CN105062715A - Automatic domestic dishwasher rinsing agent with sterilization effect - Google Patents
Automatic domestic dishwasher rinsing agent with sterilization effect Download PDFInfo
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Abstract
The invention discloses an automatic domestic dishwasher rinsing agent with a sterilization effect. The rinsing agent comprises components of raw materials in percentage by weight as follows: 5.0%-15.0% of a non-ionic surfactant, 1.0%-5.0% of a chelating agent, 0.05%-2.0% of a preservative, 2.0%-10.0% of a suspension dispersing agent, 1.0%-10.0% of a hydrotropic agent, 0.1%-10.0% of a solvent, 0.1%-8.0% of an anti-corrosion aid, 0.5%-3% of a pH value regulator and 0.1%-0.3% of essence. Specific anti-corrosion and sterilization components are added to the rinsing agent, Escherichia coli or staphylococcus aureus possibly existing on tableware can be removed effectively while the product safety is guaranteed, the removal rate for the Escherichia coli and the staphylococcus aureus is higher than 99.00%, and the rinsing agent can be used in home life, is energy-saving and environment-friendly and has bright application prospect.
Description
Technical field
The present invention relates to household automatic dishwasher purificant, belong to daily chemical product technical field, specifically, the present invention relates to a kind of household automatic dishwasher purificant with efficient degerming effect.
Background technology
Automatic dishwasher purificant is a kind of weakly acidic washing composition, its effect is after completed washings, the residual water droplet on tableware and Bowl rack surface is reduced as far as possible, to carry out drying, each consumption is very few, tableware surface can be caused to leave water mark and white trace, use excessive meeting to make tableware surface seem greasy.Therefore functionally, its design is needs based on following several respects: 1, and the residual alkali of scavenging solution.2, drying is accelerated.3, reduce water stain, improve the outward appearance of tableware, especially to transparent glass cylinder etc.4, wash the dishes froth breaking in trough/press down bubble.
During routine use automatic dishwasher cleaning tableware, special dishwasher washing composition can be used wash, the master of cleaning tableware washes the stage, it is the dirt that washes away of emulsified flushing or Betengent product itself all inevitably has some dirts, or raw material remains on tableware or in the washing soln of cleaning, general dishwasher all can be provided with rinsing program, rinses out residual spot as far as possible.In this stage, with the use of upper special bleaching of dish washing machine agent, this purpose can be reached more efficiently, and if purificant recipe ingredient has rinsing and degerming effect concurrently, bring more guarantees can to our daily life.
Daily tableware after the meal, particularly remains the tableware of meat, if cleaned not in time, is often subject to microbiological contamination, especially some pathogenic bacterium, and contacting more two kinds is intestinal bacteria and streptococcus aureus.Colon bacillus (E.coli) is commonly called intestinal bacteria, that Escherich found in 1885, more colibacillary special serotypes have pathogenic to humans and animals, especially to baby and cub (fowl), often cause severe diarrhea and septicemia.Streptococcus aureus (StaphylococcusaureusRosenbach) is a kind of important pathogen of the mankind, can cause multiple severe infections.There is the another name of " addicted to meat bacterium ".Streptococcus aureus is ubiquitous at occurring in nature, all can find in the movement of air, water, dust and humans and animals.Thus, food is a lot of by the chance of its pollution.
In recent years, the Center for Disease Control is reported, the infection caused by streptococcus aureus accounts for second, is only second to intestinal bacteria.For these two kinds common pathogenic bacterium, how to be removed in dishwashing procedure, be industry urgent problem.China Patent Publication No. CN1070421A discloses a kind of rinsing drying brightener for tableware, uses the tensio-active agents such as aliphatic alcohol polyoxyethylene phosphate ester salt and alkylphenol polyoxyethylene as its main emulsification decontamination composition in invention.China Patent Publication No. CN101018850A discloses a kind of purificant containing hydrophobically modified polycarboxylate, mainly through adding polycarboxylate polymer in invention, the wash-out of improved formulations in bleaching of dish washing machine process, effectively disperse or dirt common in emulsification dishwashing process, divide breaking up to bring the insoluble salt of the metal ion of the water hardness, finally obtain without point and do not contain sedimental dish.US Patent No. 03941713A1 discloses a kind of detergent composition, main component equally using monoalkyl polyoxyethylene ethers phosphoric acid ester as invention, for emulsion dispersion decontamination, raw material is using phosphoric acid salt as main component, in microbial decomposition process, phosphoric may cause the eutrophication of water body.
Thus, the special dishwasher washing composition of prior art still requires further improvement necessity of its formula.
Summary of the invention
The object of the present invention is to provide a kind of household automatic dishwasher purificant with efficient degerming effect, while the good rinsing of guarantee and quick-drying effect, can make product in storage process, keep stable, not by microbial contamination, effectively remove the microbial pathogens that may remain in tableware surface.
Another object of the present invention is to provide a kind of above-mentioned preparation method with the household automatic dishwasher purificant of efficient degerming effect.
A kind of household automatic dishwasher purificant with degerming effect that the present invention proposes, it contains each feed composition of following weight percent:
The sequestrant of 1.0-5.0%; The nonionogenic tenside of 5.0-15.0%; The suspension dispersive agent of 2.0-10.0%; The hydrotropic agent of 1.0%-10.0%; The anticorrosion degerming agent of 0.05-2.0%; The quick-drying solvent of 0.1%-10.0%; The anticorrosive auxiliary agent of 0.1-8.0%; The pH value regulator of 0.5-3%; The essence of 0.1-0.3%; And surplus is deionized water.
Household automatic dishwasher purificant of the present invention, described sequestrant is glutamic acid N, N, one or both mixture in oxalic acid four sodium, MDGA and Trisodium Citrate, wherein be more preferably MDGA, MDGA is that a kind of novel sequestrant has excellent sequestering power, use safety, do not produce any harmful material, biological degradability is good, have higher solubility property to inorganic sediment, adds somewhat to the wash effect of product, preferential addition is 2%-3%.
Household automatic dishwasher purificant of the present invention, described nonionogenic tenside is the mixture of more than at least one or two in fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-7, Pluronic PE 6800.Wherein preferred Pluronic PE 6800, it has excellent emulsification clean effect, and foam volume is low, can not produce a large amount of foam in automatic dishwasher operational process, and cause washing burden to machine, preferred addition is 10.0%-15.0%.
Household automatic dishwasher purificant of the present invention, described suspension dispersive agent is the mixture of more than at least one or two in toxilic acid/acrylic copolymer sodium salt, toxilic acid/olefin copolymer sodium salt and polyacrylic acid sodium salt, wherein preferred toxilic acid/acrylic copolymer sodium salt, preferential addition is 2%-5%.
Household automatic dishwasher purificant of the present invention, described hydrotropic agent is one or both the mixture in cumene sodium sulfonate and sodium xylene sulfonate, and be wherein more preferably cumene sodium sulfonate, preferred addition is 2%-4%.
Household automatic dishwasher purificant of the present invention, described anticorrosion degerming agent is one or more the mixture in methylisothiazolinone, methylchloroisothiazandnone, Phenoxyethanol and potassium sorbate.
Household automatic dishwasher purificant of the present invention, described quick-drying solvent is one or both the mixture in ethanol and Virahol; Described anticorrosive auxiliary agent is the mixture of magnesium chloride and zinc chloride at least one or two; Described pH value regulator is citric acid.
Household automatic dishwasher purificant of the present invention, described essence is not particularly limited requirement, preferred addition 0.1%-0.3%.
Household automatic dishwasher purificant of the present invention, its pH value is between 3.0-6.0.
The present invention has the preparation method of the household automatic dishwasher purificant of efficient degerming effect, and it comprises the following steps:
1) first in ingredients pot, add a certain amount of deionized water, drop into sequestrant, nonionogenic tenside, hydrotropic agent, quick-drying solvent, stir;
2) drop into suspension dispersive agent and anticorrosive auxiliary agent, stir;
3) add citric acid, adjust ph, to proper range, stirs;
4) in ingredients pot, drop into essence and anticorrosion degerming agent, stir;
5) in ingredients pot, add other auxiliary agent, stir;
6) water adding surplus in ingredients pot is continued, through being up to the standards and packing.
Tool of the present invention has the following advantages and beneficial effect:
1, the present invention is added with anticorrosion degerming composition, while ensureing stable, the security of product, effectively removes intestinal bacteria or the streptococcus aureus that may remain existence, reaches more than 99.00% to both clearances.
2, do not add use in the present invention containing phosphide, can not pollute water body, bring burden to environment.
3, the low bubble table of nonionic comprehensively employing EO-PO block in the present invention is lived and antiredeposition composition, for rinsing solution provides good spreading wetting ability, and effectively takes away the composition that may remain or deposit.
4, the preferred sequestrant of the present invention is a kind of novel sequestrant, there is excellent sequestering power, use safety, do not produce any harmful material, biological degradability is good, has higher solubility property to inorganic sediment, there is collaborative rot-resistant effect, product of the present invention can use in life staying idle at home, energy-conserving and environment-protective, has good application prospect.
5, the present invention surprisingly, intestinal bacteria and streptococcus aureus can be removed efficiently containing the mixture more than at least one or two in methylisothiazolinone, methylchloroisothiazandnone, Phenoxyethanol and potassium sorbate as the dishwasher detergent composition of degerming agent, there is the clean effect of good decontamination simultaneously.Purificant composition of the present invention does not add phosphide, while maintenance product primary demand, reduces the pollution to water body, meets the demand of environmental protection.
Embodiment
Household automatic dishwasher purificant of the present invention, its feed composition comprised has: sequestrant, nonionogenic tenside, suspension dispersive agent, hydrotropic agent, anticorrosion degerming agent, quick-drying solvent, anticorrosive auxiliary agent, pH value regulator and other auxiliary agents are as essence etc.
Utilize that tensio-active agent reduces water surface tension and its distinctive wetting, dispersion, emulsification, solublization can weaken the bonding strength of dirt at tableware surface, easily depart from from tableware surface and be distributed to water.Prevent soil redeposition to the effect of tableware surface in addition, dirt after cleaning can be avoided to form again spot and film at tableware surface.
Sequestrant is mainly used in calcium, magnesium ion in chelating water, prevents from generating a large amount of calcium carbonate or magnesiumcarbonate precipitation, is attached to final phase of a chess game surface, also has collaborative rot-resistant effect simultaneously.
Suspension dispersive agent is well dispersed in water body the material of removal or impurity, along with the process of draining is got rid of outside automatic dishwasher.Hydrotropic agent can improve the cloud point of nonionogenic tenside in system, and in high-temperature wash process, table work can not be separated out because temperature is too high, cannot play its effect.
Quick-drying solvent can accelerate the drying rate of tableware surface moisture in automatic dishwasher drying course, and makes not produce stable foam in rinse cycle, is convenient to rinsing.
Introduce anticorrosion degerming composition in purificant formula, certain guaranteeing role can be played to the quality safety of product in storage process.
Without phosphorus referring to of the present invention is not added containing the compound of phosphoric artificially in the composition, and particularly, the weight content of polycarboxylate in detergent composition of the present invention be not higher than 0.0001%; Degerming agent refers to remove or kill the preparation of specified microorganisms, and the degerming main finger in invention is for the removal of intestinal bacteria and streptococcus aureus; Pathogenic bacterium (Pathogenicbacteria) refer to cause the microorganism of disease to be called pathogenic micro-organism or pathogenic bacterium; The efficiently degerming clearance referring to for intestinal bacteria and streptococcus aureus reaches 99.00% or more.
Below by way of concrete preferred embodiment, the present invention is expressed in further detail, but the present invention is not limited in following embodiment.
embodiment 1 ~ 4
According to the composition of raw materials of following table 1, first in ingredients pot, add a certain amount of deionized water, drop into MDGA, EO/PE segmented copolymer, cumene sodium sulfonate, ethanol, stir; Drop into acrylic copolymer and magnesium chloride, stir; Add citric acid, adjust ph, to proper range, stirs; In ingredients pot, drop into essence and sanitas, stir; In ingredients pot, add other auxiliary agent, stir; Continue the water adding surplus in ingredients pot, through being up to the standards and packing.
The household automatic dishwasher purificant formula composition of table 1 embodiment 1 ~ 4
embodiment 5 ~ 8
According to the composition of raw materials of following table 2, first in ingredients pot, add a certain amount of deionized water, drop into glutamic acid N, N, oxalic acid four sodium, PE6200, sodium xylene sulfonate, ethanol, stir; Drop into acrylic copolymer and zinc chloride, stir; Add citric acid, adjust ph, to proper range, stirs; In ingredients pot, drop into essence and sanitas, stir; In ingredients pot, add other auxiliary agent, stir; Continue the water adding surplus in ingredients pot, through being up to the standards and packing.
The household automatic dishwasher purificant formula composition of table 2 embodiment 5 ~ 8
effect test example
1, composition stability test
Pass through above-described embodiment, in order to test the compatibility stability of degerming composition in invention component, contrast commercially available brand automatic dishwasher purificant, carried out thimble test, be sub-packed in the transparent PET bottle of 250ml by compound composition, be placed in the baking oven one month of 45 DEG C, take out and contrast with RT sample, observation test sample appearance, and antiseptic content change in test composition, color appearance is without obvious flavescence, and sanitas conservation rate is greater than 50% for qualified product.
Table 3 purificant component high-temperature stability test data
Table 3 data presentation, in the component of embodiment 1-8, the compatibleness of degerming composition and other component is good, stable storing, effectively can keep the stability of product.
2, rinsing performance test
In order to measure the rinsing performance of detergent composition in invention further, setting testing method is as follows: the wash effect of tableware cannot embody by concrete correlation data, can be evaluated and tested by macroscopic form.Look for the crowd (M-F is close to 1:1) of 30 Different age group to carry out Blind Test to tableware wash effect respectively, and mark to tableware rinsing effect, 5 points of effect the bests, mark is lower, tableware rinsing effect is poorer, is 4 successively, and 3,2,1 point, 0 point indicates without rinsing effect.It is qualified that the rinsing performance that scoring is more than or equal to 2 is judged to be.
Table 4 rinsing performance evaluation and test data
Above data show, the rinsing performance of Example formulations reaches the wash effect of needs.
3, wash effect test
Bacteria-eliminating efficacy (main test bacterial classification is intestinal bacteria and streptococcus aureus) detection method is as follows:
Prepare before 1 experiment:
1.1 preparation artificial dirts, the formula of artificial dirt is as follows: mixing oil 15%, wheat-flour 15%, whole milk powder 7.5%, fresh full egg liquid 30%, distilled water 32.5%; Dirt compound method is with reference to GB9985-2000 manual dishwashing washing composition;
1.2 prepare dirt bacteria suspension (intestinal bacteria, golden yellow glucose coccus are prepared respectively), and artificial dirt adds in sterilized water by 1%, and the tween 80 of 0.05%, adds bacteria suspension, and making the initial bacterium of dirt bacteria suspension dense is 105CFU/mL;
1.3 preparation washingss, accurately take 0.8g liquid detergent and are dissolved in containing in 2000mL250mg/L hard water, hard water commercially available basin (bore 34cm, footpath, end 24cm) splendid attire.
The degerming rate of 2 service plate measures
2.1 instrument
(1) balance;
(2) commercially available basin (bore 34cm, footpath, end 24cm);
(3) white porcelain vegetable dish (external diameter 200mm, smeared portion of trying to get to the heart of a matter is about 140mm);
(4) pig palm fibre paint brush, 102mm;
(5) graduated cylinder, 1000ml;
(6) stopwatch;
Microorganism detection required equipment is with reference to QB/T2738-2012.
Reagent: required reagent is with reference to QB/T2738-2012 and GB9985-2000.
2.2 experimental arrangement
2.2.1 dirt bacteria suspension is dipped dish surface (bottom service plate) uniform application 3 times with aseptic cotton carrier, often be coated with and once rotate 60 °, rotate 1 week around plate for the last time, smear 4 plates altogether, leave standstill 20 minutes, wherein 2 for inoculating time live bacterial count, 2 for washing rear live bacterial count, require inoculation after viable bacteria reclaim concentration be not less than 104CFU/mL;
2.2.2 the service plate scribbling dirt is put into and washings basin is housed, scrub with 102mm bristles paint brush subsequently, first clockwise brush five times, another mistake hour hands brush five times, so in triplicate, the dirt major part be applied on service plate is washed down, finally the dirt under not washing and foam brush is washed off, about 50s consuming time again; After washing, rush 30 seconds with tap water (flow velocity 90-100mL/S), natural air drying 20 minutes, with aseptic cotton carrier uniform application service plate surface, microbe population (with water 10mL normal saline dilution, being designated as 100) on plate count cotton swab, obtains washing rear microbial count;
2.2.3 use another 2 the service plate surfaces of aseptic cotton carrier uniform application equally, the microbe population (with water 10mL normal saline dilution, being designated as 100) on plate count cotton swab, obtains washing front microbial count;
2.3 experimental result
Degerming rate=(wash front microbial count mean value-wash rear microbial count mean value)/wash front microbial count mean value * 100%
The degerming test result of table 5 purificant
The test data of upper table shows, the clearance of Example formulations component to intestinal bacteria and streptococcus aureus all reaches more than 99.00%, reaches effectively degerming requirement significantly better than common control's sample.
In sum, the household automatic dishwasher purificant with efficient degerming effect of the present invention, while the good rinsing of guarantee and quick-drying effect, can make product in storage process, keep stable, not by microbial contamination, effective removal may remain in the microbial pathogens of tableware surface, reaches more than 99.00% to the clearance of intestinal bacteria and streptococcus aureus; And in order to can calcium, magnesium ion etc. in chelating water body in rinse cycle, avoid depositional phenomenon, and do not cause negative impact to environment, introduce the sequestering ingredient that biological degradability is good in invention, it has collaborative rot-resistant effect concurrently.
The above be only preferred embodiment of the present invention, but embodiments of the present invention is not limited thereto.It is to be noted; cited embodiment is only used to further illustrate the present invention; can not be interpreted as limiting the scope of the invention, these those skilled in the art content according to the present invention can do some nonessential improvement and adjustment. also belong in protection scope of the present invention.
Claims (10)
1. there is the household automatic dishwasher purificant of degerming effect, it is characterized in that: it also contains each feed composition of following weight percent:
2. the household automatic dishwasher purificant with degerming effect according to claim 1, it is characterized in that: the preferential addition of described sequestrant is 2%-3%, it is glutamic acid N, N, the mixture in what Trisodium Citrate of oxalic acid four sodium, MDGA more than at least one or two.
3. the household automatic dishwasher purificant with degerming effect according to claim 1, it is characterized in that: the preferred addition of described nonionogenic tenside is 10.0%-15.0%, it is the mixture of more than at least one or two in fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-7, Pluronic PE 6800.
4. the household automatic dishwasher purificant with degerming effect according to claim 1, it is characterized in that: the preferential addition of described suspension dispersive agent is 2%-5%, it is the mixture of any one or more in toxilic acid/acrylic copolymer sodium salt, toxilic acid/ethylene monomer copolymer sodium salt and polyacrylic acid sodium salt.
5. the household automatic dishwasher purificant with degerming effect according to claim 1, is characterized in that: the preferred addition of described hydrotropic agent is 2%-4%, and it is the mixture of cumene sodium sulfonate or sodium xylene sulfonate or two kinds.
6. the household automatic dishwasher purificant with degerming effect according to claim 1, is characterized in that: described anticorrosion degerming agent is the mixture of any one or more in methylisothiazolinone, methylchloroisothiazandnone, Phenoxyethanol and potassium sorbate.
7. the household automatic dishwasher purificant with degerming effect according to claim 1, is characterized in that: described quick-drying solvent is the mixture of ethanol or Virahol or two kinds.
8. the household automatic dishwasher purificant with degerming effect according to claim 1, is characterized in that: described anticorrosive auxiliary agent is the mixture of magnesium chloride or zinc chloride or two kinds; Described pH value regulator is citric acid.
9. the household automatic dishwasher purificant with degerming effect according to claim 1, is characterized in that: the pH value of described purificant is between 3.0-6.0.
10. the preparation method with the household automatic dishwasher purificant of degerming effect according to any one of claim 1-9, is characterized in that comprising the following steps:
1) first in ingredients pot, add a certain amount of deionized water, drop into sequestrant, nonionogenic tenside, hydrotropic agent, quick-drying solvent, stir;
2) drop into suspension dispersive agent and anticorrosive auxiliary agent, stir;
3) add citric acid, adjust ph, to proper range, stirs;
4) in ingredients pot, drop into essence and sanitas, stir;
5) in ingredients pot, add other auxiliary agent, stir;
6) water adding surplus in ingredients pot is continued, through being up to the standards and packing.
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| CN201510490708.4A CN105062715B (en) | 2015-08-11 | 2015-08-11 | A kind of household automatic dishwasher purificant for having high degerming effect and excellent rinsing effect concurrently |
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| CN201510490708.4A CN105062715B (en) | 2015-08-11 | 2015-08-11 | A kind of household automatic dishwasher purificant for having high degerming effect and excellent rinsing effect concurrently |
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| CN106833935A (en) * | 2016-12-23 | 2017-06-13 | 镇江华域环保设备制造有限公司 | The preparation method of fluid is gone in a kind of decontamination for kitchen use |
| CN107384619A (en) * | 2017-08-02 | 2017-11-24 | 广州立白企业集团有限公司 | It is a kind of have remove effervescent table for cleaning of residual, the degerming effect of agriculture and preparation method thereof |
| CN107523430A (en) * | 2017-09-26 | 2017-12-29 | 深圳市洁力士化工产品有限公司 | A kind of glass washing machine special glass cup brightener |
| CN109570162A (en) * | 2018-11-26 | 2019-04-05 | 蓝思科技股份有限公司 | The cleaning method of vacuum formed box |
| CN111073762A (en) * | 2019-12-27 | 2020-04-28 | 佛山市顺德区美的洗涤电器制造有限公司 | Liquid detergent composition suitable for automatic dosing in a dishwasher |
| CN112625809A (en) * | 2020-12-18 | 2021-04-09 | 广州立白企业集团有限公司 | Liquid detergent composition for dishwasher and preparation method thereof |
| CN113046192A (en) * | 2019-12-27 | 2021-06-29 | 佛山市顺德区美的洗涤电器制造有限公司 | Curing agent composition suitable for dish-washing machine |
| CN114774209A (en) * | 2022-05-16 | 2022-07-22 | 佛山市顺德区美的洗涤电器制造有限公司 | Special detergent composition for household automatic dish-washing machine |
| CN115386437A (en) * | 2022-08-31 | 2022-11-25 | 中山百科清洁用品制造有限公司 | Special rinsing agent for automatic dish-washing machine and preparation method thereof |
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| CN106833935A (en) * | 2016-12-23 | 2017-06-13 | 镇江华域环保设备制造有限公司 | The preparation method of fluid is gone in a kind of decontamination for kitchen use |
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| CN107384619B (en) * | 2017-08-02 | 2020-09-11 | 广州立白企业集团有限公司 | Cleaning effervescent tablet with pesticide residue removing and bacterium removing effects and preparation method thereof |
| CN107523430A (en) * | 2017-09-26 | 2017-12-29 | 深圳市洁力士化工产品有限公司 | A kind of glass washing machine special glass cup brightener |
| CN109570162A (en) * | 2018-11-26 | 2019-04-05 | 蓝思科技股份有限公司 | The cleaning method of vacuum formed box |
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| CN112625809A (en) * | 2020-12-18 | 2021-04-09 | 广州立白企业集团有限公司 | Liquid detergent composition for dishwasher and preparation method thereof |
| CN114774209A (en) * | 2022-05-16 | 2022-07-22 | 佛山市顺德区美的洗涤电器制造有限公司 | Special detergent composition for household automatic dish-washing machine |
| CN114774209B (en) * | 2022-05-16 | 2023-08-22 | 佛山市顺德区美的洗涤电器制造有限公司 | Special detergent composition for household automatic dish-washing machine |
| CN115386437A (en) * | 2022-08-31 | 2022-11-25 | 中山百科清洁用品制造有限公司 | Special rinsing agent for automatic dish-washing machine and preparation method thereof |
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