0.5 weight portion, embryo nelumbinis quintessence oil 0.1-0.5 weight portion.
Preferably, the preparation method of described Radix Betae extracting solution comprises: at 5-15 DEG C, the Radix Betae of fresh clean is cut into 1-3cm
3square fragment, use long wave ultraviolet, the far infrared of 800 μm and the X-ray of 0.5 dust that wavelength is 350nm to irradiate 10-20min simultaneously, send into squeezing in double-screw type squeezer, pH extract and press liquor is regulated to be transferred in Microwave Extraction Apparatus after 7.5, filter after microwave extracting 60min under the condition of 800W and be extracted liquid, at 30 DEG C, vacuum concentration to density is 1.1-1.3g/m
3, obtain Radix Betae extracting solution.
Preferably, the preparation method of described Flos Lonicerae extractive solution comprises: the Flos Lonicerae powder of 20 weight portions is broken to 20-50 order, and is added to the soak by water 1 hour of 200 weight portions after the mixing of 1 weight portion Sal, filters and obtains Aqueous extracts, for subsequent use; To filter gained Flos Lonicerae and add the alcohol heating reflux 3 times of 200 weight portions, and collect alcohol extract, mix with described Aqueous extracts, vacuum concentration is to without alcohol and density is 1.1-1.3g/cm
3, obtain Flos Lonicerae extractive solution.
Preferably, the preparation method of described embryo nelumbinis extracting solution comprises: embryo nelumbinis is crushed to 10 orders, adds 80 DEG C of water soakings and decocts 1 hour at 90 DEG C after 3 hours, filter to obtain embryo nelumbinis Aqueous extracts, for subsequent use; By decocting, to filter the embryo nelumbinis that obtains and volumetric concentration be afterwards soak 5 hours at the alcoholic solution of 80 weight portions is blended in 60 DEG C, filter, collect embryo nelumbinis and soak respectively, embryo nelumbinis is put into percolating device, use soak to carry out percolation, controlling percolation flow velocity is 5L/h, obtains embryo nelumbinis percolate, mix with described embryo nelumbinis Aqueous extracts, vacuum concentration is to without alcohol and density is 1.1-1.3g/cm
3, obtain embryo nelumbinis extracting solution.
Preferably, also need to carry out low-frequency vibration process 30min that frequency be the electronic impulse of 0.9KHz after filtering in described step 3, regulate pH to be 7.1, density is 1.1g/cm
3be finished product.
Beneficial effect
1, chemical products is relied on to improve the problem of skin quality for existing beauty and skin care product, the innate efficacy of Radix Betae, embryo nelumbinis and Flos Lonicerae extractive solution is utilized to nourish skin, in outward appearance, Radix Betae extracting solution is aubergine, last finished product is claret, there is great identification, achieve unique aesthetic feeling that this embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid outward appearance is beautiful, due to people use time, good replenishing water and preserving moisture, tender white beautiful skin can not only be reached, moisten smooth, effect, good psychological cosmetic result can also be reached.
2, by the mixed proportion of embryo nelumbinis extracting solution and Flos Lonicerae extractive solution is adjusted to optimal proportion, make the effective ingredient optimization from described two kinds of medical materials, detect described extract component in acne-removing inflammation-diminishing, the effect recovering impaired skin barrier function, and on the basis of described testing result, provide the compositions of a kind of acne-removing inflammation-diminishing and the differentiation of induced skin keratinocyte.
3, by the long wave ultraviolet of proper strength, far infrared and X-ray, Radix Betae is irradiated, coerce the betanin accumulated in beet cell matter to be secreted, and the cell wall of Radix Betae is destroyed, the nitrate in Radix Betae, folic acid and the vitamin B12 with nature redness at utmost discharge.
4, by carrying out low-frequency vibration process before obtained finished product, the hydrogen bond angle of liquid will broaden significantly, combines to manufacture stronger molecule.This can reduce acidity and the basicity of water effectively, and its pH pH-value reached between 6.9-7.2 is balanced.By the change of hydrogen bond, water can reassemble into the frequency of similar human body cell in order to absorption of human body, effectively can increase the water content of skin.
Part is embodied by explanation below by other advantage of the present invention, target and feature, part also will by research and practice of the present invention by those skilled in the art is understood.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, can implement according to this with reference to description word to make those skilled in the art.
Should be appreciated that used hereinly such as " to have ", other element one or more do not allotted in " comprising " and " comprising " term or the existence of its combination or interpolation.
Embodiment 1
A preparation method for embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid, comprises the following steps:
Step one, pour emulsifying pot into by 8/10 of activated water described in 97.9 weight portions, again polyacrylic acid and glycerol are added in emulsifying pot successively, stir with the speed of 900 revs/min and insulation after being warming up to 70 DEG C, stir and within 15 minutes, obtain A material, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: surfactant 0.1 weight portion, glycerol 1 weight portion;
Step 2, the emulsifying pot in step one is evacuated to-0.06Mpa, suction vitamin E and lact albumin hydrolysate after temperature is down to 60 DEG C, insulated and stirred obtains B material for 10 minutes, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: vitamin E 0.1 weight portion, lact albumin hydrolysate 0.1 weight portion; And
Step 3, germall and allantoin are dissolved in 1/10 of magnetic water described in 97.9 weight portions respectively, temperature in pot to be emulsified is down to 45 DEG C, by germall, allantoin, Radix Betae extracting solution, Aloe extraction solution, embryo nelumbinis extracting solution and Flos Lonicerae extractive solution are once fed in emulsifying pot, stir 30 minutes under the pressure of-0.08Mpa, get product through 100 order single layer filter cloth impurity screenings, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: Radix Betae extracting solution 0.1 weight portion, Aloe extraction solution 0.1 weight portion, embryo nelumbinis extracting solution 0.1 weight portion, Flos Lonicerae extractive solution 0.1 weight portion, germall 0.1 weight portion, allantoin 0.1 weight portion, Flos Lonicerae quintessence oil 0.1 weight portion, embryo nelumbinis quintessence oil 0.1 weight portion.
The preparation method of described Flos Lonicerae extractive solution comprises: the Flos Lonicerae powder of 20 weight portions is broken to 20 orders, and is added to the soak by water 1 hour of 200 weight portions after the mixing of 1 weight portion Sal, filters and obtains Aqueous extracts, for subsequent use; To filter gained Flos Lonicerae and add the alcohol heating reflux 3 times of 200 weight portions, and collect alcohol extract, mix with described Aqueous extracts, vacuum concentration is to without alcohol and density is 1.1g/cm
3, obtain Flos Lonicerae extractive solution.
The preparation method of described embryo nelumbinis extracting solution comprises: embryo nelumbinis is crushed to 10 orders, adds 80 DEG C of water soakings and decocts 1 hour at 90 DEG C after 3 hours, filter to obtain embryo nelumbinis Aqueous extracts, for subsequent use; By decocting, to filter the embryo nelumbinis that obtains and volumetric concentration be afterwards soak 5 hours at the alcoholic solution of 80 weight portions is blended in 60 DEG C, filter, collect embryo nelumbinis and soak respectively, embryo nelumbinis is put into percolating device, use soak to carry out percolation, controlling percolation flow velocity is 5L/h, obtains embryo nelumbinis percolate, mix with described embryo nelumbinis Aqueous extracts, vacuum concentration is to without alcohol and density is 1.1g/cm
3, obtain embryo nelumbinis extracting solution.
Embodiment 2
A preparation method for embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid, comprises the following steps:
Step one, pour emulsifying pot into by 8/10 of activated water described in 80 weight portions, again C13-14 isoparaffin and glycerol are added in emulsifying pot successively, stir with the speed of 900 revs/min and insulation after being warming up to 73 DEG C, stir and within 15 minutes, obtain A material, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: surfactant 0.6 weight portion, glycerol 8 weight portion;
Step 2, the emulsifying pot in step one is evacuated to-0.05Mpa, suction vitamin E and Herba bromi japonici aminoacid after temperature is down to 60 DEG C, insulated and stirred obtains B material for 10 minutes, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: vitamin e1 weight portion, Herba bromi japonici amino acid/11 weight portion; And
Step 3, germall and allantoin are dissolved in 1/10 of magnetic water described in 80 weight portions respectively, temperature in pot to be emulsified is down to 45 DEG C, by germall, allantoin, Radix Betae extracting solution, Aloe extraction solution, embryo nelumbinis extracting solution and Flos Lonicerae extractive solution are once fed in emulsifying pot, stir 30 minutes under the pressure of-0.07Mpa, get product through 100 order single layer filter cloth impurity screenings, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: Radix Betae extracting solution 1 weight portion, Aloe extraction solution 1 weight portion, embryo nelumbinis extracting solution 4 weight portion, Flos Lonicerae extractive solution 3 weight portion, germall 0.3 weight portion, allantoin 0.5 weight portion, Flos Lonicerae quintessence oil 0.3 weight portion, embryo nelumbinis quintessence oil 0.3 weight portion.
The preparation method of described Flos Lonicerae extractive solution comprises: the Flos Lonicerae powder of 20 weight portions is broken to 30 orders, and is added to the soak by water 1 hour of 200 weight portions after the mixing of 1 weight portion Sal, filters and obtains Aqueous extracts, for subsequent use; To filter gained Flos Lonicerae and add the alcohol heating reflux 3 times of 200 weight portions, and collect alcohol extract, mix with described Aqueous extracts, vacuum concentration is to without alcohol and density is 1.2g/cm
3, obtain Flos Lonicerae extractive solution.
The preparation method of described embryo nelumbinis extracting solution comprises: embryo nelumbinis is crushed to 10 orders, adds 80 DEG C of water soakings and decocts 1 hour at 90 DEG C after 3 hours, filter to obtain embryo nelumbinis Aqueous extracts, for subsequent use; By decocting, to filter the embryo nelumbinis that obtains and volumetric concentration be afterwards soak 5 hours at the alcoholic solution of 80 weight portions is blended in 60 DEG C, filter, collect embryo nelumbinis and soak respectively, embryo nelumbinis is put into percolating device, use soak to carry out percolation, controlling percolation flow velocity is 5L/h, obtains embryo nelumbinis percolate, mix with described embryo nelumbinis Aqueous extracts, vacuum concentration is to without alcohol and density is 1.2g/cm
3, obtain embryo nelumbinis extracting solution.
Embodiment 3
Step one, pour emulsifying pot into by 8/10 of activated water described in 68.5 weight portions, again tridecyl alcohol and glycerol are added in emulsifying pot successively, stir with the speed of 900 revs/min and insulation after being warming up to 75 DEG C, stir and within 15 minutes, obtain A material, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: tridecyl alcohol 1 weight portion, glycerol 10 weight portion;
Step 2, the emulsifying pot in step one is evacuated to-0.04Mpa, suction vitamin E and lact albumin hydrolysate after temperature is down to 60 DEG C, insulated and stirred obtains B material for 10 minutes, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: vitamin E2 weight portion, lact albumin hydrolysate 2 weight portion; And
Step 3, it is in 1/10 of described magnetic water that germall and allantoin are dissolved in weight portion respectively, temperature in pot to be emulsified is down to 45 DEG C, by germall, allantoin, Radix Betae extracting solution, Aloe extraction solution, embryo nelumbinis extracting solution and Flos Lonicerae extractive solution are once fed in emulsifying pot, stir 30 minutes under the pressure of-0.06Mpa, get product through 100 order single layer filter cloth impurity screenings, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: Radix Betae extracting solution 2 weight portion, Aloe extraction solution 2 weight portion, embryo nelumbinis extracting solution 5 weight portion, Flos Lonicerae extractive solution 5 weight portion, germall 0.5 weight portion, allantoin 1 weight portion, Flos Lonicerae quintessence oil 0.5 weight portion, embryo nelumbinis quintessence oil 0.5 weight portion.
The preparation method of described Flos Lonicerae extractive solution comprises: the Flos Lonicerae powder of 20 weight portions is broken to 50 orders, and is added to the soak by water 1 hour of 200 weight portions after the mixing of 1 weight portion Sal, filters and obtains Aqueous extracts, for subsequent use; To filter gained Flos Lonicerae and add the alcohol heating reflux 3 times of 200 weight portions, and collect alcohol extract, mix with described Aqueous extracts, vacuum concentration is to without alcohol and density is 1.3g/cm
3, obtain Flos Lonicerae extractive solution.
The preparation method of described embryo nelumbinis extracting solution comprises: embryo nelumbinis is crushed to 10 orders, adds 80 DEG C of water soakings and decocts 1 hour at 90 DEG C after 3 hours, filter to obtain embryo nelumbinis Aqueous extracts, for subsequent use; By decocting, to filter the embryo nelumbinis that obtains and volumetric concentration be afterwards soak 5 hours at the alcoholic solution of 80 weight portions is blended in 60 DEG C, filter, collect embryo nelumbinis and soak respectively, embryo nelumbinis is put into percolating device, use soak to carry out percolation, controlling percolation flow velocity is 5L/h, obtains embryo nelumbinis percolate, mix with described embryo nelumbinis Aqueous extracts, vacuum concentration is to without alcohol and density is 1.3g/cm
3, obtain embryo nelumbinis extracting solution.
Embodiment 4
Step one, pour emulsifying pot into by 8/10 of activated water described in 68.5 weight portions, again polyacrylic acid, tridecyl alcohol and glycerol are added in emulsifying pot successively, stir with the speed of 900 revs/min and insulation after being warming up to 75 DEG C, stir and within 15 minutes, obtain A material, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: polyacrylic acid 0.5 weight portion, tridecyl alcohol 0.6 weight portion, glycerol 10 weight portion;
Step 2, the emulsifying pot in step one is evacuated to-0.04Mpa, suction vitamin E, lact albumin hydrolysate and Herba bromi japonici aminoacid after temperature is down to 60 DEG C, insulated and stirred obtains B material for 10 minutes, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: vitamin E2 weight portion, lact albumin hydrolysate 1 weight portion, Herba bromi japonici amino acid/11 weight portion; And
Step 3, it is in 1/10 of described magnetic water that germall and allantoin are dissolved in weight portion respectively, temperature in pot to be emulsified is down to 45 DEG C, by germall, allantoin, Radix Betae extracting solution, Aloe extraction solution, embryo nelumbinis extracting solution and Flos Lonicerae extractive solution are once fed in emulsifying pot, stir 30 minutes under the pressure of-0.06Mpa, get product through 100 order single layer filter cloth impurity screenings, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: Radix Betae extracting solution 2 weight portion, Aloe extraction solution 2 weight portion, embryo nelumbinis extracting solution 5 weight portion, Flos Lonicerae extractive solution 5 weight portion, germall 0.5 weight portion, allantoin 1 weight portion, Flos Lonicerae quintessence oil 0.5 weight portion, embryo nelumbinis quintessence oil 0.5 weight portion.
The preparation method of described Flos Lonicerae extractive solution comprises: the Flos Lonicerae powder of 20 weight portions is broken to 50 orders, and is added to the soak by water 1 hour of 200 weight portions after the mixing of 1 weight portion Sal, filters and obtains Aqueous extracts, for subsequent use; To filter gained Flos Lonicerae and add the alcohol heating reflux 3 times of 200 weight portions, and collect alcohol extract, mix with described Aqueous extracts, vacuum concentration is to without alcohol and density is 1.3g/cm
3, obtain Flos Lonicerae extractive solution.
The preparation method of described embryo nelumbinis extracting solution comprises: embryo nelumbinis is crushed to 10 orders, adds 80 DEG C of water soakings and decocts 1 hour at 90 DEG C after 3 hours, filter to obtain embryo nelumbinis Aqueous extracts, for subsequent use; By decocting, to filter the embryo nelumbinis that obtains and volumetric concentration be afterwards soak 5 hours at the alcoholic solution of 80 weight portions is blended in 60 DEG C, filter, collect embryo nelumbinis and soak respectively, embryo nelumbinis is put into percolating device, use soak to carry out percolation, controlling percolation flow velocity is 5L/h, obtains embryo nelumbinis percolate, mix with described embryo nelumbinis Aqueous extracts, vacuum concentration is to without alcohol and density is 1.3g/cm
3, obtain embryo nelumbinis extracting solution.
Embodiment 5
The difference of the present embodiment and embodiment 4 is that the preparation method of described Radix Betae extracting solution is: at 5 DEG C, the Radix Betae of fresh clean is cut into 1cm
3square fragment, use long wave ultraviolet, the far infrared of 800 μm and the X-ray of 0.5 dust that wavelength is 350nm to irradiate 10min simultaneously, send into squeezing in double-screw type squeezer, pH extract and press liquor is regulated to be transferred in Microwave Extraction Apparatus after 7.5, filter after microwave extracting 60min under the condition of 800W and be extracted liquid, at 30 DEG C, vacuum concentration to density is 1.1g/m
3, obtain Radix Betae extracting solution.
Embodiment 6
The difference of the present embodiment and embodiment 4 is that the preparation method of described Radix Betae extracting solution is: at 12 DEG C, the Radix Betae of fresh clean is cut into 2cm
3square fragment, use long wave ultraviolet, the far infrared of 800 μm and the X-ray of 0.5 dust that wavelength is 350nm to irradiate 15min simultaneously, send into squeezing in double-screw type squeezer, pH extract and press liquor is regulated to be transferred in Microwave Extraction Apparatus after 7.5, filter after microwave extracting 60min under the condition of 800W and be extracted liquid, at 30 DEG C, vacuum concentration to density is 1.2g/m
3, obtain Radix Betae extracting solution.
Embodiment 7
The difference of the present embodiment and embodiment 4 is, the preparation method of described Radix Betae extracting solution is: at 12 DEG C, the Radix Betae of fresh clean is cut into 3cm
3square fragment, use long wave ultraviolet, the far infrared of 800 μm and the X-ray of 0.5 dust that wavelength is 350nm to irradiate 20min simultaneously, send into squeezing in double-screw type squeezer, pH extract and press liquor is regulated to be transferred in Microwave Extraction Apparatus after 7.5, filter after microwave extracting 60min under the condition of 800W and be extracted liquid, at 30 DEG C, vacuum concentration to density is 1.2g/m
3, obtain Radix Betae extracting solution.
Embodiment 8
The difference of the present embodiment and embodiment 7 is, also needs to carry out low-frequency vibration process 30min that frequency be the electronic impulse of 0.9KHz after filtering in described step 3, and regulate pH to be 7.1, density is 1.1g/cm
3be finished product.
Effect example
Severally utilize roentgenization Radix Betae 15min below by way of listing, checking ray is on the impact of Radix Betae secretion betanin and vitamin B12, and in test, Radix Betae is, at 5-15 DEG C, the beet root of fresh clean is cut into 1-3cm
3square fragment, long wave ultraviolet is the long wave ultraviolet of wavelength 350nm, and far infrared is the far infrared of wavelength 800 μm, and X-ray is the X-ray of wavelength 0.5 dust.
Betanin dissolution rate adopts colorimetry to identify, its principle is that beet alkali hydrochlorate can produce red precipitate with Reinecke salt when pH1.0, by precipitation through centrifugal abandon supernatant after, be dissolved in pinkiness solution in 70 pbw acetone, maximum light absorption value is had at 525nm place, beet alkali hydrochlorate meets Beer law when 0.1-12.5mg: because vitamin B12 is for red, can be obtained the roughly secretory volume of vitamin B12 by the color of the press liquor observing Radix Betae.
Do not adopt the Radix Betae of roentgenization, betanin dissolution rate is 1240mg/kg, and the color of press liquor is red.
Adopt the Radix Betae after UVA Radiation, betanin dissolution rate is 1250mg/kg, and the color of press liquor is red.
Adopt the Radix Betae after far-infrared radiation, betanin dissolution rate is 1253mg/kg, and the color of press liquor is red.
Adopt the Radix Betae after x-ray bombardment, betanin dissolution rate is 1262mg/kg, and the color of press liquor is red.
Adopt the Radix Betae after long wave ultraviolet and far-infrared radiation, betanin dissolution rate is 1320mg/kg, and the color of press liquor is light red.
Adopt far infrared and the postradiation Radix Betae of X-ray mixed exposure, betanin dissolution rate is 1330mg/kg, and the color of press liquor is peony.
Adopt long wave ultraviolet, far infrared and the postradiation Radix Betae of X-ray mixed exposure, betanin dissolution rate is 1350mg/kg, and the color of press liquor is aubergine.
Found by contrast test, adopt long wave ultraviolet, far infrared and X-ray mixed exposure Radix Betae greatly can improve the dissolution rate of betanin, the dissolution rate of vitamin B12 also improves accordingly.
The detection of moistening effect
Keratodermatitis hydration rate is tested: operation principle take capacitor as instrument probe, because water is the material that on skin, dielectric constant is maximum, when skin moisture content changes, the capacitance of skin also changes, so can by measuring skin pricktest capacitance, analyzing skin surface moisture content.Conventional instrument is CorneometerCM825.By measuring the change using the change of keratodermatitis capacitance before and after product to weigh water content of stratum corneum, thus evaluate the moisture-keeping efficacy of cosmetics, this kind of method carries out quantification to the moisture of keratodermatitis, the change of skin moisture content can be reacted delicately, and favorable reproducibility, be one of method that current moisture-keeping cosmetics efficacy assessments is conventional.
Experimental technique: bend side at candidate left and right forearm and mark 3 × 3cm
2the square Experimental Area of size, at the test zone of left arm as moisturizer, the corresponding symmetrical region of right arm is blank, then the moisture at each test position is detected with CorneometerCM825 test, repeat 5 times respectively, draw meansigma methods, with following formulae discovery hydration rate.
Hydration rate=(test value-blank value) × 100%
Moistening effect experiment is as shown in table 1.
Table 2 embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is to skin hydration rate result of the test
As shown in table 2, embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid of the present invention can effectively moisturizing, for the user, the moistening effect after 8 hours that works is still remarkable, and the moistening effect of embodiment 8 is best, this may be because after low-frequency vibration process, the hydrogen bond angle of liquid broadens, and manufactures stronger molecule and combines, effectively reduce acidity and the basicity of water with this, its pH pH-value reached between 6.9-7.2 is balanced.By the change of hydrogen bond, water can reassemble into the frequency of similar human body cell in order to absorption of human body, effectively can increase the water content of skin.And embodiment 5-7 also illustrates, the Radix Betae extracting solution obtained after Radix Betae is carried out multiple rays irradiation has excellent moistening effect in application the present invention.
The detection of anti-acne effect
Beneficial effect of the present invention is further illustrated below by way of listing several example of the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid of embodiment 5 that utilizes.
Li Mafan, sex man, 25 years old, pox print was darker on the face, use the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid in embodiment 2, morning every day, evening respectively smear once, and applying amount is consistent with conventional skin care item, after 20 days, small pox starts detumescence, and after 40 days, small pox is not taken off entirely, does not leave pox print on the face.
Wang Yu, sex female, 23 years old, length had funny lighter on the face, use the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid in embodiment 2, morning every day, evening respectively smear once, and the amount of painting probably can cover funny, and after 4 days, small pox starts detumescence, after 15 days, small pox is all got rid of, and skin does not leave pox print.
Chen Zhuanzhuan, sex man, 28 years old, length had a small amount of pox on the face, used the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid in embodiment 2, morning every day, evening respectively smear once, the amount skin care item be than usual coated with are few, and after 5 days, small pox starts detumescence, after 1 month, small pox is all got rid of, and skin does not leave pox print.
Skin irritation detects
Laboratory animal
20 healthy white mouse are used for acute skin irritation experiment, and the body weight of white mouse is 300-500g.
Method and result
Acute skin irritation test Methods and steps all carries out according to the irritation test Methods and steps in " cosmetics health specification 2007 editions ".Wherein, test group 1 is for smearing the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid of the present embodiment 6, and experimental group 2 is for smearing the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid of the present embodiment 8, and matched group is not for smear any sample.
Acute skin irritation result of the test is as shown in table 3
Table 3 embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is to white mouse acute skin irritation result of the test
As can be seen from Table 3, the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid of embodiment 6 and embodiment 8 is tested white mouse acute skin irritation, acute skin irritation reaction top is 0.15, stimulus intensity evaluation is less than 0.5, for non-stimulated, the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid nonirritant of embodiment 6 and embodiment 8 is described, safety is high, but the top of the embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid of embodiment 8 is lower, and zest is less.
Although embodiment of the present invention are open as above, but it is not restricted to listed in description and embodiment utilization, it can be applied to various applicable the field of the invention completely, for those skilled in the art, can easily realize other amendment, therefore do not deviating under the general concept that claim and equivalency range limit, the present invention is not limited to specific details and illustrates here and the embodiment described.
Claims (8)
1. an embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid, it is characterized in that, be made up of the component of following weight proportion: surfactant 0.1-1 weight portion, glycerol 1-10 weight portion, vitamin E 0.1-2 weight portion, aminoacid 0.1-2 weight portion, Radix Betae extracting solution 0.1-2 weight portion, Aloe extraction solution 0.1-2 weight portion, embryo nelumbinis extracting solution 0.1-5 weight portion, Flos Lonicerae extractive solution 0.1-5 weight portion, germall 0.1-0.5 weight portion, allantoin 0.1-1 weight portion, Flos Lonicerae quintessence oil 0.1-0.5 weight portion, embryo nelumbinis quintessence oil 0.1-0.5 weight portion and activated water 68.5-97.9 weight portion.
2. embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid as claimed in claim 1, is characterized in that, described surfactant is one or more in polyacrylic acid, C13-14 isoparaffin and tridecyl alcohol.
3. embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid as claimed in claim 2, is characterized in that, described aminoacid is one or more in lact albumin hydrolysate and Herba bromi japonici aminoacid.
4. a preparation method for embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid as claimed in claim 3, is characterized in that, comprise the following steps:
Step one, weight portion is got 8/10 of described activated water pour emulsifying pot into, again surfactant and glycerol are added in emulsifying pot successively, stir with the speed of 900 revs/min and insulation after being warming up to 70-75 DEG C, stir and within 15 minutes, obtain A material, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: surfactant 0.1-1 weight portion, glycerol 1-10 weight portion;
Step 2, the emulsifying pot in step one is evacuated to-0.06 ~-0.04Mpa, suction vitamin E and aminoacid after temperature is down to 60 DEG C, insulated and stirred obtains B material for 10 minutes, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: vitamin E 0.1-2 weight portion, aminoacid 0.1-2 weight portion; And
Step 3, it is in 1/10 of described magnetic water that germall and allantoin are dissolved in weight portion respectively, temperature in pot to be emulsified is down to 45 DEG C, by germall, allantoin, Radix Betae extracting solution, Aloe extraction solution, embryo nelumbinis extracting solution and Flos Lonicerae extractive solution are once fed in emulsifying pot, stir 30 minutes under the pressure of-0.08 ~-0.06Mpa, get product through 100 order single layer filter cloth impurity screenings, wherein, the additional proportion of the gross mass of above-mentioned substance relative embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid is: Radix Betae extracting solution 0.1-2 weight portion, Aloe extraction solution 0.1-2 weight portion, embryo nelumbinis extracting solution 0.1-5 weight portion, Flos Lonicerae extractive solution 0.1-5 weight portion, germall 0.1-0.5 weight portion, allantoin 0.1-1 weight portion, Flos Lonicerae quintessence oil 0.1-0.5 weight portion, embryo nelumbinis quintessence oil 0.1-0.5 weight portion.
5. the preparation method of embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid as claimed in claim 4, it is characterized in that, the preparation method of described Radix Betae extracting solution comprises: at 5-15 DEG C, the Radix Betae of fresh clean is cut into 1-3cm
3square fragment, use long wave ultraviolet, the far infrared of 800 μm and the X-ray of 0.5 dust that wavelength is 350nm to irradiate 10-20min simultaneously, send into squeezing in double-screw type squeezer, pH extract and press liquor is regulated to be transferred in Microwave Extraction Apparatus after 7.5, filter after microwave extracting 60min under the condition of 800W and be extracted liquid, at 30 DEG C, vacuum concentration to density is 1.1-1.3g/m
3, obtain Radix Betae extracting solution.
6. the preparation method of embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid as claimed in claim 4, it is characterized in that, the preparation method of described Flos Lonicerae extractive solution comprises: the Flos Lonicerae powder of 20 weight portions is broken to 20-50 order, with the soak by water 1 hour being added to 200 weight portions after 1 weight portion Sal mixing, filtration obtains Aqueous extracts, for subsequent use; To filter gained Flos Lonicerae and add the alcohol heating reflux 3 times of 200 weight portions, and collect alcohol extract, mix with described Aqueous extracts, vacuum concentration is to without alcohol and density is 1.1-1.3g/cm
3, obtain Flos Lonicerae extractive solution.
7. the preparation method of embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid as claimed in claim 4, it is characterized in that, the preparation method of described embryo nelumbinis extracting solution comprises: embryo nelumbinis is crushed to 10 orders, adds 80 DEG C of water soakings and decocts 1 hour at 90 DEG C after 3 hours, filter to obtain embryo nelumbinis Aqueous extracts, for subsequent use; By decocting, to filter the embryo nelumbinis that obtains and volumetric concentration be afterwards soak 5 hours at the alcoholic solution of 80 weight portions is blended in 60 DEG C, filter, collect embryo nelumbinis and soak respectively, embryo nelumbinis is put into percolating device, use soak to carry out percolation, controlling percolation flow velocity is 5L/h, obtains embryo nelumbinis percolate, mix with described embryo nelumbinis Aqueous extracts, vacuum concentration is to without alcohol and density is 1.1-1.3g/cm
3, obtain embryo nelumbinis extracting solution.
8. the preparation method of embryo nelumbinis honeysuckle honey skin-moisturizing, skin liquid as claimed in claim 4, is characterized in that, also needs to carry out low-frequency vibration process 30min that frequency be the electronic impulse of 0.9KHz after filtering in described step 3, and regulate pH to be 7.1, density is 1.1g/cm
3be finished product.
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| CN103156801A (en) * | 2013-02-23 | 2013-06-19 | 皖南医学院 | Whitening tendering skin-maintaining toner and preparing method thereof |
| CN104887556A (en) * | 2015-05-06 | 2015-09-09 | 绥阳县吉帮金银花科技发展有限公司 | Honeysuckle flower mask lotion and preparation method thereof |
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