CN105220486A - A kind of anti-crease finishing auxiliary agent of silk fabric - Google Patents

A kind of anti-crease finishing auxiliary agent of silk fabric Download PDF

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Publication number
CN105220486A
CN105220486A CN201510778492.1A CN201510778492A CN105220486A CN 105220486 A CN105220486 A CN 105220486A CN 201510778492 A CN201510778492 A CN 201510778492A CN 105220486 A CN105220486 A CN 105220486A
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China
Prior art keywords
ultrasonic wave
silk fabric
auxiliary agent
crease finishing
finishing auxiliary
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CN201510778492.1A
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Chinese (zh)
Inventor
丁玉平
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Changxing Sanxing Textile Co Ltd
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Changxing Sanxing Textile Co Ltd
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Priority to CN201510778492.1A priority Critical patent/CN105220486A/en
Publication of CN105220486A publication Critical patent/CN105220486A/en
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Abstract

The invention discloses a kind of anti-crease finishing auxiliary agent of silk fabric, it comprises pretreatment solution and ultrasonic wave finisher solution: be mass percent below; Pretreatment solution: nanometer sericite in powder 0.08%, fibroin 0.5%, pigskin collagen 0.3-0.5%, malic acid 0.02%, ultrasonic wave finisher solution: nano zine oxide 0.05%, fibroin 0.8%, pigskin collagen 1.5-1.9%.It makes full use of multiple means and combines, and comprise native protein, mineral powder, ultrasonic wave process means etc., its natural environmental-protective, without the need to high temperature, does not need chemical reagent, and the real silk after process has excellent wrinkle resistance and drapability.

Description

A kind of anti-crease finishing auxiliary agent of silk fabric
Technical field
The present invention relates to a kind of anti-crease finishing auxiliary agent of silk fabric, belong to field of textiles.
Background technology
The real silk fabric wearability that to have that gloss is soft, feel is soft and smooth, moisture absorption is breathed freely etc. excellent, is particularly suitable for making the products such as the underwear that has higher requirements to antibiotic property and infant clothing.But the shortcomings such as real silk fabric creases easily, easily shrink, difficulty is arranged, have impact on its result of use.In order to overcome the deficiency of real silk fabric, for many years, scientific and technical personnel constantly explore the technological approaches improving silk broadcloth wearability, wherein adopt finishing agent to be one of main research direction of raising real silk fabric performance both at home and abroad at present.
The drapability of yarn-dyed fabric is the song that produces due to its deadweight and degree of crook when taking of fabric and characteristic, and the fabric that draping property is good, can form the surface modeling of smooth smoothness, has good conformability, gives visual enjoyment.So the drapability of fabric is the main contents in appearance style.
The present invention aims to provide a kind of anti-crease finishing auxiliary agent of silk fabric, and it makes full use of multiple means and combines, and comprises native protein, mineral powder, ultrasonic wave process means etc., its natural environmental-protective, without the need to high temperature, do not need chemical reagent, and the real silk after process have excellent wrinkle resistance and drapability.
Summary of the invention
Based on the technical problem that background technology exists, the present invention is directed to background technology Problems existing, there is provided a kind of anti-crease finishing auxiliary agent of silk fabric, it makes full use of multiple means and combines, and comprises native protein, mineral powder, ultrasonic wave process means etc., its natural environmental-protective, without the need to high temperature, do not need chemical reagent, and the real silk after process have excellent wrinkle resistance and drapability.
Object of the present invention is achieved through the following technical solutions:
An anti-crease finishing auxiliary agent for silk fabric, it comprises pretreatment solution and ultrasonic wave finisher solution:
Below be mass percent;
Pretreatment solution: nanometer sericite in powder 0.08%, fibroin 0.5%, pigskin collagen 0.3-0.5%, malic acid 0.02%,
The particle diameter of described nanometer sericite in powder is 80-100nm;
Pretreating process is: get real silk fabric, bath raio 1:50, keeps constant temperature 55 DEG C concussion 25-35min, is then rapidly heated to 80 DEG C of maintenance 2s with the speed of 10 DEG C/s, then removes thermal source, be certainly cooled to 45 DEG C to keep 8-10min; Process rear 50 DEG C of oven dry;
Ultrasonic wave finisher solution:
Nano zine oxide 0.05%, fibroin 0.8%, pigskin collagen 1.5-1.9%;
The particle diameter of described nano zine oxide is 30-50nm;
The molecular weight of described collagen is 5000 dalton;
Ultrasonic wave finishing technique flow process is: bath raio 1:30, puts into thermostatic ultrasonic wave producer, keeps constant temperature 45 DEG C process 5-8min; Process latter 60 DEG C and cure 12-15s, then with the clean residue of washed with de-ionized water, 30 DEG C of oven dry.
Usefulness of the present invention is:
The invention provides a kind of anti-crease finishing auxiliary agent of silk fabric, it makes full use of multiple means and combines, and comprises native protein, mineral powder, ultrasonic wave process means etc., its natural environmental-protective, without the need to high temperature, do not need chemical reagent, and the real silk after process have excellent wrinkle resistance and drapability.
Detailed description of the invention
Embodiment 1:
The present invention's real silk fabric used is the plain crepe-back satin sample of silk broadcloth 14654.
The use of the anti-crease finishing auxiliary agent of silk fabric:
(1) preliminary treatment:
Be equipped with pretreatment solution: nanometer sericite in powder 0.08%, fibroin 0.5%, pigskin collagen 0.3%, malic acid 0.02%,
The particle diameter of described nanometer sericite in powder is 80nm;
Pretreating process is: get real silk fabric, bath raio 1:50, keeps constant temperature 55 DEG C concussion 25min, is then rapidly heated to 80 DEG C of maintenance 2s with the speed of 10 DEG C/s, then removes thermal source, be certainly cooled to 45 DEG C to keep 8min; Process rear 50 DEG C of oven dry;
(2) ultrasonic wave arranges:
Pretreated real silk is proceeded ultrasonic wave to arrange;
Be equipped with ultrasonic wave finisher solution:
Nano zine oxide 0.05%, fibroin 0.8%, pigskin collagen 1.9%;
The particle diameter of described nano zine oxide is 30nm;
The molecular weight of described collagen is 5000 dalton;
Ultrasonic wave finishing technique flow process is: bath raio 1:30, puts into thermostatic ultrasonic wave producer, keeps constant temperature 45 DEG C process 5min; Process latter 60 DEG C and cure 12s, then with the clean residue of washed with de-ionized water, 30 DEG C of oven dry.
Embodiment 2:
The use of the anti-crease finishing auxiliary agent of silk fabric:
(1) preliminary treatment:
Be equipped with pretreatment solution: nanometer sericite in powder 0.08%, fibroin 0.5%, pigskin collagen 0.5%, malic acid 0.02%,
The particle diameter of described nanometer sericite in powder is 100nm;
Pretreating process is: get real silk fabric, bath raio 1:50, keeps constant temperature 55 DEG C concussion 35min, is then rapidly heated to 80 DEG C of maintenance 2s with the speed of 10 DEG C/s, then removes thermal source, be certainly cooled to 45 DEG C to keep 8min; Process rear 50 DEG C of oven dry;
(2) ultrasonic wave arranges:
Pretreated real silk is proceeded ultrasonic wave to arrange;
Be equipped with ultrasonic wave finisher solution:
Nano zine oxide 0.05%, fibroin 0.8%, pigskin collagen 1.9%;
The particle diameter of described nano zine oxide is 50nm;
The molecular weight of described collagen is 5000 dalton;
Ultrasonic wave finishing technique flow process is: bath raio 1:30, puts into thermostatic ultrasonic wave producer, keeps constant temperature 45 DEG C process 5-8min; Process latter 60 DEG C and cure 15s, then with the clean residue of washed with de-ionized water, 30 DEG C of oven dry.
Embodiment 3:
The use of the anti-crease finishing auxiliary agent of silk fabric:
(1) preliminary treatment:
Be equipped with pretreatment solution: nanometer sericite in powder 0.08%, fibroin 0.5%, pigskin collagen 0.4%, malic acid 0.02%,
The particle diameter of described nanometer sericite in powder is 90nm;
Pretreating process is: get real silk fabric, bath raio 1:50, keeps constant temperature 55 DEG C concussion 30min, is then rapidly heated to 80 DEG C of maintenance 2s with the speed of 10 DEG C/s, then removes thermal source, be certainly cooled to 45 DEG C to keep 9min; Process rear 50 DEG C of oven dry;
(2) ultrasonic wave arranges:
Pretreated real silk is proceeded ultrasonic wave to arrange;
Be equipped with ultrasonic wave finisher solution:
Nano zine oxide 0.05%, fibroin 0.8%, pigskin collagen 1.6%;
The particle diameter of described nano zine oxide is 40nm;
The molecular weight of described collagen is 5000 dalton;
Ultrasonic wave finishing technique flow process is: bath raio 1:30, puts into thermostatic ultrasonic wave producer, keeps constant temperature 45 DEG C process 6min; Process latter 60 DEG C and cure 14s, then with the clean residue of washed with de-ionized water, 30 DEG C of oven dry.
Embodiment 4:
The use of the anti-crease finishing auxiliary agent of silk fabric:
(1) preliminary treatment:
Be equipped with pretreatment solution: nanometer sericite in powder 0.08%, fibroin 0.5%, pigskin collagen 0.4%, malic acid 0.02%,
The particle diameter of described nanometer sericite in powder is 80-100nm;
Pretreating process is: get real silk fabric, bath raio 1:50, keeps constant temperature 55 DEG C concussion 29min, is then rapidly heated to 80 DEG C of maintenance 2s with the speed of 10 DEG C/s, then removes thermal source, be certainly cooled to 45 DEG C to keep 10min; Process rear 50 DEG C of oven dry;
(2) ultrasonic wave arranges:
Pretreated real silk is proceeded ultrasonic wave to arrange;
Be equipped with ultrasonic wave finisher solution:
Nano zine oxide 0.05%, fibroin 0.8%, pigskin collagen 1.5-1.9%;
The particle diameter of described nano zine oxide is 50nm;
The molecular weight of described collagen is 5000 dalton;
Ultrasonic wave finishing technique flow process is: bath raio 1:30, puts into thermostatic ultrasonic wave producer, keeps constant temperature 45 DEG C process 7min; Process latter 60 DEG C and cure 13s, then with the clean residue of washed with de-ionized water, 30 DEG C of oven dry.
Embodiment 5:
The applicant finds, in processing procedure, effect is not linear, has very large randomness, and any modified parameter all will cause the reduction greatly of effect, only in specific scope, have obvious synergy, and comparative example be only demonstration.
Comparative example:
The use of the anti-crease finishing auxiliary agent of silk fabric:
(1) preliminary treatment:
Be equipped with pretreatment solution: nanometer sericite in powder 0.1%, fibroin 0.8%, pigskin collagen 0.8%
The particle diameter of described nanometer sericite in powder is 120nm;
Pretreating process is: get real silk fabric, bath raio 1:50, keeps constant temperature 55 DEG C concussion 40min, processes rear 50 DEG C of oven dry;
(2) ultrasonic wave arranges:
Pretreated real silk is proceeded ultrasonic wave to arrange;
Be equipped with ultrasonic wave finisher solution:
Nano zine oxide 0.05%, fibroin 0.8%, pigskin collagen 1.5%;
The particle diameter of described nano zine oxide is 80nm;
The molecular weight of described collagen is 3000 dalton;
Ultrasonic wave finishing technique flow process is: bath raio 1:50, puts into thermostatic ultrasonic wave producer, keeps constant temperature 45 DEG C process 10min; Process latter 80 DEG C and cure 5s, then with the clean residue of washed with de-ionized water, 30 DEG C of oven dry.
Embodiment 6:
Effect is tested and assessed:
The drapability of yarn-dyed fabric is the song that produces due to its deadweight and degree of crook when taking of fabric and characteristic, and the fabric that draping property is good, can form the surface modeling of smooth smoothness, has good conformability, gives visual enjoyment.So the drapability of fabric is the main contents in appearance style.
Suspended coefficient divides static drape coefficient and dynamic suspended coefficient, and the suspended coefficient of general fabrics is less, and the drapability of fabric is better, and flexibility is better.
Experimental result is as shown in the table:
Table 1
This detects data only for above-mentioned detection sample.
As can be seen here, the invention provides the silk fabric that a kind of crease-resistant drapability is good, it makes full use of multiple means and combines, comprise native protein, mineral powder, ultrasonic wave process means etc., its natural environmental-protective, without the need to high temperature, do not need chemical reagent, and the real silk after process have excellent wrinkle resistance and drapability.
Especially the excellent of embodiment 3 is most preferred embodiments of the present invention.
The above; be only the present invention's preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.

Claims (5)

1. an anti-crease finishing auxiliary agent for silk fabric, it comprises pretreatment solution and ultrasonic wave finisher solution:
Below be mass percent;
Pretreatment solution: nanometer sericite in powder 0.08%, fibroin 0.5%, pigskin collagen 0.3-0.5%, malic acid 0.02%,
Ultrasonic wave finisher solution:
Nano zine oxide 0.05%, fibroin 0.8%, pigskin collagen 1.5-1.9%.
2. the anti-crease finishing auxiliary agent of silk fabric according to claim 1, is characterized in that:
The particle diameter of described nano zine oxide is 30-50nm;
The molecular weight of described collagen is 5000 dalton.
3. the anti-crease finishing auxiliary agent of the silk fabric described in claim 1-2, is characterized in that:
The particle diameter of described nanometer sericite in powder is 80-100nm.
4. the anti-crease finishing auxiliary agent of the silk fabric described in claim 1-2, is characterized in that:
Described pretreating process is: get real silk fabric, bath raio 1:50, keeps constant temperature 55 DEG C concussion 25-35min, is then rapidly heated to 80 DEG C of maintenance 2s with the speed of 10 DEG C/s, then removes thermal source, be certainly cooled to 45 DEG C to keep 8-10min; Process rear 50 DEG C of oven dry.
5. the anti-crease finishing auxiliary agent of the silk fabric described in claim 1-2, is characterized in that:
Described ultrasonic wave finishing technique flow process is: bath raio 1:30, puts into thermostatic ultrasonic wave producer, keeps constant temperature 45 DEG C process 5-8min; Process latter 60 DEG C and cure 12-15s, then with the clean residue of washed with de-ionized water, 30 DEG C of oven dry.
CN201510778492.1A 2015-11-13 2015-11-13 A kind of anti-crease finishing auxiliary agent of silk fabric Pending CN105220486A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106120334A (en) * 2016-07-06 2016-11-16 德清县新鑫达丝绸炼染有限公司 A kind of true silk crease-resistant increases the finishing auxiliaries hung down
CN108486882A (en) * 2018-04-08 2018-09-04 苏州经贸职业技术学院 A kind of preparation method of antibacterial crease-resistant Silk Finishing agent
CN109162100A (en) * 2018-08-10 2019-01-08 常州依丝特纺织服饰有限公司 A kind of shirt fabric crease-shedding finishing agent and its application

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101974850A (en) * 2010-10-18 2011-02-16 南通曙光染织有限公司 Preparation method of ecological non-ironing silk fabric
CN103031733A (en) * 2012-12-03 2013-04-10 鑫缘茧丝绸集团股份有限公司 Preparation method of anti-crease antimicrobial complex-function true silk
CN103334292A (en) * 2013-06-27 2013-10-02 江苏华艺服饰有限公司 Real silk fabric nano-zinc oxide antibacterial production method
CN104294583A (en) * 2014-10-20 2015-01-21 南通大学 Preparation method of composite functional fabric with antimicrobial, anti-ultraviolet, deodorization and self-cleaning functions

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101974850A (en) * 2010-10-18 2011-02-16 南通曙光染织有限公司 Preparation method of ecological non-ironing silk fabric
CN103031733A (en) * 2012-12-03 2013-04-10 鑫缘茧丝绸集团股份有限公司 Preparation method of anti-crease antimicrobial complex-function true silk
CN103334292A (en) * 2013-06-27 2013-10-02 江苏华艺服饰有限公司 Real silk fabric nano-zinc oxide antibacterial production method
CN104294583A (en) * 2014-10-20 2015-01-21 南通大学 Preparation method of composite functional fabric with antimicrobial, anti-ultraviolet, deodorization and self-cleaning functions

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106120334A (en) * 2016-07-06 2016-11-16 德清县新鑫达丝绸炼染有限公司 A kind of true silk crease-resistant increases the finishing auxiliaries hung down
CN106120334B (en) * 2016-07-06 2018-09-25 德清县新鑫达丝绸炼染有限公司 A kind of finishing auxiliaries that true silk crease-resistant increasing is vertical
CN108486882A (en) * 2018-04-08 2018-09-04 苏州经贸职业技术学院 A kind of preparation method of antibacterial crease-resistant Silk Finishing agent
CN109162100A (en) * 2018-08-10 2019-01-08 常州依丝特纺织服饰有限公司 A kind of shirt fabric crease-shedding finishing agent and its application

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Application publication date: 20160106