CN105176359A - Environment-friendly antistatic anti-corrosion paint and preparation method thereof - Google Patents
Environment-friendly antistatic anti-corrosion paint and preparation method thereof Download PDFInfo
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- CN105176359A CN105176359A CN201510717071.8A CN201510717071A CN105176359A CN 105176359 A CN105176359 A CN 105176359A CN 201510717071 A CN201510717071 A CN 201510717071A CN 105176359 A CN105176359 A CN 105176359A
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Abstract
The invention discloses environment-friendly antistatic anti-corrosion paint and a preparation method thereof. The environment-friendly antistatic anti-corrosion paint is prepared from, by weight, 40-65 parts of waterborne polyurethane emulsion, 30-45 parts of waterborne acrylic resin, 5-15 parts of copper sulphide, 5-15 parts of montmorillonite, 3-12 parts of conductive mica powder, 10-20 parts of potassium titanate whiskers, 10-20 parts of zinc oxide whiskers, 3-12 parts of calcium carbonate, 3-8 parts of zinc oleate, 3-8 parts of poly[oxy(methyl-1,2-ethanediyl)], 3-6 parts of lauryl sodium sulfate, 1-2 parts of flatting agents, 0.3-2 parts of defoaming agents, 10-25 parts of ethyl alcohol and 80-100 parts of deionized water. The surface resistance of the prepared paint is large, and good anti-static capacity is displayed. Besides, the conductive mica powder and the copper sulphide are low in cost of raw materials, easy to obtain and suitable for being widely used. The prepared paint has good water resistance and acid resistance, shows excellent corrosion resistance, and is long in actual service life and stable.
Description
Technical field
The invention belongs to protective system field, particularly relate to a kind of Environmental-friendantistatic antistatic protective system and preparation method thereof.
Background technology
In numerous safeguard procedures, application is one of the most simple and efficient effective safeguard procedures.Application is that paint is surperficial in device product, can play isolation action to reduce the corrosion of external environment to device product, the work-ing life of extension device, reduces use cost.Along with the requirement of people to living environment is more and more higher, more and more attaching importance to environmental protection problem.But current most protective system on the market contains volatile organic solvent, some volatile matters are poisonous even can be carcinogenic, drastically influence the health of people; In addition, along with popularizing of electronic product, the electromagnetic wave signal of surrounding environment is more and more stronger, and radiation interference is also more and more serious, thus it is also proposed higher requirement to the antistatic effect of device product.
Summary of the invention
The technical problem solved is: in order to improve the resisting radiation interference ability of electronic product and avoid volatile organic solvent not environmentally, provide a kind of Environmental-friendantistatic antistatic protective system and preparation method thereof.
Technical scheme: in order to solve the problem, the invention provides Environmental-friendantistatic antistatic protective system, comprise following raw material, according to weight parts: aqueous polyurethane emulsion 40 ~ 65 parts, water-borne acrylic resin 30 ~ 45 parts, cupric sulfide 5 ~ 15 parts, polynite 5 ~ 15 parts, conductive mica powder 3 ~ 12 parts, potassium titanate crystal whisker 10 ~ 20 parts, ZnOw 10 ~ 20 parts, 3 ~ 12 parts, calcium carbonate, zinc oleate 3 ~ 8 parts, lauric acid polyoxypropylene ester 3 ~ 8 parts, sodium lauryl sulphate 3 ~ 6 parts, flow agent 1 ~ 2 part, defoamer 0.3 ~ 2 part, ethanol 10 ~ 25 parts and 80 ~ 100 parts of deionized waters.
Further scheme, comprise following raw material, according to weight parts: aqueous polyurethane emulsion 50 parts, water-borne acrylic resin 40 parts, cupric sulfide 10 parts, polynite 10 parts, conductive mica powder 8 parts, potassium titanate crystal whisker 15 parts, ZnOw 15 parts, 8 parts, calcium carbonate, zinc oleate 6 parts, lauric acid polyoxypropylene ester 5 parts, sodium lauryl sulphate 5 parts, flow agent 1.5 parts, defoamer 1.2 parts, ethanol 15 parts and 90 parts of deionized waters.
Further scheme, also comprises pigment 0.2 ~ 3 part.
Further scheme, described pigment is iron oxide red, chrome yellow, chrome green, aluminium powder, cobalt blue or carbon black.
Further scheme, described flow agent is silanol acid resin class or acetate butyrate fiber-like.
Further scheme, described defoamer is silicone antifoam agent.
Further scheme, the preparation method of described potassium titanate crystal whisker is: take K by certain molfraction
2cO
3, TiO
2, boric acid, water glass and silicon oxide, each raw material is added in ball grinder, adds agate ball, with rotating speed 500r/min, ball milling 2 hours, is then placed in crucible by the batch mixing after ball milling, crucible is put into resistance furnace, the mode of temperature programming is adopted to be warming up to 900 DEG C, be incubated 2 hours, be cooled to room temperature, pulverize, sieve, obtain potassium titanate crystal whisker; The length of described potassium titanate crystal whisker is 20-50 μm; The length of described ZnOw is 30-50 μm.
The preparation method of above-mentioned Environmental-friendantistatic antistatic protective system, concrete preparation process comprises:
Step one: take raw material by certainweight number;
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then cupric sulfide, polynite, conductive mica powder, potassium titanate crystal whisker, ZnOw, calcium carbonate and ethanol is added, be uniformly mixed 1 ~ 4h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 3 ~ 5h, get product.
Further scheme, described step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent, pigment and defoamer are added in the slurry in step 2, mix, disperse in grinding machine for grinding, at left at room temperature one night after grinding 3 ~ 5h, get product.
The present invention has following beneficial effect: the surface resistivity of the coating prepared by the present invention is large, shows good antistatic effect, in addition, conductive mica powder and copper sulfide materials cost low and be easy to get, be applicable to widely using.In coating, also use the potassium titanate crystal whisker and ZnOw with superior electrical conductivity energy simultaneously, organic/inorganic electro-conductive material in coating is cooperatively interacted, and each raw material adopts specific proportioning, the coating obtained thus not only has excellent static electricity resistance, has good solidity to corrosion simultaneously.Coating prepared by the present invention has good water tolerance and acid resistance, shows outstanding antiseptic property, and actual service life is long and stable.
Embodiment
In order to understand the present invention further, below in conjunction with embodiment, invention preferred embodiment is described, but should be appreciated that these describe just for further illustrating the features and advantages of the present invention, instead of limiting to the claimed invention.
Embodiment 1
The preparation method of Environmental-friendantistatic antistatic protective system, concrete preparation process comprises:
Step one: take raw material by certainweight number: according to weight parts: aqueous polyurethane emulsion 40 parts, water-borne acrylic resin 30 parts, cupric sulfide 5 parts, polynite 5 parts, conductive mica powder 3 parts, potassium titanate crystal whisker 10 parts, ZnOw 10 parts, 3 parts, calcium carbonate, zinc oleate 3 parts, lauric acid polyoxypropylene ester 3 parts, sodium lauryl sulphate 3 parts, flow agent 1 part, defoamer 0.3 part, ethanol 10 parts and 80 parts of deionized waters.；
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then adds cupric sulfide, polynite, conductive mica powder, calcium carbonate and ethanol, is uniformly mixed 1h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 3h, get product.
Also can comprise pigment 0.2 part, described pigment can be iron oxide red; Described flow agent can be silanol acid resin class; Described defoamer can be silicone antifoam agent.
Embodiment 2
The preparation method of Environmental-friendantistatic antistatic protective system, concrete preparation process comprises:
Step one: take raw material by certainweight number: according to weight parts: aqueous polyurethane emulsion 65 parts, water-borne acrylic resin 45 parts, cupric sulfide 15 parts, polynite 15 parts, conductive mica powder 12 parts, potassium titanate crystal whisker 20 parts, ZnOw 20 parts, 12 parts, calcium carbonate, zinc oleate 8 parts, lauric acid polyoxypropylene ester 8 parts, sodium lauryl sulphate 6 parts, flow agent 2 parts, defoamer 2 parts, ethanol 25 parts and 100 parts of deionized waters.；
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then adds cupric sulfide, polynite, conductive mica powder, calcium carbonate and ethanol, is uniformly mixed 4h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 5h, get product.
Also can comprise pigment 3 parts, described pigment can be chrome yellow; Described flow agent can be acetate butyrate fiber-like; Described defoamer can be silicone antifoam agent.
Embodiment 3
The preparation method of Environmental-friendantistatic antistatic protective system, concrete preparation process comprises:
Step one: take raw material by certainweight number: according to weight parts: aqueous polyurethane emulsion 45 parts, water-borne acrylic resin 33 parts, cupric sulfide 8 parts, polynite 8 parts, conductive mica powder 5 parts, potassium titanate crystal whisker 12 parts, ZnOw 12 parts, 5 parts, calcium carbonate, zinc oleate 4 parts, lauric acid polyoxypropylene ester 4 parts, sodium lauryl sulphate 4 parts, flow agent 1.2 parts, defoamer 0.5 part, ethanol 12 parts and 82 parts of deionized waters;
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then adds cupric sulfide, polynite, conductive mica powder, calcium carbonate and ethanol, is uniformly mixed 2.5h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 4h, get product.
Also can comprise pigment 1.6 parts, described pigment can be chrome green; Described flow agent can be silanol acid resin class; Described defoamer can be silicone antifoam agent.
Embodiment 4
The preparation method of Environmental-friendantistatic antistatic protective system, concrete preparation process comprises:
Step one: take raw material by certainweight number: according to weight parts: aqueous polyurethane emulsion 60 parts, water-borne acrylic resin 42 parts, cupric sulfide 14 parts, polynite 13 parts, conductive mica powder 11 parts, potassium titanate crystal whisker 18 parts, ZnOw 18 parts, 10 parts, calcium carbonate, zinc oleate 7 parts, lauric acid polyoxypropylene ester 7 parts, sodium lauryl sulphate 5 parts, flow agent 1.8 parts, defoamer 1.8 parts, ethanol 22 parts and 96 parts of deionized waters.；
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then adds cupric sulfide, polynite, conductive mica powder, calcium carbonate and ethanol, is uniformly mixed 4h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 4h, get product.
Also can comprise pigment 1.4 parts, described pigment can be aluminium powder; Described flow agent can be silanol acid resin class; Described defoamer can be silicone antifoam agent.
Embodiment 5
The preparation method of Environmental-friendantistatic antistatic protective system, concrete preparation process comprises:
Step one: take raw material by certainweight number: according to weight parts: aqueous polyurethane emulsion 50 parts, water-borne acrylic resin 40 parts, cupric sulfide 10 parts, polynite 10 parts, conductive mica powder 8 parts, potassium titanate crystal whisker 15 parts, ZnOw 15 parts, 8 parts, calcium carbonate, zinc oleate 6 parts, lauric acid polyoxypropylene ester 5 parts, sodium lauryl sulphate 5 parts, flow agent 1.5 parts, defoamer 1.2 parts, ethanol 15 parts and 90 parts of deionized waters;
Also can comprise pigment 1 part, described pigment can be cobalt blue.Described flow agent can be acetate butyrate fiber-like; Described defoamer can be silicone antifoam agent.
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then adds cupric sulfide, polynite, conductive mica powder, calcium carbonate and ethanol, is uniformly mixed 4h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent, pigment and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 5h, get product.
Comparative example 1
The preparation of the coating in this comparative example comprises the steps:
Step one: take raw material by certainweight number: according to weight parts: aqueous polyurethane emulsion 46 parts, cupric sulfide 7 parts, polynite 6 parts, conductive mica powder 8 parts, 6 parts, calcium carbonate, lauric acid polyoxypropylene ester 2 parts, sodium lauryl sulphate 1 part, flow agent 1 part, defoamer 0.8 part, ethanol 20 parts and 60 parts of deionized waters;
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then adds cupric sulfide, polynite, conductive mica powder, calcium carbonate and ethanol, is uniformly mixed 4h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, lauric acid polyoxypropylene ester, flow agent and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 3h, gets product.
Comparative example 2
The preparation of the coating in this comparative example comprises the steps:
Step one: take raw material by certainweight number: according to weight parts: aqueous polyurethane emulsion 46 parts, water-borne acrylic resin 35 parts, polynite 6 parts, 6 parts, calcium carbonate, zinc oleate 3 parts, lauric acid polyoxypropylene ester 2 parts, sodium lauryl sulphate 1 part, flow agent 1 part, defoamer 0.8 part, ethanol 20 parts and 120 parts of deionized waters;
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then adds polynite, calcium carbonate and ethanol, is uniformly mixed 4h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 3h, get product.
Performance test
By above-mentioned prepared paint in polishing iron plate surface, carry out various performance test after to be dried, following table is the performance test results of coating prepared in embodiment 1 ~ 5 and comparative example 1, comparative example 2:
| Surface resistivity/Ω | Sticking power grade | Water tolerance | Acid resistance (15% hydrochloric acid, 100h) | |
| Embodiment 1 | 4.1×10 7 | ≤ 3 grades | Unchanged | Unchanged |
| Embodiment 2 | 4.3×10 7 | ≤ 3 grades | Unchanged | Unchanged |
| Embodiment 3 | 5.1×10 7 | ≤ 3 grades | Unchanged | Unchanged |
| Embodiment 4 | 7.2×10 7 | ≤ 3 grades | Unchanged | Unchanged |
| Embodiment 5 | 9.1×10 7 | ≤ 3 grades | Unchanged | Unchanged |
| Comparative example 1 | 1.3×10 5 | ≤ 3 grades | Bubble, wrinkling | Bubble, wrinkling |
| Comparative example 2 | 4.9×10 5 | ≤ 3 grades | Unchanged | Unchanged |
Embodiment 5 is most preferred embodiment of the present invention.
Compared to comparative example 2, the surface resistivity of the coating prepared by the present invention is larger, shows better antistatic effect, in addition, conductive mica powder and copper sulfide materials cost low and be easy to get, be applicable to widely using.Compared to comparative example 1, the coating prepared by the present invention has more water tolerance and acid resistance, and show more excellent antiseptic property, actual service life is longer and more stable.
Claims (9)
1. Environmental-friendantistatic antistatic protective system, it is characterized in that, comprise following raw material, according to weight parts: aqueous polyurethane emulsion 40 ~ 65 parts, water-borne acrylic resin 30 ~ 45 parts, cupric sulfide 5 ~ 15 parts, polynite 5 ~ 15 parts, conductive mica powder 3 ~ 12 parts, potassium titanate crystal whisker 10 ~ 20 parts, ZnOw 10 ~ 20 parts, 3 ~ 12 parts, calcium carbonate, zinc oleate 3 ~ 8 parts, lauric acid polyoxypropylene ester 3 ~ 8 parts, sodium lauryl sulphate 3 ~ 6 parts, flow agent 1 ~ 2 part, defoamer 0.3 ~ 2 part, ethanol 10 ~ 25 parts and 80 ~ 100 parts of deionized waters.
2. Environmental-friendantistatic antistatic protective system according to claim 1, it is characterized in that, comprise following raw material, according to weight parts: aqueous polyurethane emulsion 50 parts, water-borne acrylic resin 40 parts, cupric sulfide 10 parts, polynite 10 parts, conductive mica powder 8 parts, potassium titanate crystal whisker 15 parts, ZnOw 15 parts, 8 parts, calcium carbonate, zinc oleate 6 parts, lauric acid polyoxypropylene ester 5 parts, sodium lauryl sulphate 5 parts, flow agent 1.5 parts, defoamer 1.2 parts, ethanol 15 parts and 90 parts of deionized waters.
3. Environmental-friendantistatic antistatic protective system according to claim 1 and 2, is characterized in that, also comprises pigment 0.2 ~ 3 part.
4. Environmental-friendantistatic antistatic protective system according to claim 3, is characterized in that, described pigment is iron oxide red, chrome yellow, chrome green, aluminium powder or cobalt blue.
5. the Environmental-friendantistatic antistatic protective system according to claim 1 or 2 or 3, is characterized in that, described flow agent is silanol acid resin class or acetate butyrate fiber-like.
6. the Environmental-friendantistatic antistatic protective system according to claim 1 or 2 or 3, is characterized in that, described defoamer is silicone antifoam agent.
7. the Environmental-friendantistatic antistatic protective system according to claim 1 or 2 or 3, is characterized in that, the preparation method of described potassium titanate crystal whisker is: take K by certain molfraction
2cO
3, TiO
2, boric acid, water glass and silicon oxide, each raw material is added in ball grinder, adds agate ball, with rotating speed 500r/min, ball milling 2 hours, is then placed in crucible by the batch mixing after ball milling, crucible is put into resistance furnace, the mode of temperature programming is adopted to be warming up to 900 DEG C, be incubated 2 hours, be cooled to room temperature, pulverize, sieve, obtain potassium titanate crystal whisker; The length of described potassium titanate crystal whisker is 20-50 μm; The length of described ZnOw is 30-50 μm.
8. a preparation method for the Environmental-friendantistatic antistatic protective system as described in claim arbitrary in claim 1-7, is characterized in that, is prepared from by the raw material in claim 1, and concrete preparation process comprises:
Step one: take raw material by certainweight number;
Step 2: the sodium lauryl sulphate in raw material is placed in deionized water and dissolves, then cupric sulfide, polynite, conductive mica powder, potassium titanate crystal whisker, ZnOw, calcium carbonate and ethanol is added, be uniformly mixed 1 ~ 4h, then by slurry grinding distribution to 2500 order fineness;
Step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent and defoamer are added in the slurry in step 2, mix, in grinding machine for grinding dispersion, at left at room temperature one night after grinding 3 ~ 5h, get product.
9. the preparation method of an Environmental-friendantistatic antistatic protective system as described in claim 8, it is characterized in that, described step 3: aqueous polyurethane emulsion, water-borne acrylic resin, zinc oleate, lauric acid polyoxypropylene ester, flow agent, pigment and defoamer are added in the slurry in step 2, mix, disperse in grinding machine for grinding, at left at room temperature one night after grinding 3 ~ 5h, get product.
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| CN201510717071.8A CN105176359A (en) | 2015-10-29 | 2015-10-29 | Environment-friendly antistatic anti-corrosion paint and preparation method thereof |
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| CN201510717071.8A CN105176359A (en) | 2015-10-29 | 2015-10-29 | Environment-friendly antistatic anti-corrosion paint and preparation method thereof |
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| CN105936802A (en) * | 2016-06-12 | 2016-09-14 | 雄子（上海）新材料科技有限公司 | Antistatic polyurethane paint and preparation method thereof |
| CN110330830A (en) * | 2019-06-05 | 2019-10-15 | 安徽蓝德正华电子有限公司 | A kind of power distribution cabinet surface layer antistatic coating and preparation method thereof |
| CN113337194A (en) * | 2021-05-31 | 2021-09-03 | 江南大学 | Preparation method of coated conductive whisker/composite antistatic coating |
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