CN105088743A - Preparation method for negative ion bamboo carbon fiber textile fabric - Google Patents
Preparation method for negative ion bamboo carbon fiber textile fabric Download PDFInfo
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- CN105088743A CN105088743A CN201510584708.0A CN201510584708A CN105088743A CN 105088743 A CN105088743 A CN 105088743A CN 201510584708 A CN201510584708 A CN 201510584708A CN 105088743 A CN105088743 A CN 105088743A
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Abstract
The invention relates to a preparation method for a negative ion bamboo carbon fiber textile fabric, and belongs to the technical field of processing of textile products. The preparation method comprises the following steps: taking the middle four sections of a moso bamboo, and splitting up and cutting into bamboo strips; after the bamboo strips are insolated under the sunshine and yellowed, performing preliminary carbonization, and performing twice heating, heat preservation and the like to form a bamboo carbon material; grinding the bamboo carbon material in an efficient nano ball grinding machine to form nano bamboo carbon fiber particles, mixing the activated nano bamboo carbon fiber particles and substances such as CaCl2 to form a bamboo carbon fiber coagulating bath turbidity solution, finally putting fibers to be spun into the bamboo carbon fiber coagulating bath turbidity solution to finally form preliminary bamboo carbon fibers, and performing stretching, sizing, drying and oiling. The preparation method has the beneficial effects that the effects of germ removal, insect prevention and health protection are achieved; inorganic substance negative ions are uniformly dispersed in the fibers, so that the negative ion bamboo carbon fiber textile fabric is high in wearability and firmness; the process of the preparation technology is simple, and the cost is low.
Description
Technical field
The present invention relates to a kind of preparation method of anion bamboo-carbon fibre weaving face fabric, belong to textile processing technical field.
Background technology
Functional anion textile is researched and developed successfully at first by Japan, and it integrates negative ion-releasing function, far-infrared radiation, antibacterial, antibacterial, deodorizing, removes the several functions such as peculiar smell, anti-electromagnetic-radiation, is a kind of high-tech product.The formation of this product relies in fiber production process or in fabric finishing process, with the addition of a kind of pure natural mineral additive, and its main component is a kind of negative ion of typical polar crystal structure.It is a kind of far-infrared radiation material be highly profitable to health.
Along with the development of anion-generating material, greatly widen Negative ionic textile and put into Application Areas.The anionic plus material developed has the advantages such as, water-wash resistance good, anion generation successful soft with skin contact, be widely used in taking, household with and medical etc.Anion weaving face fabric it can promote blood circulation of human body, help for sleep, there is the health-care effect of product more.But, also there is the place in not evening and problem anxious to be resolved, inorganic matter anion generation particulate dispersing uniformity in the fibre, fastness, the problem that durability is all not high.
Summary of the invention
The technical problem that the present invention mainly solves: for current inorganic matter anion generation particulate dispersing uniformity in the fibre, easily lump in the fibre, drop, cause inorganic matter anion generation particulate cannot the problem of effective for a long time anion releasing, provide a kind of preparation method of anion bamboo-carbon fibre weaving face fabric, mao bamboon is heated by the method repeatedly, charing, calcining, form anion bamboo-carbon fibre, weaving face fabric is made again with it, in the weaving face fabric that the present invention obtains with anion have degerming, desinsection, the effect of health care, simultaneously inorganic matter anion being uniformly dispersed in the fibre, there is ABRASION RESISTANCE and fastness.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention:
(1) the growth mao bamboon of more than 4 years is got, broken apart by chopping from root 1 ~ 2m place, four whole joints are taken again apart from 2 ~ 3m place of the place of breaking apart by chopping, rived and cut off and grown into 5cm, thick is the thin bamboo strips used for weaving of 2 ~ 3mm, tan by the sun 20 ~ 30 days in the sun, after preliminarily dried to yellowish, thin bamboo strips used for weaving is collected at being placed in 100 ~ 150 DEG C and dry 2 ~ 3h;
(2) after thin bamboo strips used for weaving is dried, be placed in 150 ~ 270 DEG C of Muffle furnaces and tentatively carbonize, control time is 5 ~ 8h, after preliminary charing, again slowly heat up with the speed of 10 DEG C/min, 270 ~ 450 DEG C to be achieved, pass into after nitrogen to pressure is 1 ~ 2MPa to it, insulation makes it carbonize 8 ~ 10h completely, form bamboo charcoal, finally slowly heat up with the speed of 10 DEG C/min again, after 450 ~ 600 DEG C to be achieved, bamboo charcoal after carbonizing completely is incubated calcining 3 ~ 5h, and after calcining completes, make it naturally cool to 20 ~ 30 DEG C can be worth bamboo charcoal material;
(3) milled in efficient nano ball mill by above-mentioned bamboo charcoal material, mill 3 ~ 5h repeatedly, forms the nanometer bamboo carbon fiber particle that particle size is 5 ~ 10 μm, subsequently the nanometer bamboo carbon fiber particle of preparation is activated 2 ~ 3h at 700 ~ 900 DEG C;
(4) by mass percentage, the nanometer bamboo carbon fiber particle of the above-mentioned preparation of 5 ~ 10% is chosen, the CaCl of 7 ~ 9%
2, 10 ~ 11%KCl becomes the turbid liquid of bamboo-carbon fibre coagulating bath with the water of 60 ~ 70% with the dispersant proportioning of 8 ~ 10%; Described dispersant counts the sodium pyrophosphate mixed dispersant of the sodium phosphate trimer of 40 ~ 50 parts, the calgon of 10 ~ 25 parts and 25 ~ 50 parts by weight;
(5) by the fiber of required weaving by the turbid liquid of bamboo-carbon fibre coagulating bath, finally form bamboo-carbon fibre as-spun fibre, more stretched, sizing and drying oil, and can weave and form a kind of anion bamboo-carbon fibre weaving face fabric.
application of the present invention: the anion bamboo-carbon fibre weaving face fabric obtained by the present invention can be applicable to the field such as clothes, household bedding, and no matter the product made is in use, still lays up, all can not be mouldy, infested, has insect protected effect.
The invention has the beneficial effects as follows:
(1) have degerming, effect of insect protected and health care;
(2) inorganic matter anion being uniformly dispersed in the fibre, has ABRASION RESISTANCE and fastness;
(3) manufacture craft process is simple, and required cost is low.
Detailed description of the invention
Get the growth mao bamboon of more than 4 years, broken apart by chopping from root 1 ~ 2m place, four whole joints are taken again apart from 2 ~ 3m place of the place of breaking apart by chopping, rived and cut off and grown into 5cm, thick is the thin bamboo strips used for weaving of 2 ~ 3mm, tan by the sun 20 ~ 30 days in the sun, after preliminarily dried to yellowish, thin bamboo strips used for weaving is collected at being placed in 100 ~ 150 DEG C and dry 2 ~ 3h; After thin bamboo strips used for weaving is dried, be placed in 150 ~ 270 DEG C of Muffle furnaces and tentatively carbonize, control time is 5 ~ 8h, after preliminary charing, again slowly heat up with the speed of 10 DEG C/min, 270 ~ 450 DEG C to be achieved, pass into after nitrogen to pressure is 1 ~ 2MPa to it, insulation makes it carbonize 8 ~ 10h completely, form bamboo charcoal, finally slowly heat up with the speed of 10 DEG C/min again, after 450 ~ 600 DEG C to be achieved, bamboo charcoal after carbonizing completely is incubated calcining 3 ~ 5h, and after calcining completes, make it naturally cool to 20 ~ 30 DEG C can be worth bamboo charcoal material;
Milled in efficient nano ball mill by above-mentioned bamboo charcoal material, mill 3 ~ 5h repeatedly, forms the nanometer bamboo carbon fiber particle that particle size is 5 ~ 10 μm, subsequently the nanometer bamboo carbon fiber particle of preparation is activated 2 ~ 3h at 700 ~ 900 DEG C; By mass percentage, the nanometer bamboo carbon fiber particle of the above-mentioned preparation of 5 ~ 10% is chosen, the CaCl of 7 ~ 9%
2, 10 ~ 11%KCl becomes the turbid liquid of bamboo-carbon fibre coagulating bath with the water of 60 ~ 70% with the dispersant proportioning of 8 ~ 10%; Described dispersant counts the sodium pyrophosphate mixed dispersant of the sodium phosphate trimer of 40 ~ 50 parts, the calgon of 10 ~ 25 parts and 25 ~ 50 parts by weight; By the fiber of required weaving by the turbid liquid of bamboo-carbon fibre coagulating bath, finally form bamboo-carbon fibre as-spun fibre, more stretched, sizing and drying oil, and can weave and form a kind of anion bamboo-carbon fibre weaving face fabric.
Example 1
First get the growth mao bamboon of more than 4 years, broken apart by chopping from root 2m place, then take four whole joints apart from 3m place of the place of breaking apart by chopping, rived and cut off and grow into 5cm, thick is the thin bamboo strips used for weaving of 3mm, tans by the sun 30 days in the sun, after preliminarily dried to yellowish, thin bamboo strips used for weaving is collected at being placed in 150 DEG C and dry 3h; After thin bamboo strips used for weaving is dried, be placed in 270 DEG C of Muffle furnaces and tentatively carbonize, the control time is 8h, after preliminary charing, again slowly heat up with the speed of 10 DEG C/min, 450 DEG C to be achieved, pass into after nitrogen to pressure is 1MPa to it, insulation makes it carbonize 10h completely, form bamboo charcoal, finally slowly heat up with the speed of 10 DEG C/min again, after 600 DEG C to be achieved, 5h is calcined in bamboo charcoal insulation after carbonizing completely, and after calcining completes, make it naturally cool to 20 DEG C can be worth bamboo charcoal material; Milled in efficient nano ball mill by above-mentioned bamboo charcoal material, mill 5h repeatedly, forms the nanometer bamboo carbon fiber particle that particle size is 10 μm, subsequently the nanometer bamboo carbon fiber particle of preparation is activated 3h at 700 DEG C; By gross mass 100g, choose the nanometer bamboo carbon fiber particle of the above-mentioned preparation of 5g, the CaCl of 7g
2, the water of 10gKCl with 70g becomes the turbid liquid of bamboo-carbon fibre coagulating bath with the dispersant proportioning of 8g; Described dispersant counts the sodium pyrophosphate mixed dispersant of the sodium phosphate trimer of 50 parts, the calgon of 25 parts and 25 parts by weight; By the fiber of required weaving by the turbid liquid of bamboo-carbon fibre coagulating bath, final formation bamboo-carbon fibre as-spun fibre, again stretched, sizing and drying oil, can weave and form a kind of anion bamboo-carbon fibre weaving face fabric, the anion bamboo-carbon fibre weaving face fabric obtained by the present invention can be applicable to apparel industry, and no matter the clothes made is at wearing, or in placing, all can not be mouldy, infested, there is insect protected effect.
example 2
First get the growth mao bamboon of more than 4 years, broken apart by chopping from root 1m place, then take four whole joints apart from 2m place of the place of breaking apart by chopping, rived and cut off and grow into 5cm, thick is the thin bamboo strips used for weaving of 2mm, tans by the sun 20 days in the sun, after preliminarily dried to yellowish, thin bamboo strips used for weaving is collected at being placed in 100 DEG C and dry 2h; After thin bamboo strips used for weaving is dried, be placed in 150 DEG C of Muffle furnaces and tentatively carbonize, the control time is 5h, after preliminary charing, again slowly heat up with the speed of 10 DEG C/min, after 270 DEG C to be achieved, insulation makes it carbonize 8h completely, form bamboo charcoal, finally slowly heat up with the speed of 10 DEG C/min again, 450 DEG C to be achieved, pass into after nitrogen to pressure is 2MPa to it, 3h is calcined in bamboo charcoal insulation after carbonizing completely, and after calcining completes, make it naturally cool to 20 DEG C can be worth bamboo charcoal material; Milled in efficient nano ball mill by above-mentioned bamboo charcoal material, mill 3h repeatedly, forms the nanometer bamboo carbon fiber particle that particle size is 5 μm, subsequently the nanometer bamboo carbon fiber particle of preparation is activated 2h at 900 DEG C; By gross mass 200g, choose the nanometer bamboo carbon fiber particle of the above-mentioned preparation of 20g, the CaCl of 18g
2, the water of 22gKCl with 120g becomes the turbid liquid of bamboo-carbon fibre coagulating bath with the dispersant proportioning of 20g; Described dispersant counts the sodium pyrophosphate mixed dispersant of the sodium phosphate trimer of 40 parts, the calgon of 10 parts and 50 parts by weight; By the fiber of required weaving by the turbid liquid of bamboo-carbon fibre coagulating bath, final formation bamboo-carbon fibre as-spun fibre, again stretched, sizing and drying oil, can weave and form a kind of anion bamboo-carbon fibre weaving face fabric, the anion bamboo-carbon fibre weaving face fabric obtained by the present invention can apply household bedding, and no matter the product made is in use, still lay up, all can not be mouldy, infested, there is insect protected effect.
Example 3
First get the growth mao bamboon of more than 4 years, broken apart by chopping from root 1m place, then take four whole joints apart from 3m place of the place of breaking apart by chopping, rived and cut off and grow into 5cm, thick is the thin bamboo strips used for weaving of 2mm, tans by the sun 25 days in the sun, after preliminarily dried to yellowish, thin bamboo strips used for weaving is collected at being placed in 120 DEG C and dry 2h; After thin bamboo strips used for weaving is dried, be placed in 200 DEG C of Muffle furnaces and tentatively carbonize, the control time is 7h, after preliminary charing, again slowly heat up with the speed of 10 DEG C/min, 300 DEG C to be achieved, pass into after nitrogen to pressure is 1MPa to it, insulation makes it carbonize 9h completely, form bamboo charcoal, finally slowly heat up with the speed of 10 DEG C/min again, after 500 DEG C to be achieved, 4h is calcined in bamboo charcoal insulation after carbonizing completely, and after calcining completes, make it naturally cool to 25 DEG C can be worth bamboo charcoal material; Milled in efficient nano ball mill by above-mentioned bamboo charcoal material, mill 4h repeatedly, forms the nanometer bamboo carbon fiber particle that particle size is 7 μm, subsequently the nanometer bamboo carbon fiber particle of preparation is activated 2h at 800 DEG C; By gross mass 300g percentages, choose the nanometer bamboo carbon fiber particle of the above-mentioned preparation of 21g, the CaCl of 24g
2, the water of 30gKCl with 195g becomes the turbid liquid of bamboo-carbon fibre coagulating bath with the dispersant proportioning of 30g; Described dispersant counts the sodium pyrophosphate mixed dispersant of the sodium phosphate trimer of 45 parts, the calgon of 20 parts and 35 parts by weight; By the fiber of required weaving by the turbid liquid of bamboo-carbon fibre coagulating bath, final formation bamboo-carbon fibre as-spun fibre, again stretched, sizing and drying oil, can weave and form a kind of anion bamboo-carbon fibre weaving face fabric, the anion bamboo-carbon fibre weaving face fabric obtained by the present invention can apply household bedding, and no matter the product made is in use, still lay up, all can not be mouldy, infested, there is insect protected effect.
Claims (1)
1. a preparation method for anion bamboo-carbon fibre weaving face fabric, is characterized in that concrete preparation process is:
(1) the growth mao bamboon of more than 4 years is got, broken apart by chopping from root 1 ~ 2m place, four whole joints are taken again apart from 2 ~ 3m place of the place of breaking apart by chopping, rived and cut off and grown into 5cm, thick is the thin bamboo strips used for weaving of 2 ~ 3mm, tan by the sun 20 ~ 30 days in the sun, after preliminarily dried to yellowish, thin bamboo strips used for weaving is collected at being placed in 100 ~ 150 DEG C and dry 2 ~ 3h;
(2) after thin bamboo strips used for weaving is dried, be placed in 150 ~ 270 DEG C of Muffle furnaces and tentatively carbonize, control time is 5 ~ 8h, after preliminary charing, again slowly heat up with the speed of 10 DEG C/min, 270 ~ 450 DEG C to be achieved, pass into after nitrogen to pressure is 1 ~ 2MPa to it, insulation makes it carbonize 8 ~ 10h completely, form bamboo charcoal, finally slowly heat up with the speed of 10 DEG C/min again, after 450 ~ 600 DEG C to be achieved, bamboo charcoal after carbonizing completely is incubated calcining 3 ~ 5h, and after calcining completes, make it naturally cool to 20 ~ 30 DEG C can be worth bamboo charcoal material;
(3) milled in efficient nano ball mill by above-mentioned bamboo charcoal material, mill 3 ~ 5h repeatedly, forms the nanometer bamboo carbon fiber particle that particle size is 5 ~ 10 μm, subsequently the nanometer bamboo carbon fiber particle of preparation is activated 2 ~ 3h at 700 ~ 900 DEG C;
(4) by mass percentage, the nanometer bamboo carbon fiber particle of the above-mentioned preparation of 5 ~ 10% is chosen, the CaCl of 7 ~ 9%
2, 10 ~ 11%KCl becomes the turbid liquid of bamboo-carbon fibre coagulating bath with the water of 60 ~ 70% with the dispersant proportioning of 8 ~ 10%; Described dispersant counts the sodium pyrophosphate mixed dispersant of the sodium phosphate trimer of 40 ~ 50 parts, the calgon of 10 ~ 25 parts and 25 ~ 50 parts by weight;
(5) by the fiber of required weaving by the turbid liquid of bamboo-carbon fibre coagulating bath, finally form bamboo-carbon fibre as-spun fibre, more stretched, sizing and drying oil, and can weave and form a kind of anion bamboo-carbon fibre weaving face fabric.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106835324A (en) * | 2017-01-18 | 2017-06-13 | 肇庆新盈泰环境材料有限公司 | A kind of polypropylene fibre nano-bamboo carbon chopped fiber and preparation method thereof |
| CN110541244A (en) * | 2019-09-05 | 2019-12-06 | 韩建华 | Antibacterial non-woven fabric, preparation method thereof and mask with antibacterial non-woven fabric |
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| CN101195932A (en) * | 2007-12-18 | 2008-06-11 | 盛虹集团有限公司 | Method for producing bamboo charcoal fibre |
| CN102817098A (en) * | 2011-06-10 | 2012-12-12 | 上海欧迪芬内衣精品股份有限公司 | Method for manufacturing bamboo charcoal antibacterial fiber |
| CN103643534A (en) * | 2013-11-20 | 2014-03-19 | 苏州工业园区友顺制衣厂 | Making technology of bamboo charcoal fiber cloth |
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2015
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Patent Citations (3)
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|---|---|---|---|---|
| CN101195932A (en) * | 2007-12-18 | 2008-06-11 | 盛虹集团有限公司 | Method for producing bamboo charcoal fibre |
| CN102817098A (en) * | 2011-06-10 | 2012-12-12 | 上海欧迪芬内衣精品股份有限公司 | Method for manufacturing bamboo charcoal antibacterial fiber |
| CN103643534A (en) * | 2013-11-20 | 2014-03-19 | 苏州工业园区友顺制衣厂 | Making technology of bamboo charcoal fiber cloth |
Non-Patent Citations (2)
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| 水产部供销司等: "《水产品综合利用 第四辑（海藻类）》", 31 August 1959, 轻工业出版社 * |
| 郝新敏等: "《功能纺织材料和防护服装》", 30 November 2010, 中国纺织出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106835324A (en) * | 2017-01-18 | 2017-06-13 | 肇庆新盈泰环境材料有限公司 | A kind of polypropylene fibre nano-bamboo carbon chopped fiber and preparation method thereof |
| CN110541244A (en) * | 2019-09-05 | 2019-12-06 | 韩建华 | Antibacterial non-woven fabric, preparation method thereof and mask with antibacterial non-woven fabric |
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Application publication date: 20151125 |