CN105131484A - Waterproof flame retardant anti-microbial mildew-resistant pigment - Google Patents
Waterproof flame retardant anti-microbial mildew-resistant pigment Download PDFInfo
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- CN105131484A CN105131484A CN201510560097.6A CN201510560097A CN105131484A CN 105131484 A CN105131484 A CN 105131484A CN 201510560097 A CN201510560097 A CN 201510560097A CN 105131484 A CN105131484 A CN 105131484A
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Abstract
The invention relates to a waterproof flame retardant anti-microbial mildew-resistant pigment. The waterproof flame retardant anti-microbial mildew-resistant pigment is composed of the following ingredients, by weight, 30-34 parts of acrylic acid, 32-36 parts of ceramic glaze, 28-32 parts of polystyrene diol, 32-36 parts of walnut oil, 28-32 parts of zinc oxide powder, 32-36 parts of pine-soot ink, 28-32 parts of mica powder, 34-38 parts of polyacrylic acid emulsion, 28-32 parts of polyester carbamate resins, 32-36 parts of aluminum stearate, 28-32 parts of glyceryl stearate, 32-36 parts of octamethylcyclotetrasiloxane, 28-32 parts of acrylamide, 32-36 parts of phosalone, 28-32 parts of chlorhexidine, 32-36 parts of imidacloprid, 28-32 parts of tetramethrin, 32-36 parts of diafenthiuron and 1000-2000 parts of water. The preparation technology method is simple, and the prepared product has excellent waterproof anti-microbial mildew-resistant performances, has good flame retardant performance, and is suitable for usage in a plurality of fields. The product performances are improved, and the processing and usage are convenient.
Description
Technical field
The present invention relates to a kind of water proof fire retardant antibacterial and mouldproof pigment, belong to pigment formula technical field.
Background technology
Pigment is exactly the material that object can be made to catch color.Pigment have a solubility with insolubility, have inorganic and organically difference.Mineral dye is generally mineral material, and the mankind know use mineral dye very early, utilizes coloured soil and ore, crag is drawn a picture and smears health.Pigment dyestuff generally takes from plant and marine animal, as the purple that alizarin indigo plant, gamboge and ancient Roman refine from shellfish.
Summary of the invention
The object of the present invention is to provide a kind of water proof fire retardant antibacterial and mouldproof pigment, to realize the function of the antibacterial deinsectization of pigment water proof fire retardant better.
To achieve these goals, technical scheme of the present invention is as follows.
A kind of water proof fire retardant antibacterial and mouldproof pigment, be made up of the component of following mass fraction: 30 ~ 34 parts, vinylformic acid, ceramic glaze 32 ~ 36 parts, polystyrene glycol 28 ~ 32 parts, walnut oil 32 ~ 36 parts, zinc white 28 ~ 32 parts, pine-soot ink 32 ~ 36 parts, mica powder 28 ~ 32 parts, polyacrylate emulsion 34 ~ 38 parts, polyester urethane resin 28 ~ 32 parts, aluminum stearate 32 ~ 36 parts, glyceryl stearate 28 ~ 32 parts, octamethylcyclotetrasiloxane 32 ~ 36 parts, acrylamide 28 ~ 32 parts, kill sulphur P 32 ~ 36 part, Tubulicid 28 ~ 32 parts, Provado 32 ~ 36 parts, Tetramethrin 28 ~ 32 parts, diafenthiuron 32 ~ 36 parts, 1000 ~ 2000 parts, water.
Further, above-mentioned water proof fire retardant antibacterial and mouldproof pigment, is made up of the component of following mass fraction: 30 parts, vinylformic acid, ceramic glaze 32 parts, polystyrene glycol 28 parts, walnut oil 32 parts, zinc white 28 parts, pine-soot ink 32 parts, mica powder 28 parts, polyacrylate emulsion 34 parts, polyester urethane resin 28 parts, aluminum stearate 32 parts, glyceryl stearate 28 parts, octamethylcyclotetrasiloxane 32 parts, acrylamide 28 parts, kill sulphur P 32 part, Tubulicid 28 parts, Provado 32 parts, Tetramethrin 28 parts, diafenthiuron 32 parts, 1000 parts, water.
Further, above-mentioned water proof fire retardant antibacterial and mouldproof pigment, is made up of the component of following mass fraction: 32 parts, vinylformic acid, ceramic glaze 34 parts, polystyrene glycol 30 parts, walnut oil 34 parts, zinc white 30 parts, pine-soot ink 34 parts, mica powder 30 parts, polyacrylate emulsion 36 parts, polyester urethane resin 30 parts, aluminum stearate 34 parts, glyceryl stearate 30 parts, octamethylcyclotetrasiloxane 34 parts, acrylamide 30 parts, kill 34 parts, sulphur phosphorus, Tubulicid 30 parts, Provado 34 parts, Tetramethrin 30 parts, diafenthiuron 34 parts, 1500 parts, water.
Further, above-mentioned water proof fire retardant antibacterial and mouldproof pigment, is made up of the component of following mass fraction: 34 parts, vinylformic acid, ceramic glaze 36 parts, polystyrene glycol 32 parts, walnut oil 36 parts, zinc white 32 parts, pine-soot ink 36 parts, mica powder 32 parts, polyacrylate emulsion 38 parts, polyester urethane resin 32 parts, aluminum stearate 36 parts, glyceryl stearate 32 parts, octamethylcyclotetrasiloxane 36 parts, acrylamide 32 parts, kill 36 parts, sulphur phosphorus, Tubulicid 32 parts, Provado 36 parts, Tetramethrin 32 parts, diafenthiuron 36 parts, 2000 parts, water.
Further, above-mentioned water proof fire retardant antibacterial and mouldproof method for preparing pigment step is as follows:
(1) by the vinylformic acid of described mass fraction, polystyrene glycol, walnut oil, zinc white, pine-soot ink, mica powder, polyacrylate emulsion, aluminum stearate, glyceryl stearate, octamethylcyclotetrasiloxane, acrylamide, kill sulphur phosphorus, Tubulicid, Provado, Tetramethrin, diafenthiuron add in the water of above-mentioned mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20 ~ 40KHz, rate of dispersion about 5000 ~ 5400r/min, jitter time is 30 ~ 60min;
(2) add the polyester urethane resin of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20 ~ 35KHz, rate of dispersion about 4800 ~ 5200r/min, and jitter time is 30 ~ 50min;
(3) add the ceramic glaze of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20 ~ 30KHz, rate of dispersion about 4600 ~ 4800r/min, and jitter time is 20 ~ 40min; Mix this product that rear obtained solid content is about 20 ~ 70%.
Above-mentioned each component function is as follows:
(1) vinylformic acid: important organic synthesis raw material and synthetic resins monomer is polymerization velocity vinyl monomer quickly.Great majority are in order to manufacture the esters of acrylic acids such as methyl acrylate, ethyl ester, butyl ester, hydroxyl ethyl ester.
(2) ceramic glaze: classification and purposes can rough classification as follows: lead glaze and leadless glaze; Raw glaze and fritted glaze; Once-firing or twice firing glaze; Ceramic tile, tableware, snitaryware and electroceramics glaze; By enameling method divide leaching glaze, glaze spraying, water glaze; High melting glaze and low temperature glaze; High expansion glaze and Low Thermal Expantion Glaze; Coloured glaze and colourless glaze; Transparent and opaque glaze; Bright glaze, matt glaze, semi-mat glaze or figure glaze etc.
(3) polystyrene glycol: water-intake rate is extremely low is moistureproof and anti-permeability is splendid.
(4) walnut oil: light yellow transparent liquid, main component is unsaturated fatty acids.
(5) zinc white: there is good wear resistance, resistance to tearing and elasticity.In pigment industry, this product, except having tinting strength and opacifying power, is again the sanitas in pigment and luminous agent.
(6) pine-soot ink: thick ink is unglazed, matter is carefully easily ground.
(7) mica powder: ultrafine mica powder makes the functional fillers such as plastics, pigment, paint, rubber, can improve its physical strength, strengthens toughness, sticking power, anti-aging and erosion resistance etc.
(8) polyacrylate emulsion: thickening material, dispersion agent, flocculation agent, sizing agent and membrane-forming agent etc. can be made.Be widely used in the industry such as pigment, papermaking, weaving, oil recovery, mining, food, medicine, makeup and water treatment.
(9) polyester urethane resin: its goods have the excellent properties such as wear-resisting, heatproof, sealing, sound insulation, good processability, degradable.Purposes is very wide, can replace rubber, plastics, nylon etc.The pigment made has strong tackiness, and film has excellent wear resistance, water tolerance and resistance to chemical reagents etc.
(10) aluminum stearate: white or micro-yellow powder, water insoluble, ethanol, ether, be dissolved in alkali, turps, Dormant oils, oil, kerosene and benzene equal solvent.As thermo-stabilizer and the lubricant of igelite, the anti-settling agent of paint industry, siccative, the water-resisting agent of fabric, the intensifier etc. of lubricating oil.
(11) glyceryl stearate: for the emulsifying agent of industrial yarn finish and the lubricant of textiles; Drip agent and antifogging agent is used as in plastics film; In plastic working, make lubricant and static inhibitor, can be used as defoamer, dispersion agent, thickening material, wetting agent etc. in other respects.
(12) octamethylcyclotetrasiloxane: main application comprises Organosilicon Polymers such as preparing methyl-silicone oil, the insulation of radio components and protection against the tide, gas-chromatography glass capillary column surface deactivator etc.
(13) acrylamide: be mainly used in water purification process, the processing of paper pulp and the undercoat etc. of pipeline, also for polyacrylamide gel electrophoresis.
(14) kill sulphur phosphorus: killing insects by touching, miticide, without systemic action, insecticidal spectrum is wide, and the lasting period is long, and meta-bolites still has an insecticidal activity.
(15) Tubulicid: have great broad-spectrum antibacterial, germicidal action is a kind of sterilization and disinfection medicine preferably, to the anti-microbial effect of Gram-positive and negative bacterium, stronger than Herb of Common violet such as bromogeramine, even if still effective when having serum, blood etc. to exist.
(16) Provado: nicotinoids ultra-high efficiency sterilant, have wide spectrum, efficient, low toxicity, low residue, insect not easily produces resistance, to features such as people, animal, plant and natural enemies securities, and have tag, the multiple action such as stomach toxicity and interior suction.
(17) Tetramethrin: a kind of powerful synthetic pesticide, belongs to pyrethroid.The fusing point of this white crystalline solid is 65-80 degree Celsius.Its mixing steric isomer is applied to commerical prod.Be generally used for manufacturing sterilant, it can affect the central nervous system of insect.To the sanitary insect pest such as mosquito, fly, there is quick down effect, but lethal poor performance, there is anabiosis, therefore will use with the medicament mixture of other good disinsection effect.
(18) diafenthiuron: a kind of new sulfur ureas efficient insecticide, miticide, have tag, stomach toxicity, interior suction and fumigation action, and there is certain ovicidal effect.Low toxicity, but to fish, the high poison of honeybee.Changing the material with insecticidal activity under ultraviolet light into, to vegetables having produced serious drug-fast insect, there is stronger activity.The aphid on various crop and ornamental plant, aleyrodid, leafhopper, noctuidae pests and evil mite can be prevented and treated.
This beneficial effect of the invention is: this water proof fire retardant antibacterial and mouldproof pigment process of preparing is simple, prepared product has comparatively superior water-proof antibiotic fungicidal properties, and flame retardant properties is better, is adapted at multiple fields and uses, improve product performance, process easy to use.
Embodiment
Below in conjunction with embodiment, the specific embodiment of the present invention is described, better to understand the present invention.
embodiment 1
Water proof fire retardant antibacterial and mouldproof pigment in the present embodiment, is made up of the component of following mass fraction: 30 parts, vinylformic acid, ceramic glaze 32 parts, polystyrene glycol 28 parts, walnut oil 32 parts, zinc white 28 parts, pine-soot ink 32 parts, mica powder 28 parts, polyacrylate emulsion 34 parts, polyester urethane resin 28 parts, aluminum stearate 32 parts, glyceryl stearate 28 parts, octamethylcyclotetrasiloxane 32 parts, acrylamide 28 parts, kill sulphur P 32 part, Tubulicid 28 parts, Provado 32 parts, Tetramethrin 28 parts, diafenthiuron 32 parts, 1000 parts, water.
Above-mentioned water proof fire retardant antibacterial and mouldproof method for preparing pigment step is as follows:
(1) by the vinylformic acid of described mass fraction, polystyrene glycol, walnut oil, zinc white, pine-soot ink, mica powder, polyacrylate emulsion, aluminum stearate, glyceryl stearate, octamethylcyclotetrasiloxane, acrylamide, kill sulphur phosphorus, Tubulicid, Provado, Tetramethrin, diafenthiuron add in the water of above-mentioned mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20kHz, rate of dispersion about 5400r/min, jitter time is 60min;
(2) add the polyester urethane resin of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20kHz, rate of dispersion about 5200r/min, and jitter time is 50min;
(3) add the ceramic glaze of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20kHz, rate of dispersion about 4800r/min, and jitter time is 40min; Mix this product that rear obtained solid content is about 20%.
embodiment 2
Water proof fire retardant antibacterial and mouldproof pigment in the present embodiment, is made up of the component of following mass fraction: 32 parts, vinylformic acid, ceramic glaze 34 parts, polystyrene glycol 30 parts, walnut oil 34 parts, zinc white 30 parts, pine-soot ink 34 parts, mica powder 30 parts, polyacrylate emulsion 36 parts, polyester urethane resin 30 parts, aluminum stearate 34 parts, glyceryl stearate 30 parts, octamethylcyclotetrasiloxane 34 parts, acrylamide 30 parts, kill 34 parts, sulphur phosphorus, Tubulicid 30 parts, Provado 34 parts, Tetramethrin 30 parts, diafenthiuron 34 parts, 1500 parts, water.
Above-mentioned water proof fire retardant antibacterial and mouldproof method for preparing pigment step is as follows:
(1) by the vinylformic acid of described mass fraction, polystyrene glycol, walnut oil, zinc white, pine-soot ink, mica powder, polyacrylate emulsion, aluminum stearate, glyceryl stearate, octamethylcyclotetrasiloxane, acrylamide, kill sulphur phosphorus, Tubulicid, Provado, Tetramethrin, diafenthiuron add in the water of above-mentioned mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 30kHz, rate of dispersion about 5200r/min, jitter time is 45min;
(2) add the polyester urethane resin of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 27kHz, rate of dispersion about 5000r/min, and jitter time is 40min;
(3) add the ceramic glaze of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 25kHz, rate of dispersion about 4700r/min, and jitter time is 30min; Mix this product that rear obtained solid content is about 35%.
embodiment 3
Water proof fire retardant antibacterial and mouldproof pigment in the present embodiment, is made up of the component of following mass fraction: 34 parts, vinylformic acid, ceramic glaze 36 parts, polystyrene glycol 32 parts, walnut oil 36 parts, zinc white 32 parts, pine-soot ink 36 parts, mica powder 32 parts, polyacrylate emulsion 38 parts, polyester urethane resin 32 parts, aluminum stearate 36 parts, glyceryl stearate 32 parts, octamethylcyclotetrasiloxane 36 parts, acrylamide 32 parts, kill 36 parts, sulphur phosphorus, Tubulicid 32 parts, Provado 36 parts, Tetramethrin 32 parts, diafenthiuron 36 parts, 2000 parts, water.
Above-mentioned water proof fire retardant antibacterial and mouldproof method for preparing pigment step is as follows:
(1) by the vinylformic acid of described mass fraction, polystyrene glycol, walnut oil, zinc white, pine-soot ink, mica powder, polyacrylate emulsion, aluminum stearate, glyceryl stearate, octamethylcyclotetrasiloxane, acrylamide, kill sulphur phosphorus, Tubulicid, Provado, Tetramethrin, diafenthiuron add in the water of above-mentioned mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 40kHz, rate of dispersion 5000r/min, jitter time is 30min;
(2) add the polyester urethane resin of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 35kHz, rate of dispersion 4800r/min, and jitter time is 30min;
(3) add the ceramic glaze of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 30kHz, rate of dispersion about 4600r/min, and jitter time is 20min; Mix this product that rear obtained solid content is about 70%.
Carry out performance measurement for the pigment in embodiment 1, embodiment 2 and embodiment 3 and certain commercially available pigment, measured data are as shown in table 1.Fire protection flame retarding level estimate adopts UL94 standard.
Table 1 the performance test results
Table 1 the performance test results
Visible, material of the present invention has good fire protection flame retarding, waterproof, antibacterial and mouldproof performance.
The above is the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention; can also make some improvements and modifications, these improvements and modifications are also considered as protection scope of the present invention.
Claims (5)
1. a water proof fire retardant antibacterial and mouldproof pigment, it is characterized in that: be made up of the component of following mass fraction: 30 ~ 34 parts, vinylformic acid, ceramic glaze 32 ~ 36 parts, polystyrene glycol 28 ~ 32 parts, walnut oil 32 ~ 36 parts, zinc white 28 ~ 32 parts, pine-soot ink 32 ~ 36 parts, mica powder 28 ~ 32 parts, polyacrylate emulsion 34 ~ 38 parts, polyester urethane resin 28 ~ 32 parts, aluminum stearate 32 ~ 36 parts, glyceryl stearate 28 ~ 32 parts, octamethylcyclotetrasiloxane 32 ~ 36 parts, acrylamide 28 ~ 32 parts, kill sulphur P 32 ~ 36 part, Tubulicid 28 ~ 32 parts, Provado 32 ~ 36 parts, Tetramethrin 28 ~ 32 parts, diafenthiuron 32 ~ 36 parts, 1000 ~ 2000 parts, water.
2. water proof fire retardant antibacterial and mouldproof pigment according to claim 1, it is characterized in that: described water proof fire retardant antibacterial and mouldproof pigment is made up of the component of following mass fraction: 30 parts, vinylformic acid, ceramic glaze 32 parts, polystyrene glycol 28 parts, walnut oil 32 parts, zinc white 28 parts, pine-soot ink 32 parts, mica powder 28 parts, polyacrylate emulsion 34 parts, polyester urethane resin 28 parts, aluminum stearate 32 parts, glyceryl stearate 28 parts, octamethylcyclotetrasiloxane 32 parts, acrylamide 28 parts, kill sulphur P 32 part, Tubulicid 28 parts, Provado 32 parts, Tetramethrin 28 parts, diafenthiuron 32 parts, 1000 parts, water.
3. according to the water proof fire retardant antibacterial and mouldproof pigment described in claim 1 to 2, it is characterized in that: described water proof fire retardant antibacterial and mouldproof pigment is made up of the component of following mass fraction: 32 parts, vinylformic acid, ceramic glaze 34 parts, polystyrene glycol 30 parts, walnut oil 34 parts, zinc white 30 parts, pine-soot ink 34 parts, mica powder 30 parts, polyacrylate emulsion 36 parts, polyester urethane resin 30 parts, aluminum stearate 34 parts, glyceryl stearate 30 parts, octamethylcyclotetrasiloxane 34 parts, acrylamide 30 parts, kill 34 parts, sulphur phosphorus, Tubulicid 30 parts, Provado 34 parts, Tetramethrin 30 parts, diafenthiuron 34 parts, 1500 parts, water.
4. the water proof fire retardant antibacterial and mouldproof pigment according to claims 1 to 3, it is characterized in that: described water proof fire retardant antibacterial and mouldproof pigment is made up of the component of following mass fraction: 34 parts, vinylformic acid, ceramic glaze 36 parts, polystyrene glycol 32 parts, walnut oil 36 parts, zinc white 32 parts, pine-soot ink 36 parts, mica powder 32 parts, polyacrylate emulsion 38 parts, polyester urethane resin 32 parts, aluminum stearate 36 parts, glyceryl stearate 32 parts, octamethylcyclotetrasiloxane 36 parts, acrylamide 32 parts, kill 36 parts, sulphur phosphorus, Tubulicid 32 parts, Provado 36 parts, Tetramethrin 32 parts, diafenthiuron 36 parts, 2000 parts, water.
5. the water proof fire retardant antibacterial and mouldproof pigment according to claim 1 or 4, is characterized in that: described water proof fire retardant antibacterial and mouldproof method for preparing pigment step is as follows:
(1) by the vinylformic acid of described mass fraction, polystyrene glycol, walnut oil, zinc white, pine-soot ink, mica powder, polyacrylate emulsion, aluminum stearate, glyceryl stearate, octamethylcyclotetrasiloxane, acrylamide, kill sulphur phosphorus, Tubulicid, Provado, Tetramethrin, diafenthiuron add in the water of above-mentioned mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20 ~ 40KHz, rate of dispersion about 5000 ~ 5400r/min, jitter time is 30 ~ 60min;
(2) add the polyester urethane resin of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20 ~ 35KHz, rate of dispersion about 4800 ~ 5200r/min, and jitter time is 30 ~ 50min;
(3) add the ceramic glaze of described mass fraction, ultrasonic high speed dispersion, ultrasonic frequency is 20 ~ 30KHz, rate of dispersion about 4600 ~ 4800r/min, and jitter time is 20 ~ 40min; Mix this product that rear obtained solid content is about 20 ~ 70%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510560097.6A CN105131484A (en) | 2015-09-07 | 2015-09-07 | Waterproof flame retardant anti-microbial mildew-resistant pigment |
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| CN201510560097.6A CN105131484A (en) | 2015-09-07 | 2015-09-07 | Waterproof flame retardant anti-microbial mildew-resistant pigment |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106147333A (en) * | 2016-07-20 | 2016-11-23 | 新乡学院 | A kind of dubbin paint |
| CN106496972A (en) * | 2016-11-18 | 2017-03-15 | 佛山市天顺科技有限公司 | A kind of multifunction power safeguards glove material |
| CN108034355A (en) * | 2018-01-15 | 2018-05-15 | 傅雨菲 | A kind of blueness oil painting composite pigment and its preparation method and application |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1045014A2 (en) * | 1999-04-16 | 2000-10-18 | MERCK PATENT GmbH | Pigment mixture |
| CN102503567A (en) * | 2011-10-12 | 2012-06-20 | 上海高诚艺术包装有限公司 | Wood grain glaze as well as preparation method and using method thereof |
| CN104592797A (en) * | 2015-01-24 | 2015-05-06 | 南阳理工学院 | Formula of quick-drying water-proof art painting paint |
-
2015
- 2015-09-07 CN CN201510560097.6A patent/CN105131484A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1045014A2 (en) * | 1999-04-16 | 2000-10-18 | MERCK PATENT GmbH | Pigment mixture |
| CN102503567A (en) * | 2011-10-12 | 2012-06-20 | 上海高诚艺术包装有限公司 | Wood grain glaze as well as preparation method and using method thereof |
| CN104592797A (en) * | 2015-01-24 | 2015-05-06 | 南阳理工学院 | Formula of quick-drying water-proof art painting paint |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106147333A (en) * | 2016-07-20 | 2016-11-23 | 新乡学院 | A kind of dubbin paint |
| CN106496972A (en) * | 2016-11-18 | 2017-03-15 | 佛山市天顺科技有限公司 | A kind of multifunction power safeguards glove material |
| CN108034355A (en) * | 2018-01-15 | 2018-05-15 | 傅雨菲 | A kind of blueness oil painting composite pigment and its preparation method and application |
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