CN105155177A - Supercritical carbon dioxide ox horn button dyeing kettle and dyeing technology - Google Patents
Supercritical carbon dioxide ox horn button dyeing kettle and dyeing technology Download PDFInfo
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- CN105155177A CN105155177A CN201510412594.1A CN201510412594A CN105155177A CN 105155177 A CN105155177 A CN 105155177A CN 201510412594 A CN201510412594 A CN 201510412594A CN 105155177 A CN105155177 A CN 105155177A
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- dyeing
- carbon dioxide
- kettle
- supercritical carbon
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B19/00—Treatment of textile materials by liquids, gases or vapours, not provided for in groups D06B1/00 - D06B17/00
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
- D06B23/14—Containers, e.g. vats
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Treatment Of Fiber Materials (AREA)
Abstract
The invention discloses a supercritical carbon dioxide ox horn button dyeing kettle and a dyeing technology. The dyeing kettle comprises a kettle body. A carbon oxide fluid and dye inlet and a carbon oxide fluid and dye outlet are formed in the bottom of the kettle body; during the dying, the carbon oxide fluid and dye flow into the kettle body from the bottom to impact the button and drive the button to dye in a non-static way, so the button can move due to air flow impact; and dying flaws of overlapped parts between buttons can be avoided. The cylindrical bottom of the dyeing kettle is in an inverted trapezoidal structure to enable the buttons to have contact with carbon oxide fluid with dying paint and finish dying. Buttons with rich colors can be acquired by the use of the dying technology; dyed products require no cleaning and drying operations; a water-free dying process is achieved; production cost is reduced; and dying quality is improved and environment pollution is reduced.
Description
Technical field
The invention belongs to technical field of textile printing, relate to supercritical CO 2 dyeing still, particularly supercritical carbon dioxide ox horn button dyeing caldron and dyeing thereof.
Background technology
China is the country of a shortage of water resources, and water resource environment is also in continuous deterioration, and add the waste with water, Situation of water resources allows of no optimist especially.The traditional water bath dyeing of button, main is medium with water, in dyeing course, the chemical substances such as a large amount of dyestuffs, auxiliary agent and surfactant cause severe contamination to environment, resistant to elevated temperatures colouring agent kind is few, colour system is incomplete, add Masterbatch causes button production process unstable, governs the sustainable development of garment accessories industry.The requirement of 2l century commute controlling, high efficiency, nonstaining property and reusable edible is more and more outstanding.The supercritical carbon dioxide waterless staining technique developed in last century end is considered to a kind of " green, sustainable development " technology because of outstanding features such as it is pollution-free, short route, high efficiency, and enjoys favor.
At present, supercritical CO 2 dyeing technology has obtained interim progress as a kind of novel green dyeing-finishing technology, comparatively ripe to the associating exploratory development of its process conditions, dyeing mechanism and dyeing installation.And the supercritical fluid dyeing research of garment accessories seldom, supercritical CO 2 dyeing technology is not also adopted to carry out the dyeing of the garment accessories such as button at present.On the other hand, because button compact structure, quality are comparatively large, the mode according to the static state of routine is deposited in and dyes together, can cause forcing together of button and button consolidation, the overlapping of button and button there will be uneven dyeing and contaminates not saturating phenomenon, causes button dyeing speck.
Summary of the invention
An object of the present invention is to provide supercritical carbon dioxide ox horn button dyeing caldron, button is driven to dye in non-static mode by CO 2 fluid, thus the overlapping solving button and button when adopting the supercritical CO 2 dyeing still of prior art there will be uneven dyeing and contaminates not saturating, causes the problem of button dyeing speck.
Above-mentioned purpose of the present invention adopts following technical scheme to realize.
A kind of supercritical carbon dioxide ox horn button dyeing caldron, comprise kettle, the upper end of described kettle is provided with sealing kettle cover, and the bottom of described kettle is provided with CO 2 fluid and dyestuff entrance, and the top of described kettle is provided with CO 2 fluid and dyestuff outlet.
As preferred technical scheme, described dyeing caldron also comprises cylindrical shell, and described cylindrical shell is placed in kettle, and the bottom of described cylindrical shell is provided with opening, described opening is corresponding with described CO 2 fluid and dyestuff entrance, and described opening part is provided with the curved surface netware protruded to inner barrel.During dyeing, described ox horn button is placed in cylindrical shell, and the supercritical carbon dioxide fluid carrying dyestuff flows into cylindrical shell by bottom opening, impacts button and drives button to dye in non-static mode.Flow velocity also by controlling supercritical carbon dioxide fluid realizes the change of air-flow, thus button is moved under the gear shift shock of air-flow, avoids the dyeing speck of button and button overlapping.The mesh aperture preferably 1 ~ 2mm of curved surface netware, the preferred stainless steel of material.Curved surface netware dispersibles CO 2 fluid and dyestuff, thus dyeing evenly.
As preferred technical scheme, the bottom of described cylindrical shell is inverted trapezoidal structure, adopts this structure that button can be avoided to be deposited in cylinder body bottom and occurs dead angle, to prevent uneven dyeing.The bottom of wherein said cylindrical shell refers to the periphery of curved surface netware.
As preferred technical scheme, the hypotenuse of described inverted trapezoidal structure and the angle of horizontal plane are 20 ~ 50 degree, and CO 2 fluid impacts button to adopt this angle effectively to ensure, thus avoid button overlap and pile up, and effectively prevent uneven dyeing.
As preferred technical scheme, the bottom opening place of described cylindrical shell is provided with chassis with holes, is positioned at the below of described curved surface netware.The aperture on described chassis with holes is preferably 3mm, the preferred stainless steel of material.Chassis with holes can, to CO 2 fluid and dyestuff filtration, avoid impurity etc. to enter cylindrical shell.
As preferred technical scheme, described chassis with holes and curved surface netware are all dynamically connected with the opening movable of cylinder body bottom, adopt this structure to be convenient to dismounting and washing, improve staining efficiency.
As preferred technical scheme, the upper end of described cylindrical shell is provided with lid with holes.Adopting this structure, be convenient to dress and get button, namely when not opening lid, directly can load button by the hole of lid with holes during practical application, after dyeing terminates, also when not opening lid, directly can take out button by the hole of lid with holes.On the other hand, described lid with holes also can the rate of outflow of moderate control CO 2 fluid and dyestuff.
As preferred technical scheme, described lid with holes is provided with draw ring, is conveniently pulled out by cylindrical shell.
As preferred technical scheme, described sealing kettle cover is flexibly connected with described kettle by opening clip soon.
As preferred technical scheme, the periphery of described kettle is provided with heating jacket, and in order to heating and insulation, the bottom of described heating jacket is provided with thermal medium entrance, and top is provided with thermal medium outlet.
As preferred technical scheme, described cylindrical shell is provided with cylindrical shell twist portion, described kettle is provided with kettle twist portion, described cylindrical shell and kettle, is connected with kettle twist portion by cylindrical shell twist portion.
Another object of the present invention is to provide the technique adopting above-mentioned supercritical carbon dioxide ox horn button dyeing caldron to carry out the dyeing of ox horn button.
As preferred technical scheme, the dyeing condition of described ox horn button dyeing is: the dyeing condition of described dyeing is: supercritical carbon dioxide fluid flow velocity is 10 ~ 40g/min, dyeing temperature in the kettle is 80 ~ 100 DEG C, in dyeing caldron, pressure is 15 ~ 25MPa, and dyeing time is 30 ~ 60min; The dyestuff that wherein said dyeing adopts is direct dyes, before described ox horn button dyeing, carry out preliminary treatment, described preprocess method is: be placed on by ox horn button in reaction of low temperature plasma device, vacuumize, pass into oxygen, at pressure 25 ~ 70Pa, discharge process 5 ~ 30min under power 25 ~ 300W.Dyeing terminates rear step-down makes dyestuff be separated with carbon dioxide, reclaims respectively, and take out stained specimens, sample is without post processings such as cleaning-dryings.The change that the color sample depth accounts for the factors such as the mass percent of ox horn button mainly through dyeing time, dyeing temperature, direct dyes controls.The metering of described supercritical carbon dioxide fluid flow velocity is for standard with the supercritical carbon dioxide that flows through per minute and the common quality of direct dyes.
As preferred technical scheme, the quality of described direct dyes accounts for 1 ~ 5% of ox horn button quality, is preferably 2 ~ 3%.
As preferred technical scheme, the compound method of the dye liquor of described direct dyes is: after direct dyes being dissolved with water, then add levelling agent and obtain, the addition of described levelling agent accounts for 0.5% ~ 2% of dye liquor gross mass.Wherein, the addition of deionized water of dissolving direct dyes will not be particularly limited to, can the water yield of dissolving dye completely, and the water yield generally added is 2 ~ 5 times of the direct dyes quality as solute.For levelling agent, will not be particularly limited to, those skilled in the art can be adopted can to realize commercially available levelling agent of the present invention and all can use, the present invention preferably adopts paregal O.
In technique scheme, the kind of described direct dyes will not be particularly limited to, and the direct dyes for protein fiber dyeing in this area are all available.In the present invention, direct dyes are preferably Direct Red 23, directly Huang 28, directly indigo plant 72.
When undressed ox horn button dyes in supercritical carbon dioxide, dyestuff is difficult to dispersion and enters in button fiber molecule, and therefore Color is not obvious, and Dry Sack is very shallow.The present invention by carrying out preliminary treatment by ox horn button in the plasma reactor of certain pressure, power, and make button surface produce ion, be convenient to react with dyestuff, Color significantly improves, and obtains color depth and obviously deepens.
Described above in Supercritical carbon dioxide fluid dyeing process, the supercritical carbon dioxide carrying DISPERSE DYES enters dyeing autoclave body bottom by certain speed by carbon dioxide and dyestuff entrance, the chassis with holes be provided with by dyeing caldron cylinder body bottom and curved surface netware enter cylindrical shell, form eddy airstream to dye, the carbon dioxide carrying part DISPERSE DYES flows out from carbon dioxide outlet, form circulation, in dyeing caldron, button circulating along with supercritical carbon dioxide, completes dyeing gradually.The molecular dynamics mechanism that the supercritical carbon dioxide carrying DISPERSE DYES carries out button dyeing in cylindrical shell is: the dyestuff be dissolved in supercritical carbon dioxide fluid enters Dynamic Boundary layer near material interface gradually, when dyestuff is after material interface, rely on the diffusion of self close to material, when molecular force is enough large, dyestuff is by materials adsorption, inside and outside material, form dye strength difference, complete the absorption set of dyestuff, thus realize the non-aqueous dyeing of supercritical carbon dioxide fluid.
Beneficial effect of the present invention: the invention provides a kind of new supercritical carbon dioxide ox horn button dyeing caldron, this dyeing caldron is provided with CO 2 fluid and dyestuff entrance in the bottom of kettle, and top is provided with outlet, during dyeing, bottom silicon dioxide carbon fluid and dyestuff flow into kettle, impact button and drive button to dye in non-static mode, flow velocity also by controlling supercritical carbon dioxide fluid realizes the change of air-flow, thus button is moved under the gear shift shock of air-flow, avoid the dyeing speck of button and button overlapping.Simultaneously the cylinder body bottom of dyeing caldron of the present invention is designed to inverted trapezoidal structure, effectively prevents from button from not reaching carrying the CO 2 fluid of DISPERSE DYES and the problem that cannot dye.Adopt dyeing of the present invention, can obtain color and luster and enrich complete button, the product after dyeing does not need to carry out post processings such as cleaning, dry, realizes overall process non-aqueous dyeing, saves production cost, and improves dyeing quality, reduces environmental pollution.
Accompanying drawing explanation
Fig. 1 is the structural representation of supercritical carbon dioxide ox horn button dyeing caldron of the present invention;
Wherein, 1, kettle, 2, sealing kettle cover, 3, cylindrical shell, 4, CO 2 fluid and dyestuff entrance, 5, CO 2 fluid and dyestuff outlet, 6, curved surface netware, 7, inverted trapezoidal structure, 8, lid with holes, 9, chassis with holes, 10, draw ring, 11, open clip soon, 12, heating jacket, 13, thermal medium entrance, 14, thermal medium outlet, 15, cylindrical shell twist portion, 16, kettle twist portion, 17, opening.
Detailed description of the invention
Following non-limiting example can make the present invention of those of ordinary skill in the art's comprehend, but does not limit the present invention in any way.
In following embodiment: plasma reactor is the HPD-2400 type plasma reactor of Nanjing Su Man Electronics Co., Ltd.; Levelling agent is paregal O.
Embodiment 1 ~ 8
A kind of supercritical carbon dioxide ox horn button dyeing caldron, as shown in Figure 1, this dyeing caldron comprises kettle and cylindrical shell, the upper end of described kettle is provided with sealing kettle cover, sealing kettle cover is flexibly connected with described kettle by opening clip soon, and the periphery of described kettle is provided with heating jacket, in order to heating and insulation, the bottom of described heating jacket is provided with thermal medium entrance, and top is provided with thermal medium outlet; Described cylindrical shell is placed in kettle, and the bottom of described kettle is provided with CO 2 fluid and dyestuff entrance, and the top of described kettle is provided with CO 2 fluid and dyestuff outlet; The bottom of described cylindrical shell is provided with opening, described opening is corresponding with described CO 2 fluid and dyestuff entrance, described opening part is provided with the curved surface netware protruded to inner barrel and the chassis with holes be positioned at below it, the mesh aperture of described curved surface netware is 1 ~ 2mm, the aperture on described chassis with holes is 3mm, described curved surface netware and chassis with holes are all movably connected on the bottom of cylindrical shell, are convenient to dismounting and cleaning.The bottom of described cylindrical shell is inverted trapezoidal structure, and the angle of its hypotenuse and horizontal plane is 40 degree.The upper end of described cylindrical shell is provided with lid with holes, and described lid with holes is provided with draw ring.Cylindrical shell is provided with cylindrical shell twist portion, described kettle is provided with kettle twist portion, described cylindrical shell and kettle, is connected with kettle twist portion by cylindrical shell twist portion.When practical application, dyestuff still is outside equipped with at dyeing caldron, reaching supercritical carbon dioxide passes in dyestuff still, dissolve dyestuff wherein, then the supercritical carbon dioxide with DISPERSE DYES is passed into certain speed in the cylindrical shell of dyeing caldron and dye, form eddy airstream to dye, the carbon dioxide carrying part DISPERSE DYES flows out from carbon dioxide outlet, get back in dyeing caldron, form circulation, in dyeing caldron, button circulating along with supercritical carbon dioxide, completes dyeing gradually.Miss the season when carbon dioxide damages, in dyestuff still, supplement supercritical carbon dioxide, the supercritical carbon dioxide carrying dyestuff reenters dyeing caldron by carbon dioxide entrance.
Adopt supercritical carbon dioxide ox horn button dyeing caldron as shown in Figure 1 to carry out the dyeing of ox horn button, dyeing comprises the steps:
(1) preliminary treatment of ox horn button: ox horn button is placed in reaction of low temperature plasma device, vacuumizes, pass into oxygen, at pressure 25 ~ 70Pa, discharge process 5 ~ 30min under power 25 ~ 300W, after electric discharge terminates, recover normal pressure, take out button, for subsequent use;
(2) open the dyeing caldron of supercritical carbon dioxide ox horn button dyeing apparatus, the draw ring utilizing the lid with holes of dyeing caldron inner barrel to be provided with proposes whole cylindrical shell, is evenly placed in cylindrical shell by ox horn button good for preliminary treatment, puts back to cylindrical shell;
(3) open refrigeration system and high-pressure system, more than carbon dioxide pressurization to critical pressure, then by heater, carbon dioxide is heated to more than critical point temperature, makes carbon dioxide reach supercriticality;
(4) the dye liquor preparation of direct dyes: after direct dyes being dissolved with deionized water, then add levelling agent and obtain, the addition of described levelling agent accounts for 0.5% ~ 2% of dye liquor gross mass;
(5) dye liquor is poured in dyestuff still, supercritical carbon dioxide dissolving dye is passed in dyestuff still, supercritical carbon dioxide with dyestuff to be passed in the cylindrical shell in dyeing caldron by dyestuff still with the speed of 10 ~ 40g/min simultaneously, utilize heater to make dyeing temperature in the kettle reach 80 ~ 100 DEG C, keep temperature constant; Open high-pressure system, pressure in dyeing caldron is made to reach 15 ~ 25MPa, keep constant pressure, dye 30 ~ 60min under constant temperature and pressure, high-pressure pump, the circulatory system and heating system is closed, then release of pressure make fluid remain on 7.9Mpa, carry out the recovery of carbon dioxide and dyestuff under 30 degree after reaching setting dyeing time; Continue release of pressure to normality, take out dyeing button; The speed wherein passing into the supercritical carbon dioxide in dyestuff still is identical with the speed that the supercritical carbon dioxide with dyestuff passes into dyeing caldron cylindrical shell by dyestuff still, ensures the dynamic equilibrium of CO 2 fluid in dyestuff still with this.
Table 1 is the dyeing condition adopted in embodiment 1 ~ 8, is specially: plasma treatment time, dyestuff account for percentage composition (" dye content " in table 1), fluid flow, dyeing pressure, dyeing temperature and the dyeing time etc. of ox horn button quality.In embodiment 1 ~ 8, the direct dyes of use are Direct Red 23, and the levelling agent of use is paregal O, and levelling agent use amount is 1% of dye liquor gross mass.In the embodiment 1 ~ 8 of table 1, the pretreatment condition of ox horn button is: pressure 50Pa, power 250W.
Table 2 is the characterisitic parameter of the product obtained of dyeing under adopting the dyeing condition of embodiment 1 ~ 8, is specially: use Color-Eye7000A fabric color measurement and color match instrument to record its apparent color depth K/S value; The fastness to soaping of dyeing button is detected according to GB-T3921, and the variable color fastness recording button by GB-T250, the staining fastness of fabric is recorded by GB-T251; Detect the colour fastness to rubbing of dyeing button according to GB-T3920, recorded dry, the wet staining fastness of button by GB-T251; Detected the sunlight fastness of button by GB730, and record the colour fasteness to sunlight of button; Detect the color fastness to hot pressing of dyeing button according to GB-T6152, the variable color fastness recording button by GB-T250, is recorded the staining fastness of fabric by GB-T251.
The dyeing condition adopted in table 1. embodiment 1 ~ 8
Table 2. dyes under adopting the dyeing condition of embodiment 1-8 the characterisitic parameter of the product obtained
The result of table 2 is visible, method of the present invention is adopted to carry out the dyeing of ox horn button, it is apparent that color depth K/S value can reach 6 ~ 18, illustrate that this method can obtain the button of various depth color by adjusting process condition, and its color fastness to washing, colour fastness to rubbing major part can reach 4 or 3 ~ 4 grades, it has good washability and crocking resistance, and its color fastness to hot pressing and colour fasteness to sunlight all reach 3-4 or 4 grade, illustrate its resistance to hot pressing and colour fasteness to sunlight better.
Claims (10)
1. supercritical carbon dioxide ox horn button dyeing caldron, comprise kettle (1), the upper end of described kettle (1) is provided with sealing kettle cover (2), it is characterized in that: the bottom of described kettle (1) is provided with CO 2 fluid and dyestuff entrance (4), the top of described kettle is provided with CO 2 fluid and dyestuff outlet (5).
2. supercritical carbon dioxide ox horn button dyeing caldron according to claim 1, it is characterized in that: described dyeing caldron also comprises cylindrical shell (3), described cylindrical shell (3) is placed in kettle (1), the bottom of described cylindrical shell (3) is provided with opening (17), described opening (17) is corresponding with described CO 2 fluid and dyestuff entrance (4), and described opening (17) place is provided with the curved surface netware (6) protruded to cylindrical shell (3) inside.
3. supercritical carbon dioxide ox horn button dyeing caldron according to claim 2, is characterized in that: the bottom of described cylindrical shell (3) is inverted trapezoidal structure (7).
4. supercritical carbon dioxide ox horn button dyeing caldron according to claim 3, is characterized in that: the hypotenuse of described inverted trapezoidal structure (7) and the angle of horizontal plane are 20 ~ 50 degree.
5. supercritical carbon dioxide ox horn button dyeing caldron according to claim 2, it is characterized in that: opening (17) place of described cylindrical shell (3) is provided with chassis with holes (9), described chassis with holes (9) is positioned at the below of described curved surface netware (6).
6. supercritical carbon dioxide ox horn button dyeing caldron according to claim 2, it is characterized in that: the upper end of described cylindrical shell (3) is provided with lid with holes (8), described lid with holes (8) is provided with draw ring (10).
7. supercritical carbon dioxide ox horn button dyeing caldron according to claim 2, is characterized in that: the mesh aperture of described curved surface netware (6) is 1 ~ 2mm.
8. an ox horn button supercritical CO 2 dyeing technique, is characterized in that: adopt the supercritical carbon dioxide ox horn button dyeing caldron described in any one of claim 1 ~ 7 to dye.
9. dyeing according to claim 8, it is characterized in that: the dyeing condition of described dyeing is: supercritical carbon dioxide fluid flow velocity is 10 ~ 40g/min, dyeing temperature in the kettle is 80 ~ 100 DEG C, and in dyeing caldron, pressure is 15 ~ 25MPa, and dyeing time is 30 ~ 60min;
The dyestuff that wherein said dyeing adopts is direct dyes, before described ox horn button dyeing, carry out preliminary treatment, described preprocess method is: be placed on by ox horn button in reaction of low temperature plasma device, vacuumize, pass into oxygen, at pressure 25 ~ 70Pa, discharge process 5 ~ 30min under power 25 ~ 300W.
10. dyeing according to claim 9, it is characterized in that, the quality of described direct dyes accounts for 1 ~ 5% of ox horn button quality, the compound method of the dye liquor of described direct dyes is: after direct dyes being dissolved with deionized water, add levelling agent again to obtain, the addition of described levelling agent accounts for 0.5% ~ 2% of dye liquor gross mass.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510412594.1A CN105155177B (en) | 2015-07-14 | 2015-07-14 | Supercritical carbon dioxide ox horn button dyeing caldron and its dyeing |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510412594.1A CN105155177B (en) | 2015-07-14 | 2015-07-14 | Supercritical carbon dioxide ox horn button dyeing caldron and its dyeing |
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| CN105155177A true CN105155177A (en) | 2015-12-16 |
| CN105155177B CN105155177B (en) | 2017-06-27 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105755711A (en) * | 2016-05-04 | 2016-07-13 | 青岛即发集团股份有限公司 | Supercritical CO2 waterless staining dye pot and waterless staining method |
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| CN1944762A (en) * | 2006-10-27 | 2007-04-11 | 美晨集团股份有限公司 | Dyeing caldron in supercritical CO2 dyeing device |
| CN201485677U (en) * | 2009-07-21 | 2010-05-26 | 东莞市彩之虹化工有限公司 | Dyeing kettle |
| CN102776738A (en) * | 2012-07-17 | 2012-11-14 | 大连工业大学 | Supercritical carbon dioxide hairball dyeing kettle and waterless dyeing method thereof |
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2015
- 2015-07-14 CN CN201510412594.1A patent/CN105155177B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW200420798A (en) * | 2002-10-31 | 2004-10-16 | Uhde High Pressure Tech Gmbh | Process for dyeing materials in compressed carbon dioxide |
| CN1944762A (en) * | 2006-10-27 | 2007-04-11 | 美晨集团股份有限公司 | Dyeing caldron in supercritical CO2 dyeing device |
| CN201485677U (en) * | 2009-07-21 | 2010-05-26 | 东莞市彩之虹化工有限公司 | Dyeing kettle |
| CN102776738A (en) * | 2012-07-17 | 2012-11-14 | 大连工业大学 | Supercritical carbon dioxide hairball dyeing kettle and waterless dyeing method thereof |
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| CN105755711A (en) * | 2016-05-04 | 2016-07-13 | 青岛即发集团股份有限公司 | Supercritical CO2 waterless staining dye pot and waterless staining method |
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Effective date of registration: 20221213 Address after: 362212 Fengchi Industrial Zone, tangcuo village, Chidian Town, Jinjiang City, Quanzhou City, Fujian Province Patentee after: JINJIANG GUOSHENG SHOE MATERIAL LTD. Address before: 116034 No. 1 light industry garden, Ganjingzi District, Liaoning, Dalian Patentee before: DALIAN POLYTECHNIC University |
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