CN105238274A - Compound-wax type automobile polish and preparing method thereof - Google Patents
Compound-wax type automobile polish and preparing method thereof Download PDFInfo
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- CN105238274A CN105238274A CN201510776268.9A CN201510776268A CN105238274A CN 105238274 A CN105238274 A CN 105238274A CN 201510776268 A CN201510776268 A CN 201510776268A CN 105238274 A CN105238274 A CN 105238274A
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Abstract
The invention discloses a compound-wax type automobile polish and a preparing method thereof. The compound-wax type automobile polish is prepared from 5 parts to 20 parts of compound wax, 2 parts to 6 parts of polyvinyl alcohol, 0.6 part to 1.4 parts of triethanolamine oleate, 0.03 part to 0.1 part of carboxyethyl cellulose, 2.1 parts to 3.6 parts of amino silicon oil, 0.3 part to 0.8 part of ethoxy dodecyl alcohol, 0.12 part to 0.54 part of nitrous acid diisopropylamine, 0.25 part to 0.55 part of dimethylaniline, 0.07 part to 0.12 part of N-methyl pyrrolidone, 0.13 part to 0.25 part of trihydroxyethyl methyI ammonium methosulfate, 0.45 part to 1.25 parts of glyceryl tristearate, 0.5 part to 1.8 parts of oil-based amino acid sodium, 0.01 part to 0.08 part of sodium dodecyl benzene sulfonate, 0.06 part to 0.15 part of potassium sorbate, 0.1 part to 0.4 part of simethicone and 15 parts to 30 parts of water. The polishing effect is good in stability, finishing paint is not corroded, and present imported products can be replaced.
Description
Technical field
The invention belongs to Motor Maintenance product technical field, be specifically related to a kind of compound wax pattern vehicle glazing agent and preparation method thereof.
Background technology
Automobile external finish paint often adopts acrylic acid or the like or polyurethanes coating, and these finish paints are comparatively large because of the pollution effect caused by hydro carbons, hydrocarbons, dust etc. in air, clean-out system, lustering agent need be adopted to carry out cleaning, glazing, protection etc. " beauty treatment ".Along with the attention of people to social environment and the raising of cultural taste, automobile " beauty treatment " is not confined to sedan limousine.People can see the billboard of " carwash ", " waxing " everywhere.The quietly rise of automobile " beauty treatment " industry, brings good opportunity to develop to the production of automobile washing lustering agent.
The development of cleaning polishing wax technology can be divided into two stages: one is the development and production of unifunctional clean-out system or lustering agent; Two is difunctional and Development and Production that is multifunctional product.With single function clean-out system that EDAT, fluorinated alkyl carboxylic acid potassium, oxalic acid, sodium alkyl benzene sulfonate, potato juice, sodium stearyl fumarate etc. are component, and to be component single after functionally photo etching is used widely with silicone oil (be conventional with methyl-silicone oil), wax, kerosene etc., from the security used and effect, traditional measure wax amount of first cleaning glazing of waxing again is many, labour intensity is large, upper ray velocity is slow, low in glossiness.Develop difunctional and multifunctional product and become the market requirement, especially neutral cleaning, glazing, protection hold concurrently can multifunctional product be subject to the favor of society.
The dual function product being component with rubber viscous oil and potassium hydroxide, sylvite of domestic early stage research and development, fails widespread use owing to being corrosive, along with the development of Domestic Automotive Industry, and the research constantly progress of automobile washing lustering agent.The end of the eighties is domestic develops the cleaning formed with trolamine, oleic acid, Trisodium Citrate, white oil, methyl-silicone oil, sherwood oil and water etc. and to add lustre to emulsion, has without advantages such as electrostatic, corrosion-free, not dust suctions, thus saves a large amount of paraffin resources.At the beginning of the nineties, domesticly to develop with silicone oil, paraffin and solubilizing agent thereof etc. for effective constituent, transparent cleaning wax polish easy to use, not only consumption is few, has good decontamination, polishing effect, and has incoagulable advantage more than-15 DEG C.The automobile washing lustering agent that latest domestic is developed, with mineral oil, polysiloxane, clean-out system, lipid acid, emulsifying agent etc. for raw material, has the functions such as cleaning, level and smooth, bright and clean and protection to car body.Through stability, rust-preventing characteristic, corrodibility and paint film impact test, there is non-volatile, good stability, to advantages such as lacquer painting are corrosion-free.But this domestic technique not yet forms high volume product supply market.In current domestic big and medium-sized cities, more and more simple carwash industry develops into professional car detailing center, and they and client earnestly expect to have energy and the same the having good quality of imported product and the lower home made article of price.
Summary of the invention
The object of this invention is to provide a kind of compound wax pattern vehicle glazing agent and preparation method thereof, by the composite vehicle glazing agent obtained of different sorts wax, there are good decontamination, polishing effect, good stability, corrosion-free to finish paint, and preparation method is simple, cost is lower, can substitute current imported product.
To achieve these goals, the technical solution used in the present invention is:
The agent of a kind of compound wax pattern vehicle glazing, component and each constituent mass number as follows: compound wax 5 ~ 20 parts, polyvinyl alcohol 2 ~ 6 parts, triethanolamine oleate 0.6 ~ 1.4 part, carboxyethyl cellulose 0.03 ~ 0.1 part, amido silicon oil 2.1 ~ 3.6 parts, hydroxyethyl dodecyl alcohol 0.3 ~ 0.8 part, nitrous acid Diisopropylamine 0.12 ~ 0.54 part, xylidine 0.25 ~ 0.55 part, N-Methyl pyrrolidone 0.07 ~ 0.12 part, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt 0.13 ~ 0.25 part, Tristearoylglycerol 0.45 ~ 1.25 part, oil base amino acid sodium 0.5 ~ 1.8 part, Sodium dodecylbenzene sulfonate 0.01 ~ 0.08 part, potassium sorbate 0.06 ~ 0.15 part, dimethyl silicone oil 0.1 ~ 0.4 part, 15 ~ 30 parts, water.
Described compound wax is by vegetable wax, animal wax and mineral wax 1:(1 ~ 3 in mass ratio): (1 ~ 5) is composited.
Described vegetable wax is flax wax or tealight.
Described animal wax is beeswax.
Described mineral wax is at least one in paraffin, ceresine or Microcrystalline Wax.
Described compound wax preferably by vegetable wax, animal wax and mineral wax in mass ratio 1:2:4 be composited.
Described a kind of compound wax pattern vehicle glazing agent, component and each constituent mass number as follows: vegetable wax 2 parts, animal wax 4 parts, mineral wax 9 parts, polyvinyl alcohol 4 parts, triethanolamine oleate 1.0 parts, carboxyethyl cellulose 0.06 part, amido silicon oil 2.8 parts, hydroxyethyl dodecyl alcohol 0.5 part, nitrous acid Diisopropylamine 0.35 part, xylidine 0.4 part, N-Methyl pyrrolidone 0.9 part, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt 0.18 part, Tristearoylglycerol 0.85 part, oil base amino acid sodium 1.2 parts, Sodium dodecylbenzene sulfonate 0.05 part, potassium sorbate 0.09 part, dimethyl silicone oil 0.25 part, 28 parts, water.
The preparation method of described a kind of compound wax pattern vehicle glazing agent, comprises the steps:
1) vegetable wax, animal wax and mineral wax are mixed in proportion, be heated to 100 ~ 120 DEG C melt to wax, add triethanolamine oleate, carboxyethyl cellulose, amido silicon oil, hydroxyethyl dodecyl alcohol, nitrous acid Diisopropylamine, xylidine, N-Methyl pyrrolidone, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt, Tristearoylglycerol, oil base amino acid sodium, Sodium dodecylbenzene sulfonate, potassium sorbate and dimethyl silicone oil, at 80 ~ 100 DEG C, stir 1 ~ 5h;
2) water is mixed with polyvinyl alcohol, be heated to 80 ~ 90 DEG C;
3) mixing solutions of step 1) is joined step 2) solution in, namely stirring and emulsifying to room temperature obtains the agent of compound wax pattern vehicle glazing.
The chemical composition of wax is different, its physicals is also just different, at certain wax of selection or several wax as raw material with while obtaining performance complement, also to control the indexs such as melting range, oxygen level and the saponification value be suitable for reach best result of use, the present invention finds under study for action, the compound of different types of wax can bring the collaborative effect improved, and makes polishing effect better, more stable.
Beneficial effect: the invention provides a kind of compound wax pattern vehicle glazing agent and preparation method thereof, by the composite synergy of different sorts wax, the vehicle glazing agent obtained, there are good decontamination, polishing effect, good stability, corrosion-free to finish paint, and preparation method is simple, cost is lower, can substitute current imported product.
Embodiment
Embodiment 1
The agent of a kind of compound wax pattern vehicle glazing, component and each constituent mass number as follows: compound wax 5 parts, polyvinyl alcohol 2 parts, triethanolamine oleate 0.6 part, carboxyethyl cellulose 0.03 part, amido silicon oil 2.1 parts, hydroxyethyl dodecyl alcohol 0.3 part, nitrous acid Diisopropylamine 0.12 part, xylidine 0.25 part, N-Methyl pyrrolidone 0.07 part, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt 0.13 part, Tristearoylglycerol 0.45 part, oil base amino acid sodium 0.5 part, Sodium dodecylbenzene sulfonate 0.01 part, potassium sorbate 0.06 part, dimethyl silicone oil 0.1 part, 15 parts, water.Described compound wax by tealight, beeswax, paraffin in mass ratio 1:1:5 be composited.
Preparation method, comprises the steps:
1) vegetable wax, animal wax and mineral wax are mixed in proportion, be heated to 110 DEG C melt to wax, add triethanolamine oleate, carboxyethyl cellulose, amido silicon oil, hydroxyethyl dodecyl alcohol, nitrous acid Diisopropylamine, xylidine, N-Methyl pyrrolidone, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt, Tristearoylglycerol, oil base amino acid sodium, Sodium dodecylbenzene sulfonate, potassium sorbate and dimethyl silicone oil, at 90 DEG C, stir 3h;
2) water is mixed with polyvinyl alcohol, be heated to 85 DEG C;
3) mixing solutions of step 1) is joined step 2) solution in, namely stirring and emulsifying to room temperature obtains the agent of compound wax pattern vehicle glazing.
Embodiment 2
The agent of a kind of compound wax pattern vehicle glazing, component and each constituent mass number as follows: compound wax 20 parts, polyvinyl alcohol 6 parts, triethanolamine oleate 1.4 parts, carboxyethyl cellulose 0.1 part, amido silicon oil 3.6 parts, hydroxyethyl dodecyl alcohol 0.8 part, nitrous acid Diisopropylamine 0.54 part, xylidine 0.55 part, N-Methyl pyrrolidone 0.12 part, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt 0.25 part, Tristearoylglycerol 1.25 parts, oil base amino acid sodium 1.8 parts, Sodium dodecylbenzene sulfonate 0.08 part, potassium sorbate 0.15 part, dimethyl silicone oil 0.4 part, 30 parts, water.Described compound wax by tealight, beeswax, paraffin, Microcrystalline Wax in mass ratio 1:2:2:2 be composited.
Preparation method, comprises the steps:
1) vegetable wax, animal wax and mineral wax are mixed in proportion, be heated to 110 DEG C melt to wax, add triethanolamine oleate, carboxyethyl cellulose, amido silicon oil, hydroxyethyl dodecyl alcohol, nitrous acid Diisopropylamine, xylidine, N-Methyl pyrrolidone, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt, Tristearoylglycerol, oil base amino acid sodium, Sodium dodecylbenzene sulfonate, potassium sorbate and dimethyl silicone oil, at 90 DEG C, stir 3h;
2) water is mixed with polyvinyl alcohol, be heated to 85 DEG C;
3) mixing solutions of step 1) is joined step 2) solution in, namely stirring and emulsifying to room temperature obtains the agent of compound wax pattern vehicle glazing.
Embodiment 3
The agent of a kind of compound wax pattern vehicle glazing, component and each constituent mass number as follows: compound wax 15 parts, polyvinyl alcohol 4 parts, triethanolamine oleate 1.0 parts, carboxyethyl cellulose 0.06 part, amido silicon oil 2.8 parts, hydroxyethyl dodecyl alcohol 0.5 part, nitrous acid Diisopropylamine 0.35 part, xylidine 0.4 part, N-Methyl pyrrolidone 0.9 part, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt 0.18 part, Tristearoylglycerol 0.85 part, oil base amino acid sodium 1.2 parts, Sodium dodecylbenzene sulfonate 0.05 part, potassium sorbate 0.09 part, dimethyl silicone oil 0.25 part, 28 parts, water, described compound wax by tealight, beeswax, paraffin, ceresine, Microcrystalline Wax in mass ratio 1:2:1:2:1 be composited.
Preparation method, comprises the steps:
1) vegetable wax, animal wax and mineral wax are mixed in proportion, be heated to 110 DEG C melt to wax, add triethanolamine oleate, carboxyethyl cellulose, amido silicon oil, hydroxyethyl dodecyl alcohol, nitrous acid Diisopropylamine, xylidine, N-Methyl pyrrolidone, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt, Tristearoylglycerol, oil base amino acid sodium, Sodium dodecylbenzene sulfonate, potassium sorbate and dimethyl silicone oil, at 90 DEG C, stir 3h;
2) water is mixed with polyvinyl alcohol, be heated to 85 DEG C;
3) mixing solutions of step 1) is joined step 2) solution in, namely stirring and emulsifying to room temperature obtains the agent of compound wax pattern vehicle glazing.
Comparative example 1:
With the difference of embodiment 3, comparative example 1 is only that wax used in lustering agent is all tealight, all the other components and preparation method are all identical with embodiment 3.
Comparative example 2:
With the difference of embodiment 3, comparative example 2 is only that wax used in lustering agent is all beeswax, all the other components and preparation method are all identical with embodiment 3.
Comparative example 3:
With the difference of embodiment 3, comparative example 3 is only that wax used in lustering agent is all paraffin, all the other components and preparation method are all identical with embodiment 3.
Comparative example 4:
Comparative example 4 and the difference of embodiment 3 be only wax used in lustering agent be tealight and paraffin in mass ratio 1:4 be composited, all the other components and preparation method are all identical with embodiment 3.
Comparative example 5:
Comparative example 5 and the difference of embodiment 3 be only wax used in lustering agent be beeswax and paraffin in mass ratio 1:2 be composited, all the other components and preparation method are all identical with embodiment 3.
Comparative example 6:
Comparative example 6 and the difference of embodiment 3 be only wax used in lustering agent be tealight and beeswax in mass ratio 1:2 be composited, all the other components and preparation method are all identical with embodiment 3.
Carry out performance test to the lustering agent of embodiment 1 ~ 3 and comparative example 1 ~ 6, physical and chemical index and testing method are:
High-temperature stability (50 ± 0.5 DEG C): constant temperature recovers room temperature in 4 hours, does not affect result of use;
Low-temperature stability (-12 ± 0.5 DEG C): freezing 3 hours, recovers room temperature, does not affect result of use;
Product is put into container, take out keep placing male 0.3 hour in the thermostatic bath of (50 ± 0.5 DEG C) and (-12 ± 0.5 DEG C) in temperature after, place 2 hours at normal temperatures again, take off lid, by eyes and the state studying surface with hand touch.
Gloss increase degree: more than 5, employing digital display glossiness gauge measures, digital display glossiness gauge is 20 °, 60 °, 80 ° of fixed angle type glossiness testing tools, the measurement window of instrument is placed on black standard plate, calibrate standard glossiness, after pending data is stable, again the measurement window of instrument is placed on tested model (not smearing photo etching), pointer indication data are exactly the gloss value of tested model itself, then on tested model, lustering agent is smeared, Deng it done after to wipe clean again, now apparatus measures window is placed on tested model again, the data of pointer indication are exactly the gloss value of now model, the difference of former and later two data is the glossiness that polishing wax improves, i.e. glossiness increment.
Impact on spray-coating surface: film does not peel off, crackle, wrinkle, expansion, softening or variable color; Be placed on setting-out in the test piece on smooth horizontal stand, with finger comprehensively, spreadable equably, after normal temperature places 4 hours, wipe remaining sample, the then spraying that press...withes one's finger away with pieces of cloth cotton, with eyes and with hand touch whether research film peels off, crackle, wrinkle, expansion, softening or variable color.
Test result is:
The lustering agent of embodiment 1 ~ 3 is all very stable when high temperature and low temperature, does not have the separation of solvent or composition, does not have obvious change of state, and returning to room temperature 1h after taking-up can normally use.The lustering agent of comparative example 1,2,3 has the separation of composition, obvious demixing phenomenon when high temperature, returning to room temperature after taking-up can not normally use; The lustering agent of comparative example 4,5,6 is comparatively stable when high temperature and low temperature, the separation phenomenon of a small amount of solvent and composition, and returning to room temperature 5h after taking-up can normally use.
Glossiness increased value is respectively:
Glossiness increased value is respectively:
| Example 1 | Example 2 | Example 3 | Contrast 1 | Contrast 2 | Contrast 3 | Contrast 4 | Contrast 5 | Contrast 6 |
| 8 | 9 | 12 | 4 | 5 | 5 | 6 | 5 | 7 |
Embodiment 1 ~ 3 on the impact of spray-coating surface is: film does not peel off, crackle, wrinkle, expansion, softening or variable color; The lustering agent of comparative example 1 ~ 6 on the impact of spray-coating surface is: the lustering agent film of comparative example 1 ~ 3 has crackle, peeling phenomenon; The lustering agent film of comparative example 4 ~ 6 has a little wrinkle, softens.
From above-mentioned experimental result, compound wax of the present invention has synergy each other, and in lustering agent, wax consumption is few, and glossiness increased value is high, and result of use is good, and cost is lower, and preparation method is simple.
Claims (8)
1. compound wax pattern vehicle glazing agent, it is characterized in that, component and each constituent mass number as follows: compound wax 5 ~ 20 parts, polyvinyl alcohol 2 ~ 6 parts, triethanolamine oleate 0.6 ~ 1.4 part, carboxyethyl cellulose 0.03 ~ 0.1 part, amido silicon oil 2.1 ~ 3.6 parts, hydroxyethyl dodecyl alcohol 0.3 ~ 0.8 part, nitrous acid Diisopropylamine 0.12 ~ 0.54 part, xylidine 0.25 ~ 0.55 part, N-Methyl pyrrolidone 0.07 ~ 0.12 part, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt 0.13 ~ 0.25 part, Tristearoylglycerol 0.45 ~ 1.25 part, oil base amino acid sodium 0.5 ~ 1.8 part, Sodium dodecylbenzene sulfonate 0.01 ~ 0.08 part, potassium sorbate 0.06 ~ 0.15 part, dimethyl silicone oil 0.1 ~ 0.4 part, 15 ~ 30 parts, water.
2. a kind of compound wax pattern vehicle glazing according to claim 1 agent, is characterized in that, described compound wax is by vegetable wax, animal wax and mineral wax 1:(1 ~ 3 in mass ratio): (1 ~ 5) is composited.
3. a kind of compound wax pattern vehicle glazing according to claim 2 agent, is characterized in that, described vegetable wax is flax wax or tealight.
4. a kind of compound wax pattern vehicle glazing according to claim 2 agent, is characterized in that, described animal wax is beeswax.
5. a kind of compound wax pattern vehicle glazing according to claim 2 agent, is characterized in that, described mineral wax is at least one in paraffin, ceresine or Microcrystalline Wax.
6. a kind of compound wax pattern vehicle glazing according to claim 2 agent, is characterized in that, described compound wax by vegetable wax, animal wax and mineral wax in mass ratio 1:2:4 be composited.
7. a kind of compound wax pattern vehicle glazing according to claim 2 agent, it is characterized in that, component and each constituent mass number as follows: vegetable wax 2 parts, animal wax 4 parts, mineral wax 9 parts, polyvinyl alcohol 4 parts, triethanolamine oleate 1.0 parts, carboxyethyl cellulose 0.06 part, amido silicon oil 2.8 parts, hydroxyethyl dodecyl alcohol 0.5 part, nitrous acid Diisopropylamine 0.35 part, xylidine 0.4 part, N-Methyl pyrrolidone 0.9 part, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt 0.18 part, Tristearoylglycerol 0.85 part, oil base amino acid sodium 1.2 parts, Sodium dodecylbenzene sulfonate 0.05 part, potassium sorbate 0.09 part, dimethyl silicone oil 0.25 part, 28 parts, water.
8. the preparation method of a kind of compound wax pattern vehicle glazing agent in claim 1 to 7 described in any one, is characterized in that, comprise the steps:
1) vegetable wax, animal wax and mineral wax are mixed in proportion, be heated to 100 ~ 120 DEG C melt to wax, add triethanolamine oleate, carboxyethyl cellulose, amido silicon oil, hydroxyethyl dodecyl alcohol, nitrous acid Diisopropylamine, xylidine, N-Methyl pyrrolidone, trihydroxyethyl methyl quaternary ammonium methyl sulfate salt, Tristearoylglycerol, oil base amino acid sodium, Sodium dodecylbenzene sulfonate, potassium sorbate and dimethyl silicone oil, at 80 ~ 100 DEG C, stir 1 ~ 5h;
2) water is mixed with polyvinyl alcohol, be heated to 80 ~ 90 DEG C;
3) mixing solutions of step 1) is joined step 2) solution in, namely stirring and emulsifying to room temperature obtains the agent of compound wax pattern vehicle glazing.
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| CN201510776268.9A CN105238274A (en) | 2015-11-14 | 2015-11-14 | Compound-wax type automobile polish and preparing method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106398545A (en) * | 2016-08-27 | 2017-02-15 | 安徽天瞳智能科技有限公司 | Composite material with superhydrophobic performance |
| CN106479437A (en) * | 2016-08-27 | 2017-03-08 | 安徽天瞳智能科技有限公司 | A kind of antistatic high brightness aqueouss composite and preparation method thereof |
| WO2017161510A1 (en) * | 2016-03-23 | 2017-09-28 | 江阴樱花梦家庭用品有限公司 | Spraying liquid vehicle wax composition and preparation method therefor |
| CN109852252A (en) * | 2017-11-30 | 2019-06-07 | 菏泽海诺知识产权服务有限公司 | A kind of automobile-used scratch wax and preparation method thereof |
| CN109852258A (en) * | 2017-11-30 | 2019-06-07 | 菏泽海诺知识产权服务有限公司 | A kind of decontamination wax and preparation method thereof |
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