CN105200686B - Supercritical fluid is to spray dyeing installation - Google Patents

Supercritical fluid is to spray dyeing installation Download PDF

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Publication number
CN105200686B
CN105200686B CN201510733238.XA CN201510733238A CN105200686B CN 105200686 B CN105200686 B CN 105200686B CN 201510733238 A CN201510733238 A CN 201510733238A CN 105200686 B CN105200686 B CN 105200686B
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pairs
combinations
sealing gland
unit
spray
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CN105200686A (en
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王威强
王明禄
刘燕
曲延鹏
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Shandong University
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Shandong University
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Abstract

The present invention relates to textile dyeing apparatus field, more particularly to a kind of supercritical fluid is to spray dyeing installation.Constituted by cleaning unit, to spray-painting color element, rinse unit, return channel, working fluid sealing gland unit, air sealing gland unit, connecting plate, sealed letter body, seal and pressure-regulating valve;According to supercritical fluid to spray-painting color technological process, install successively air sealing gland unit, working fluid sealing gland unit, return channel, cleaning unit, return channel, working fluid sealing gland unit, return channel, to spray-painting color element, return channel, working fluid sealing gland unit, return channel, rinse unit, return channel, working fluid sealing gland unit, air sealing gland unit.Supercritical fluid of the invention sprays to pollutant simultaneously from both sides, and it is zero that fluid injection power is offset, even dyeing, eliminates the deformation and tension failure produced to pollutant under high-pressure jet effect;Using the air seal structure for depressurizing step by step, continuous dyeing is realized, its simple structure, tightly beaten, manufacturability is excellent.

Description

Supercritical fluid is to spray dyeing installation
First, technical field
The present invention relates to textile dyeing apparatus field, more particularly to a kind of supercritical fluid is to spray dyeing installation.
2nd, technical background
Water pollution problems seriously governs traditional dyeing industrial expansion.Supercritical fluid dyeing utilizes supercritical fluid, Especially supercritical carbon dioxide is dyeed instead of water as the carrier of dyestuff, realizes non-aqueous dyeing, so that fundamentally Solve the problems, such as to dye industrial water pollution, there is good development prospect.
The characteristics of summarizing existing supercritical fluid dyeing device can be seen that by supercritical fluid that feature is determined in itself Fixed, the stainer of supercritical fluid dyeing must use high-tension apparatus, and the sealing property simultaneously for stainer is required also very Height, also requires to have to open soon or commutating structure well, this adds increased the complexity and cost of investment of apparatus structure, and nothing Method realizes high-volume continuous dyeing, seriously constrains the popularization and application of this new technology.
Patent Office of China national Department of Intellectual Property authorized announcement number on November 23rd, 2011 CN101798735B, the patent of entitled " supercritical fluid spray-dyeing device ", device incorporates supercritical fluid spraying technology With the advantage of traditional spray-painting technology, overcoming existing supercritical fluid dyeing device must use the shortcoming of high pressure dyeing device.With Afterwards, Patent Office of China national Department of Intellectual Property first disclosed announcement number on the 13rd for CN103981661A after August in 2014, Entitled " a kind of Novel supercritical fluid spray-painting injector " and September in 2015 authorize announcement number on 30th and are A kind of CN103866515B, the patent of entitled " supercritical fluid spray-dyeing injector ", deposits to supercritical fluid spray-dyeing technology Problem carried out some improvement.Cannot be while carrying out two-sided spray to pollutant but the problem that above-mentioned three patents are present is Dye, there is aberration in the two sides of pollutant;In addition, in the presence of high-speed jet, pollutant may be damaged because deformation is excessive Or the final upper dye effect of influence.
3rd, the content of the invention
The purpose of the present invention is the defect for overcoming existing supercritical fluid spray-dyeing equipment to exist, there is provided a kind of technological process letter Just, production efficiency is high, good level-dyeing property and to the undamaged supercritical fluid of pollutant to spray dyeing installation.
The technical scheme is that by cleaning unit, to spray-painting color element, rinse unit, return channel, working fluid gas Envelope unit, air sealing gland unit, connecting plate, sealed letter body, seal and pressure-regulating valve are constituted.
Cleaning unit is constituted by one or more structure identical to spray-painting color element or rinse unit to spray apparatus, by It is two or more when being constituted to spray apparatus, to being connected with each other by connecting plate between spray apparatus, to the number of spray apparatus by specific dyer Skill condition determines;Spray apparatus is made up of a pair of half tubulars of combinations of pairs to spray canister and a pair of distribution grids, in the diameter to spray canister Distribution grid is installed at split surface, it is corresponding to being respectively provided with supercritical fluid entrance in spray canister in two just to distribution grid center Pipe;Two and half tubulars after combinations of pairs are respectively mounted end socket to the two ends end of spray canister;Connecting plate is the structure of combinations of pairs, Connection corresponding to the axial edge at spray canister combinations of pairs with half tubular to spray apparatus respectively, the connecting plate of combinations of pairs is along dyeing Two opposite sides in technological process direction seal against each other connection respectively;Gap and combinations of pairs between the distribution grid of combinations of pairs Connecting plate between gap constitute pollutant passage.
Return channel is made up of the backflow cylinder of a pair of half tubulars of combinations of pairs, in two backflow cylinders of corresponding half tubular Center is respectively provided with operative fluid outlet pipe;The two ends end of the two and half tubulars backflow cylinder after combinations of pairs is respectively mounted End socket;Space between two backflow cylinders of combinations of pairs constitutes pollutant passage.
Working fluid sealing gland unit or air sealing gland unit are constituted by one or more structure identical air seal, by two When individual or more air seal is constituted, connected by sealed letter body phase between air seal, the number of air seal is by specific sealed letter The sealing characteristics of internal seal determine;Air seal is made up of the half tubular sealing gland cylinder of a pair of combinations of pairs, in two matched groups The center of the sealing gland cylinder of conjunction is respectively provided with fluid inlet tube;The two ends end of the two and half tubular sealing glands cylinder after combinations of pairs It is respectively mounted end socket;Sealed letter body is the structure of combinations of pairs, respectively with half tubular sealing gland of air seal cylinder combinations of pairs at Axial edge correspondence is connected, and the seal of combinations of pairs is installed in the sealed letter body of pairing;The sealed letter body of combinations of pairs is along dye Two opposite sides in color technological process direction seal against each other connection respectively;Gap and matched group between the seal of combinations of pairs Space between the sealing gland cylinder of conjunction constitutes pollutant passage.
According to supercritical fluid to spray-painting color technological process, install successively air sealing gland unit, working fluid sealing gland unit, Return channel, cleaning unit, return channel, working fluid sealing gland unit, return channel, to spray-painting color element, return channel, working fluid gas Envelope unit, return channel, rinse unit, return channel, working fluid sealing gland unit, air sealing gland unit;Return channel and cleaning unit Or to spray-painting color element or rinse unit between spray apparatus, by the connecting plate of combinations of pairs by the backflow of the tubular of return channel half Axial edge at cylinder combinations of pairs with to spray apparatus half tubular to the corresponding connection of axial edge at spray canister combinations of pairs;Work Make between the air seal and return channel of fluid sealing gland unit, by the sealed letter body of combinations of pairs by the sealing gland of the tubular of air seal half Axial edge connection corresponding with the axial edge at the backflow cylinder combinations of pairs of the tubular of return channel half at cylinder combinations of pairs;Work Make between the air seal of fluid sealing gland unit and the air seal of air sealing gland unit, by the sealed letter body of combinations of pairs by sealing gland The corresponding connection of axial edge at the sealing gland cylinder combinations of pairs of the tubular of device half;Along first air sealing gland in technological process direction It is not connected with other air seals in first air seal of unit or second last air seal of air sealing gland unit Axial edge at the half tubular sealing gland cylinder combinations of pairs of side installs the sealed letter body of combinations of pairs;The sealed letter of combinations of pairs Body seals against each other connection respectively along two opposite sides of dyeing flow direction;Combinations of pairs is installed in the sealed letter body of pairing Seal, the gap between the seal in the sealed letter body of combinations of pairs constitutes pollutant passage.
Each supercritical fluid inlet tube in cleaning unit or rinse unit, and each work in working fluid sealing gland unit Make pipeline of the fluid inlet tube with supercritical fluid generation subsystem to be connected, supercritical fluid generates the opposite side of subsystem Pipeline is connected with the pipeline of working fluid storage subsystem;Each supercritical fluid inlet tube in spray-painting color element and dyestuff are dissolved The pipeline of subsystem is connected, and another lateral line of dyestuff dissolving subsystem is connected with the pipeline of supercritical fluid generation subsystem Connect;The fluid inlet tube of air sealing gland unit is connected with compressed air unit;The working fluid of cleaning unit two ends return channel Outlet and working fluid are connected with the pipeline of impurity isolated subsystem, to spray-painting color element or rinse unit two ends return channel Operative fluid outlet pipe and working fluid be connected with the pipeline of dye separation subsystem, working fluid separates subsystem with impurity Another lateral line of system and another lateral line of working fluid and dye separation subsystem with working fluid storage subsystem Pipeline connection.
In supercritical fluid inlet tube to spray apparatus, the operative fluid outlet pipe of return channel, working fluid sealing gland unit Pressure-regulating valve is respectively mounted at fluid inlet tube, the fluid inlet tube of air sealing gland unit.
The excellent effect that the present invention is produced:Supercritical fluid sprays to pollutant simultaneously from both sides so that even dyeing, while It is zero to act on the fluid injection power on pollutant and offset, and is effectively eliminated under high-pressure jet effect to produced by pollutant Deformation and tension failure, it is its simple structure, tight while using the air seal structure for depressurizing step by step, be truly realized continuous dyeing Beat, manufacturability is excellent.
4th, illustrate
Fig. 1 is structural representation of the present invention to spray apparatus;
Fig. 2 is the structural representation of return channel of the present invention;
Fig. 3 is the structural representation of air seal of the present invention;
Fig. 4 is the overall structure diagram of single pair of spray apparatus of the present invention and single air seal combination;
Fig. 5 is double overall structure diagrams combined to spray apparatus and double air seals of the invention;
Fig. 6 is the overall structure diagram of three pairs of spray apparatus of the invention and the combination of three air seals;
Fig. 7 is present invention implementation to spray-painting color process flow diagram.
Reference:
1st, pollutant 2, to spray apparatus 2-1-1, to spray canister A 2-1-2, to spray canister B 2-2-1, supercritical fluid inlet tube A 2-2-2, supercritical fluid inlet tube B 2-3-1, distribution grid A 2-3-2, distribution grid B 3-1, connecting plate A 3-2, connecting plate B 4th, return channel 4-1-1, backflow cylinder A 4-1-2, backflow cylinder B 4-2-1, operative fluid outlet pipe A 4-2-2, operative fluid outlet Pipe B 5, air seal 5-1-1, sealing gland cylinder A 5-1-2, sealing gland cylinder B 5-2-1, fluid inlet tube A 5-2-2, fluid inlet tube B 6-1, sealed letter body A 6-2 sealed letter body B 7-1, seal A 7-2 seals B 8, pressure-regulating valve 8-1, pressure-regulating valve A 8-2, pressure-regulating valve B 8-3, pressure-regulating valve C 8-4, pressure-regulating valve D 9, cleaning unit 10, to spray-painting color element 11st, rinse unit 12, working fluid sealing gland unit 13, air sealing gland unit 14, working fluid storage subsystem 15, super face Boundary fluid generation subsystem 16, dyestuff dissolving subsystem 17, working fluid and impurity isolated subsystem 18, working fluid with Dye separation subsystem 19, compressed air unit.
5th, specific embodiment
Describe implementation process of the invention in detail below in conjunction with the accompanying drawings.
Embodiment one:Single injector and the supercritical fluid of single air seal combination to spray dyeing installation, such as Fig. 1~Fig. 4 institutes Show.
Supercritical fluid to spray dyeing installation by cleaning unit 9, to spray-painting color element 10, rinse unit 11, return channel 4, Working fluid sealing gland unit 12, the connecting plate A3-1 of air sealing gland unit 13, pairing structure and connecting plate B3-2, pairing structure Sealed letter body A 6-1 and sealed letter body B6-2, seal A7-1, seal B7-2 and pressure-regulating valve 8 are constituted.
Required according to dyeing condition, determine cleaning unit 9 or to spray-painting color element 10 or rinse unit 11 by one Individual structure identical is constituted to spray apparatus 2;To spray apparatus 2 by a pair of half tubulars of combinations of pairs to spray canister A2-1-1 and to spray canister B2- 1-2, a pair of distribution grid A2-3-1 and distribution grid B2-3-2 are constituted, to spray canister A2-1-1 and the diameter subdivision to spray canister B2-1-2 Distribution grid A2-3-1 and distribution grid B2-3-2 is respectively mounted at face, just to distribution grid A2-3-1 and distribution grid B2-3-2 centers To spray canister A2-1-1 and to being correspondingly arranged supercritical fluid inlet tube A2-2-1 respectively on spray canister B2-1-2 and supercritical fluid enters Mouth pipe B2-2-2;Two and half tubulars after combinations of pairs are pacified respectively to spray canister A2-1-1 and to the two ends end of spray canister B2-1-2 Dress end socket;Gap between the distribution grid A2-3-1 and distribution grid B2-3-2 of combinations of pairs constitutes the passage of pollutant 1.
Return channel 4 is made up of the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of a pair of half tubulars of combinations of pairs, in backflow The centre position of cylinder A4-1-1 sets operative fluid outlet pipe A4-2-1, and workflow is set in the centre position of backflow cylinder B4-1-2 Body outlet B4-2-2, the two ends end part of the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of two and half tubulars after combinations of pairs End socket is not installed;Space between the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of combinations of pairs constitutes the passage of pollutant 1.
According to the sealing characteristics of the seal in sealed letter body, working fluid sealing gland unit 12 or air sealing gland unit are determined 13 are constituted by an air seal 5;Air seal 5 is by a pair of gentle sealed tube B5-1-2 of half tubular sealing gland cylinder A5-1-1 of combinations of pairs Constitute, fluid inlet tube A5-2-1 is respectively provided with the center of the gentle sealed tube B5-1-2 of sealing gland cylinder A5-1-1 of combinations of pairs With fluid inlet tube B5-2-2;The two ends end of the gentle sealed tube B5-1-2 of sealing gland cylinder A5-1-1 of two and half tubulars after combinations of pairs Portion is respectively mounted end socket;Space between the gentle sealed tube B5-1-2 of sealing gland cylinder A5-1-1 of combinations of pairs constitutes the logical of pollutant 1 Road.
The annexation of each unit of the present invention:Along the traffic direction of pollutant 1, air sealing gland unit 13, work is installed successively Make fluid sealing gland unit 12, return channel 4, cleaning unit 9, return channel 4, working fluid sealing gland unit 12, return channel 4, to spray-painting Color element 10, return channel 4, working fluid sealing gland unit 12, return channel 4, rinse unit 11, return channel 4, working fluid sealing gland list Unit 12, air sealing gland unit 13;Return channel 4 and cleaning unit 9 or to spray-painting color element 10 or rinse unit 11 to spray apparatus 2 it Between, by the connecting plate A3-1 and connecting plate B3-2 of combinations of pairs by the backflow cylinder A4-1-1 of half tubular of return channel 4 and backflow Axial edge at cylinder B4-1-2 combinations of pairs is matched somebody with somebody with half tubular to spray apparatus 2 to spray canister A 2-1-1 and to spray canister B 2-1-2 To the corresponding connection of axial edge at combination;Between the air seal 5 and return channel 4 of working fluid sealing gland unit 12, by matching somebody with somebody To the sealed letter body A6-1 that combines and sealed letter body A6-2 by the gentle sealed tube B5- of the sealing gland of half tubular of air seal 5 cylinder A5-1-1 The backflow cylinder A4-1-1 and backflow cylinder B4-1-2 combinations of pairs of half tubular of axial edge and return channel 4 at 1-2 combinations of pairs The axial edge correspondence at place is connected;The air seal 5 of working fluid sealing gland unit 12 and the air seal 5 of air sealing gland unit 13 it Between, by the sealed letter body A 6-1 and sealed letter body A 6-2 of combinations of pairs by the sealing gland cylinder A5-1-1 of half tubular of air seal 5 The corresponding connection of axial edge at gentle sealed tube B5-1-2 combinations of pairs;Along first air sealing gland list in technological process direction Unit 13 first air seal 5 or second last air seal 5 of air sealing gland unit 13 in not with other phases of air seal 5 Axial edge at the sealing gland cylinder gentle sealed tube B5-1-2 combinations of pairs of A5-1-1 of half tubular for connecting side is respectively mounted sealing Letter body A6-1 and sealed letter body A6-2;The sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs are along dyeing flow direction Two opposite sides seal against each other connection respectively;Sealing is respectively mounted in the sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs Part A7-1 and seal B7-2, the sealing in seal A7-1 and sealed letter body B6-2 in the sealed letter body A6-1 of combinations of pairs Gap between part B7-2 constitutes the passage of pollutant 1.
Each supercritical fluid inlet tube A2-2-1 and supercritical fluid inlet tube in cleaning unit 9 or rinse unit 11 Each fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 in B2-2-2, and working fluid sealing gland unit 12 face with super The pipeline connection of boundary's fluid generation subsystem 15, another lateral line of supercritical fluid generation subsystem 15 is stored with working fluid The pipeline connection of subsystem 14;To each supercritical fluid inlet tube A2-2-1 and supercritical fluid inlet tube in spray-painting color element 10 B2-2-2 is connected with the pipeline of dyestuff dissolving subsystem 16, and another lateral line of dyestuff dissolving subsystem 16 is given birth to supercritical fluid Pipeline into subsystem 15 is connected;The fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 and air of air sealing gland unit 13 Compression device 19 is connected;The operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe of the both sides return channel 4 of cleaning unit 9 B4-2-2 and working fluid are connected with the pipeline of impurity isolated subsystem 17, and spray-painting color element 10 and the both sides of cleaning unit 9 are returned Flow the operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe B4-2-2 and working fluid and dye separation subsystem 18 of device 4 Pipeline connection, another lateral line and working fluid and the dye separation subsystem of working fluid and impurity isolated subsystem 17 Pipeline of the 18 another lateral line with working fluid storage subsystem 14 is connected.
Pressure regulation is installed in the supercritical fluid inlet tube A2-2-1 to spray apparatus 2 and supercritical fluid inlet tube B2-2-2 Valve A8-1;Pressure-regulating valve B8- is installed in the operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe B4-2-2 of return channel 4 2;Pressure-regulating valve C8-3 is installed in the fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 of working fluid sealing gland unit 12; Pressure-regulating valve D8- is respectively mounted at the fluid inlet tube A 5-2-1 and fluid inlet tube B5-2-2 of air sealing gland unit 13 4。
Embodiment two:Dual jet and the supercritical fluid of double air seals combination to spray dyeing installation, such as Fig. 1~Fig. 3 and Shown in Fig. 5.
Supercritical fluid to spray dyeing installation by cleaning unit 9, to spray-painting color element 10, rinse unit 11, return channel 4, Working fluid sealing gland unit 12, the connecting plate A3-1 of air sealing gland unit 13, pairing structure and connecting plate B3-2, pairing structure Sealed letter body A6-1 and sealed letter body B6-2, seal A7-1, seal B7-2 and pressure-regulating valve 8 are constituted.
Required according to dyeing condition, determine cleaning unit 9 or to spray-painting color element 10 or rinse unit 11 by two Individual structure identical is constituted to spray apparatus 2, and two to connecting plate A 3-1 and connecting plate the B 3-2 between spray apparatus 2 by pairing structure It is formed by connecting;To spray apparatus 2 by a pair of half tubulars of combinations of pairs to spray canister A 2-1-1 and to spray canister B2-1-2, a pair of distribution grids A2-3-1 and distribution grid B2-3-2 are constituted, and are respectively mounted at the diameter split surface to spray canister A2-1-1 and to spray canister B2-1-2 point Fabric swatch A2-3-1 and distribution grid B2-3-2, just to distribution grid A2-3-1 and distribution grid B2-3-2 centers to spray canister A2-1-1 and To supercritical fluid inlet tube A2-2-1 and supercritical fluid inlet tube B2-2-2 is correspondingly arranged on spray canister B2-1-2 respectively;Pairing Two and half tubulars after combination are respectively mounted end socket to spray canister A2-1-1 and to the two ends end of spray canister B2-1-2;Pairing structure Connecting plate A3-1 and connecting plate A3-2 respectively with half tubular to spray apparatus 2 to spray canister A2-1-1 and to spray canister B2-1-2 match The corresponding connection of axial edge at combination, the connecting plate A3-1 and connecting plate A3-2 of combinations of pairs are along dyeing flow direction Two opposite sides seal against each other connection respectively;Gap between the distribution grid A2-3-1 and distribution grid B2-3-2 of combinations of pairs and Gap between the connecting plate A3-1 and connecting plate A3-2 of combinations of pairs constitutes the passage of pollutant 1.
Return channel 4 is made up of the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of a pair of half tubulars of combinations of pairs, in backflow The centre position of cylinder A4-1-1 sets operative fluid outlet pipe A4-2-1, and workflow is set in the centre position of backflow cylinder B4-1-2 Body outlet B4-2-2, the two ends end part of the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of two and half tubulars after combinations of pairs End socket is not installed;Space between the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of combinations of pairs constitutes the passage of pollutant 1.
According to the sealing characteristics of the seal B7-2 in the seal A7-1 in sealed letter body A6-1 and sealed letter body B6-2, Determine that working fluid sealing gland unit 12 or air sealing gland unit 13 are constituted by two air seals 5, pass through between two air seals 5 The sealed letter body A6-1 and sealed letter body A6-2 of pairing structure are formed by connecting;Air seal 5 is by a pair of half tubular gas of combinations of pairs The gentle sealed tube B5-1-2 of sealed tube A5-1-1 are constituted, in the center of the gentle sealed tube B5-1-2 of sealing gland cylinder A5-1-1 of combinations of pairs It is respectively provided with fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2;The sealing gland cylinder A5- of two and half tubulars after combinations of pairs The two ends end of the gentle sealed tube B5-1-2 of 1-1 is respectively mounted end socket;The sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs Company corresponding with the axial edge at the sealing gland of half tubular of the air seal 2 cylinder gentle sealed tube B5-1-2 combinations of pairs of A5-1-1 respectively Connect, the sealed letter body A6-1 and sealed letter body A 6-2 of combinations of pairs are mutual respectively along two opposite sides of dyeing flow direction It is tightly connected;Seal A7-1 and seal A7-2 is respectively mounted in sealed letter body A6-1 and sealed letter body A 6-2;Combinations of pairs Sealed letter body A6-1 in seal A7-1 and sealed letter body B6-2 in seal B7-2 between gap and combinations of pairs Sealing gland cylinder A4-1-1 gentle sealed tube B4-1-2 between space constitute the passage of pollutant 1.
The annexation of each unit of the present invention:Along the traffic direction of pollutant 1, air sealing gland unit 13, work is installed successively Make fluid sealing gland unit 12, return channel 4, cleaning unit 9, return channel 4, working fluid sealing gland unit 12, return channel 4, to spray-painting Color element 10, return channel 4, working fluid sealing gland unit 12, return channel 4, rinse unit 11, return channel 4, working fluid sealing gland list Unit 12, air sealing gland unit 13;Return channel 4 and cleaning unit 9 or to spray-painting color element 10 or rinse unit 11 to spray apparatus 2 it Between, by the connecting plate A3-1 and connecting plate B3-2 of combinations of pairs by the backflow cylinder A4-1-1 of half tubular of return channel 4 and backflow Axial edge at cylinder B4-1-2 combinations of pairs is matched with half tubular to spray apparatus 2 to spray canister A2-1-1 and to spray canister B2-1-2 The corresponding connection of axial edge at combination;Between the air seal 5 and return channel 4 of working fluid sealing gland unit 12, by pairing The sealed letter body A6-1 and sealed letter body A6-2 of combination are by the gentle sealed tube B5-1-2 of the sealing gland of half tubular of air seal 5 cylinder A5-1-1 At the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 combinations of pairs of half tubular of axial edge and return channel 4 at combinations of pairs Axial edge correspondence is connected;Between the air seal 5 of working fluid sealing gland unit 12 and the air seal 5 of air sealing gland unit 13, lead to Cross the sealing gland cylinder gentle sealed tubes of A5-1-1 of sealed letter body A6-1 and sealed letter body A6-2 by half tubular of air seal 5 of combinations of pairs The corresponding connection of axial edge at B5-1-2 combinations of pairs;Along the of first air sealing gland unit 13 in technological process direction Be not connected side in one air seal 5 or second last air seal 5 of air sealing gland unit 13 with other air seals 5 Half tubular sealing gland cylinder the gentle sealed tube B5-1-2 combinations of pairs of A5-1-1 at axial edge be respectively mounted sealed letter body A6-1 With sealed letter body A6-2;The sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs along dyeing flow direction two offsides Side seals against each other connection respectively;Be respectively mounted in the sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs seal A7-1 and Seal B7-2, the seal B7-2 in seal A7-1 and sealed letter body B6-2 in the sealed letter body A6-1 of combinations of pairs it Between gap constitute pollutant 1 passage.
Each supercritical fluid inlet tube A2-2-1 and supercritical fluid inlet tube in cleaning unit 9 or rinse unit 11 Each fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 in B2-2-2, and working fluid sealing gland unit 12 face with super The pipeline connection of boundary's fluid generation subsystem 15, another lateral line of supercritical fluid generation subsystem 15 is stored with working fluid The pipeline connection of subsystem 14;To each supercritical fluid inlet tube A2-2-1 and supercritical fluid inlet tube in spray-painting color element 10 B2-2-2 is connected with the pipeline of dyestuff dissolving subsystem 16, and another lateral line of dyestuff dissolving subsystem 16 is given birth to supercritical fluid Pipeline into subsystem 15 is connected;The fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 and air of air sealing gland unit 13 Compression device 19 is connected;The operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe of the both sides return channel 4 of cleaning unit 9 B4-2-2 and working fluid are connected with the pipeline of impurity isolated subsystem 17, and spray-painting color element 10 and the both sides of cleaning unit 9 are returned Flow the operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe B4-2-2 and working fluid and dye separation subsystem 18 of device 4 Pipeline connection, another lateral line and working fluid and the dye separation subsystem of working fluid and impurity isolated subsystem 17 Pipeline of the 18 another lateral line with working fluid storage subsystem 14 is connected.
Pressure regulation is installed in the supercritical fluid inlet tube A2-2-1 to spray apparatus 2 and supercritical fluid inlet tube B2-2-2 Valve A8-1;Pressure-regulating valve B8- is installed in the operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe B4-2-2 of return channel 4 2;Pressure-regulating valve C8- is installed in fluid inlet tube A5-2-1 and fluid inlet tube the B 5-2-2 of working fluid sealing gland unit 12 3;Pressure-regulating valve D8- is respectively mounted at the fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 of air sealing gland unit 13 4。
Embodiment three:Three injectors and three air seals combination supercritical fluid to spray dyeing installation, such as Fig. 1~Fig. 3 and Shown in Fig. 6.
Supercritical fluid to spray dyeing installation by cleaning unit 9, to spray-painting color element 10, rinse unit 11, return channel 4, The connecting plate A 3-1 and connecting plate B3-2, pairing structure of working fluid sealing gland unit 12, air sealing gland unit 13, pairing structure Sealed letter body A6-1 and sealed letter body B6-2, seal A7-1, seal B7-2 and pressure-regulating valve 8 constitute.
Required according to dyeing condition, determine cleaning unit 9 or to spray-painting color element 10 or rinse unit 11 by three Individual structure identical is constituted to spray apparatus 2, and three connect to the connecting plate A3-1 and connecting plate B3-2 between spray apparatus 2 by pairing structure Connect and form;To spray apparatus 2 by a pair of half tubulars of combinations of pairs to spray canister A2-1-1 and to spray canister B2-1-2, a pair of distribution grids A2-3-1 and distribution grid B2-3-2 are constituted, and are respectively mounted at the diameter split surface to spray canister A2-1-1 and to spray canister B2-1-2 point Fabric swatch A2-3-1 and distribution grid B2-3-2, just to distribution grid A2-3-1 and distribution grid B2-3-2 centers to spray canister A2-1-1 and To supercritical fluid inlet tube A2-2-1 and supercritical fluid inlet tube B2-2-2 is correspondingly arranged on spray canister B2-1-2 respectively;Pairing Two and half tubulars after combination are respectively mounted end socket to spray canister A2-1-1 and to the two ends end of spray canister B2-1-2;Combinations of pairs Connecting plate A 3-1 and connecting plate A3-2 match somebody with somebody to spray canister A2-1-1 and to spray canister B2-1-2 with half tubular to spray apparatus 2 respectively To the corresponding connection of axial edge at combination, the connecting plate A3-1 and connecting plate A3-2 of combinations of pairs are along dyeing flow side To two opposite sides seal against each other connection respectively;Gap between the distribution grid A2-3-1 and distribution grid B2-3-2 of combinations of pairs with And the gap between the connecting plate A3-1 and connecting plate A3-2 of combinations of pairs constitutes the passage of pollutant 1.
Return channel 4 is made up of the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of a pair of half tubulars of combinations of pairs, in backflow The centre position of cylinder A4-1-1 sets operative fluid outlet pipe A4-2-1, and workflow is set in the centre position of backflow cylinder B4-1-2 Body outlet B4-2-2, the two ends end part of the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of two and half tubulars after combinations of pairs End socket is not installed;Space between the backflow cylinder A4-1-1 and backflow cylinder B4-1-2 of combinations of pairs constitutes the passage of pollutant 1.
According to the sealing characteristics of the seal B7-2 in the seal A7-1 in sealed letter body A6-1 and sealed letter body B6-2, Determine that working fluid sealing gland unit 12 and air sealing gland unit 13 are constituted by three air seals 5, pass through between three air seals 5 The sealed letter body A6-1 and sealed letter body A6-2 of pairing structure are formed by connecting;Air seal 5 is by a pair of half tubular gas of combinations of pairs The gentle sealed tube B5-1-2 of sealed tube A5-1-1 are constituted, in the center of the gentle sealed tube B5-1-2 of sealing gland cylinder A5-1-1 of combinations of pairs It is respectively provided with fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2;The sealing gland cylinder A 5- of two and half tubulars after combinations of pairs The two ends end of the gentle sealed tube B5-1-2 of 1-1 is respectively mounted end socket;The sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs Company corresponding with the axial edge at the sealing gland of half tubular of the air seal 2 cylinder gentle sealed tube B5-1-2 combinations of pairs of A5-1-1 respectively Connect, the sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs are mutually close respectively along two opposite sides of dyeing flow direction Envelope connection;Seal A 7-1 and seal A 7-2 are respectively mounted in sealed letter body A6-1 and sealed letter body A 6-2;Combinations of pairs Sealed letter body A6-1 in seal A7-1 and sealed letter body B6-2 in seal B7-2 between gap and combinations of pairs Sealing gland cylinder A4-1-1 gentle sealed tube B4-1-2 between space constitute the passage of pollutant 1.
The annexation of each unit of the present invention:Along the traffic direction of pollutant 1, air sealing gland unit 13, work is installed successively Make fluid sealing gland unit 12, return channel 4, cleaning unit 9, return channel 4, working fluid sealing gland unit 12, return channel 4, to spray-painting Color element 10, return channel 4, working fluid sealing gland unit 12, return channel 4, rinse unit 11, return channel 4, working fluid sealing gland list Unit 12, air sealing gland unit 13;Return channel 4 and cleaning unit 9 or to spray-painting color element 10 or rinse unit 11 to spray apparatus 2 it Between, by the connecting plate A3-1 and connecting plate B3-2 of combinations of pairs by the backflow cylinder A4-1-1 of half tubular of return channel 4 and backflow Axial edge at cylinder B4-1-2 combinations of pairs is matched somebody with somebody with half tubular to spray apparatus 2 to spray canister A2-1-1 and to spray canister B 2-1-2 To the corresponding connection of axial edge at combination;Between the air seal 5 and return channel 4 of working fluid sealing gland unit 12, by matching somebody with somebody To the sealed letter body A6-1 that combines and sealed letter body A6-2 by the gentle sealed tube B5- of the sealing gland of half tubular of air seal 5 cylinder A5-1-1 The backflow cylinder A4-1-1 and backflow cylinder B4-1-2 combinations of pairs of half tubular of axial edge and return channel 4 at 1-2 combinations of pairs The axial edge correspondence at place is connected;The air seal 5 of working fluid sealing gland unit 12 and the air seal 5 of air sealing gland unit 13 it Between, by the sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs by the sealing gland cylinder A5-1-1 of half tubular of air seal 5 and The corresponding connection of axial edge at sealing gland cylinder B5-1-2 combinations of pairs;Along first air sealing gland unit in technological process direction It is not connected with other air seals 5 in 13 first air seal 5 or second last air seal 5 of air sealing gland unit 13 Axial edge at the sealing gland cylinder gentle sealed tube B5-1-2 combinations of pairs of A5-1-1 of half tubular for connecing side is respectively mounted sealed letter Body A6-1 and sealed letter body A6-2;The sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs are along dyeing flow direction Two opposite sides seal against each other connection respectively;Seal is respectively mounted in the sealed letter body A6-1 and sealed letter body A6-2 of combinations of pairs A7-1 and seal B7-2, the sealing in seal A7-1 and sealed letter body B6-2 in the sealed letter body A 6-1 of combinations of pairs Gap between part B7-2 constitutes the passage of pollutant 1.
Each supercritical fluid inlet tube A2-2-1 and supercritical fluid inlet tube in cleaning unit 9 or rinse unit 11 Each fluid inlet tube A 5-2-1 and fluid inlet tube B5-2-2 in B2-2-2, and working fluid sealing gland unit 12 with it is super The pipeline connection of critical fluids generation subsystem 15, another lateral line of supercritical fluid generation subsystem 15 is deposited with working fluid Store up the pipeline connection of subsystem 14;To each supercritical fluid inlet tube A2-2-1 and supercritical fluid entrance in spray-painting color element 10 Pipe B2-2-2 is connected with the pipeline of dyestuff dissolving subsystem 16, and dyestuff dissolves another lateral line and supercritical fluid of subsystem 16 Generate the pipeline connection of subsystem 15;The fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 of air sealing gland unit 13 and sky Gas compression device 19 is connected;The operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe of the both sides return channel 4 of cleaning unit 9 B4-2-2 and working fluid are connected with the pipeline of impurity isolated subsystem 17, and spray-painting color element 10 and the both sides of cleaning unit 9 are returned Flow the operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe B4-2-2 and working fluid and dye separation subsystem 18 of device 4 Pipeline connection, another lateral line and working fluid and the dye separation subsystem of working fluid and impurity isolated subsystem 17 Pipeline of the 18 another lateral line with working fluid storage subsystem 14 is connected.
Pressure regulation is installed in the supercritical fluid inlet tube A2-2-1 to spray apparatus 2 and supercritical fluid inlet tube B2-2-2 Valve A8-1;Pressure-regulating valve B8- is installed in the operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe B4-2-2 of return channel 4 2;Pressure-regulating valve C8-3 is installed in the fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 of working fluid sealing gland unit 12; Pressure-regulating valve D8-4 is respectively mounted at the fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 of air sealing gland unit 13.
Example IV:Using supercritical fluid of the present invention to spray dyeing installation, the supercritical fluid of implementation is to spray dyer The implementation process of skill, such as Fig. 7, and shown in Fig. 4 or Fig. 5 or Fig. 6.
First, the operating fluid crosses supercritical fluid generation subsystem 15 in working fluid storage subsystem 14, generation Meet the supercritical fluid of spray-painting process conditions;
Second, pollutant 1 runs along technological process direction, sequentially passes through air sealing gland unit 13, working fluid sealing gland list Unit 12, return channel 4, cleaning unit 9, return channel 4, working fluid sealing gland unit 12, return channel 4, to spray-painting color element 10, backflow Device 4, working fluid sealing gland unit 12, return channel 4, rinse unit 11, return channel 4, working fluid sealing gland unit 12, air sealing gland Unit 13;
3rd, the pure supercritical fluid in supercritical fluid generation subsystem 15 is flowed separately through in cleaning unit 9 to spray apparatus 2 Supercritical fluid inlet tube A2-2-1 and supercritical fluid inlet tube B2-2-2, into spray canister A 2-1-1 and to spray canister B2- 1-2, and through distribution grid A2-3-1 and distribution grid B2-3-2 it is uniform after, correspondence spray to pollutant 1, it is extracted and is cleaned, To go the removal of impurity;At this moment the pressure differential that the both sides of pollutant 1 are born is zero, supercritical fluid work of the step-down as non-supercritical state Make fluid;The working fluid for carrying impurity enters return channel by the pollutant passage between connecting plate A3-1 and connecting plate B3-2 4, working fluid after step-down through operative fluid outlet pipe A4-2-1 and operative fluid outlet pipe B4-2-2 enter working fluid with Impurity isolated subsystem 17, it is separated after working fluid be stored in working fluid storage subsystem 14, be provided with Posterior circle and use; Cleaning pressure is controlled by pressure-regulating valve A 8-1 and pressure-regulating valve B 8-2;
4th, the pure supercritical fluid in supercritical fluid generation subsystem 15 flows through dyestuff dissolving subsystem 16, carries The dyestuff of saturation solubility pass through in spray-painting color element 10 to the supercritical fluid inlet tube A2-2-1 and supercritical fluid of spray apparatus 2 Inlet tube B2-2-2 enters to spray canister A2-1-1 and to spray canister B2-1-2, and through distribution grid A2-3-1 and distribution grid B2-3-2 to it After uniform, correspondence sprays to pollutant 1, pollutant 1 is carried out to spray-painting color, and the pressure differential that at this moment both sides of pollutant 1 are born is zero; The supercritical fluid for carrying excess dye enters return channel by the pollutant passage between connecting plate A3-1 and connecting plate B3-2 4, and the working fluid as non-supercritical state is depressured, the working fluid after step-down is through operative fluid outlet pipe A4-2-1 and work Make fluid outlet pipe B4-2-2 and flow back to working fluid and dye separation subsystem 18, it is separated after, working fluid is stored in work Fluid storage subsystem 14, is provided with Posterior circle and uses;Dyestuff after separation is available for multiplexing;Dyeing pressure is by pressure-regulating valve A8-1 Controlled with pressure-regulating valve B8-2;
5th, the pure supercritical fluid in supercritical fluid generation subsystem 15 is flowed through in rinse unit 11 to spray apparatus 2 Supercritical fluid inlet tube 2-2-1 and supercritical fluid inlet tube B2-2-2 enters to spray canister A 2-1-1 and to spray canister B2-1-2, And through distribution grid A2-3-1 and distribution grid B2-3-2 to its it is uniform after, spray to pollutant 1, it is rinsed, at this moment pollutant 1 The pressure differential that both sides are born is zero, supercritical fluid working fluid of the step-down as non-supercritical state.Carry the lower loose colour of rinsing The working fluid of dyestuff enters return channel 4 by the pollutant passage between connecting plate A 3-1 and connecting plate B3-2, after step-down Working fluid enters working fluid with dye separation through operative fluid outlet pipe A 4-2-1 and operative fluid outlet pipe B4-2-2 System 18, it is separated after working fluid be stored in working fluid storage subsystem 14, be provided with Posterior circle and use;Dye after separation Material is available for multiplexing;Rinsing pressure is controlled by pressure-regulating valve A 8-1 and pressure-regulating valve B8-2;
6th, while above-mentioned three, the 4th and the 5th step is carried out, the working fluid of different pressures is by working fluid sealing gland The fluid inlet tube A5-2-1 and fluid inlet tube B5-2-2 of unit 12 enter, and sealing gland step by step is carried out to equipment, prevent workflow Body circulates between different return channels 4;Working fluid sealing gland pressure at different levels are controlled by pressure-regulating valve C8-3;
7th, it is installed on the working fluid step pressure reducing that the working fluid sealing gland unit 12 at process route most two ends will leak out To certain pressure, finally leak to air sealing gland unit 13, air by air sealing gland unit 13 fluid inlet tube A5-2-1 Enter with fluid inlet tube B5-2-2, air sealing gland step by step is proceeded to the working fluid that leakage comes, until pressure is down to Normal pressure;Air sealing gland pressure at different levels are controlled by pressure-regulating valve D8-4.
Simple structure of the present invention, easy to operate, good level-dyeing property, pollutant are injury-free, can continuously produce, and greatly improve Dyeing quality and staining efficiency.

Claims (1)

1. supercritical fluid to spray dyeing installation, it is characterized by by cleaning unit, to spray-painting color element, rinse unit, return channel, Working fluid sealing gland unit, air sealing gland unit, connecting plate, sealed letter body, seal and pressure-regulating valve are constituted;
Cleaning unit is constituted by one or more structure identical to spray-painting color element or rinse unit to spray apparatus, by two Or more when being constituted to spray apparatus, to being connected with each other by connecting plate between spray apparatus, to the number of spray apparatus by specific dyeing bar Part determines;Spray apparatus is made up of a pair of half tubulars of combinations of pairs to spray canister and a pair of distribution grids, in the diameter subdivision to spray canister Distribution grid is installed at face, it is corresponding to being respectively provided with supercritical fluid inlet tube in spray canister in two just to distribution grid center; Two and half tubulars after combinations of pairs are respectively mounted end socket to the two ends end of spray canister;Connecting plate is the structure of combinations of pairs, point Connection not corresponding to the axial edge at spray canister combinations of pairs with half tubular to spray apparatus, the connecting plate of combinations of pairs is along dyer Two opposite sides of skill flow direction seal against each other connection respectively;Gap and combinations of pairs between the distribution grid of combinations of pairs Gap between connecting plate constitutes pollutant passage;
Return channel is made up of the backflow cylinder of a pair of half tubulars of combinations of pairs, at two centers of the backflow cylinder of corresponding half tubular Position is respectively provided with operative fluid outlet pipe;The two ends end of the two and half tubulars backflow cylinder after combinations of pairs is respectively mounted envelope Head;Space between two backflow cylinders of combinations of pairs constitutes pollutant passage;
Working fluid sealing gland unit or air sealing gland unit are constituted by one or more structure identical air seal, by two or When above air seal is constituted, connected by sealed letter body phase between air seal, the number of air seal is by specific sealed letter body The sealing characteristics of seal determine;Air seal is made up of the half tubular sealing glands cylinder of a pair of combinations of pairs, in two combinations of pairs The center of sealing gland cylinder is respectively provided with fluid inlet tube;The two ends end difference of the two and half tubular sealing glands cylinder after combinations of pairs End socket is installed;Sealed letter body is the structure of combinations of pairs, respectively with half tubular sealing gland of air seal cylinder combinations of pairs at axial direction Edge correspondence is connected, and the seal of combinations of pairs is installed in the sealed letter body of pairing;The sealed letter body of combinations of pairs is along dyer Two opposite sides of skill flow direction seal against each other connection respectively;Gap and combinations of pairs between the seal of combinations of pairs Space between sealing gland cylinder constitutes pollutant passage;
According to supercritical fluid to spray-painting color technological process, air sealing gland unit, working fluid sealing gland unit, backflow are installed successively Device, cleaning unit, return channel, working fluid sealing gland unit, return channel, to spray-painting color element, return channel, working fluid sealing gland list Unit, return channel, rinse unit, return channel, working fluid sealing gland unit, air sealing gland unit;Return channel and cleaning unit or right Spray-painting color element or rinse unit between spray apparatus, the backflow cylinder of the tubular of return channel half being matched somebody with somebody by the connecting plate of combinations of pairs To the axial edge at combination with to spray apparatus half tubular to the corresponding connection of axial edge at spray canister combinations of pairs;Workflow Between the air seal and return channel of body sealing gland unit, the sealing gland cylinder of the tubular of air seal half is matched somebody with somebody by the sealed letter body of combinations of pairs To the corresponding connection of axial edge at the backflow cylinder combinations of pairs of the axial edge at combination and the tubular of return channel half;Workflow Between the air seal of body sealing gland unit and the air seal of air sealing gland unit, by the sealed letter body of combinations of pairs by air seal half The corresponding connection of axial edge at the sealing gland cylinder combinations of pairs of tubular;Along first air sealing gland unit in technological process direction First air seal or second last air seal of air sealing gland unit in be not connected with other air seals side Half tubular sealing gland cylinder combinations of pairs at axial edge install combinations of pairs sealed letter body;The sealed letter body edge of combinations of pairs Two opposite sides of dyeing flow direction seal against each other connection respectively;The sealing of combinations of pairs is installed in the sealed letter body of pairing Part, the gap between the seal in the sealed letter body of combinations of pairs constitutes pollutant passage;
Each supercritical fluid inlet tube in cleaning unit or rinse unit, and each workflow in working fluid sealing gland unit Pipeline of the body inlet tube with supercritical fluid generation subsystem is connected, and supercritical fluid generates another lateral line of subsystem Pipeline with working fluid storage subsystem is connected;Subsystem is dissolved to each supercritical fluid inlet tube in spray-painting color element and dyestuff The pipeline of system is connected, and another lateral line of dyestuff dissolving subsystem is connected with the pipeline of supercritical fluid generation subsystem; The fluid inlet tube of air sealing gland unit is connected with compressed air unit;The operative fluid outlet of cleaning unit two ends return channel Pipe and working fluid are connected with the pipeline of impurity isolated subsystem, to spray-painting color element or the work of rinse unit two ends return channel Make fluid outlet pipe and working fluid to be connected with the pipeline of dye separation subsystem, working fluid and impurity isolated subsystem Another lateral line of another lateral line and working fluid and dye separation subsystem with the pipe of working fluid storage subsystem Road connects;
The supercritical fluid inlet tube to spray apparatus, the operative fluid outlet pipe of return channel, working fluid sealing gland unit fluid Pressure-regulating valve is respectively mounted at inlet tube, the fluid inlet tube of air sealing gland unit.
CN201510733238.XA 2015-10-30 2015-10-30 Supercritical fluid is to spray dyeing installation Expired - Fee Related CN105200686B (en)

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CN107034702A (en) * 2017-04-14 2017-08-11 三明通用科技孵化有限公司 A kind of supercritical carbon-dioxicle dyeing method of poly butylene succinate fabric
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CN111020938B (en) * 2019-12-06 2021-03-26 山东大学 Retractable supercritical fluid counter-jet dyeing device and counter-jet dyeing process
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