CN105147735A - Bath product containing dark jade - Google Patents
Bath product containing dark jade Download PDFInfo
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- CN105147735A CN105147735A CN201510665968.0A CN201510665968A CN105147735A CN 105147735 A CN105147735 A CN 105147735A CN 201510665968 A CN201510665968 A CN 201510665968A CN 105147735 A CN105147735 A CN 105147735A
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Abstract
The invention relates to a bath product containing dark jade, and belongs to the technical field of health care and health preserving. The bath product is prepared from dark jade, salt, talcum powder, pearl powder and agilawood, has the characteristics of killing bacteria, diminishing inflammation, relieving itching, detoxifying, keeping freshness, easing pain, dissipating blood stasis, activating cells, quickly opening microcirculation and the like, can remove acidic metabolites in a human body to promote and strengthen the human body metabolism. The bath product adopts natural dark jade as a main ingredient serving as a parent body and uses natural water as a carrier to realize natural energy conversion through an exchange effect between an external temperature field and a human body temperature field, so as to realize the natural energy health effect on the human body. In addition, through a preparation method for the bath product, effective components in materials such as dark jade can be extracted to the utmost extent, so that the effectiveness of rare and precious materials such as dark jade is improved, unordered use and waste are avoided, the environment is protected, and an epoch-marking significance is realized.
Description
Technical field
The present invention relates to a kind of bathing goods, particularly relate to a kind of bathing goods containing black jade stone, belong to health care, health promotion technology field.
Background technology
Black jade is a kind of preciousness and rare natural resources, only originate in the black jade of Mountainous Area of North, Fuping County, Shaanxi Province, its color heavy is greasy, texture is careful, balck like ink, bright and clean lovely, extremely well-known, its hardness is about Mohs4o, and element is for controlling excellent treasure's material of inkstone, cutter work, and ancients are by itself and diamond, gem, colored stone being called " expensive U.S. stone ".Black jade, refer to a famous and precious kind in XinjiangArid area, it possesses the one's best quality of Khotan jade, and heavily fortified point causes gentle, wherein pure person balck like ink, and it is balck like ink, and color heavy is greasy, and texture is careful, bright and clean elegance.
Black jade has water purification, invigorates blood circulation, effect of toxin expelling; with medical science monumental works such as Shennong's Herbal, Tang Materia Medica, Compendium of Material Medica for foundation; detect through modern science and technology and find that jet god tea can change molecular structure water; the blood fat reducing of energy purified blood matter, each large physiological system normalization of conditioning human body, clears up human body waste effectively; vessel softening; blood circulation promoting accelerates circulation, under specified temp (90 DEG C), effectively can discharge self trace element in drinking-water.Have effect of dredge the meridian passage, black jade is undertaken massaging by human body subcutaneous cell and acupuncture point, footpath, portion and infiltrates human body, thus improves immune function of human body, makes microcirculqtory system each mechanism balance, to reach, dredging the meridian, QI and blood are smooth, internal organs peace and effect.There is effect of improving eyesight lung moistening, often wear black jade ornaments, blood circulation can be impelled, negative and positive can be regulated, can treatment palpitate with fear, the diseases such as heat in the heart, acute conjunctivitis, tooth are swollen, cough, pain in the lung, hyperthyroidism, have the functions such as improving eyesight, lung moistening, convenient, blood pressure lowering, and have certain prophylactic-therapeutic effect to breast carcinoma, long periods of wear can prevent relieving the pain caused by diseases, make people energetic, body parts is coordinated more, sucks black green onyx, by the merit of nutrition contained by saliva and lyase, energy promoting the production of body fluid to quench thirst, grows cardiopulmonary except gastric heat, has special effect to oral ulcer.There is effect of anti-inflammatory analgesic, there is B, S element in black jade and compound has sterilization, antipruritic effect.This is the operation of nature of the natural products that the Nature is given.Have effect of anti-corrosive fresh-keeping, black jade contains vegetable oil base, and penetration is also very strong, therefore there is cleaning function, paint on hand can be washed off, the greasy dirt of smoke exhaust ventilator, also can wash fine fabrics, avoid the bad smell of paint scrubber, detergent, infuse tea with black jade, can prevent tannin from discharging, make tea flavour more glycol, not puckery, cool might as well to drink, with black jade god tea bubble milk, dissolve not easily become sour completely; Cook with black jade god tea, color whiten is tender, and sweet-smelling is good to eat, not easily becomes sour; Soup is boiled, Tang Gengxian with the refreshing tea of blackish green jade; With the refreshing tea Scalded Green Vegetable of blackish green jade, original color and taste can be kept; Make coffee with jet god tea, taste is denseer more fragrant; Fragrance can be kept for a long time, and reduce zest; Water flowers with black jade god tea, HUAMU can be made without fertilizer also gorgeous fragrance; With the flower arrangement of black jade god tea, can flowering time be extended, more long more luxuriant; Breed fish with black jade god tea, fish jar tongue not green for a long time, fish is eaten less also can be active.
In view of black jade has so many health care, health preserving effect, black jade is developed to easy to use, and can the product of efficiency utilization, be current problem demanding prompt solution.
Summary of the invention
Technical problem to be solved by this invention is that the defect overcoming prior art provides a kind of bathing goods containing black jade stone, these bathing goods have sterilization, antiinflammatory, antipruritic, toxin expelling, fresh-keeping, analgesia scattered silt, activating cell, open the features such as microcirculation fast, also can remove human body inner acidic metabolite, promote and strengthen body metabolism.
Technical problem of the present invention is realized by following technical scheme.
Bathing goods containing black jade stone, it is prepared from by the component of following weight portion:
Prepare a method for the above-mentioned bathing goods containing black jade stone, comprise the steps: that black jade stone is after polishing becomes fine powder, is mixed in proportion with salt, Pulvis Talci, Margarita powder.
In order to improve the effectiveness of black jade stone, salt, Pulvis Talci, Margarita powder, further,
The above-mentioned method having the bathing goods of black jade stone, comprise the steps: that (1) takes black jade stone, salt, Pulvis Talci, the Margarita powder of recipe quantity, micronization processes is carried out after mix homogeneously, particle size distribution after micronization processes is that D90 is less than 5 microns, D50 is less than 2 microns, obtain the former powder of material, for subsequent use;
(2) add in the dilute alkaline soln containing diethanolamine by the former powder of step (1) gained material, the volume mL of described dilute alkaline soln is 3 ~ 5 times of the former grain weight amount g of material, through microwave treatment after jolting, obtains alkaline hydrolysis sample solution, for subsequent use;
(3) by the dilute acid soln containing peracetic acid, join rapidly in the alkaline hydrolysis sample solution of step (2) gained under agitation, after equaling 5.8 to pH, carry out supersound extraction, centrifugal, the dilute acid soln of residue containing peracetic acid washs, centrifugal, merge supernatant filtering with microporous membrane, obtain filtrate, for subsequent use;
(4) filtrate step (3) obtained adopts rotary evaporating device to concentrate, being condensed into relative density at 60 DEG C is the extractum of 1.20, drying under reduced pressure at 80 DEG C, particle size distribution after dry extract micronization processes is that D90 is less than 10 microns, D50 is less than 5 microns, obtain extract powder, for subsequent use;
(5) by step (4) gained extract powder and 1,3-two (2,4,6-trimethylphenyl)-4,5-glyoxalidine tetrafluoroborate add pH value be 6.8 containing pancreatin phosphate buffer in stirring and dissolving disperse to obtain solution, wherein the volume mL of phosphate buffer and the weight g of the former powder of material are than being 12.5:1,1,3-two (2,4,6-trimethylphenyl)-4, the weight g of 5-glyoxalidine tetrafluoroborate and the weight g of the former powder of material are than being 2:1, and by this solution lyophilization, flaggy temperature is down to-15 DEG C from room temperature, 1 hour time used, keep 6 hours; Continue to be down to-30 DEG C, 23 minutes time used, keep 2.5 hours; When rear cabinet temperature is down to below-40 DEG C, be evacuated to below 35Pa, freeze drying box flaggy is slowly warming up to-12 DEG C, 100 minutes time used, keeps 8.5 hours; Flaggy continues to be warming up to 1 DEG C, 60 minutes time used, keeps 4 hours, treats that product temperature is elevated to close to flaggy temperature, and obviously reducing appears in rear cabinet temperature, and distillation terminates; Continue to be warming up to plate temperature 40 DEG C, 80 minutes time used, keep 3.5 hours; When in drying baker vacuum rise ease up, without significant change time, lyophilizing terminates, by the powder of lyophilization gained load packaging bag namely obtain black jade lithophysa bathe goods.
Preferably, above-mentioned preparation contains the method for the bathing goods of black jade stone, and described in step (2), dilute alkaline soln is triethylamine solution, and concentration is 0.6moL/L, and the concentration of described diethanolamine is mass fraction 10%; Described microwave power is 800W, and the microwave time is 30s.Above-mentioned preparation contains the method for the bathing goods of black jade stone, and described in step (3), dilute acid soln is L MALIC ACID solution, and concentration is 0.2moL/L; The concentration of described peracetic acid is mass fraction 5%; The described supersound extraction time is 20min; Described microporous filter membrane is PEFT material.
In addition, the present invention further provides black jade stone for the preparation of the application in bathing goods.
Above-mentioned black jade stone is for the preparation of the application in bathing goods, and described bathing goods are prepared from by the component of following weight portion:
Above-mentioned black jade stone is for the preparation of the application in bathing goods, and described bathing goods are prepared from by following methods:
(1) take black jade stone, salt, Pulvis Talci, the Margarita powder of recipe quantity, carry out micronization processes after mix homogeneously, the particle size distribution after micronization processes is that D90 is less than 5 microns, D50 is less than 2 microns, obtains the former powder of material, for subsequent use;
(2) add in the dilute alkaline soln containing diethanolamine by the former powder of step (1) gained material, the volume mL of described dilute alkaline soln is 3 ~ 5 times of the former grain weight amount g of material, through microwave treatment after jolting, obtains alkaline hydrolysis sample solution, for subsequent use;
(3) by the dilute acid soln containing peracetic acid, join rapidly in the alkaline hydrolysis sample solution of step (2) gained under agitation, after equaling 5.8 to pH, carry out supersound extraction, centrifugal, the dilute acid soln of residue containing peracetic acid washs, centrifugal, merge supernatant filtering with microporous membrane, obtain filtrate, for subsequent use;
(4) filtrate step (3) obtained adopts rotary evaporating device to concentrate, being condensed into relative density at 60 DEG C is the extractum of 1.20, drying under reduced pressure at 80 DEG C, particle size distribution after dry extract micronization processes is that D90 is less than 10 microns, D50 is less than 5 microns, obtain extract powder, for subsequent use;
(5) by step (4) gained extract powder and 1,3-two (2,4,6-trimethylphenyl)-4,5-glyoxalidine tetrafluoroborate add pH value be 6.8 containing pancreatin phosphate buffer in stirring and dissolving disperse to obtain solution, wherein the volume mL of phosphate buffer and the weight g of the former powder of material are than being 12.5:1,1,3-two (2,4,6-trimethylphenyl)-4, the weight g of 5-glyoxalidine tetrafluoroborate and the weight g of the former powder of material are than being 2:1, and by this solution lyophilization, flaggy temperature is down to-15 DEG C from room temperature, 1 hour time used, keep 6 hours; Continue to be down to-30 DEG C, 23 minutes time used, keep 2.5 hours; When rear cabinet temperature is down to below-40 DEG C, be evacuated to below 35Pa, freeze drying box flaggy is slowly warming up to-12 DEG C, 100 minutes time used, keeps 8.5 hours; Flaggy continues to be warming up to 1 DEG C, 60 minutes time used, keeps 4 hours, treats that product temperature is elevated to close to flaggy temperature, and obviously reducing appears in rear cabinet temperature, and distillation terminates; Continue to be warming up to plate temperature 40 DEG C, 80 minutes time used, keep 3.5 hours; When in drying baker vacuum rise ease up, without significant change time, lyophilizing terminates, by the powder of lyophilization gained load packaging bag namely obtain black jade lithophysa bathe goods.
Preferably, above-mentioned black jade stone is for the preparation of the application in bathing goods, and described in step (2), dilute alkaline soln is triethylamine solution, and concentration is 0.6moL/L, and the concentration of described peracetic acid is mass fraction 10%; Described microwave power is 800W, and the microwave time is 30s.Above-mentioned black jade stone is for the preparation of the application in bathing goods, and described in step (3), dilute acid soln is L MALIC ACID solution, and concentration is 0.2moL/L; The concentration of described peracetic acid is mass fraction 5%; The described supersound extraction time is 20min; Described microporous filter membrane is PEFT material.
The equipment used in micronization processes described in the present invention can be jet mill, ball mill or fluid energy mill, and other equipment that this area routine also can be used to use, are not particularly limited to.
In use, get more than 1 liter water boil, bathing goods containing black jade stone of the present invention for 8g are poured into water, continue to boil 3 ~ 5 minutes, be blended in the warm water of about 40 DEG C that mix up in advance, regulate water temperature to carry out bathing according to personal considerations, this using method is referred to as bathing once in the present invention.
These bathing goods containing black jade stone of the present invention, ground by the pure natural effect type black jade stone containing micro-(grand) secondary element such as 6.73% active Magnet and needed by human body chromium, zinc, calcium, manganese, strontium, selenium, and be prepared from specific consumption proportion with compositions such as salt, Pulvis Talci, Margarita powder.Bathing goods containing black jade stone of the present invention, its effective ingredient is mutually collaborative to be annotated and applies to ultimate attainment by " the beautiful people of supporting, people support beautiful ".Bathing goods active constituent content containing black jade stone of the present invention is high, penetration is strong, conduction of heat is fast, there is sterilization, antiinflammatory, antipruritic, toxin expelling, fresh-keeping, analgesia scattered silt, activating cell, open effect of microcirculation fast, and human body inner acidic metabolite can be removed, promote and strengthen body metabolism.Bathing goods containing black jade stone of the present invention using natural black jade for main component is as parent, using natural water source as carrier, by the exchange interaction of ambient temperature field and human body temperature field, reach and utilize natural energy to change and the natural energy health-care effect that carries out human body.In addition; these bathing goods containing black jade stone of the present invention; with specific proportionings of composition such as black jade stone and salt, Pulvis Talci, Margarita powder; in addition the specific operating procedure such as micronization, alkali liquor hydrolysis, acid solution extraction, lyophilization, and the specific material such as alkali liquor, acid solution, can extract the effective ingredient in the materials such as black jade stone to greatest extent; improve the effectiveness of this your resource uncommon of black jade stone; avoid and unorderedly use and waste, protect environment, be with historically new significance.
Detailed description of the invention
Below by detailed description of the invention, the invention will be further described, but just understand the present invention for helping, and professional and technical personnel in the field realized or uses the present invention, not forming any restriction to the present invention.
The preparation of the embodiment 1 bathing goods containing black jade stone of the present invention
Composition and ratio:
Preparation method:
Black jade stone, after 60 ~ 80 object sieves are crossed in polishing powder delivery, is mixed in proportion rear use salt, Pulvis Talci, Margarita powder, specification 8g/ bag.
Bathing goods containing black jade stone prepared by embodiment 2 commonsense method
Composition and ratio:
Preparation method:
Black jade stone, after 60 ~ 80 object sieves are crossed in polishing powder delivery, is mixed in proportion rear use salt, Pulvis Talci, Margarita powder, specification 8g/ bag.
The preparation of the embodiment 3 bathing goods containing black jade stone of the present invention
Composition and ratio:
Preparation method:
Black jade stone, after 60 ~ 80 object sieves are crossed in polishing powder delivery, is mixed in proportion rear use salt, Pulvis Talci, Margarita powder, specification 8g/ bag.
The preparation of the embodiment 4 bathing goods containing black jade stone of the present invention
Composition and ratio:
Preparation method:
(1) take black jade stone, salt, Pulvis Talci, the Margarita powder of recipe quantity, carry out micronization processes after mix homogeneously, the particle size distribution after micronization processes is that D90 is less than 5 microns, D50 is less than 2 microns, obtains the former powder of material, for subsequent use;
(2) the former powder of step (1) gained material is added in the dilute alkaline soln containing diethanolamine, the volume of described dilute alkaline soln is 234mL, described dilute alkaline soln is triethylamine solution, and concentration is 0.6moL/L, and the concentration of described diethanolamine is mass fraction 10%; Through microwave treatment after jolting, described microwave power is 800W, and the microwave time is 30s, obtains alkaline hydrolysis sample solution, for subsequent use;
(3) by the dilute acid soln containing peracetic acid, join rapidly in the alkaline hydrolysis sample solution of step (2) gained under agitation, after equaling 5.8 to pH, carry out supersound extraction, the supersound extraction time is 20min, centrifugal, and the dilute acid soln of residue containing peracetic acid washs, described dilute acid soln is L MALIC ACID solution, and concentration is 0.2moL/L; The concentration of described peracetic acid is mass fraction 5%, and centrifugal merging supernatant PEFT material filtering with microporous membrane, obtains filtrate, for subsequent use;
(4) filtrate step (3) obtained adopts rotary evaporating device to concentrate, being condensed into relative density at 60 DEG C is the extractum of 1.20, drying under reduced pressure at 80 DEG C, particle size distribution after dry extract micronization processes is that D90 is less than 10 microns, D50 is less than 5 microns, obtain extract powder 26.6g, for subsequent use;
(5) by step (4) gained extract powder and 1,3-two (2,4,6-trimethylphenyl)-4,5-glyoxalidine tetrafluoroborate add pH value be 6.8 containing pancreatin phosphate buffer in stirring and dissolving disperse to obtain solution, wherein the volume of phosphate buffer is 975mL, 1,3-two (2,4,6-trimethylphenyl)-4, the weight g of 5-glyoxalidine tetrafluoroborate and the weight of the former powder of material are 156g, and by this solution lyophilization, flaggy temperature is down to-15 DEG C from room temperature, 1 hour time used, keep 6 hours; Continue to be down to-30 DEG C, 23 minutes time used, keep 2.5 hours; When rear cabinet temperature is down to below-40 DEG C, be evacuated to below 35Pa, freeze drying box flaggy is slowly warming up to-12 DEG C, 100 minutes time used, keeps 8.5 hours; Flaggy continues to be warming up to 1 DEG C, 60 minutes time used, keeps 4 hours, treats that product temperature is elevated to close to flaggy temperature, and obviously reducing appears in rear cabinet temperature, and distillation terminates; Continue to be warming up to plate temperature 40 DEG C, 80 minutes time used, keep 3.5 hours; When in drying baker vacuum rise ease up, without significant change time, lyophilizing terminates, by the powder 178.3g of lyophilization gained load packaging bag namely obtain black jade lithophysa bathe goods, specification 8g/ bag.
The preparation of the embodiment 5 bathing goods containing black jade stone of the present invention
Composition and ratio:
Preparation method:
(1) take black jade stone, salt, Pulvis Talci, the Margarita powder of recipe quantity, carry out micronization processes after mix homogeneously, the particle size distribution after micronization processes is that D90 is less than 5 microns, D50 is less than 2 microns, obtains the former powder of material, for subsequent use;
(2) the former powder of step (1) gained material is added in the dilute alkaline soln containing diethanolamine, the volume 400mL of described dilute alkaline soln, described dilute alkaline soln is triethylamine solution, and concentration is 0.6moL/L, and the concentration of described peracetic acid is mass fraction 10%; Through microwave treatment after jolting; Described microwave power is 800W, and the microwave time is 30s, obtains alkaline hydrolysis sample solution, for subsequent use;
(3) by the dilute acid soln containing peracetic acid, join rapidly in the alkaline hydrolysis sample solution of step (2) gained under agitation, after equaling 5.8 to pH, carry out supersound extraction, the described supersound extraction time is 20min, centrifugal, the dilute acid soln of residue containing peracetic acid washs, described dilute acid soln is L MALIC ACID solution, and concentration is 0.2moL/L, and the concentration of described peracetic acid is mass fraction 5%, merge supernatant PEFT material filtering with microporous membrane, centrifugal, obtain filtrate, for subsequent use;
(4) filtrate step (3) obtained adopts rotary evaporating device to concentrate, being condensed into relative density at 60 DEG C is the extractum of 1.20, drying under reduced pressure at 80 DEG C, particle size distribution after dry extract micronization processes is that D90 is less than 10 microns, D50 is less than 5 microns, obtain extract powder 41.2g, for subsequent use;
(5) by step (4) gained extract powder and 1,3-two (2,4,6-trimethylphenyl)-4,5-glyoxalidine tetrafluoroborate add pH value be 6.8 containing pancreatin phosphate buffer in stirring and dissolving disperse to obtain solution, the wherein volume 1250mL of phosphate buffer, 1,3-two (2,4,6-trimethylphenyl)-4, the weight 200g of 5-glyoxalidine tetrafluoroborate, by this solution lyophilization, flaggy temperature is down to-15 DEG C from room temperature, 1 hour time used, keep 6 hours; Continue to be down to-30 DEG C, 23 minutes time used, keep 2.5 hours; When rear cabinet temperature is down to below-40 DEG C, be evacuated to below 35Pa, freeze drying box flaggy is slowly warming up to-12 DEG C, 100 minutes time used, keeps 8.5 hours; Flaggy continues to be warming up to 1 DEG C, 60 minutes time used, keeps 4 hours, treats that product temperature is elevated to close to flaggy temperature, and obviously reducing appears in rear cabinet temperature, and distillation terminates; Continue to be warming up to plate temperature 40 DEG C, 80 minutes time used, keep 3.5 hours; When in drying baker vacuum rise ease up, without significant change time, lyophilizing terminates, by the powder 239.6g of lyophilization gained load packaging bag namely obtain black jade lithophysa bathe goods, specification 8g/ bag.
The preparation of the embodiment 6 bathing goods containing black jade stone of the present invention
Composition and ratio:
Preparation method:
(1) take black jade stone, salt, Pulvis Talci, the Margarita powder of recipe quantity, carry out micronization processes after mix homogeneously, the particle size distribution after micronization processes is that D90 is less than 5 microns, D50 is less than 2 microns, obtains the former powder of material, for subsequent use;
(2) the former powder of step (1) gained material is added in the dilute alkaline soln containing diethanolamine, the volume of described dilute alkaline soln is 605mL, described dilute alkaline soln is triethylamine solution, and concentration is 0.6moL/L, and the concentration of described diethanolamine is mass fraction 10%; Through microwave treatment after jolting, described microwave power is 800W, and the microwave time is 30s, obtains alkaline hydrolysis sample solution, for subsequent use;
(3) by the dilute acid soln containing peracetic acid, join rapidly in the alkaline hydrolysis sample solution of step (2) gained under agitation, after equaling 5.8 to pH, carry out supersound extraction, the supersound extraction time is 20min, centrifugal, and the dilute acid soln of residue containing peracetic acid washs, described dilute acid soln is L MALIC ACID solution, and concentration is 0.2moL/L; The concentration of described peracetic acid is mass fraction 5%, and centrifugal merging supernatant PEFT material filtering with microporous membrane, obtains filtrate, for subsequent use;
(4) filtrate step (3) obtained adopts rotary evaporating device to concentrate, being condensed into relative density at 60 DEG C is the extractum of 1.20, drying under reduced pressure at 80 DEG C, particle size distribution after dry extract micronization processes is that D90 is less than 10 microns, D50 is less than 5 microns, obtain extract powder 39.8g, for subsequent use;
(5) by step (4) gained extract powder and 1,3-two (2,4,6-trimethylphenyl)-4,5-glyoxalidine tetrafluoroborate add pH value be 6.8 containing pancreatin phosphate buffer in stirring and dissolving disperse to obtain solution, wherein the volume of phosphate buffer is 1512.5mL, 1,3-two (2,4,6-trimethylphenyl)-4, the weight g of 5-glyoxalidine tetrafluoroborate and the weight of the former powder of material are 242g, and by this solution lyophilization, flaggy temperature is down to-15 DEG C from room temperature, 1 hour time used, keep 6 hours; Continue to be down to-30 DEG C, 23 minutes time used, keep 2.5 hours; When rear cabinet temperature is down to below-40 DEG C, be evacuated to below 35Pa, freeze drying box flaggy is slowly warming up to-12 DEG C, 100 minutes time used, keeps 8.5 hours; Flaggy continues to be warming up to 1 DEG C, 60 minutes time used, keeps 4 hours, treats that product temperature is elevated to close to flaggy temperature, and obviously reducing appears in rear cabinet temperature, and distillation terminates; Continue to be warming up to plate temperature 40 DEG C, 80 minutes time used, keep 3.5 hours; When in drying baker vacuum rise ease up, without significant change time, lyophilizing terminates, by the powder 278g of lyophilization gained load packaging bag namely obtain black jade lithophysa bathe goods, specification 8g/ bag.
Checking embodiment 1
Enter the routine male diabetic patient of group 30,45 ~ 55 years old age, ill history 5 ~ 8 years, be divided into A group, B group, C group at random; A group uses the bathing goods bathing containing black jade stone prepared by the embodiment of the present invention 5; The bathing goods bathing containing black jade stone that B group uses embodiment 2 to prepare.C group only uses black jade stone powder bathing, and three groups use same dose 8g at every turn.
Result: during bathing to 3 time, A group has 7 patient blood glucose to recover normal; B group has 5 patient blood glucose to recover normal; C group has 2 patient blood glucose to recover normal.
During bathing to 4 time, A group all patients blood sugar recovery is normal; B group has 8 patient blood glucose to recover normal, and C group has 5 patient blood glucose to recover normal.
During bathing to 5 time, A group all patients blood glucose is normal, unchanged; B group all patients blood sugar recovery is normal, and C group has 8 patient blood glucose to recover normal.
Visible, the bathing goods containing black jade stone prepared by the present invention, wherein, black jade stone powder and salt, Pulvis Talci, Margarita powder serve so that specific ratio is mutually collaborative the effect improving respective effectiveness.In addition, bathing goods containing black jade stone of the present invention, with specific proportionings of composition such as black jade stone and salt, Pulvis Talci, Margarita powder, in addition the specific operating procedure such as micronization, alkali liquor hydrolysis, acid solution extraction, lyophilization, and the specific material such as alkali liquor, acid solution, the effective ingredient in the materials such as black jade stone can be extracted to greatest extent, there is the advantages such as active constituent content is higher, penetration is stronger, conduction of heat is faster, use amount is less compared with alone black jade stone powder.
Case example takes passages 1
Wang: female, 75 years old, suffers from serious prolapse of lumbar intervertebral disc, cervical spondylosis, hypertension, hyperlipidemia, also has the bone of rheumatoid arthritis whole body to be almost out of shape, with originally walking, with regard to two point form life, on daytime sofa, on evening bed.After suffer from again lung Nang swell, every day all will have plenty kind of a Chinese medicine and western medicine, but disease still without any improvement.The bathing goods bathing containing black jade stone prepared by the use embodiment of the present invention 21 time, just can throw off crutch and walk, then steeped 10 times again, whole people seems very spiritedness, and blood pressure blood fat is normal, does not also eat any medicine again.
What certain: man, 56 years old.Because of long-term high protein, higher fatty acid excessive, suffer from diabetes 8 years, fasting glucose 12.Use the bathing goods bathing containing black jade stone prepared by the embodiment of the present invention 1, after 12 times, blood sugar recovery is normal, has no recurrence so far 2 years more.
Liu: man, 54 years old, type 2 diabetes mellitus, blood glucose is up to more than 13 o'clock, and blood pressure, and blood fat is all high, take medicine and reach 10 years, beat Insulin 3 year, the bathing goods bathing containing black jade stone prepared by the use embodiment of the present invention 2 13 times, not needing now to beat insulin does not need to eat any medicine yet, present three indexs are normal, health is very light, and not weak, the mental status is also very good.
Clock: man, 43 years old.Because of bad life style, suffer from serious subhealth state, listless, immunity is low, often catches a cold.Use the bathing goods bathing containing black jade stone prepared by the embodiment of the present invention 2, only 8 times, people just spirit changes, and comes one year over, does not occur once to catch a cold.
Cai: man, 43 years old, drinks and causes severe gout, there is the time of 3 years, the outbreak of each gout, all with the hyperpyrexia of about 39 degree and hurt like hell, suffer from can not normally walking of the foot pain of gout, use the bathing goods bathing containing black jade stone prepared by the embodiment of the present invention 2, water temperature greatly about 43 degree, bathing 1 pain relief, temperature decline, normal walking, bathing 3 body temperature are normal, and pain disappears.
Zhang: man, 72 years old.For many years, hypertension, headache and insomnia, stool constipation, also usually skin pruritus, use the bathing goods bathing containing black jade stone prepared by the embodiment of the present invention 3, just stopped skin pruritus after 2 times, 7 headache and dizzies and constipation all solve, and after 13 times, hypertension recovers normal.
Wang: man, 53 years old, blood thickness, fatty liver, serious rheumatism, above will have a rest for 4th floors 2 times, uses the bathing goods bathing containing black jade stone prepared by the embodiment of the present invention 21 to 3 time, water after bathing presents blackish green, and I feels brisk condition of mind, and need not have a rest and can go up 4th floors, the mental status is fine.
Stone: female, 65 years old.Because of long-term Fengshi Guanjie pain, foot articular sensation start distortion, sometimes pain can not walk, connect lavatory all difficult.Adhere to the bathing goods bathing containing black jade stone used prepared by the embodiment of the present invention 2, just can easily walk afterwards for 5 times, adhere to foaming foot 26 times, the joint of distortion restores to the original state substantially.
Zhao: man, 26 years old, figure was partially fat, gout outbreak often, can only jump by single lower limb time serious, can't fall asleep of pain at night, can not can not go downstairs on foot, can only starve several days, or friend brings meal, owing to following the line of least resistance conveniently, continue to eat bean product one week, gout is shown effect, hurt like hell, use the bathing goods containing black jade stone prepared by the embodiment of the present invention 2 at once, bathing complete out after, although also some pain, but alleviate and much had a rest one hour, a large amount of perspire, when instantly walking, pain perception completely without.
Bai: female, 61 years old, causes femoral head break because falling down by bike, go home to rest in hospital, lain in bed three months, play a lot of skin ulcer on the face owing to getting angry after one month.Use the bathing goods containing black jade stone prepared by the embodiment of the present invention 2, the 1st time bathing feels unobstructed from head to foot, very comfortable, conscientious employ two weeks after, skin ulcer on the face disappears, and lower limb also can be walked with descending.
In certain: female, 22 years old, before bathing, whole face was all purple pox, the time of several years takes a lot of time and money does not all have effect, uses the bathing goods containing black jade stone prepared by the embodiment of the present invention 2, the time of one month, face purple pox disappears, peach and cream.
Pay certain: 34 years old, serious striae gravidarum patient, also with obesity, the symptoms such as hypoimmunity, the bathing goods bathing 3 times containing black jade stone prepared by the continuous embodiment of the present invention 2, striae gravidarum calms down, smooth, and waistline has also subtracted.
Only certain: 49 years old, the patient of weakened immune system, had serious seborrheic skin problem, can not perm, dye head, through the bathing goods bathing containing black jade stone prepared by 5 embodiment of the present invention 2, can perm, dye head.
Rely certain: man, 45 years old, serious splenic and gastric incoordination, deficiency of vital energy blood deficiency patient, weak all over, through using the bathing goods bathing containing black jade stone prepared by the embodiment of the present invention 23 times, complexion takes a turn for the better, and whole body is strong.
Xu certain: female, 24 years old, because job specification is bowed for a long time, cause serious cervical spondylosis, make a definite diagnosis cervical vertebra 4,5 and save distortion, often dizzy, headache of feeling sick, refers to fiber crops, the bathing goods bathing containing black jade stone prepared by the process use embodiment of the present invention 27 times, symptom fades away, and complexion is not gloomy as before yet, and the cervical spondylosis that how to work now is not also violated, also do not have a dizzy spell, and successful weight loss 10 kilograms.
Yan: female, 56 years old, suffers from the diseases such as cerebral hemorrhage, peripheral neuritis, hypertension, arthritis, ache all over the body is unable, walks tired, by through using the bathing goods bathing containing black jade stone prepared by the embodiment of the present invention 2 15 times, health is without pain symptom, and whole body is strong.
Below be only the preferred embodiment of the present invention; not in order to limit the present invention, to those skilled in the art, under the premise without departing from the principles of the invention; the some improvement that can also make, retouching, equivalent replacement, all should be included within protection scope of the present invention.
Claims (6)
1. the bathing goods containing black jade stone, it is characterized in that, it is prepared from by the component of following weight portion:
2. prepare a method for the bathing goods containing black jade stone as claimed in claim 1, it is characterized in that, comprise the steps: that black jade stone is after polishing becomes fine powder, is mixed in proportion with salt, Pulvis Talci, Margarita powder.
3. the method for the bathing goods containing black jade stone according to claim 2, is characterized in that, comprise the steps:
(1) take black jade stone, salt, Pulvis Talci, the Margarita powder of recipe quantity, carry out micronization processes after mix homogeneously, the particle size distribution after micronization processes is that D90 is less than 5 microns, D50 is less than 2 microns, obtains the former powder of material, for subsequent use;
(2) the former powder of step (1) gained material is added in the dilute alkaline soln containing diethanolamine, the volume mL of described dilute alkaline soln is 3 ~ 5 times of the former grain weight amount g of material, described dilute alkaline soln is triethylamine solution, concentration is 0.6moL/L, and the concentration of described diethanolamine is mass fraction 10%; Through microwave treatment after jolting, described microwave power is 800W, and the microwave time is 30s, obtains alkaline hydrolysis sample solution, for subsequent use;
(3) by the dilute acid soln containing peracetic acid, join rapidly in the alkaline hydrolysis sample solution of step (2) gained under agitation, after equaling 5.8 to pH, carry out supersound extraction, the supersound extraction time is 20min, centrifugal, and the dilute acid soln of residue containing peracetic acid washs, described dilute acid soln is L MALIC ACID solution, and concentration is 0.2moL/L; The concentration of described peracetic acid is mass fraction 5%, centrifugal, merges supernatant PEFT material filtering with microporous membrane, obtains filtrate, for subsequent use;
(4) filtrate step (3) obtained adopts rotary evaporating device to concentrate, being condensed into relative density at 60 DEG C is the extractum of 1.20, drying under reduced pressure at 80 DEG C, particle size distribution after dry extract micronization processes is that D90 is less than 10 microns, D50 is less than 5 microns, obtain extract powder, for subsequent use;
(5) by step (4) gained extract powder and 1,3-two (2,4,6-trimethylphenyl)-4,5-glyoxalidine tetrafluoroborate add pH value be 6.8 containing pancreatin phosphate buffer in stirring and dissolving disperse to obtain solution, wherein the volume mL of phosphate buffer and the weight g of the former powder of material are than being 12.5:1,1,3-two (2,4,6-trimethylphenyl)-4, the weight g of 5-glyoxalidine tetrafluoroborate and the weight g of the former powder of material are than being 2:1, and by this solution lyophilization, flaggy temperature is down to-15 DEG C from room temperature, 1 hour time used, keep 6 hours; Continue to be down to-30 DEG C, 23 minutes time used, keep 2.5 hours; When rear cabinet temperature is down to below-40 DEG C, be evacuated to below 35Pa, freeze drying box flaggy is slowly warming up to-12 DEG C, 100 minutes time used, keeps 8.5 hours; Flaggy continues to be warming up to 1 DEG C, 60 minutes time used, keeps 4 hours, treats that product temperature is elevated to close to flaggy temperature, and obviously reducing appears in rear cabinet temperature, and distillation terminates; Continue to be warming up to plate temperature 40 DEG C, 80 minutes time used, keep 3.5 hours; When in drying baker vacuum rise ease up, without significant change time, lyophilizing terminates, by the powder of lyophilization gained load packaging bag namely obtain black jade lithophysa bathe goods.
4. black jade stone is for the preparation of the application in bathing goods.
5. black jade stone according to claim 4 is for the preparation of the application in bathing goods, it is characterized in that, described bathing goods are prepared from by the component of following weight portion:
6. black jade stone according to claim 5 is for the preparation of the application in bathing goods, it is characterized in that, described bathing goods are prepared from by following methods:
(1) take black jade stone, salt, Pulvis Talci, the Margarita powder of recipe quantity, carry out micronization processes after mix homogeneously, the particle size distribution after micronization processes is that D90 is less than 5 microns, D50 is less than 2 microns, obtains the former powder of material, for subsequent use;
(2) the former powder of step (1) gained material is added in the dilute alkaline soln containing diethanolamine, the volume mL of described dilute alkaline soln is 3 ~ 5 times of the former grain weight amount g of material, described dilute alkaline soln is triethylamine solution, concentration is 0.6moL/L, and the concentration of described diethanolamine is mass fraction 10%; Through microwave treatment after jolting, described microwave power is 800W, and the microwave time is 30s, obtains alkaline hydrolysis sample solution, for subsequent use;
(3) by the dilute acid soln containing peracetic acid, join rapidly in the alkaline hydrolysis sample solution of step (2) gained under agitation, after equaling 5.8 to pH, carry out supersound extraction, the supersound extraction time is 20min, centrifugal, and the dilute acid soln of residue containing peracetic acid washs, described dilute acid soln is L MALIC ACID solution, and concentration is 0.2moL/L; The concentration of described peracetic acid is mass fraction 5%, centrifugal, merges supernatant PEFT material filtering with microporous membrane, obtains filtrate, for subsequent use;
(4) filtrate step (3) obtained adopts rotary evaporating device to concentrate, being condensed into relative density at 60 DEG C is the extractum of 1.20, drying under reduced pressure at 80 DEG C, particle size distribution after dry extract micronization processes is that D90 is less than 10 microns, D50 is less than 5 microns, obtain extract powder, for subsequent use;
(5) by step (4) gained extract powder and 1,3-two (2,4,6-trimethylphenyl)-4,5-glyoxalidine tetrafluoroborate add pH value be 6.8 containing pancreatin phosphate buffer in stirring and dissolving disperse to obtain solution, wherein the volume mL of phosphate buffer and the weight g of the former powder of material are than being 12.5:1,1,3-two (2,4,6-trimethylphenyl)-4, the weight g of 5-glyoxalidine tetrafluoroborate and the weight g of the former powder of material are than being 2:1, and by this solution lyophilization, flaggy temperature is down to-15 DEG C from room temperature, 1 hour time used, keep 6 hours; Continue to be down to-30 DEG C, 23 minutes time used, keep 2.5 hours; When rear cabinet temperature is down to below-40 DEG C, be evacuated to below 35Pa, freeze drying box flaggy is slowly warming up to-12 DEG C, 100 minutes time used, keeps 8.5 hours; Flaggy continues to be warming up to 1 DEG C, 60 minutes time used, keeps 4 hours, treats that product temperature is elevated to close to flaggy temperature, and obviously reducing appears in rear cabinet temperature, and distillation terminates; Continue to be warming up to plate temperature 40 DEG C, 80 minutes time used, keep 3.5 hours; When in drying baker vacuum rise ease up, without significant change time, lyophilizing terminates, by the powder of lyophilization gained load packaging bag namely obtain black jade lithophysa bathe goods.
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|---|---|---|---|
| CN201510665968.0A CN105147735A (en) | 2015-10-15 | 2015-10-15 | Bath product containing dark jade |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510665968.0A CN105147735A (en) | 2015-10-15 | 2015-10-15 | Bath product containing dark jade |
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| CN107050222A (en) * | 2017-04-20 | 2017-08-18 | 乔丕凯 | A kind of health products containing black jade powder and preparation method thereof |
| CN107137266A (en) * | 2017-05-02 | 2017-09-08 | 石京涛 | A kind of bathing product containing black jade stone and preparation method thereof, application method |
| CN107397705A (en) * | 2017-09-27 | 2017-11-28 | 兰军胜 | Black jade plant mask and preparation method thereof, skin condition product and its preparation method and application |
| CN107496261A (en) * | 2017-10-09 | 2017-12-22 | 兰军胜 | Black jade plant is soaked cream and preparation method thereof |
| CN109125147A (en) * | 2017-06-16 | 2019-01-04 | 北京丰仁源科技发展有限公司 | Contain blackish green jade bathing product with health care function and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107137266A (en) * | 2017-05-02 | 2017-09-08 | 石京涛 | A kind of bathing product containing black jade stone and preparation method thereof, application method |
| CN109125147A (en) * | 2017-06-16 | 2019-01-04 | 北京丰仁源科技发展有限公司 | Contain blackish green jade bathing product with health care function and preparation method thereof |
| CN107397705A (en) * | 2017-09-27 | 2017-11-28 | 兰军胜 | Black jade plant mask and preparation method thereof, skin condition product and its preparation method and application |
| CN107496261A (en) * | 2017-10-09 | 2017-12-22 | 兰军胜 | Black jade plant is soaked cream and preparation method thereof |
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