CN1051164A - A kind of forming method of black ceramic plate used in building decoration - Google Patents

A kind of forming method of black ceramic plate used in building decoration Download PDF

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Publication number
CN1051164A
CN1051164A CN 89106840 CN89106840A CN1051164A CN 1051164 A CN1051164 A CN 1051164A CN 89106840 CN89106840 CN 89106840 CN 89106840 A CN89106840 A CN 89106840A CN 1051164 A CN1051164 A CN 1051164A
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CN
China
Prior art keywords
ceramic plate
black ceramic
forming method
pug
building decoration
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Pending
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CN 89106840
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Chinese (zh)
Inventor
王树忠
王振林
李永光
白桂福
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ZHUCHENG CERAMICS FACTORY SHANDONG PROV
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ZHUCHENG CERAMICS FACTORY SHANDONG PROV
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Priority to CN 89106840 priority Critical patent/CN1051164A/en
Publication of CN1051164A publication Critical patent/CN1051164A/en
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  • Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)

Abstract

A kind of forming method whole process of black ceramic plate of architectural decoration comprises that (1) ingredient inspection (2) batching (3) pulverizes (4) and stir (5) filter mud (6) old (7) puggings (8) cutting (9) extrusion moldings (10) dry (11) and burn till (12) polishing check; The present invention has mechanize, serialization degree height, and labour intensity is little, labour productivity height, the advantage that product percent of pass is high; The high-grade construction decoration material that " black ceramic plate " that present method is produced is a kind of hardness height, thin thickness, color is shiny black, glossiness is high.

Description

A kind of forming method of black ceramic plate used in building decoration
The invention belongs to the forming method of porcelain finishing material for building, the forming method of more definite a kind of black ceramic plate used in building decoration of saying so.
The black decorative porcelain is a kind of high-grade finishing material, and it is mainly used in decorative wall, floor and puts the platform of instrument; Sometimes also available its unit's of manufacturing famous brand.
The forming method of porcelain decorative sheet mainly contains two kinds at present:
1. slip casting: the main drawback of this kind method is: (1) takes up an area of many, needs the gypsum mold amount big, (2) are interrupted production technique, manual operations is many, the production cycle long, labour intensity greatly, labour productivity and product percent of pass be all low.
2. shaping method to suppress: the shortcoming of this kind method is that product percent of pass is low.
Task of the present invention be study that successfully a kind of production technique mechanize serialization degree is higher, labour intensity is little, floor space is little, labour productivity and all high processing method of manufacturing the black decorative porcelain of product percent of pass.
Content of the present invention:
Accompanying drawing is a process flow sheet of the present invention.With reference to accompanying drawing that detailed description of the present invention is as follows:
1. the inspection of raw and process materials:
At first test to the present invention is raw materials used, make every kind of raw material must reach following index request, can put into production use:
(1) tailings in vanadium extraction: contain Fe 2O 3: 54.04~64.42%, TiO 2: 5.94~8.58%, V 2O 5: 0.92~1.7%, MnO:4.14~6.74%.Cr 2O 5: 0.02~2.14%.
(2) clay: contain SiO 2〉=52%, Al 2O 3〉=30%.
(3) talcum powder: contain MgO 〉=30%, Fe 2O 3+ TiO 2≤ 0.3%.
(4) bowl kiln hood soil: contain SiO 2〉=53%, Al 2O 3〉=30%.
(5) laterite: contain SiO 2〉=58%, Al 2O 3〉=16%.
2. prepare burden:
To prepare burden by following prescription through " ingredient inspection " qualified raw material; Batching error requirements≤± 5%,
Prescription: tailings in vanadium extraction: 65%, clay: 11%, talcum powder: 3%, bowl kiln hood soil: 11%, laterite: 10%.
3. pulverize:
In 1.5 tons of ball mills of packing into of qualified batching that will transfer from " batching ", then in material: ball: the ratio of water=1: 2: 1.8 adding ballstone and water in the ball mill.After adding, start ball mill again, its rotating speed is controlled in 23 ± 2 rev/mins of scopes.Material is pulverized.When the pulverizing time reaches 10 ± 0.5 hours, it is stopped operating, will pulverize and expect that storage was good standby behind 80~120 mesh sieves.
4. stir:
To put into suction pit by the qualified mud that " pulverizing " transfers, even in order to make pug, in suction pit with stirrer stir be no less than 20 minutes after, stop to stir, mud has stored up standby.
5. filter mud:
The mud that " stirring " is good carries out press filtration with pressure filter, is qualified mud cake when moisture content is 20 ± .5%.
6. old:
To send into room temperature from the qualified pug that " filter mud " transfers is to carry out " old " 20-35 ℃ the pug worker-house, and after the old time reached 24-48 hour, pug can change down and uses.
7. pugging:
To put into " vacuum deairing machine " that vacuum tightness is 750 ± 10 millimeter water column through " old " qualified pug, and pug be carried out " pugging " handle twice.
8. cutting:
To handle qualified pug through " pugging ", with " single-lead-screw extruding briquetting machine knife plate cutter " on request size (general requirement cut into 600 millimeters rectangular) cut.
9. extrusion molding:
The strip pug that " cutting " is good, by being that 280 millimeters rollers of φ are formed by diameter, rotating speed is 3 meter per seconds " two roll presses ", through after four compactings more in accordance with regulations size (general base substrate dimensional requirement is: length * wide * thick=605 ± 5 * 404 ± 5 * 11 ± 2 millimeter) cut, promptly get " base substrate " of manufacturing black ceramic plate.
10. dry:
" base substrate " of " extrusion molding " sent in the oven dry road, and dry under 40 °~60 ℃ temperature 〉=48 hours, dried " base substrate " requires not ftracture moisture content≤4%.
11. burn till:
Qualified " base substrate " that drying is good sent in 42 meters long " coal electricity mix roller kiln " and burnt till, and top temperature is 1060~1100 ℃ in the kiln, and firing time is 108~120 minutes; " base substrate " after burning till requires to be forbidden that cracking is arranged, gives birth to defectives such as burning, burning and bubble.
12. the qualified product after will " burning till ", polish by polishing machine again, the polishing time is five minutes, and the product behind the mill is tested by DB/3707 Q32001~88 specified standardss, is " decorate and use black ceramic plate " that the present invention will manufacture through goods after the assay was approved.
" decorate and use black ceramic plate " that the present invention is made, its shape is regular, be rectangle, the quality exquisiteness, look black, and hardness (Morse) is that 8(is higher by 2 than artificial granite stone), glossiness is (stonite's glossiness is 60 degree) more than 80 degree, surface-brightening is like mirror, thereby porcelain decorative plate is a kind of ideal flawless finish material of construction.
The present invention has following advantage and characteristics:
1. mechanize of the present invention, serialization degree height has been saved large quantities of labor forces.
Because of whole process of the present invention is mechanize and serialization production substantially, therefore large quantities of labor forces have been saved, for example: produce 40000 meters per year 2Black porcelain plate can be saved 50 people.
2. alleviate labour intensity, improved labour productivity:
Because of each operation of the present invention realizes power operation substantially, so that the operator from the manual work of heaviness, free.Also because of the present invention has realized mechanize substantially, serialization production so shortened the production cycle, has improved labour productivity.
For example: it is 1/3~1/4 of shaping method to suppress that the present invention whenever manufactures a used time of black ceramic plate.The present invention manufacture 1 used time of black ceramic plate only be " slip casting " 1/60.
3. improved product percent of pass
Product percent of pass of the present invention is up to more than 80%, and the product percent of pass of " slip casting " is only 70%, and the product percent of pass of " shaping method to suppress " is 75%.
4. the present invention is taken up an area of less, can save a large amount of gypsum molds.
To produce 40000 meters per year 2The production line of black ceramic plate is an example, and main worker-house of the present invention takes up an area of 450 meters 2, " slip casting " main worker-house takes up an area of 700 meters 2, " shaping method to suppress " main worker-house takes up an area of 600 meters 2; Use the present invention can save more than 1000 gypsum mold.
Most preferred embodiment:
1. technological process: " Figure of description " is process flow sheet of the present invention.
Referring now to accompanying drawing, the present embodiment technological process is described below:
(1). will prepare burden by following " prescription " through " ingredient inspection " qualified raw material:
The prescription: the batching error be≤± 5%.
Tailings in vanadium extraction: 65%, clay: 11%, talcum powder: 3%,
Bowl kiln hood soil: 11%, laterite: 10%,
(2). 1.5 tons of the blanks that will prepare by " prescription ", the model of packing into is in 2100 * 1800 the ball mill, then in material: ball: the ratio of water=1: 2: 1.8 in the ball mill adding ballstone and water when all adding, starting ball mill, to make rotating speed be 23 ± 2 rev/mins, when the ball milling time reaches 10 hours, it is stopped operating.
(3) will send in the suction pit with stirrer with " ball mill pulverizing " good pug and stir 15 minutes, and stop to stir, pug is stand-by.
(4) pug that will stir in " suction pit " carries out press filtration with pressure filter moisture content reaches at 20 ± 1.5% o'clock in the pug to making, and promptly stops press filtration, and mud cake is stand-by.
(5) mud cake that press filtration is qualified was sent into room temperature and is in 20~35 ℃ the pug worker-house " old " 48 hours.
(6) old 48 hours pug being put into vacuum tightness is that " vacuum deairing machine " of 750 ± 10 millimeter water column handled pug twice totally.
(7) will in " pug mill ", handle qualified pug and pug be cut into 600 millimeters rectangular with " single-lead-screw extruding briquetting machine knife plate cutter ".
(8) will send into diameter by the rectangular pug of " extrusion molding knife plate cutter " cutting is that 280 millimeters rollers of φ are formed, rotating speed is 3 meter per seconds " two roll presses ", after four compactings, by long * wide * thick=605 ± 5 * 404 ± 5 * 11 ± 2 mm sizes cutting, the moulded pottery not yet put in a kiln to bake after the cutting promptly is the required base substrate of black ceramic plate again.
(9) will be through " two roll press " compacting back and cut into " base substrate " of certain size again, sent into 50 ± 10 ℃ of oven dry inherences, road dry 48 hours down, moisture content≤4% is not ftractureed in dried base substrate requirement.
(10) 48 hours qualified base substrates of drying are sent into 42 meters long, maximum sintering temperature is to burn till in 1100 ℃ " the coal electricity is in conjunction with roller kiln ", firing time is 110 minutes, and the base substrate after burning till requires to be forbidden that cracking is arranged, gives birth to problems such as burning, burning and bubble.
(11) will polish with polishing machine through the salable product after burning till and reach mirror-like to product in five minutes, and then, test by DB/3707Q32001~88 standards, qualified back product is qualified product of the present invention.
2. effect:
The described decoration of this most preferred embodiment with the forming method of black ceramic plate except that this method itself has mechanize, serialization degree height, labour productivity height, product percent of pass height, labour intensity is little and the production line floor space little, the product that this method system is carried also has following advantage and characteristics: black ceramic plate is the oblong-shaped of rule, surface-brightening such as mirror, hardness (Mohs) is up to 8, and the folding strength height is (greater than 400Kg/cm 2), water-intake rate low (≤0.3%), glossiness height (more than 80 degree), Heat stability is good (20~150 ℃ of heat exchanges are not fried).The prepared black ceramic plate of embodiment is a kind of high-grade architectural constructional materials in summary.

Claims (12)

1, a kind of forming method of black ceramic plate used in building decoration is characterized in that this method comprises (1) ingredient inspection, (2) batching, (3) pulverize, stir (4), (5) filter mud, (6) old, (7) pugging, (8) cutting, (9) extrusion molding, (10) drying, (11) burn till (12) polishing, check.
2, the forming method according to the described a kind of black ceramic plate used in building decoration of claim 1 is characterized in that (2) batching in this method is to allocate by following prescription through " ingredient inspection " qualified raw material:
Prescription: batching error requirements≤± 5%.
Tailings in vanadium extraction: 65%, clay: 11%, laterite: 10%,
Talcum powder: 3%, bowl kiln hood soil: 11%,
3, it is characterized in that according to the forming method of the described a kind of black ceramic plate used in building decoration of claim 1 (3) in this method pulverize, be will be from the deployed pug that " batching " transfers is packed ball mill into, then in material: ball: the ratio of water=1: 2: 1.8 adds ballstone and water again in ball mill, after all adding, start ball mill, make its rotating speed be 23 ± 2 rev/mins material carried out " pulverizing ", reach 10 ± 0.5 hours when the ball milling time, ball mill is stopped operating, and will expect 80~120 mesh sieves, then material is stored for future use.
4, according to the forming method of the described a kind of black ceramic plate used in building decoration of claim 1, it is characterized in that stir (4) in this method is to put into suction pit through " pulverizings " qualified pug, mix the machine stirring and be not less than 20 minutes with stirring to tremble.
5, according to the forming method of the described a kind of black ceramic plate used in building decoration of claim 1, it is characterized in that (5) filter mud in this method, to be pug that " stirring " is good carry out press filtration moisture content to the pug with pressure filter is to be qualified " mud cake " at 20 ± 1.5% o'clock.
6, according to the forming method of the described a kind of black ceramic plate used in building decoration of claim 1 it is characterized in that (6) in this method old be that the qualified pug that transfers from " filter mud " is sent into room temperature is to carry out " old " 20~35 ℃ the pug worker-house, the old time is 〉=24 hours.
7, it is characterized in that (7) pugging in this method according to the forming method of the described a kind of black ceramic plate used in building decoration of claim 2, is to be that " vacuum deairing machine " of 750 ± 10 millimeter water column carries out " pugging " to pug and handle twice with put into vacuum tightness through old qualified pug.
8, it is characterized in that (8) cutting in this method according to the forming method of the described a kind of black ceramic plate used in building decoration of claim 1, is to handle qualified pug through " pugging " with " single-lead-screw extruding briquetting machine knife plate cutter " size cut growth strip as requested.
9, it is characterized in that (9) extrusion molding in this method according to the forming method of wanting the described a kind of black ceramic plate used in building decoration of claim 1, be will be " cutting " pug into strips, by being that 280 millimeters rollers of φ are formed by diameter, rotating speed is 3 meter per seconds " two roll presses ", through four times the compacting after more in accordance with regulations size cut into needed porcelain plate base substrate.
10, it is characterized in that (10) drying in this method according to the described a kind of forming method of decorating with black ceramic plate of claim 1, is that the base substrate of " extrusion molding " is sent in the oven dry road, dry more than 48 hours under 40~60 ℃ the temperature.
11, it is characterized in that according to the described a kind of forming method of decorating with black ceramic plate of claim 1 (11) in this method burn till, be the base substrate after " drying " to be sent in " the coal electricity is in conjunction with roller kiln " burn till, the kiln highest temperature is 1060~1100 ℃, firing time is 108~120 minutes
12, it is characterized in that (12) polishing, check in this method according to the forming method of the black ceramic plate of the described a kind of architectural decoration of claim 1, is the goods that will " burn till ", polishes by polishing machine again, and the polishing time is five minutes; Grinded product standard is in accordance with regulations tested.
CN 89106840 1989-10-21 1989-10-21 A kind of forming method of black ceramic plate used in building decoration Pending CN1051164A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 89106840 CN1051164A (en) 1989-10-21 1989-10-21 A kind of forming method of black ceramic plate used in building decoration

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 89106840 CN1051164A (en) 1989-10-21 1989-10-21 A kind of forming method of black ceramic plate used in building decoration

Publications (1)

Publication Number Publication Date
CN1051164A true CN1051164A (en) 1991-05-08

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CN 89106840 Pending CN1051164A (en) 1989-10-21 1989-10-21 A kind of forming method of black ceramic plate used in building decoration

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102363316A (en) * 2011-06-30 2012-02-29 德清县建明坩埚厂 Clay crucible forming method
CN106631043A (en) * 2015-11-02 2017-05-10 曾建平 Superior ultrathin white ceramic plate and manufacturing process thereof
CN112939567A (en) * 2019-12-11 2021-06-11 辽宁省轻工科学研究院有限公司 Black ceramic tile prepared by using vanadium extraction tailings and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102363316A (en) * 2011-06-30 2012-02-29 德清县建明坩埚厂 Clay crucible forming method
CN106631043A (en) * 2015-11-02 2017-05-10 曾建平 Superior ultrathin white ceramic plate and manufacturing process thereof
CN112939567A (en) * 2019-12-11 2021-06-11 辽宁省轻工科学研究院有限公司 Black ceramic tile prepared by using vanadium extraction tailings and preparation method thereof

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