CN105136602B - Activated carbon comprehensive gas adsorption instrument - Google Patents
Activated carbon comprehensive gas adsorption instrument Download PDFInfo
- Publication number
- CN105136602B CN105136602B CN201510562342.7A CN201510562342A CN105136602B CN 105136602 B CN105136602 B CN 105136602B CN 201510562342 A CN201510562342 A CN 201510562342A CN 105136602 B CN105136602 B CN 105136602B
- Authority
- CN
- China
- Prior art keywords
- gas
- adsorption
- weighing
- tube
- activated carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Landscapes
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Separation Of Gases By Adsorption (AREA)
Abstract
The invention relates to an active carbon comprehensive gas adsorption instrument which comprises a gas generating device (1), a gas heating device (2), an adsorption weighing device (3) and a control computer (4), wherein adsorption gas is generated by the gas generating device, enters the gas heating device for heating through metering and filtering, is introduced into the adsorption weighing device for adsorption reaction and real-time weighing, continuously feeds back weighing data in the reaction to the control computer through a data transmission line, the control computer judges a reaction starting point and a reaction finishing point according to the change of detection data, controls the adsorption instrument to stop recording work at the finishing point, and outputs an operation result. The adsorption apparatus has the advantages of high speed, high efficiency, simple operation, large handling capacity, compact structure, high accuracy and the like, can realize the process automation of temperature control, ventilation, heating, drying, weighing, final calculation and the like in the detection process of the gas adsorption capacity of the activated carbon, simplifies the manual detection operation steps, and improves the detection accuracy and efficiency.
Description
Technical Field
The invention belongs to the field of gas adsorption capacity detection and treatment equipment of activated carbon, and particularly relates to an activated carbon comprehensive gas adsorption instrument.
Background
At present, the activated carbon industry is developing vigorously, and in the related detection field, a common experimental device for detecting the adsorption rate is operated in an artificial chemical detection mode, specifically, gas with a certain flow is introduced into activated carbon in certain equipment, the activated carbon before and after adsorption is weighed by balance, the adsorption reaction process is timed by a stopwatch, and then the adsorption rate of the activated carbon is calculated by a formula. The method has the advantages of complex operation, long time consumption, multiple human factors and large error range.
Disclosure of Invention
In view of the above prior art, the technical problem to be solved by the present invention is to provide a device with higher speed, higher efficiency, simple operation, large processing capacity, compact structure and high accuracy, which simplifies the manual detection operation steps and improves the detection efficiency.
In order to solve the technical problem, the invention provides an active carbon comprehensive gas adsorption instrument, which comprises a gas generating device, a gas heating device, an adsorption weighing device and a control computer, wherein:
the gas generating device comprises an air purifier, an adsorbed gas generating bottle and a float flowmeter which are connected in turn through a gas pipeline;
the gas heating device comprises an adsorbed gas inlet pipe, a constant-temperature heat insulation box for containing hot water bath, a constant-temperature water bath control panel, an adsorbed gas constant-temperature pipe arranged in the hot water bath, a gas heating device and a water circulating pump;
the adsorption weighing device comprises a real-time weighing platform, a weighing pipe arranged above the weighing platform, a sample pipe and an air outlet pipe, wherein the sample pipe and the air outlet pipe are arranged on the upper opening of the weighing pipe in a matching way;
the control computer comprises a data processing and control unit which is connected with the real-time weighing platform through a data transmission line.
The active carbon comprehensive gas adsorption instrument has the advantages of being fast, efficient, simple to operate, large in treatment capacity, compact in structure, high in accuracy and the like, and the automation of the active carbon gas adsorption capacity detection process can be realized by using the adsorption instrument, so that the manual detection operation steps are simplified, and the detection accuracy and efficiency are improved.
As an improvement of the activated carbon comprehensive gas adsorption instrument, the side wall of the constant-temperature heat insulation box is provided with a water outlet pipe and a water inlet pipe, the water outlet pipe is positioned at the lowest position of the water surface of the control water bath, and the water inlet pipe is positioned at the highest position of the water surface of the control water bath. By adopting the structure, water can be conveniently added, drained or changed for the hot water bath, and when the temperature of the hot water bath is higher than a set value, the temperature can be rapidly reduced by adding cold water into the water inlet and draining hot water from the water outlet.
As a further improvement of the activated carbon comprehensive gas adsorption instrument, the sample tube comprises a tube part for accommodating a sample, a bottom part with a small hole, a matching part with a frosted outer surface and a tube plug communicated with an exhaust tube. The structure can ensure the gas circulation, is convenient for the active carbon to fully adsorb and react, and prevents gas leakage.
As a further improvement of the activated carbon comprehensive gas adsorption instrument, the constant-temperature heat insulation box is provided with a top cover, and the top cover is covered after the operation, so that the hot water bath can be prevented from being influenced by the environment, and the water temperature is kept stable.
As a further improvement of the activated carbon comprehensive gas adsorption instrument, the sample tube is made of a glass material, and the weighing tube is made of a copper material, so that the influence of certain corrosive gases is avoided.
In conclusion, the integrated activated carbon gas adsorption instrument has the advantages of being rapid, efficient, simple to operate, large in treatment capacity, compact in structure, high in accuracy and the like, and the automatic detection process of the gas adsorption capacity of the activated carbon can be realized by using the integrated activated carbon gas adsorption instrument, so that the manual detection operation steps are simplified, and the detection accuracy and efficiency are improved.
Drawings
FIG. 1 is a schematic structural diagram of an activated carbon integrated gas adsorption apparatus according to the present invention;
FIG. 2 is a schematic diagram of a control computer of the integrated activated carbon gas adsorption apparatus of the present invention;
fig. 3 is a schematic view of an adsorption device of the activated carbon comprehensive gas adsorption apparatus of the present invention.
In the figure: 1-gas generating device, 11-air purifier, 12-adsorbed gas generating bottle, 13-float flowmeter, 2-gas heating device, 21-adsorbed gas inlet pipe, 22-constant temperature heat insulation box, 23-constant temperature water bath control panel, 24-adsorbed gas constant temperature pipe, 25-water bath heating pipe, 26-water circulating pump, 27-water outlet pipe, 28-water inlet pipe, 29-top cover, 3-adsorption weighing device, 31-real-time weighing platform, 32-weighing pipe, 33-sample pipe, 331-pipe part, 332-bottom part, 333-matching part, 334-pipe plug, 34-power line, 35-data transmission line, 36-exhaust pipe, 37-waterproof heat insulation layer, 4-control computer
Detailed Description
The following detailed description of embodiments of the invention refers to the accompanying drawings in which:
as shown in fig. 1 to 3, an activated carbon comprehensive gas adsorption instrument comprises a gas generating device 1, a gas heating device 2, an adsorption weighing device 3 and a control computer 4, wherein:
the gas generating device 1 comprises an air purifier 11, an adsorbed gas generating bottle 12 and a floater flowmeter 13 which are connected in sequence through a gas pipeline;
the gas heating device 2 comprises an air inlet pipe 21 for absorbing gas, a constant-temperature heat insulation box 22 for containing hot water bath, a constant-temperature water bath control panel 23, an air constant-temperature tube 24 for absorbing gas, a water bath heating tube 25 and a water circulating pump 26, wherein the constant-temperature heat insulation box 22 is arranged in the hot water bath, the side wall of the constant-temperature heat insulation box is provided with a water outlet pipe 27 and a water inlet pipe 28, the water outlet pipe 27 is positioned at the lowest part of the water surface of the control water bath;
the adsorption weighing device 3 comprises a real-time weighing platform 31, a weighing tube 32 placed above the weighing platform, a sample tube 33 and an exhaust tube 36 which are arranged on the upper opening of the weighing tube in a matching way, a power line 34 and a data transmission line 35 are connected to the real-time weighing platform, the adsorption weighing device 3 and the gas heating device 2 are arranged in a constant-temperature heat insulation box 22 and connected through a gas pipeline, the adsorption weighing device 3 is separated from the gas heating device 2 through a waterproof heat insulation layer 37, and the sample tube 33 comprises a tube part 331 for accommodating a sample, a bottom 332 with small holes, a matching part 333 with the outer surface subjected to frosting treatment and a tube plug 334 communicated with the exhaust tube 36;
the control computer 4 comprises a data processing and control unit and is connected with the real-time weighing platform 31 by a data transmission line 35. The data processing and control unit is designed to: controlling the comprehensive adsorption instrument to complete the whole detection process of the adsorption rate of the activated carbon gas; controlling a reading operation, which can be continuously performed and in which the weighing value can be recorded and an adsorption curve can be made according to the value; and data processing, namely judging according to the data read and recorded in the detection process, controlling the start and the end of the detection process, and automatically calculating a detection result according to the recorded data.
The working principle of the activated carbon comprehensive gas adsorption instrument of the invention is as follows: the adsorption gas is generated by the gas generating device 1, enters the gas heating device 2 for heating after being metered and filtered, then enters the adsorption weighing device 3 for adsorption reaction and real-time weighing, the weighing data of the real-time weighing platform 31 in the reaction is continuously fed back to the control computer 4 through the data transmission line 35, the control computer judges the starting point and the end point of the reaction according to the change of the detection data, and controls the adsorption instrument to stop recording work at the end point, and the operation result is output.
When the device is used, the switch of the constant-temperature water bath control panel 23 is firstly turned on, the temperature of the hot water bath is set, the water bath heating pipe 25 is started to heat, the water circulating pump 26 is started to stir and circulate, when the real-time temperature of the hot water bath reaches a set value, air purified by the air purifier 11 is introduced into the adsorption gas generation bottle 12, generated gas is taken out and mixed, the flow is controlled by the float flowmeter 13, the air enters the gas heating device 2 through the adsorption gas inlet pipe 21, the air is heated and insulated by the hot water bath in the adsorption gas constant-temperature pipe 24, enters the sample pipe 33 and is exhausted by the exhaust pipe 36 after being adsorbed by activated carbon. The mass of the activated carbon in the sample tube 33 after adsorbing gas is measured in real time by the real-time weighing platform 31 and is transmitted to the control computer by the data transmission line, the control computer judges a reaction starting point and a reaction finishing point according to the change of the detected data, the adsorption instrument is controlled to stop recording at the finishing point, and the adsorption rate of the activated carbon sample is obtained through calculation.
The embodiments of the present invention have been described in detail with reference to the drawings, but the present invention is not limited to the embodiments and various changes can be made thereto within the knowledge of those skilled in the art.
Claims (5)
1. The utility model provides a gaseous absorption appearance is synthesized to active carbon, its characterized in that, includes gas generator (1), gas heating device (2), adsorbs weighing device (3) and control computer (4), wherein:
the gas generating device (1) comprises an air purifier (11), an adsorbed gas generating bottle (12) and a float flowmeter (13) which are sequentially connected through a gas pipeline;
the gas heating device (2) comprises an adsorption gas inlet pipe (21), a constant-temperature heat insulation box (22) for containing hot water bath, a constant-temperature water bath control panel (23), an adsorption gas constant-temperature pipe (24) arranged in the hot water bath, a water bath heating pipe (25) and a water circulating pump (26);
the adsorption weighing device (3) comprises a real-time weighing platform (31), a weighing tube (32) arranged above the weighing platform (31), a sample tube (33) and an exhaust tube (36) which are arranged on an upper opening of the weighing tube (32) in a matching way, wherein the real-time weighing platform (31) is connected with a power line (34) and a data transmission line (35), the adsorption weighing device (3) and the gas heating device (2) are in the same constant-temperature heat insulation box (22) and are connected through a gas pipeline, and the adsorption weighing device (3) is separated from the gas heating device (2) through a waterproof heat insulation layer (37);
the sample tube (33) comprises a tube part (331) for accommodating a sample, a bottom part (332) with a small hole, a matching part (333) with a frosted outer surface and a tube plug (334) communicated with the exhaust tube (36);
the control computer (4) comprises a data processing and control unit and is connected with the real-time weighing platform (31) through a data transmission line (35).
2. The activated carbon comprehensive gas adsorption instrument according to claim 1, wherein a water outlet pipe (27) and a water inlet pipe (28) are installed on the side wall of the constant-temperature heat insulation box (22), the water outlet pipe (27) is located at the lowest position of the water surface of the control water bath, and the water inlet pipe (28) is located at the highest position of the water surface of the control water bath.
3. The activated carbon integrated gas adsorption apparatus of claim 1, wherein the constant temperature heat insulation box (22) has a top cover (29).
4. The integrated activated carbon gas adsorber according to claim 1, wherein the sample tube (33) is made of a glass material.
5. The activated carbon integrated gas adsorber of claim 1, wherein the weighing tube (32) is made of copper material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510562342.7A CN105136602B (en) | 2015-09-07 | 2015-09-07 | Activated carbon comprehensive gas adsorption instrument |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510562342.7A CN105136602B (en) | 2015-09-07 | 2015-09-07 | Activated carbon comprehensive gas adsorption instrument |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105136602A CN105136602A (en) | 2015-12-09 |
| CN105136602B true CN105136602B (en) | 2020-08-04 |
Family
ID=54722032
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510562342.7A Expired - Fee Related CN105136602B (en) | 2015-09-07 | 2015-09-07 | Activated carbon comprehensive gas adsorption instrument |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105136602B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106918526A (en) * | 2017-04-14 | 2017-07-04 | 中国石油化工股份有限公司 | The quick method for determining petroleum vapor recovery sorbing material adsorption desorption performance |
| CN109030116B (en) * | 2018-06-08 | 2021-06-18 | 海南大学 | Adsorption tube for gas adsorption |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2408800A (en) * | 2003-10-24 | 2005-06-08 | Surface Measurement Systems Lt | Method and apparatus for investigating the properties of a solid material |
| CN201438170U (en) * | 2009-06-26 | 2010-04-14 | 上海梅山钢铁股份有限公司 | Measuring device of crystal water in inorganic material |
| CN102288689A (en) * | 2011-04-26 | 2011-12-21 | 广东工业大学 | Device and method for testing adsorption property of activated semi-coke adsorbent |
| CN102401771A (en) * | 2010-09-21 | 2012-04-04 | 淮阴工学院 | Apparatus for testing work ability of activated carbon canister used for vehicle |
| CN103278433A (en) * | 2013-05-16 | 2013-09-04 | 北京林业大学 | Device and method for researching particle absorbing capability of plants |
| CN103335913A (en) * | 2013-07-05 | 2013-10-02 | 株洲南方燃气轮机成套制造安装有限公司 | Apparatus and method used for testing oil mist adsorbability of adsorption fillings |
| CN203811496U (en) * | 2014-04-01 | 2014-09-03 | 贝士德仪器科技(北京)有限公司 | Weight-method physical adsorption instrument |
| CN104849169A (en) * | 2015-05-26 | 2015-08-19 | 中国石油化工股份有限公司 | Method for testing adsorption and desorption performance of adsorption materials for oil gas recovery |
| CN204924838U (en) * | 2015-09-07 | 2015-12-30 | 宁夏出入境检验检疫局检验检疫综合技术中心 | Gas absorption appearance is synthesized to active carbon |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101721878A (en) * | 2010-01-18 | 2010-06-09 | 哈尔滨工业大学 | Method and system for capturing CO2 by temperature-lowering absorption and low-voltage desorption |
| CN101934221B (en) * | 2010-10-14 | 2012-10-10 | 厦门大学 | Modified adsorbent and preparation method thereof |
| CN203275231U (en) * | 2013-05-21 | 2013-11-06 | 江苏核电有限公司 | Device for measuring dynamic adsorption coefficient of material in vacuum |
| CN204159185U (en) * | 2014-09-29 | 2015-02-18 | 中能东讯新能源科技(大连)有限公司 | A kind of thermostatic type oil gas adsorbent equipment |
-
2015
- 2015-09-07 CN CN201510562342.7A patent/CN105136602B/en not_active Expired - Fee Related
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2408800A (en) * | 2003-10-24 | 2005-06-08 | Surface Measurement Systems Lt | Method and apparatus for investigating the properties of a solid material |
| CN201438170U (en) * | 2009-06-26 | 2010-04-14 | 上海梅山钢铁股份有限公司 | Measuring device of crystal water in inorganic material |
| CN102401771A (en) * | 2010-09-21 | 2012-04-04 | 淮阴工学院 | Apparatus for testing work ability of activated carbon canister used for vehicle |
| CN102288689A (en) * | 2011-04-26 | 2011-12-21 | 广东工业大学 | Device and method for testing adsorption property of activated semi-coke adsorbent |
| CN103278433A (en) * | 2013-05-16 | 2013-09-04 | 北京林业大学 | Device and method for researching particle absorbing capability of plants |
| CN103335913A (en) * | 2013-07-05 | 2013-10-02 | 株洲南方燃气轮机成套制造安装有限公司 | Apparatus and method used for testing oil mist adsorbability of adsorption fillings |
| CN203811496U (en) * | 2014-04-01 | 2014-09-03 | 贝士德仪器科技(北京)有限公司 | Weight-method physical adsorption instrument |
| CN104849169A (en) * | 2015-05-26 | 2015-08-19 | 中国石油化工股份有限公司 | Method for testing adsorption and desorption performance of adsorption materials for oil gas recovery |
| CN204924838U (en) * | 2015-09-07 | 2015-12-30 | 宁夏出入境检验检疫局检验检疫综合技术中心 | Gas absorption appearance is synthesized to active carbon |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105136602A (en) | 2015-12-09 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103983748B (en) | A kind of active coke desulphurizing denitration performance characterization test method and device thereof | |
| CN103115941A (en) | Novel closed heat conductivity coefficient testing device | |
| Su et al. | Experimental study on the performance of an improved dehumidification system integrated with precooling and recirculated regenerative rotary desiccant wheel | |
| CN105136602B (en) | Activated carbon comprehensive gas adsorption instrument | |
| CN204904049U (en) | Multi -functional environmental simulation cabin | |
| CN110064302A (en) | A kind of honeycomb type denitrification catalyst SO2Oxygenation efficiency real-time on-line detecting method and device | |
| CN203376244U (en) | High temperature-resistant aqueous vapor oxidization property simulation and acceleration testing device | |
| CN108195993A (en) | A kind of SCR denitration full-scale performance detection evaluating apparatus and its application process | |
| CN104849167A (en) | Device for detecting isothermal adsorption and desorption of moisture of tobacco slice or cut tobacco biomass | |
| CN106568897A (en) | Device and measuring method used for continuous measuring of content of mercury of different valence states in flue gas | |
| CN202655009U (en) | Device for detecting fluid ion parameters in generation process of gas hydrate in real time | |
| CN203870075U (en) | Active coke desulfurization and denitration performance characterization test device | |
| CN204924838U (en) | Gas absorption appearance is synthesized to active carbon | |
| CN107219086B (en) | Test platform and test method for evaluating performance of organic waste gas treatment device based on gas path automatic control | |
| CN210021745U (en) | Honeycomb denitration catalyst SO2Real-time on-line detection device for oxidation rate | |
| CN205352824U (en) | Intelligent COD of integration clears up appearance | |
| CN206161504U (en) | Test device that historical relic corrodes under simulation museum environment | |
| CN203365290U (en) | Simple chemical corrosion testing device | |
| CN205941252U (en) | Graininess oil absorption material adsorptivity can environmental suitability testing arrangement | |
| CN216816567U (en) | Absorbent performance detection device | |
| CN114755384A (en) | Heat supply heat exchanger and pipe network scaling tendency online measuring device and method thereof | |
| CN107860706A (en) | A kind of sulfidation corrosion experimental rig | |
| CN114531745A (en) | Fluoride purification system, explosion-proof heater in fluoride purification system and use method | |
| CN108896474B (en) | Corrosion evaluation device and method for monitoring concentration of dissolved oxygen at high temperature in real time | |
| CN207438885U (en) | A kind of Full automatic stepping type energy-saving and purifying boiler |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20200804 Termination date: 20210907 |