CN105220455A - A kind of fragrant citrus taste releases fragrant fabric and preparation method thereof - Google Patents
A kind of fragrant citrus taste releases fragrant fabric and preparation method thereof Download PDFInfo
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- CN105220455A CN105220455A CN201510595747.0A CN201510595747A CN105220455A CN 105220455 A CN105220455 A CN 105220455A CN 201510595747 A CN201510595747 A CN 201510595747A CN 105220455 A CN105220455 A CN 105220455A
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- sodium sulfate
- lauryl sodium
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- fragrant
- bamboo fibre
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Abstract
The invention provides one and release fragrant fabric, described fabric is formed by the bamboo fibre of 80% and the cotton fiber blending of 20%, the CNT of described bamboo fibre grafting lauryl sodium sulfate modification, is enclosed with fragrance matter in the CNT of described lauryl sodium sulfate modification; Described fragrance matter is orange limonene.The present invention selects the orange limonene that the coated threshold size of CNT of suitable lauryl sodium sulfate modification is suitable, and is grafted on bamboo fibre, obtain there is fragrant citrus smell release fragrant fabric; Bamboo fibre itself also can embed part orange limonene, more enhances the lasting release of fragrant citrus smell; The cavity of CNT inside also can embed part orange limonene matter, improves the body of fragrance and release persistence.
Description
Technical field
The invention belongs to textile material preparation field, be specifically related to a kind of fragrant citrus taste and release fragrant fabric and preparation method thereof.
Background technology
The dulcet fabric of tool is subject to the favor of consumer, but the lasting fragrance that prior art prepares the dulcet fabric of tool is poor, be difficult to long-term reservation, and the performance such as the feel of pattern-printing and dyeing fabric, rub resistance, fastness to washing, antifouling, weather resisteant should be ensured in process of production, when printing, saturating net should avoid print slurry blocking impact to produce simultaneously, and the problems referred to above are the problems that should solve in the production of aromatic home textile fabric.
This area needs to develop a kind of fabric that can discharge fragrance lastingly.
Summary of the invention
An object of the present invention is to provide a kind of fragrant citrus taste to release fragrant fabric, described fabric is formed by the bamboo fibre of 80% and the cotton fiber blending of 20%, the CNT of described bamboo fibre grafting lauryl sodium sulfate modification, is enclosed with fragrance matter in the CNT of described lauryl sodium sulfate modification;
Described fragrance matter is orange limonene.
The preparation process of the CNT of described lauryl sodium sulfate modification is: by carbon nanotube dispersed in the solution being dissolved with lauryl sodium sulfate, then add coupling agent, and spraying dry obtains the CNT of lauryl sodium sulfate modification.
The preparation method that fragrant citrus taste of the present invention releases fragrant fabric comprises the steps:
(1) CNT of lauryl sodium sulfate modification is prepared;
(2) by the CNT of bamboo fibre grafting lauryl sodium sulfate modification;
(3) fragrance matter is embedded;
(4) so air-dry that to release fragrant bamboo fibre;
(5) cotton fiber is soaked orange limonene 4 ~ 6s, after air-dry, obtain fragrant cotton fiber;
(6) fragrant bamboo fibre and fragrant cotton fiber are obtained fabric by the quality of 8:2 than blending.
The preparation method of the CNT of the described lauryl sodium sulfate modification of step (1) is: by 0.1 ~ 0.3mol/L carbon nanotube dispersed in the solution of lauryl sodium sulfate being dissolved with 1 ~ 3mol/L, then add 0.02 ~ 0.05mol/L coupling agent, spraying dry obtains the CNT of lauryl sodium sulfate modification.
Described spray drying temperature is 120 ~ 150 DEG C.
The method of the CNT of described bamboo fibre grafting lauryl sodium sulfate modification is: by the CNT of the lauryl sodium sulfate modification of mass ratio 0.1 ~ 0.5:3 ~ 5 and bamboo fibre mixing, stir, add coupling agent reaction, react complete, washing, the dry product obtaining the CNT of bamboo fibre grafting lauryl sodium sulfate modification;
The addition of described coupling agent is 0.01 ~ 0.07wt% of the carbon nanotube mass of lauryl sodium sulfate modification.
The process of the described embedding fragrance matter of step (3) is: be immersed in orange limonene by the product of step (2), applies the microwave of 100 ~ 500W, reaction 10 ~ 15min.
Described air-dry temperature is 15 ~ 20 DEG C.
Compared with prior art, the present invention has following beneficial effect:
The present invention selects the orange limonene that the coated threshold size of CNT of suitable lauryl sodium sulfate modification is suitable, and is grafted on bamboo fibre, obtain there is fragrant citrus smell release fragrant fabric; Bamboo fibre itself also can embed part orange limonene, more enhances the lasting release of fragrant citrus smell; The cavity of CNT inside also can embed part orange limonene matter, improves the body of fragrance and release persistence.
Detailed description of the invention
For better the present invention being described, be convenient to understand technical scheme of the present invention, typical but non-limiting embodiment of the present invention is as follows:
Embodiment 1
A kind of fragrant citrus taste releases fragrant fabric, prepares by the following method:
(1) by 0.1mol/L carbon nanotube dispersed in the solution of lauryl sodium sulfate being dissolved with 3mol/L, then add 0.02mol/L coupling agent, 150 DEG C of spraying dry obtain the CNT of lauryl sodium sulfate modification;
(2) by the CNT of the lauryl sodium sulfate modification of mass ratio 0.1:5 and bamboo fibre mixing, stir, add titanate coupling agent reaction, react complete, washing, the dry product obtaining the CNT of bamboo fibre grafting lauryl sodium sulfate modification; The addition of described coupling agent is the 0.07wt% of the carbon nanotube mass of lauryl sodium sulfate modification;
(3) product of the CNT of bamboo fibre grafting lauryl sodium sulfate modification step (2) obtained is dispersed in orange limonene, carries out 300W microwave irradiation 5s, obtains the bamboo fibre embedding orange limonene;
(4) 20 DEG C so air-dry that to release fragrant bamboo fibre;
(5) soak orange limonene 6s by 5 DEG C, cotton fiber, 10 DEG C air-dry after obtain fragrant cotton fiber;
(6) fragrant bamboo fibre and fragrant cotton fiber are obtained fabric by the quality of 8:2 than blending.
Release what prepare the size that fragrant fabric cuts 1m × 1m, be divided into 7 equal portions, 1 part is placed in closed container and leaves standstill 30min, and insert headspace gas chromatography absorption pin, after Thermal desorption, gas Chromatographic Determination fragrance matter, is designated as A
0; By 4 parts release under fragrant fabric hangs respectively and be placed in room temperature condition, place 1,5,10,30 day respectively, the fragrant fabric of releasing of 2 parts is placed 10 days (being equivalent to 2 years), 30 days (being equivalent to 5 years) at the ventilating opening of air output 3m/s respectively, adopt Headspace Gas Chromatography respectively, be designated as A respectively
1, A
2, A
3, A
4, A
5, A
6; Adopt A
n/ A
0obtain fragrance conservation rate, result is as table 1.
Embodiment 2
A kind of fragrant citrus taste releases fragrant fabric, prepares by the following method:
(1) by 0.3mol/L carbon nanotube dispersed in the solution of lauryl sodium sulfate being dissolved with 1 ~ 3mol/L, then add 0.02mol/L coupling agent, 120 ~ 150 DEG C of spraying dry obtain the CNT of lauryl sodium sulfate modification;
(2) by the CNT of the lauryl sodium sulfate modification of mass ratio 0.5:3 and bamboo fibre mixing, stir, add titanate coupling agent reaction, react complete, washing, the dry product obtaining the CNT of bamboo fibre grafting lauryl sodium sulfate modification; The addition of described coupling agent is the 0.01wt% of the carbon nanotube mass of lauryl sodium sulfate modification;
(3) 20 ~ 35 DEG C so air-dry that to release fragrant bamboo fibre;
(4) soak orange limonene 4s by 10 DEG C, cotton fiber, 20 DEG C air-dry after obtain fragrant cotton fiber;
(5) fragrant bamboo fibre will be released and fragrant cotton fiber blending obtains fabric.
Method of testing is with embodiment 1, and result is as table 1.
Embodiment 3
A kind of fragrant citrus taste releases fragrant fabric, prepares by the following method:
(1) by 0.2mol/L carbon nanotube dispersed in the solution of lauryl sodium sulfate being dissolved with 2mol/L, then add 0.03mol/L coupling agent, 140 DEG C of spraying dry obtain the CNT of lauryl sodium sulfate modification;
(2) by the CNT of the lauryl sodium sulfate modification of mass ratio 0.3:4 and bamboo fibre mixing, stir, add titanate coupling agent reaction, react complete, washing, the dry product obtaining the CNT of bamboo fibre grafting lauryl sodium sulfate modification; The addition of described coupling agent is the 0.04wt% of the carbon nanotube mass of lauryl sodium sulfate modification;
(3) 20 ~ 35 DEG C so air-dry that to release fragrant bamboo fibre;
(4) soak orange limonene 5s by 8 DEG C, cotton fiber, 17 DEG C air-dry after obtain fragrant cotton fiber;
(5) fragrant bamboo fibre will be released and fragrant cotton fiber blending obtains fabric.
Method of testing is with embodiment 1, and result is as table 1.
Comparative example 1
Adopt the mode of surface dressing to arrange the fabric of the bamboo fibre of 80% and the cotton fiber blending of 20%, described surface dressing uses orange limonene, and method of testing is identical with embodiment 1; Result is as table 1.
Table 1 fragrance conservation rate test result
| Placement condition | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example |
| Normal temperature 1 day | 100％ | 100％ | 100％ | 99％ |
| Normal temperature 5 days | 99％ | 100％ | 100％ | 98％ |
| Normal temperature 10 days | 98％ | 99％ | 99％ | 93％ |
| Normal temperature 30 days | 95％ | 98％ | 99％ | 85％ |
| Ventilate 10 days | 92％ | 92％ | 93％ | 60％ |
| Ventilate 30 days | 88％ | 86％ | 90％ | 20％ |
As can be seen from Table 1, provided by the inventionly release fragrant fabric there is good fragrance conservation rate.
It should be noted that and understand, when not departing from the spirit and scope of the present invention required by accompanying claim, various amendment and improvement can be made to the present invention of foregoing detailed description.Therefore, the scope of claimed technical scheme is not by the restriction of given any specific exemplary teachings.
Applicant states, the present invention illustrates method detailed of the present invention by above-described embodiment, but the present invention is not limited to above-mentioned method detailed, does not namely mean that the present invention must rely on above-mentioned method detailed and could implement.Person of ordinary skill in the field should understand, any improvement in the present invention, to equivalence replacement and the interpolation of auxiliary element, the concrete way choice etc. of each raw material of product of the present invention, all drops within protection scope of the present invention and open scope.
Claims (8)
1. a fragrant citrus taste releases fragrant fabric, it is characterized in that, described fabric is formed by the bamboo fibre of 80% and the cotton fiber blending of 20%, and the CNT of described bamboo fibre grafting lauryl sodium sulfate modification, is enclosed with fragrance matter in the CNT of described lauryl sodium sulfate modification;
Described fragrance matter is orange limonene.
2. fabric as claimed in claim 1, it is characterized in that, the preparation process of the CNT of described lauryl sodium sulfate modification is: by carbon nanotube dispersed in the solution being dissolved with lauryl sodium sulfate, then add coupling agent, spraying dry obtains the CNT of lauryl sodium sulfate modification.
3. fragrant citrus taste releases the preparation method of fragrant fabric as claimed in claim 1, it is characterized in that, described method comprises the steps:
(1) CNT of lauryl sodium sulfate modification is prepared;
(2) by the CNT of bamboo fibre grafting lauryl sodium sulfate modification;
(3) fragrance matter is embedded;
(4) so air-dry that to release fragrant bamboo fibre;
(5) cotton fiber is soaked orange limonene 4 ~ 6s, after air-dry, obtain fragrant cotton fiber;
(6) fragrant bamboo fibre and fragrant cotton fiber are obtained fabric by the quality of 8:2 than blending.
4. method as claimed in claim 3, it is characterized in that, the preparation method of the CNT of the described lauryl sodium sulfate modification of step (1) is: by 0.1 ~ 0.3mol/L carbon nanotube dispersed in the solution of lauryl sodium sulfate being dissolved with 1 ~ 3mol/L, then add 0.02 ~ 0.05mol/L coupling agent, spraying dry obtains the CNT of lauryl sodium sulfate modification.
5. method as claimed in claim 4, it is characterized in that, described spray drying temperature is 120 ~ 150 DEG C.
6. method as claimed in claim 3, it is characterized in that, the method of the CNT of described bamboo fibre grafting lauryl sodium sulfate modification is: by the CNT of the lauryl sodium sulfate modification of mass ratio 0.1 ~ 0.5:3 ~ 5 and bamboo fibre mixing, stir, add coupling agent reaction, react complete, washing, the dry product obtaining the CNT of bamboo fibre grafting lauryl sodium sulfate modification;
The addition of described coupling agent is 0.01 ~ 0.07wt% of the carbon nanotube mass of lauryl sodium sulfate modification.
7. method as claimed in claim 3, it is characterized in that, the process of the described embedding fragrance matter of step (3) is: be immersed in orange limonene by the product of step (2), applies the microwave of 100 ~ 500W, reaction 3 ~ 7s.
8. method as claimed in claim 7, it is characterized in that, described air-dry temperature is 15 ~ 20 DEG C.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107299444A (en) * | 2017-06-29 | 2017-10-27 | 顾渊 | One kind releases fragrant fabric and preparation method thereof |
| CN107313247A (en) * | 2017-06-26 | 2017-11-03 | 俞秀英 | A kind of fragrant citrus taste releases fragrant fabric and preparation method thereof |
| CN107326488A (en) * | 2017-06-30 | 2017-11-07 | 周远华 | A kind of fragrant citrus taste releases fragrant fabric and preparation method thereof |
| CN111074417A (en) * | 2019-11-28 | 2020-04-28 | 江苏品创纺织科技有限公司 | Preparation method of fabric with electromagnetic shielding function |
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| CN101899723A (en) * | 2009-05-27 | 2010-12-01 | 阿克马法国公司 | Manufacturing has the method for the conductibility composite fibre of nanotube at high proportion |
| CN102286160A (en) * | 2011-07-01 | 2011-12-21 | 同济大学 | Preparation method for multi-dimensional reinforcement of carbon nano tube grafted glass fibers |
| CN202738887U (en) * | 2012-07-12 | 2013-02-20 | 泉州匹克鞋业有限公司 | Aromatic sportwear fabric |
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2015
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Patent Citations (4)
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| CN101016659A (en) * | 2007-01-26 | 2007-08-15 | 东华大学 | Method of preparing Lyocell fiber containing carbon nano tube |
| CN101899723A (en) * | 2009-05-27 | 2010-12-01 | 阿克马法国公司 | Manufacturing has the method for the conductibility composite fibre of nanotube at high proportion |
| CN102286160A (en) * | 2011-07-01 | 2011-12-21 | 同济大学 | Preparation method for multi-dimensional reinforcement of carbon nano tube grafted glass fibers |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107313247A (en) * | 2017-06-26 | 2017-11-03 | 俞秀英 | A kind of fragrant citrus taste releases fragrant fabric and preparation method thereof |
| CN107299444A (en) * | 2017-06-29 | 2017-10-27 | 顾渊 | One kind releases fragrant fabric and preparation method thereof |
| CN107326488A (en) * | 2017-06-30 | 2017-11-07 | 周远华 | A kind of fragrant citrus taste releases fragrant fabric and preparation method thereof |
| CN111074417A (en) * | 2019-11-28 | 2020-04-28 | 江苏品创纺织科技有限公司 | Preparation method of fabric with electromagnetic shielding function |
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