CN105175200B - Pyrotechnic composition for calligraphy and painting creation, and preparation method thereof - Google Patents
Pyrotechnic composition for calligraphy and painting creation, and preparation method thereof Download PDFInfo
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- CN105175200B CN105175200B CN201510425267.XA CN201510425267A CN105175200B CN 105175200 B CN105175200 B CN 105175200B CN 201510425267 A CN201510425267 A CN 201510425267A CN 105175200 B CN105175200 B CN 105175200B
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Abstract
The invention relates to a pyrotechnic composition for calligraphy and painting creation, and a preparation method thereof, and belongs to the field of calligraphy and painting creation pyrotechnic compositions. The pyrotechnic composition for calligraphy and painting creation comprises 30-50 parts of ammonium perchlorate, 15-40 parts of metaldehyde, 15-35 parts of copper chloride and 5-10 parts of shellac. The preparation method comprises the following steps: respectively weighing certain amounts of ammonium perchlorate, metaldehyde, copper chloride and shellac according to proportions of the above formula; respectively fully grinding the weighed ammonium perchlorate, metaldehyde and copper chloride in a mortar, respectively sieving by using a 100-200 mesh sieve 3 times, and carrying out full dry mixing on all the obtained sieved reagents until uniformity; and putting weighed shellac in a beaker, adding a proper amount of 95% ethanol to dissolve shellac, pouring the above obtained dry mixed uniform medicine mixture into the beaker after shellac is completely dissolved, fully stirring, and air-drying the obtained medicine in a shady place until no liquid exists. The pyrotechnic composition has the advantages of fast combustion, low combustion temperature, few combustion residues, fire delivery cross the air, short creation time, low creation cost and high safety coefficient.
Description
Technical field
The present invention relates to a kind of pyrotechnic composition and preparation method thereof for calligraphy and painting creation in pyrotechnic composition preparation field.
Background technology
Pyrotechnics calligraphy and painting is the calligraphy and painting that a kind of utilization pyrotechnic composition burns to create, and is a kind of new Creation form in fine arts field,
This Creation form has strict demand to performance parameters such as the burning velocities and ignition temperature of pyrotechnic composition.
The Chinese invention patent of Patent No. CN1036928A discloses the making that a kind of pyrotechnic composition of Mr. Cai Guoqiang is drawn
Technique, it is+10% red phosphorus of+15% sulfur of 75% potassium nitrate to describe its pyrotechnic composition composition for being used for pyrotechnics drawing, by firing
Painting creation is carried out on the carriers such as painting canvas, paper, plank directly with control device.It is characterized in that：Pyrotechnic composition used be by
Certain proportion is formed through mechanical mixture, and pyrotechnic composition is directly sprinkling upon the carriers such as painting canvas, paper, plank carries out burning creation, in order to
Protection carrier, needs to carry out pretreatment to these carriers, is allowed to not reason high-temp combustion and is damaged.But Mr. Cai Guoqiang is made
Formula is red phosphorus base pyrotechnic composition, and substantial amounts of corrosive fume is formed during burning, runs into
Fire is passed, and a large amount of combustion residues are produced on carrier, also needed to carry out artificial hypothermia in combustion process, expend a large amount of manpowers, thing
Power and financial resources, during field experimentation, safety coefficient is more low.In addition Anhui University of Science and Technology is matched somebody with somebody using potassium hyperchlorate, sulfur and activated carbon
The pyrotechnic composition of system carries out calligraphy creation research, and the formula ignition temperature is higher, easily burns creation carrier, also generates during burning
Sulfur dioxide toxic gas and a large amount of residues, this is unfavorable to pyrotechnics creation.Therefore, develop a kind of for calligraphy and painting creation
Pyrotechnic composition and preparation method thereof new problem always anxious to be resolved.
The content of the invention
It is an object of the invention to provide a kind of pyrotechnic composition for calligraphy and painting creation and preparation method thereof, the pyrotechnics of the present invention
Medicine burning is rapid, and ignition temperature is low, and combustion residue is few, can pass fire every empty, and creative time is short, creates low cost, and safety coefficient is high,
Disclosure satisfy that during use to for creating the requirement of the performance parameters such as the burning velocity and ignition temperature of the pyrotechnic composition of calligraphy and painting.
The object of the present invention is achieved like this：A kind of pyrotechnic composition for calligraphy and painting creation, described are created for calligraphy and painting
Pyrotechnic composition consist of：Ammonium perchlorate 30-65 parts, methaldehyde 15-40 parts, copper chloride 15-35 parts, Lac 5-10 parts；
Described preparation method comprises the steps：
（1）Quantitative ammonium perchlorate, the methaldehyde, copper chloride and Lac are weighed respectively according to formula proportion；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition；
Described pyrotechnic composition ignition temperature is 960K-1770K, and apparent density is 0.644g/ml-0.899g/ml, and burn rate is
10.101mm/s-139.870mm/s, residue content is 5.836%-20.046%；
When described pyrotechnic composition laying depth is 3mm, 70mm is can reach every the empty fire distance that passes；When medicament thickness is 3.3mm,
75mm be can reach every the empty fire distance that passes；With the increase of calligraphy and painting pyrotechnic composition laying depth, also can increase therewith every the empty fire distance that passes；
And calligraphy and painting pyrotechnic composition is radially propagated to surrounding every the empty fire that passes, no specific directivity；
Described calligraphy and painting pyrotechnic composition can realize the multicolour coloring of writing, can form faint yellow, Lycoperdon polymorphum Vitt, brown, black
The writing of color；
It is described pyrotechnic composition is created for calligraphy and painting operation principle be can realize at pyrotechnics calligraphy and painting creation mark of break every sky
Fire is passed, and is made production process without the need for special handling being carried out to calligraphy and painting carrier, only just can be fully completed by once being ignited, realize word
The multicolour pyrotechnics coloring of paintings product, and combustion process has good visual effect.
The present invention is characterized by a kind of pyrotechnic composition for calligraphy and painting creation and preparation method thereof.
A kind of pyrotechnic composition for calligraphy and painting creation and preparation method thereof compared with prior art, has burning with pyrotechnic composition
Rapidly, ignition temperature is low, and combustion residue is few, can pass fire every empty, and creative time is short, creation low cost, the high advantage of safety coefficient,
Calligraphy and painting will be widely used in create in pyrotechnic composition field.
Description of the drawings
Below in conjunction with the accompanying drawings and embodiment the present invention is described in detail.
Fig. 1 is the flaxen of the recipe ingredient creation of embodiment one《Head bowed, like a willing ox I serve the children》Works.
Fig. 2 is the Lycoperdon polymorphum Vitt of the recipe ingredient creation of embodiment nine《Show high ideals by simple living》Works.
Fig. 3 is the brown of the recipe ingredient creation of embodiment ten《Dragon Lord》Works.
Fig. 4 is the black of the recipe ingredient creation of embodiment 12《Good fortune》Works.
Fig. 5 is that the medicament of embodiment 14 investigates schematic diagram every the empty fire distance that passes.
Fig. 6 is that the medicament of embodiment 15 passes fiery directivity investigation schematic diagram every empty.
Specific embodiment
Referring to the drawings, following examples will be helpful to the understanding to the present invention, but these embodiments are only for the present invention
It is illustrated, the present invention is not limited to these contents.
Embodiment one
（1）42 parts of ammonium perchlorate, 28 parts of the methaldehyde, 25 parts of copper chloride and Lac are quantitatively weighed respectively according to formulation ratio
5 parts；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.899g/ml, and burn rate is 16.411mm/s, and combustion residue content is 11.750%.Jing
REAL computed in software obtains theoretical temperature combustion for 1100K, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma,
It is layed on sketch paper and lights, burning is rapid, flame has blue, red, yellow trichroism, flame is in the shape of the letter V to spray to propagate and advances, in sketch
Faint yellow writing is formed on paper, and it is 2mm fire distance to be passed every sky.Using the flaxen of calligraphy and painting pyrotechnic composition creation《Bow one's head sweet
For willing ox》Works, are shown in accompanying drawing 1.
Embodiment two
（1）40 parts of quantitative ammonium perchlorate, 15 parts of the methaldehyde, 35 parts of copper chloride, Lac are weighed respectively according to formulation ratio
10 parts；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.779g/ml, and burn rate is 13.922mm/s, and combustion residue content is 14.113%.Jing
REAL computed in software obtains theoretical temperature combustion for 1511K, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma,
It is layed on sketch paper and lights, burning is rapid, and flame has indigo plant, white dichromatism, and burning direction is seen, flame is in the shape of the letter V before injection propagation
Entering, blackness handwriting being formed on sketch paper, it is 5mm fire distance to be passed every sky.
Embodiment three
（1）40 parts of quantitative ammonium perchlorate, 38 parts of the methaldehyde are weighed respectively according to formulation ratio：Copper chloride 15g：Lac
7g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.681g/ml, and burn rate is 84.286mm/s, and combustion residue content is 9.932%.Jing
It is 980K that REAL computed in software obtains theoretical temperature combustion, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma, is spread
Light on sketch paper, burning is swift and violent quickly, produce intense white light, it is impossible to normally see flame clearly, recognize at the end of burning is fast
There is blue flame, flower blackness handwriting being formed on sketch paper, it is 20mm fire distance to be passed every sky.
Example IV
（1）Quantitative ammonium perchlorate 32g is weighed respectively according to formulation ratio：Methaldehyde 28g：Copper chloride 35g：Lac 5g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.753g/ml, and burn rate is 56.098mm/s, and combustion residue content is 19.635%.Jing
It is 964K that REAL computed in software obtains theoretical temperature combustion, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma, is spread
Light on sketch paper, burning is rapid, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V before injection propagation
Entering, light black writing being formed on sketch paper, it is 1mm fire distance to be passed every sky.
Embodiment five
（1）Quantitative ammonium perchlorate 45g is weighed respectively according to formulation ratio：Methaldehyde 25g：Copper chloride 20g：Lac 10g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.644g/ml, and burn rate is 76.671mm/s, and combustion residue content is 9.918%.Jing
REAL computed in software obtains theoretical temperature combustion for 1256K, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma,
It is layed on sketch paper and lights, burning quickly, produces intense white light, it is impossible to normally sees flame clearly, at the end of burning is fast, recognize have
Blue flame, forms light gray writing on sketch paper, and it is 20mm to pass fire distance every sky.
Embodiment six
（1）Quantitative ammonium perchlorate 30g is weighed respectively according to proportioning：Methaldehyde 40g：Copper chloride 20g：Lac 10g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.756g/ml, and burn rate is 38.334mm/s, and combustion residue content is 20.046%.Jing
It is 961K that REAL computed in software obtains theoretical temperature combustion, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma, is spread
Light on sketch paper, quickly, flame has red, yellow, blue trichroism, and burning direction is seen, flame is in the shape of the letter V before injection propagation for burning
Entering, light black writing being formed on sketch paper, it is 1mm fire distance to be passed every sky.
Embodiment seven
（1）Quantitative ammonium perchlorate 50g is weighed respectively according to proportioning：Methaldehyde 25g：Copper chloride 15g：Lac 10g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.715g/ml, and burn rate is 102.570mm/s, and combustion residue content is 6.589%.Jing
It is 1268K that REAL computed in software obtains theoretical temperature combustion, and this group of pyrotechnic composition outward appearance of the group is gray powdery, and slightly fruit is fragrant
Taste, is layed on sketch paper and lights, and burning is swift and violent quickly, produces intense white light, it is impossible to normally see flame clearly, at the end of burning is fast
Identification has blue flame, and flower brown writing is formed on sketch paper, and it is 70mm to pass fire distance every sky.
The pyrotechnic composition of 0.3g is layed in into one group of concentric circular everywhere, medicament laying depth is 3mm, tests and only draws
Light at a, can be ignited at b and every sky at c, be not ignited at d, this can reach 70mm, medicament burning after the empty fire distance that passes
Effect is shown in accompanying drawing 5.The pyrotechnic composition of 1.5g is layed at the six of same circumference, medicament laying depth is 3.3mm, is tested
Go out, remaining is ignited every sky at five, this also illustrates that medicament passes fire every empty after the empty fire distance that passes up to 75mm
Radially propagate to surrounding, no specific directivity, medicament combustion efficiency are shown in accompanying drawing 6.
Embodiment eight
（1）Quantitative ammonium perchlorate 50g is weighed respectively according to formulation ratio：Methaldehyde 18g：Copper chloride 25g：Lac 7g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.842g/ml, and burn rate is 10.101mm/s, and combustion residue content is 5.836%.Jing
It is 1770K that REAL computed in software obtains theoretical temperature combustion, and pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma, is laid
Light on sketch paper, burning is rapid, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V before injection propagation
Entering, light black writing being formed on sketch paper, it is 1mm fire distance to be passed every sky.
Embodiment nine
（1）Quantitative ammonium perchlorate 40g is weighed respectively according to formulation ratio：Methaldehyde 30g：Copper chloride 25g：Lac 5g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.878g/ml, and burn rate is 75.025mm/s, and combustion residue content is 12.685%.Jing
It is 1030K that REAL computed in software obtains theoretical temperature combustion, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, with Fructus Litchi fragrance, paving
Light on sketch paper, burning is rapid, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V before injection propagation
Entering, Lycoperdon polymorphum Vitt writing being formed on sketch paper, it is 1mm fire distance to be passed every sky.The Lycoperdon polymorphum Vitt created using the calligraphy and painting pyrotechnic composition《Rather
It is quiet to cause far》Works, are shown in accompanying drawing 2.
Embodiment ten
（1）Quantitative ammonium perchlorate 40g is weighed respectively according to formulation ratio：Methaldehyde 40g：Copper chloride 15g：Lac 5g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.685g/ml, and burn rate is 139.870mm/s, and combustion residue content is 6.589%.Jing
It is 960K that REAL computed in software obtains theoretical temperature combustion, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma, is spread
Light on sketch paper, burning is rapid, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V before injection propagation
Entering, brown writing being formed on sketch paper, colouring is preferable, it is 10mm fire distance to be passed every sky.Created using the calligraphy and painting pyrotechnic composition
Brown《Dragon Lord》Works, are shown in accompanying drawing 3.
Embodiment 11
（1）Quantitative ammonium perchlorate 35g is weighed respectively according to formulation ratio：Methaldehyde 35g：Copper chloride 25g：Lac 5g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.696g/ml, and burn rate is 47.801mm/s, and combustion residue content is 14.644%.Jing
It is 968K that REAL computed in software obtains theoretical temperature combustion, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma, is spread
Light on sketch paper, burning is rapid, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V before injection propagation
Entering, blackness handwriting being formed on sketch paper, it is 2mm fire distance to be passed every sky.
Embodiment 12
（1）Quantitative ammonium perchlorate 50g is weighed respectively according to formulation ratio：Methaldehyde 20g：Copper chloride 25g：Lac 5g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.739g/ml, and burn rate is 81.905mm/s, and combustion residue content is 6.697%.Jing
REAL computed in software obtains theoretical temperature combustion for 1601K, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma,
It is layed on sketch paper and lights, burning is rapid, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V to spray and propagates
Advancing, blackness handwriting being formed on sketch paper, it is 1mm fire distance to be passed every sky.The black created using the calligraphy and painting pyrotechnic composition
《Good fortune》Works, are shown in accompanying drawing 4.
Embodiment 13
（1）Quantitative ammonium perchlorate 50g is weighed respectively according to formulation ratio：Methaldehyde 20g：Copper chloride 20g：Lac 10g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.681g/ml, and burn rate is 100.134mm/s, and combustion residue content is 6.078%.Jing
It is 974K that REAL computed in software obtains theoretical temperature combustion, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma, is spread
Light on sketch paper, burning is rapid, and flame has red, Huang Erse, and burning direction is seen, flame is in the shape of the letter V to spray to propagate and advances,
Blackness handwriting is formed on sketch paper, and it is 30mm fire distance to be passed every sky.
Embodiment 14
（1）Quantitative ammonium perchlorate 60g is weighed respectively according to formulation ratio：Methaldehyde 20g：Copper chloride 15g：Lac 5g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.707g/ml, and burn rate is 33.334mm/s, and combustion residue content is 1.257%.Jing
REAL computed in software obtains theoretical temperature combustion for 2009K, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma,
It is layed on sketch paper and lights, burning is swift and violent quickly, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V injection
Propagating and advancing, blackness handwriting is formed on sketch paper, it is 2mm fire distance to be passed every sky.
Embodiment 15
（1）Quantitative ammonium perchlorate 65g is weighed respectively according to formulation ratio：Methaldehyde 15g：Copper chloride 15g：Lac 5g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.734g/ml, and burn rate is 47.619mm/s, and combustion residue content is 0.935%.Jing
REAL computed in software obtains theoretical temperature combustion for 2487K, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma,
It is layed on sketch paper and lights, burning is rapid, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V to spray and propagates
Advancing, blackness handwriting being formed on sketch paper, it is 1mm fire distance to be passed every sky.
Embodiment 16
（1）Quantitative ammonium perchlorate 60g is weighed respectively according to formulation ratio：Methaldehyde 20g：Copper chloride 15g：Lac 5g；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh is taken
Sieved in several sieves respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, will step
Suddenly（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, then
Dry in being put into 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, be obtained
Calligraphy and painting pyrotechnic composition.
The pyrotechnic composition apparent density is 0.715g/ml, and burn rate is 105.263mm/s, and combustion residue content is 0.586%.Jing
REAL computed in software obtains theoretical temperature combustion for 2625K, and this group of pyrotechnic composition outward appearance is yellowish-brown powder, slightly fruit aroma,
It is layed on sketch paper and lights, burning is rapid, flame has blue, red, yellow trichroism, and burning direction is seen, flame is in the shape of the letter V to spray and propagates
Advancing, blackness handwriting being formed on sketch paper, it is 2mm fire distance to be passed every sky.
The present invention is described in further detail with reference to embodiment：
Described calligraphy and painting pyrotechnic composition can realize passing every empty at pyrotechnics calligraphy and painting creation mark of break with the ability that fire is passed every sky
Fire, makes production process without the need for carrying out special handling to calligraphy and painting carrier, only just can be fully completed by once being ignited.Every the empty fire that passes it is in
It is radial to propagate to surrounding, no specific directivity, and with the increase of calligraphy and painting pyrotechnic composition laying depth, its every it is empty pass fire away from
From also increasing therewith.
Described calligraphy and painting pyrotechnic composition has burning rapid, and ignition temperature is relatively low, and combustion residue is less, can pass fire, wound every empty
It is shorter to make the time, and creation cost is relatively low, and pyrotechnic composition combustion process has good visual effect, the pyrotechnic composition calligraphy and painting works of creation
Being capable of mounting persistence.
Described pyrotechnic composition also can increase every the empty fire distance that passes therewith with the increase of calligraphy and painting pyrotechnic composition laying depth；And
Calligraphy and painting pyrotechnic composition is radially propagated to surrounding every the empty fire that passes, no specific directivity.
Described calligraphy and painting pyrotechnic composition can realize the multicolour coloring of writing, can form faint yellow (accompanying drawing 1), Lycoperdon polymorphum Vitt (attached
Fig. 2), the writing of the color such as brown (accompanying drawing 3), black (accompanying drawing 4), realizes the multicolour pyrotechnics coloring of works, creates calligraphy and painting
With very strong ornamental, embodiment and original work photo accompanying drawing are seen respectively.
Claims (6)
1. it is a kind of for calligraphy and painting creation pyrotechnic composition, it is characterised in that：The described pyrotechnic composition for calligraphy and painting creation is consisted of：It is high
Ammonium chlorate 30-65 parts, methaldehyde 15-40 parts, copper chloride 15-35 parts, Lac 5-10 parts.
2. it is according to claim 1 it is a kind of for calligraphy and painting creation pyrotechnic composition preparation method, it is characterised in that it is described
Preparation method comprises the steps：
（1）Quantitative ammonium perchlorate, the methaldehyde, copper chloride and Lac are weighed respectively according to formula proportion；
（2）Load weighted ammonium perchlorate, the methaldehyde, copper chloride are fully ground in mortar respectively, 100-200 mesh numbers are taken
Sieved in sieve respectively 3 times, each reagent after sieving is fully dry-mixed uniform；
（3）Load weighted Lac is put into into beaker, appropriate 95% ethanol dissolving is added, after Lac dissolving completely, by step
（2）Described in dry-mixed uniform medicament pour in beaker, be sufficiently stirred for, dry in the cool medicament to no liquid exist；
（4）By step（3）Described in the medicament that dries scrape beaker, being poured on the pelletize sieve of 18 mesh carries out pelletize, is then placed in
Dry in 60-70 DEG C of baking oven；
（5）By step（4）Described in dry after medicament pour into and sieve again 3 times in the sieve of 100-200 mesh numbers, calligraphy and painting is obtained
Pyrotechnic composition.
3. according to claim 1 it is a kind of for calligraphy and painting creation pyrotechnic composition, it is characterised in that：Described pyrotechnic composition burning temperature
Spend for 960K-1770K, apparent density is 0.644g/ml-0.899g/ml, burn rate is 10.101mm/s-139.870mm/s, residue
Content is 5.836%-20.046%.
4. according to claim 1 it is a kind of for calligraphy and painting creation pyrotechnic composition, it is characterised in that：Described pyrotechnic composition laying is thick
Spend for 3mm when, pass fiery distance and can reach 70mm every empty；When medicament thickness is 3.3mm, 75mm is can reach every the empty fire distance that passes；With
The increase of calligraphy and painting pyrotechnic composition laying depth, also can be increased therewith every the empty fire distance that passes；And calligraphy and painting pyrotechnic composition passes fiery in spoke every empty
Penetrate shape to propagate to surrounding, no specific directivity.
5. according to claim 1 it is a kind of for calligraphy and painting creation pyrotechnic composition, it is characterised in that：Described calligraphy and painting pyrotechnic composition energy
The multicolour coloring of writing is enough realized, faint yellow, Lycoperdon polymorphum Vitt, brown, the writing of black color is formed.
6. according to claim 1 it is a kind of for calligraphy and painting creation pyrotechnic composition, it is characterised in that：Described creates for calligraphy and painting
The operation principle of pyrotechnic composition is to realize that pyrotechnics calligraphy and painting creates fiery every empty biography at mark of break, makes production process without the need for calligraphy and painting
Carrier carries out special handling, only just can be fully completed by once being ignited, and realizes the multicolour pyrotechnics coloring of calligraphy and painting works, and
Combustion process has good visual effect.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510425267.XA CN105175200B (en) | 2015-07-20 | 2015-07-20 | Pyrotechnic composition for calligraphy and painting creation, and preparation method thereof |
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| CN201510425267.XA CN105175200B (en) | 2015-07-20 | 2015-07-20 | Pyrotechnic composition for calligraphy and painting creation, and preparation method thereof |
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| CN112811968A (en) * | 2021-02-08 | 2021-05-18 | 大连交通大学 | Red pyrotechnic composition for calligraphy and painting creation and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4169709A (en) * | 1975-07-01 | 1979-10-02 | Colgate-Palmolive Company | Artificial fireplace logs |
| CN1036928A (en) * | 1988-04-18 | 1989-11-08 | 蔡国强 | Manufactural technology of explosive paint |
| CN104626867A (en) * | 2015-01-30 | 2015-05-20 | 王嘉华 | Manufacturing process for firework carbon residue calligraphy and painting |
-
2015
- 2015-07-20 CN CN201510425267.XA patent/CN105175200B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4169709A (en) * | 1975-07-01 | 1979-10-02 | Colgate-Palmolive Company | Artificial fireplace logs |
| CN1036928A (en) * | 1988-04-18 | 1989-11-08 | 蔡国强 | Manufactural technology of explosive paint |
| CN104626867A (en) * | 2015-01-30 | 2015-05-20 | 王嘉华 | Manufacturing process for firework carbon residue calligraphy and painting |
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| CN105175200A (en) | 2015-12-23 |
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