CN105087173A - Green sea fruit and vegetable antibacterial cleaning agent and preparation method thereof - Google Patents
Green sea fruit and vegetable antibacterial cleaning agent and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a green sea fruit and vegetable antibacterial cleaning agent and a preparation method thereof. The antibacterial cleaning agent takes alkyl glycoside as a main component and comprises the following components by mass percent: 70-80% of surfactant, 3-6% of thickening agent, 6-9% of detergent assistant, 1-4% of pH regulator, 0.1-0.4% of preservative and the balance of water. The antibacterial cleaning agent has the beneficial effects that the raw materials of the product are green substances and are non-toxic, harmless, healthy and environment-friendly, thus avoiding damages of the artificially synthesized detergent to washings and residues in water; besides, the cleaning agent has stronger degreasing capability, is convenient to use, can be used for removing harmful substances on fruits and vegetables, such as residual pesticides and wax, has exquisite and stable foam and stronger antibacterial property, is pollution-free, does not cause secondary pollution and is beneficial to environment-friendly rapid development; and therefore, the antibacterial cleaning agent has the advantages of green raw materials, non-toxicity, harmlessness, healthiness, environment-friendliness, and the like.
Description
Technical field
Technical field
The present invention relates to a kind of daily cleaning agent and preparation method thereof, particularly relate to antibacterial clean-out system of green marine fruit vegetable and preparation method thereof.
Background technology
Food-safety problem becomes study hotspot, the agricultural chemicals of fruit and vegetable surfaces and the health of the existence of wax to the mankind cause certain threat, there is the fruits and vegetables washing composition of abundant species in the market, but lack the fruits and vegetables washing composition efficiently removing the objectionable impurities such as pesticide residue and wax.In existing production technology, washing composition majority is petrochemical complex synthetic products, and the application of this type of fruits and vegetables washing composition not only can not remove objectionable impurities effectively, and the chemical substance of synthesis that what its use was adjoint is causes certain harm to human body and environment.At present, the relevant report of existing many fruits and vegetables washing composition:
Application number is that the Chinese patent application of 103602528A discloses a kind of fruits and vegetables washing composition, it is characterized in that the material comprised by following parts by weight forms: coconut palm oleoyl monoethanolamine 11-16 part, sodium xylene sulfonate 14-36 part, Witco 1298 Soft Acid 9-13 part, ultraviolet absorbers 1-6 part, potassium hydrogen persulfate composite powder 8-15 part, potassium permanganate 2-8 part, sodium carbonate 6-8 part, ethanol 1-6 part, sodium phosphate 12-18 part.This invention has good emulsifying, performance of deoiling, and has stronger washing force especially to the agricultural chemicals of fruit and vegetable surface attachment, also can make common dish washing detergent and use.
Application number is the preparation method that the Chinese patent application of 103160392A discloses a kind of nontoxic fruits and vegetables washing composition, belongs to technical field of civilian industry.The main points of its technical scheme are: be for raw material with the waste water-bean curd pulp-water discharged in the bean product production processes such as bean curd, dried bean curd, the skin of soya-bean milk, simple and the eco-friendly technology separation such as centrifugation, alcohol precipitation is adopted to go out effective constituent, open with water-soluble on a small quantity, add appropriate salt and Xylo-Mucine again, stir.This reodorant effectively can wash the pesticide residue on fruit, vegetables, and has degerming, bacteriostasis efficacy preferably, and to human body and animal harmless.
Application number is that the Chinese patent application of CN104232362A provides a kind of fruits and vegetables washing composition and preparation method thereof, and described fruits and vegetables washing composition comprises: Aloe extract, quaternary surfactant, citric acid, proteolytic enzyme, dispersion agent, solubilizing agent and deionized water.The fruits and vegetables washing composition smell of this invention is pure and fresh, has good bactericidal property and pesticides removal function simultaneously, is applicable to the washing of fruit, vegetables.
Application number is the preparation method that the Chinese patent application of CN103897882A discloses a kind of fruits and vegetables washing composition, comprise the following steps: following material to add by weight in reactor: alkylol amide type nonionogenic tenside 25-35 part, AMONYL 380LC 3-5 part and ethylene glycol 8-10 part, filling speed is 20-25ml/ minute, stir after filling, stirring velocity is 35 revs/min; Leave standstill after stirring, time of repose is 35-45 minute; Cool in the process of leaving standstill, cooling temperature is lower than 10 degrees Celsius, stir in process of cooling, stirring velocity is 15 revs/min, the washing composition that method of the present invention is produced can remove the residual toxicity in the food surfacess such as veterinary antibiotics, also can remove the residual toxicity entered in food, use washing composition without any Side effect simultaneously.
But above-mentioned fruits and vegetables washing composition also exists that part material derives from synthetic chemistry, complex process, complicated components is various, efficiency is not obvious, certain pollution and injury are caused to environment and human body.Therefore this area still needs a kind of fruits and vegetables washing composition of more environmental protection.
Summary of the invention
The object of the invention is to provide that a kind of raw material is green, nontoxic for prior art, health environment-friendly, there is stronger ability of cleaning greasy dirt, the objectionable impurities such as remains of pesticide and wax above fruits and vegetables can be removed, foam exquisiteness is stablized, the antibacterial clean-out system of green marine fruit vegetable with stronger germ resistance and preparation method thereof.
The present invention solves the problems of the technologies described above adopted technical scheme: antibacterial clean-out system of green marine fruit vegetable and preparation method thereof, comprising with alkyl glycoside is main component, wherein: by mass percentage containing, for example lower component: the water of tensio-active agent 70-80%, thickening material 3-6%, detergent builder 6-9%, pH adjusting agent 1-4%, sanitas 0.1-0.4%, surplus.Raw material is all green matters, nontoxic, health environment-friendly, avoids synthetic washing composition to washes infringement and remaining in water; In addition, washing composition of the present invention have stronger ability of cleaning greasy dirt, easy to use, the objectionable impuritiess such as remains of pesticide above fruits and vegetables and wax can be removed, foam exquisiteness is stable, there is stronger germ resistance, pollution-free, can not secondary pollution be produced, be beneficial to environmentally friendly fast development.
For optimizing technique scheme, the measure taked also comprises: also containing essence 0.2-0.5%; Essence is one in grape, lemon, ocean or aloe or its combination.Add essence and can improve sensory effects.Tensio-active agent is alkyl glycoside APG0814 or alkyl glycoside APG1214 or rhamnolipid or its combination.The tensio-active agent of higher concentration and specific washing auxiliary detergent with the use of, while the good decontamination washing effect of acquisition, there is unexpected antibacterial effect, and can not to environment build-up of pressure.Thickening material is sodium alginate or xanthan gum; Sanitas is one or more the mixture in phenylformic acid, Sodium Benzoate, Sorbic Acid or potassium sorbate; Detergent builder are EDTA-2Na or metasilicate pentahydrate sodium or its combination; PH adjusting agent is citric acid.Experiment shows, the mixing formulation of the xanthan gum of specific components content, sodium alginate, EDTA-2Na, phenylformic acid, citric acid has fabulous sterilization effect.Comprise the steps:
1) join in the water of 60 DEG C by the thickening material accurately taking 3-6 weight part, make its dissolving of slowly expanding, until form the strong thickener soln of uniform flow;
2) pH adjusting agent of the washing auxiliary detergent of 6-9 weight part, 1-4 weight part and the sanitas of 0.1-0.4 weight part are added to the water one by one, stir and make it dissolve completely, form liquid;
3) by above-mentioned steps 1) and step 2) green surfactant of preparation and the liquid that obtains and thickener soln and 70-80 weight part mixes, be heated to 40-50 DEG C, stirring makes its Homogeneous phase mixing, add the essence of 0.2-0.5 weight part again, keep the skin wet to 100 weight parts, degassed, get product.The xanthan gum of specific components content, sodium alginate, EDTA-2Na, phenylformic acid, citric acid are mixed by above-mentioned steps, the mixing formulation obtained is beyond thought has fabulous sterilization effect, and has and wash cleaning effect preferably.Essence is one in grape, lemon, ocean or aloe or its combination.Tensio-active agent is alkyl glycoside APG0814 or alkyl glycoside APG1214 or rhamnolipid or its combination.Thickening material is sodium alginate or xanthan gum; Detergent builder are EDTA-2Na or metasilicate pentahydrate sodium or its combination; PH adjusting agent is citric acid.
Owing to present invention employs by mass percentage containing, for example lower component: the water of tensio-active agent 70-80%, thickening material 3-6%, detergent builder 6-9%, pH adjusting agent 1-4%, sanitas 0.1-0.4%, surplus.Raw material is all green matters, nontoxic, health environment-friendly, avoids synthetic washing composition to washes infringement and remaining in water; In addition, washing composition of the present invention have stronger ability of cleaning greasy dirt, easy to use, the objectionable impuritiess such as remains of pesticide above fruits and vegetables and wax can be removed, foam exquisiteness is stable, there is stronger germ resistance, pollution-free, can not secondary pollution be produced, be beneficial to environmentally friendly fast development.Thus the present invention there is raw material green, nontoxic, health environment-friendly, there is stronger ability of cleaning greasy dirt, the objectionable impurities such as remains of pesticide and wax above fruits and vegetables can be removed, stronger germ resistance is stablized, had to foam exquisiteness advantage.
Embodiment
Below in conjunction with attached embodiment, the present invention is described in further detail.
Embodiment 1: antibacterial clean-out system of green marine fruit vegetable and preparation method thereof, comprising with alkyl glycoside is main component, wherein: by mass percentage containing, for example lower component: the water of tensio-active agent 70-80%, thickening material 3-6%, detergent builder 6-9%, pH adjusting agent 1-4%, sanitas 0.1-0.4%, surplus.Raw material is all green matters, nontoxic, health environment-friendly, avoids synthetic washing composition to washes infringement and remaining in water; In addition, washing composition of the present invention have stronger ability of cleaning greasy dirt, easy to use, the objectionable impuritiess such as remains of pesticide above fruits and vegetables and wax can be removed, foam exquisiteness is stable, there is stronger germ resistance, pollution-free, can not secondary pollution be produced, be beneficial to environmentally friendly fast development.Also containing essence 0.2-0.5%; Essence is one in grape, lemon, ocean or aloe or its combination.Add essence and can improve sensory effects.Tensio-active agent is alkyl glycoside APG0814 or alkyl glycoside APG1214 or rhamnolipid or its combination; Preferable range includes any sub-range scope wherein and concrete numerical value, as being 70-73%, 74%-76%, 77-80%.。The tensio-active agent of higher concentration and specific washing auxiliary detergent with the use of, while the good decontamination washing effect of acquisition, there is unexpected antibacterial effect, and can not to environment build-up of pressure.Thickening material is sodium alginate or xanthan gum; Preferable range includes any sub-range scope wherein and concrete numerical value, as being 3-4%, 4-5%, 5-6%.。Sanitas is one or more the mixture in phenylformic acid, Sodium Benzoate, Sorbic Acid or potassium sorbate; Preferable range includes any sub-range scope wherein and concrete numerical value, as being 0.1-0.2%, 0.2-0.3%, 0.3-0.4%.。Detergent builder are EDTA-2Na or metasilicate pentahydrate sodium or its combination; Preferable range includes any sub-range scope wherein and concrete numerical value, as being 6-7%, 7-8%, 8-9%.PH adjusting agent is citric acid; Preferable range includes any sub-range scope wherein and concrete numerical value, as being 1-2%, 2-3%, 3-4%.。Experiment shows, the mixing formulation of the xanthan gum of specific components content, sodium alginate, EDTA-2Na, phenylformic acid, citric acid has fabulous sterilization effect.Comprise the steps:
1) join in the water of 60 DEG C by the thickening material accurately taking 3-6 weight part, make its dissolving of slowly expanding, until form the strong thickener soln of uniform flow;
2) pH adjusting agent of the washing auxiliary detergent of 6-9 weight part, 1-4 weight part and the sanitas of 0.1-0.4 weight part are added to the water one by one, stir and make it dissolve completely, form liquid;
3) by above-mentioned steps 1) and step 2) green surfactant of preparation and the liquid that obtains and thickener soln and 70-80 weight part mixes, be heated to 40-50 DEG C, stirring makes its Homogeneous phase mixing, add the essence of 0.2-0.5 weight part again, keep the skin wet to 100 weight parts, degassed, get product.The xanthan gum of specific components content, sodium alginate, EDTA-2Na, phenylformic acid, citric acid are mixed by above-mentioned steps, the mixing formulation obtained is beyond thought has fabulous sterilization effect, and has and wash cleaning effect preferably.Essence is one in grape, lemon, ocean or aloe or its combination.Tensio-active agent is alkyl glycoside APG0814 or alkyl glycoside APG1214 or rhamnolipid or its combination.Thickening material is sodium alginate or xanthan gum; Detergent builder are EDTA-2Na or metasilicate pentahydrate sodium or its combination; PH adjusting agent is citric acid.
Concrete preferred embodiment is as follows:
The preparation method of this green marine fruit vegetable clean-out system comprises the following steps:
(1) accurately take 4g sodium alginate thickening material to join in the water of 100mL60 DEG C, make its dissolving of slowly expanding, until form the strong thickener soln of uniform flow.
(2) the washing auxiliary detergent metasilicate pentahydrate sodium of 6 weight parts, 2 weight part pH adjusting agent citric acids and 0.2 potassium sorbate preservative are joined in the water of 8 weight parts in order, stir and make it dissolve completely, form liquid.
(3) APG(0814 of the liquid of 16.2 weight parts above-mentioned preparation obtained, 3 weight part sodium alginate thickening material liquid and 80 weight parts) green surfactant mixes, be heated to 50 DEG C, stirring makes its Homogeneous phase mixing, add the food grade grape essence of 0.2 weight part, keep the skin wet to 100 weight parts, degassed, obtain a kind of green marine fruit vegetable clean-out system.
Embodiment 2:
The preparation method of this green marine fruit vegetable clean-out system comprises the following steps:
(1) accurately take 4g sodium alginate thickening material to join in the water of 100mL60 DEG C, make its dissolving of slowly expanding, until form the strong thickener soln of uniform flow.
(2) the washing auxiliary detergent metasilicate pentahydrate sodium of 7 weight parts, 1 weight part pH adjusting agent citric acid and 0.1 preservative sodium benzoate are joined in the water of 9 weight parts in order, stir and make it dissolve completely, form liquid.
(3) APG(1214 of the liquid of 17.1 weight parts above-mentioned preparation obtained, 4 weight part sodium alginate thickening material liquid and 78 weight parts) green surfactant mixes, be heated to 50 DEG C, stirring makes its Homogeneous phase mixing, add the food grade lemon flavour of 0.3 weight part, keep the skin wet to 100 weight parts, degassed, obtain a kind of green marine fruit vegetable clean-out system.
Embodiment 3:
The preparation method of this green marine fruit vegetable clean-out system comprises the following steps:
(1) accurately take 4g xanthan gum thickening material to join in the water of 100mL60 DEG C, make its dissolving of slowly expanding, until form the strong thickener soln of uniform flow.
(2) by the washing auxiliary detergent EDTA-2Na of 8 weight parts, 3 weight part pH adjusting agent citric acids and 0.4
Preservative benzoic acid joins in the water of 10 weight parts in order, stirs and makes it dissolve completely, forms liquid.
(3) liquid, the 5 weight part sodium alginate thickening material liquid of 21.4 weight parts above-mentioned preparation obtained
With the APG(1214 of 70 weight parts) green surfactant mixes, and is heated to 50 DEG C, stirs and makes its Homogeneous phase mixing, add the food grade grape essence of 0.3 weight part, keep the skin wet to 100 weight parts, degassed, obtains a kind of green marine fruit vegetable clean-out system.Specific proportioning can obtain good washing effect, and obtains beyond thought sterilization effect, and its sterilization mechanism is not yet studied, but its product result of use really has the superiority that like product can not be compared.
Embodiment 4:
The preparation method of this green marine fruit vegetable clean-out system comprises the following steps:
(1) accurately take 4g xanthan gum thickening material to join in the water of 100mL60 DEG C, make its dissolving of slowly expanding, until form the strong thickener soln of uniform flow.
(2) by the washing auxiliary detergent EDTA-2Na of 9 weight parts, 4 weight part pH adjusting agent citric acids and 0.3
Preservative benzoic acid joins in the water of 7 weight parts in order, stirs and makes it dissolve completely, forms liquid.
(3) liquid, the 6 weight part sodium alginate thickening material liquid of 20.3 weight parts above-mentioned preparation obtained
Mix with the rhamnolipid green surfactant of 72 weight parts, be heated to 50 DEG C, stir and make its Homogeneous phase mixing, add the food grade aloe flavour of 0.5 weight part, keep the skin wet to 100 weight parts, degassed, obtain a kind of green marine fruit vegetable clean-out system.
effect detection:
The sterilization effect test of green marine fruit vegetable clean-out system prepared by embodiment 1-4.
Use streptococcus aureus, intestinal bacteria (being commercially available bacterial strain product) as the bacterial classification of bactericidal assay; Use the clean-out system of embodiment 1-4 prepared by the present invention as bactericidal agent.
Experimental procedure:
The preparation of streptococcus aureus bacteria suspension and intestinal bacteria bacteria suspension:
The preparation of streptococcus aureus bacteria suspension: by S. aureus Inoculate in nutrient agar (preparation: peptone 10g, extractum carnis 3g, sodium-chlor 5g, agar 20g, add distilled water to 1000mL, autoclaving 15min under 121 DEG C of conditions) in, cultivate 20 hours at 30 DEG C, then the culture 0.9wt% aseptic sodium chloride solution obtained is made bacteria suspension, wherein in bacteria suspension, the quantity of streptococcus aureus is 90CFU/mL;
(1) preparation of intestinal bacteria bacteria suspension: intestinal bacteria are inoculated in LB liquid nutrient medium, 20h is cultivated at 30 DEG C, then the culture 0.9wt% aseptic sodium chloride solution obtained is made bacteria suspension, wherein in bacteria suspension, colibacillary quantity is 90CFU/mL.
(2) in each embodiment making detergent 4.5mL, add bacteria suspension and the colibacillary bacteria suspension mixing of 0.5mL of 0.5mL streptococcus aureus respectively, leave standstill effect 10min, obtain 6 groups two kinds bacterium medicine suspensions respectively;
(3) get each group of bacterium medicine suspension 0.5mL to add the neutralizing agent of 4.5mL respectively (neutralizing agent is by Sulfothiorine, tween 80 and water formulated, in neutralizing agent, the mass percent concentration of Sulfothiorine is 0.5%, the mass percent concentration of tween 80 is 1%), after mixing, comprehensive action 8min, in each group, get 0.5mL mixing liquid is again inoculated on different solid plain agar (nutrient agar medium) substratum plates respectively, cultivate 36 hours at 37 DEG C, calculate colony number, calculate sterilizing rate, according to colony counts, dead colony counts is divided by original total number of bacterial colony.Experimental result is in table 1.
Table 1. is the green marine fruit vegetable washing composition effectiveness comparison of group respectively
From table 1 result: adopt the preferred green marine fruit vegetable clean-out system of the present invention to carry out bacteriostatic experiment and all obtain the excellent effect that sterilizing rate reaches more than 90%, the visible suitable selection by component and particular combination, make this green marine fruit vegetable clean-out system be attended by good sterilizing power.
Comprehensively above-mentioned, the green marine fruit vegetable washing composition of one of the present invention has the advantages such as component is simple, preparation is convenient, by the suitable selection of component, particular combination, synergy and show excellent sterilization effect, and be attended by good foaming simultaneously, achieve beat all effect, there is industrial production prospect and marketable value widely.
Although describe the present invention in conjunction with preferred embodiment; so itself and be not used to limit the present invention; any those skilled in the art; without departing from the spirit and scope of the present invention; can implement various change, the displacement of coordinator and amendment here to the theme listed, therefore protection scope of the present invention be as the criterion when the scope limited depending on proposed claim.
Claims (8)
1. the antibacterial clean-out system of green marine fruit vegetable, comprising with alkyl glycoside is main component, it is characterized in that: by mass percentage containing, for example lower component: the water of tensio-active agent 70-80%, thickening material 3-6%, detergent builder 6-9%, pH adjusting agent 1-4%, sanitas 0.1-0.4%, surplus.
2. the antibacterial clean-out system of green marine fruit vegetable according to claim 1, is characterized in that: also containing essence 0.2-0.5%; Described essence is one in grape, lemon, ocean or aloe or its combination.
3. the antibacterial clean-out system of green marine fruit vegetable according to claim 1, is characterized in that: described tensio-active agent is alkyl glycoside APG0814 or alkyl glycoside APG1214 or rhamnolipid or its combination.
4. the antibacterial clean-out system of green marine fruit vegetable according to claim 3, is characterized in that: described thickening material is sodium alginate or xanthan gum; Described sanitas is one or more the mixture in phenylformic acid, Sodium Benzoate, Sorbic Acid or potassium sorbate; Described detergent builder are EDTA-2Na or metasilicate pentahydrate sodium or its combination; Described pH adjusting agent is citric acid.
5. the preparation method of the antibacterial clean-out system of green marine fruit vegetable, is characterized in that: comprise the steps:
1) join in the water of 60 DEG C by the thickening material accurately taking 3-6 weight part, make its dissolving of slowly expanding, until form the strong thickener soln of uniform flow;
2) pH adjusting agent of the washing auxiliary detergent of 6-9 weight part, 1-4 weight part and the sanitas of 0.1-0.4 weight part are added to the water one by one, stir and make it dissolve completely, form liquid;
3) by above-mentioned steps 1) and step 2) green surfactant of preparation and the liquid that obtains and thickener soln and 70-80 weight part mixes, be heated to 40-50 DEG C, stirring makes its Homogeneous phase mixing, add the essence of 0.2-0.5 weight part again, keep the skin wet to 100 weight parts, degassed, get product.
6. antibacterial clean-out system of green marine fruit vegetable according to claim 5 and preparation method thereof, is characterized in that: described essence is one in grape, lemon, ocean or aloe or its combination.
7. antibacterial clean-out system of green marine fruit vegetable according to claim 5 and preparation method thereof, is characterized in that: described tensio-active agent is alkyl glycoside APG0814 or alkyl glycoside APG1214 or rhamnolipid or its combination.
8. antibacterial clean-out system of green marine fruit vegetable according to claim 7 and preparation method thereof, is characterized in that: described thickening material is sodium alginate or xanthan gum; Described detergent builder are EDTA-2Na or metasilicate pentahydrate sodium or its combination; Described pH adjusting agent is citric acid.
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| CN111019930A (en) * | 2019-12-30 | 2020-04-17 | 武汉新华扬生物股份有限公司 | Enzyme protective agent, composite enzyme liquid for pesticide degradation, preparation method of composite enzyme liquid and washing combined liquid |
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| US11713179B2 (en) | 2020-05-15 | 2023-08-01 | The Procter & Gamble Company | Refillable product containing dissolvable solid article |
| USD1005114S1 (en) | 2020-05-15 | 2023-11-21 | The Procter & Gamble Company | Dispenser with pads |
| US11826439B2 (en) | 2020-09-10 | 2023-11-28 | The Procter & Gamble Company | Dissolvable solid article containing anti-bacterial actives |
| WO2022159368A1 (en) * | 2021-01-21 | 2022-07-28 | The Procter & Gamble Company | Dissolvable solid article containing preservatives |
| CN113265304A (en) * | 2021-04-30 | 2021-08-17 | 湖北美拓日化科技有限公司 | Liquid detergent and preparation method thereof |
| CN115477981A (en) * | 2022-09-23 | 2022-12-16 | 广西壮族自治区林业科学研究院 | Liquid green fruit and vegetable washing product and preparation method thereof |
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Application publication date: 20151125 |