CN105255332A - Water-based paint for pipeline and preparing method of water-based paint - Google Patents
Water-based paint for pipeline and preparing method of water-based paint Download PDFInfo
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Abstract
The invention relates to water-based paint for a pipeline. The water-based paint for the pipeline is prepared from modified phenolic resin, pitch, alcohol acid emulsion, chromium oxide green, an anti-rusting agent, low polymer polyhydric alcohols, maleic anhydride, methyl methacrylate, hydroxyl ethyl acrylate, hydroxylated fiber resin, polyether sulfone resin, polysorbate, sodium hexametaphosphate, organic silicon emulsion, epoxy silane modified silicon sol, crosslinked polyethylene, tert-butyl peroxybenzoate, sodium silicate, melamine phosphate, pentaerythritol, aluminum silicate fibers, silicon dioxide, antibacterial preservative, titanium dioxide, Ni, Zn, water and other raw materials. Due to the fact that the ingredients such as Ni and Zn are contained in the water-based paint for the pipeline, the water-based paint for the pipeline has the high-temperature resisting and corrosion resisting performance, is suitable for coating demands of various occasions, does not contain toxic organic solvents, is free of pollution and has the advantages that a paint surface cannot crack, and the paint is resistant to aging, high in adhesive force and the like.
Description
Technical field
The present invention relates to a kind of pipeline-used water coating and preparation method thereof, belong to technical field of coatings.
Background technology
In recent years, from the viewpoint of environmental problem, carrying out by the conversion of organic solvent type coatings hydrotropisms coating.In addition, coating general requirement has the film performances such as excellent water tolerance, alkali resistance, wearability, weathering resistance.
Water-borne coatings is with the coating of water as dispersion medium and thinner, compare with the coating of organic solvent type, water-borne coatings had both decreased the discharge of volatile organic solvent, again can saving resource, the energy (produce solvent need consume the energy), simultaneously convenient transport and storage.Along with the enhancing of people's environmental consciousness, also more and more tighter to the relevant environmental regulation of the manufacture and usage of Chemicals, therefore water-borne coatings has become the main flow direction of modern coatings industrial development.
According to the dispersing morphology of resin in water, water-borne coatings can be divided into water and milk glue-type, aqueous dispersion type and water-soluble three class.The coating used on the market is at present base-material mainly with synthetic resin emulsion or vinylformic acid, and by synthesis such as various pigment, filler and auxiliary agents.The main drawback of this coating is that to be coated with film elasticity easily aging, and flintiness is bad, can not the intensity of available protecting wall plaster bottom, thus produces metope cracking, comes off, and not only affect buildings attractive in appearance, and metope ftractures, and causes metope to leak.
Summary of the invention
The technical problem to be solved in the present invention is, not enough for prior art, pipeline-used water coating proposing a kind of corrosion-resistant and high-temperature resistant and preparation method thereof.
The present invention is the technical scheme solving the problems of the technologies described above proposition: a kind of pipeline-used water coating, and in this pipeline-used water coating, the mass percent of each composition is: modified phenolic resins: 0.23-0.36%, pitch: 0.14-0.16%, alkyd emulsion: 0.53-0.66%, chromoxide green: 0.35-0.47%, rust-preventive agent: 0.53-0.58%, oligomer polyol: 0.53-0.59%, maleic anhydride: 0.16-0.19%, methyl methacrylate: 0.23-0.31%, hydroxyl ethyl acrylate: 0.13-0.15%, hydroxylation fibre resin: 0.12-0.14%, polyethersulfone resin: 0.07-0.08%, polysorbate: 0.05-0.06%, Sodium hexametaphosphate 99: 0.22-0.25%, organic silicon emulsion: 0.27-0.28%, epoxy radicals silicone hydride modified silicasol: 0.13-0.16%, crosslinked polyethylene: 0.03-0.06%, perbenzoic acid butyl ester: 0.25-0.34%, water glass: 0.15-0.18%, melamine phosphate: 0.11-0.13%, tetramethylolmethane: 0.37-0.43%, aluminum silicate fiber: 0.17-0.19%, silicon-dioxide: 0.28-0.36%, fungicidal preservative: 0.21-0.32%, film coalescence aid: 0.16-0.18%, waterborne polyurethane resin: 0.05-0.08%, acrylate: 0.03-0.07%, titanium dioxide: 0.09-0.19%, polyvinyl alcohol: 0.13-0.15%, light calcium carbonate: 0.23-0.37%, talcum powder: 0.22-0.31%, terra alba: 0.14-0.26%, titanium dioxide: 0.18-0.19%, waterborne epoxy modified resin: 0.13-0.15%, Ti:0.08-0.09%, Mn:0.06-0.07%, Cr:0.03-0.05%, Ni:0.05-0.13%, Zn:0.35-0.39%, V:0.06-0.09%, Re:0.05-0.07%, Au:0.08-0.12%, surplus is water.
The improvement of technique scheme is: fungicidal preservative is Kathon.
The improvement of technique scheme is: film coalescence aid is the combination of at least 2 kinds in propylene glycol, propylene glycol monomethyl ether, 1-Methoxy-2-propyl acetate, Lauryl Alcohol ester.
The improvement of technique scheme is: described rust-preventive agent is iron mica.
The preparation method of pipeline-used water coating, comprises the following steps:
(i) prepare burden: the mass percent of pipeline-used water coating by each composition is prepared burden;
(ii) in the reactor that water trap is housed, add oligomer polyol, be warming up to 91-95 DEG C and make it to melt, slowly add maleic anhydride, then increase the temperature to 116-120 DEG C of reaction, to fraction water device water-dividing, namely cooling obtains maleic anhydride modified polyester;
(iii) in a nitrogen environment, with methyl methacrylate and hydroxyl ethyl acrylate for solvent, maleic anhydride modified polyester, hydrophilic small molecules chainextender and the initiator of above-mentioned synthesis are added in reactor, 82 DEG C-86 DEG C are heated under whipped state, reaction 45-55min, obtains the low hydroxyl value acrylic polyester of wetting ability;
(iv) in the acrylic polyester (iii) obtained, add neutralizing agent, the system pH of making reaches 7, under whipped state, then adds distilled water performed polymer is uniformly dispersed, and obtains water-based low hydroxyl value acrylic polyester dispersion;
(v) add surplus stock in the water-based low hydroxyl value acrylic polyester dispersion (iv) obtained to step and stir, being heated to 120-130 DEG C simultaneously, controlling stirrer rotating speed is that per minute 2100-2200 turns, and mixing time is 20-25min;
(vi) defoamer, film coalescence aid and pH value regulator are added successively in the mixture that (v) step obtain, mixture is adjusted to alkalescence, and its pH value is 7.2-8.1;
(vii) mixture step (vi) obtained carries out speed lapping, and the speed lapping time is 10-12min;
(viii) pigment natural plant aqueous mill base, color adjusting agent, scratching resistant and slip(ping)agent is added;
(ix) use ultrasonic generator to carry out secondary stirring to the product after moisturizing, control hyperacoustic frequency and the sound intensity is 3KHZ-9MHZ and 2-9W/cm respectively
2;
(x) moisturizing also uses viscosity modifier adjusting viscosity to 77-85KU, obtains pipeline-used water coating.
The improvement of technique scheme is: step (iii) in hydrophilic small molecules chainextender be one or more in dihydroxy carboxylic acids, dicarboxyl half ester or dicarboxyl sulfonate.
The improvement of technique scheme is: step (iii) middle initiator is BPO.
The improvement of technique scheme is: step (iv) middle neutralizing agent is ammoniacal liquor.
The improvement of technique scheme is: step (ix) in, control hyperacoustic frequency and the sound intensity is 7MHZ and 6W/cm respectively
2.
The improvement of technique scheme is: step (x) in viscosity modifier adjusting viscosity to 82KU.
The present invention adopts the beneficial effect of technique scheme to be: (1) due in pipeline-used water coating containing compositions such as Ni, Zn, make it have the performance of corrosion-and high-temp-resistant, adapt to the coating demand of various occasion; (2) the present invention is not containing toxic organic solvents, pollution-free; (3) this pipeline-used water coating lacquer painting can not ftracture, and the paint film hand rubbing after film forming also can not split; (4) anti-aging, the strong adhesion of pipeline-used water coating of the present invention; (5) owing to adding the compositions such as water glass, melamine phosphate, silicon-dioxide, make the heat-proof quality of water-borne coatings better; (6) organic silicon emulsion and epoxy radicals silicone hydride modified silicasol interact and improve the performance of coating, and improve the sticking power of its paint film, thermotolerance and intensity further, make the strong adhesion of the paint film of this pipeline-used water coating, shock strength is good, and thermotolerance is good; (7) owing to adding fungicidal preservative, mould etc. is prevented to corrode the coated side of pipeline use coating, the coating life-span of prolongation; (8) owing to using ultrasonic generator to carry out secondary stirring to the product after moisturizing, make stock dispersion more even; (9) step (iv) in obtained water-based low hydroxyl value acrylic polyester dispersion, it is low that this dispersion has hydroxyl value, good from eliminate optical property, while ensureing desirable matte effect, effectively reduces the consumption of dumb light powder; (10) with the addition of pitch in coating and rust-preventive agent can effectively prevent spontaneous corrosion and microorganism to the corrosion of pipeline.
Embodiment
embodiment 1
In the pipeline-used water coating of the present embodiment, the mass percent of each composition is: modified phenolic resins: 0.23%, pitch: 0.14%, alkyd emulsion: 0.56%, chromoxide green: 0.37%, rust-preventive agent: 0.58%, oligomer polyol: 0.59%, maleic anhydride: 0.16%, methyl methacrylate: 0.23%, hydroxyl ethyl acrylate: 0.15%, hydroxylation fibre resin: 0.14%, polyethersulfone resin: 0.08%, polysorbate: 0.05%, Sodium hexametaphosphate 99: 0.22%, organic silicon emulsion: 0.27%, epoxy radicals silicone hydride modified silicasol: 0.13%, crosslinked polyethylene: 0.03%, perbenzoic acid butyl ester: 0.25%, water glass: 0.15%, melamine phosphate: 0.11%, tetramethylolmethane: 0.37%, aluminum silicate fiber: 0.19%, silicon-dioxide: 0.28%, fungicidal preservative: 0.21%, film coalescence aid: 0.18%, waterborne polyurethane resin: 0.05%, acrylate: 0.03%, titanium dioxide: 0.09%, polyvinyl alcohol: 0.15%, light calcium carbonate: 0.23%, talcum powder: 0.22%, terra alba: 0.14%, titanium dioxide: 0.18%, waterborne epoxy modified resin: 0.13%, Ti:0.08%, Mn:0.06%, Cr:0.03%, Ni:0.05%, Zn:0.35%, V:0.06%, Re:0.07%, Au:0.08%, surplus is water.
The preparation method of the pipeline-used water coating of the present embodiment, comprises the following steps:
(i) prepare burden: the mass percent of pipeline-used water coating by each composition is prepared burden;
(ii) in the reactor that water trap is housed, add oligomer polyol, be warming up to 95 DEG C and make it to melt, slowly add maleic anhydride, then increase the temperature to 118 DEG C of reactions, to fraction water device water-dividing, namely cooling obtains maleic anhydride modified polyester;
(iii) in a nitrogen environment, with methyl methacrylate and hydroxyl ethyl acrylate for solvent, maleic anhydride modified polyester, hydrophilic small molecules chainextender (mixture of dicarboxyl half ester and dicarboxyl sulfonate) and the initiator B PO of above-mentioned synthesis are added in reactor, 85 DEG C are heated under whipped state, reaction 55min, obtains the low hydroxyl value acrylic polyester of wetting ability;
(iv) in the acrylic polyester (iii) obtained, add neutralizing agent (ammoniacal liquor), the system pH of making reaches 7, under whipped state, then adds distilled water performed polymer is uniformly dispersed, and obtains water-based low hydroxyl value acrylic polyester dispersion;
(v) add surplus stock in the water-based low hydroxyl value acrylic polyester dispersion (iv) obtained to step and stir, being heated to 130 DEG C simultaneously, controlling stirrer rotating speed is per minute 2100 turns, and mixing time is 25min;
(vi) defoamer, film coalescence aid and pH value regulator are added successively in the mixture that (v) step obtain, mixture is adjusted to alkalescence, and its pH value is 7.8;
(vii) mixture step (vi) obtained carries out speed lapping, and the speed lapping time is 12min;
(viii) pigment natural plant aqueous mill base, color adjusting agent, scratching resistant and slip(ping)agent is added;
(ix) use ultrasonic generator to carry out secondary stirring to the product after moisturizing, control hyperacoustic frequency and the sound intensity is 7MHZ and 6W/cm respectively
2;
(x) moisturizing also uses viscosity modifier adjusting viscosity to 82KU, obtains pipeline-used water coating.
Wherein fungicidal preservative is Kathon.Film coalescence aid is the combination of propylene glycol, propylene glycol monomethyl ether, 1-Methoxy-2-propyl acetate, Lauryl Alcohol ester.Rust-preventive agent is iron mica.
The present invention is not limited to above-described embodiment.All employings are equal to the technical scheme of replacing and being formed, and all drop on the protection domain of application claims.
Claims (10)
1. a pipeline-used water coating, is characterized in that: in described pipeline-used water coating, the mass percent of each composition is: modified phenolic resins: 0.23-0.36%, pitch: 0.14-0.16%, alkyd emulsion: 0.53-0.66%, chromoxide green: 0.35-0.47%, rust-preventive agent: 0.53-0.58%, oligomer polyol: 0.53-0.59%, maleic anhydride: 0.16-0.19%, methyl methacrylate: 0.23-0.31%, hydroxyl ethyl acrylate: 0.13-0.15%, hydroxylation fibre resin: 0.12-0.14%, polyethersulfone resin: 0.07-0.08%, polysorbate: 0.05-0.06%, Sodium hexametaphosphate 99: 0.22-0.25%, organic silicon emulsion: 0.27-0.28%, epoxy radicals silicone hydride modified silicasol: 0.13-0.16%, crosslinked polyethylene: 0.03-0.06%, perbenzoic acid butyl ester: 0.25-0.34%, water glass: 0.15-0.18%, melamine phosphate: 0.11-0.13%, tetramethylolmethane: 0.37-0.43%, aluminum silicate fiber: 0.17-0.19%, silicon-dioxide: 0.28-0.36%, fungicidal preservative: 0.21-0.32%, film coalescence aid: 0.16-0.18%, waterborne polyurethane resin: 0.05-0.08%, acrylate: 0.03-0.07%, titanium dioxide: 0.09-0.19%, polyvinyl alcohol: 0.13-0.15%, light calcium carbonate: 0.23-0.37%, talcum powder: 0.22-0.31%, terra alba: 0.14-0.26%, titanium dioxide: 0.18-0.19%, waterborne epoxy modified resin: 0.13-0.15%, Ti:0.08-0.09%, Mn:0.06-0.07%, Cr:0.03-0.05%, Ni:0.05-0.13%, Zn:0.35-0.39%, V:0.06-0.09%, Re:0.05-0.07%, Au:0.08-0.12%, surplus is water.
2. pipeline-used water coating according to claim 1, is characterized in that: described fungicidal preservative is Kathon.
3. pipeline-used water coating according to claim 2, is characterized in that: described film coalescence aid is the combination of at least 2 kinds in propylene glycol, propylene glycol monomethyl ether, 1-Methoxy-2-propyl acetate, Lauryl Alcohol ester.
4. pipeline-used water coating according to claim 3, is characterized in that: described rust-preventive agent is iron mica.
5. the preparation method of the pipeline-used water coating according to claim arbitrary in Claims 1-4, is characterized in that: comprise the following steps:
(i) prepare burden: the mass percent of pipeline-used water coating by each composition is prepared burden;
(ii) in the reactor that water trap is housed, add oligomer polyol, be warming up to 91-95 DEG C and make it to melt, slowly add maleic anhydride, then increase the temperature to 116-120 DEG C of reaction, to fraction water device water-dividing, namely cooling obtains maleic anhydride modified polyester;
(iii) in a nitrogen environment, with methyl methacrylate and hydroxyl ethyl acrylate for solvent, maleic anhydride modified polyester, hydrophilic small molecules chainextender and the initiator of above-mentioned synthesis are added in reactor, 82 DEG C-86 DEG C are heated under whipped state, reaction 45-55min, obtains the low hydroxyl value acrylic polyester of wetting ability;
(iv) in the acrylic polyester (iii) obtained, add neutralizing agent, the system pH of making reaches 7, under whipped state, then adds distilled water performed polymer is uniformly dispersed, and obtains water-based low hydroxyl value acrylic polyester dispersion;
(v) add surplus stock in the water-based low hydroxyl value acrylic polyester dispersion (iv) obtained to step and stir, being heated to 120-130 DEG C simultaneously, controlling stirrer rotating speed is that per minute 2100-2200 turns, and described mixing time is 20-25min;
(vi) defoamer, film coalescence aid and pH value regulator are added successively in the mixture that (v) step obtain, mixture is adjusted to alkalescence, and its pH value is 7.2-8.1;
(vii) mixture step (vi) obtained carries out speed lapping, and the speed lapping time is 10-12min;
(viii) pigment natural plant aqueous mill base, color adjusting agent, scratching resistant and slip(ping)agent is added;
(ix) use ultrasonic generator to carry out secondary stirring to the product after moisturizing, control hyperacoustic frequency and the sound intensity is 3KHZ-9MHZ and 2-9W/cm respectively
2;
(x) moisturizing also uses viscosity modifier adjusting viscosity to 77-85KU, obtains pipeline-used water coating.
6. the preparation method of pipeline-used water coating according to claim 5, is characterized in that: described step (iii) in hydrophilic small molecules chainextender be one or more in dihydroxy carboxylic acids, dicarboxyl half ester or dicarboxyl sulfonate.
7. the preparation method of pipeline-used water coating according to claim 6, is characterized in that: described step (iii) middle initiator is BPO.
8. the preparation method of pipeline-used water coating according to claim 7, is characterized in that: described step (iv) middle neutralizing agent is ammoniacal liquor.
9. the preparation method of pipeline-used water coating according to claim 8, is characterized in that: described step (ix) in, control hyperacoustic frequency and the sound intensity is 7MHZ and 6W/cm respectively
2.
10. the preparation method of pipeline-used water coating according to claim 9, is characterized in that: described step (x) in viscosity modifier adjusting viscosity to 82KU.
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CN106085124A (en) * | 2016-07-18 | 2016-11-09 | 天长市巨龙车船涂料有限公司 | A kind of high antiseptic property epoxy iron red shop primer |
CN106189857A (en) * | 2016-07-19 | 2016-12-07 | 董芬芳 | A kind of metal thickness slurry heavy anti-corrosion antirust paint |
CN106497409A (en) * | 2016-11-25 | 2017-03-15 | 威海恒基伟业信息科技发展有限公司 | A kind of preparation method of the polyethylene pipe of anticorrosion antiwear |
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CN108047789A (en) * | 2017-12-17 | 2018-05-18 | 苏州赛斯德工程设备有限公司 | A kind of preparation method of pipeline-used water coating |
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CN112662255A (en) * | 2020-12-24 | 2021-04-16 | 浙江立盛新型墙体材料有限公司 | Process method for producing environment-friendly water-based paint |
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CN104263184A (en) * | 2014-09-06 | 2015-01-07 | 广东华澜浩宇科技创新有限公司 | Preparation method of water-based matte paint |
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CN103468130A (en) * | 2013-09-03 | 2013-12-25 | 吴江市冰心文教用品有限公司 | High temperature resistant anticorrosive paint |
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CN106189857A (en) * | 2016-07-19 | 2016-12-07 | 董芬芳 | A kind of metal thickness slurry heavy anti-corrosion antirust paint |
CN106497409A (en) * | 2016-11-25 | 2017-03-15 | 威海恒基伟业信息科技发展有限公司 | A kind of preparation method of the polyethylene pipe of anticorrosion antiwear |
CN106497408A (en) * | 2016-11-25 | 2017-03-15 | 威海恒基伟业信息科技发展有限公司 | A kind of antiseptic wearable coat of tubing |
CN106543894A (en) * | 2016-11-25 | 2017-03-29 | 威海恒基伟业信息科技发展有限公司 | A kind of preparation method of the polyethylene tube of anticorrosion antiwear |
CN106752642A (en) * | 2016-12-12 | 2017-05-31 | 浙江欣苗化工有限公司 | A kind of chassis of container soluble asphalt anticorrosive coating and preparation method thereof |
CN107189649A (en) * | 2017-05-31 | 2017-09-22 | 成都协恒科技有限公司 | A kind of corrosion resistant coating for container |
CN107163770A (en) * | 2017-07-04 | 2017-09-15 | 合肥择浚电气设备有限公司 | A kind of machinery antirust paint containing attapulgite and preparation method thereof |
CN108047640A (en) * | 2017-12-17 | 2018-05-18 | 苏州赛斯德工程设备有限公司 | A kind of formica |
CN108047789A (en) * | 2017-12-17 | 2018-05-18 | 苏州赛斯德工程设备有限公司 | A kind of preparation method of pipeline-used water coating |
CN108060358A (en) * | 2017-12-17 | 2018-05-22 | 苏州赛斯德工程设备有限公司 | A kind of processing technology of corrosion resistant flange |
CN112662255A (en) * | 2020-12-24 | 2021-04-16 | 浙江立盛新型墙体材料有限公司 | Process method for producing environment-friendly water-based paint |
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