CN105062156B - A kind of ceramic coating with antibacterial functions and preparation method thereof - Google Patents
A kind of ceramic coating with antibacterial functions and preparation method thereof Download PDFInfo
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Abstract
A kind of ceramic coating with antibacterial functions, is made up of priming paint and finish paint two parts, and the priming paint and finish paint are constituted by component A hosts, component B curing agent and component C catalyst；The component A of the priming paint and finish paint:Component B:Component C is by weight ratio:2‑4:1‑2:0.01‑0.02.Without hazardous decomposition products in coating process of the present invention, VOC emission is extremely low, meets the environmental requirement of RoHS, is a kind of new green environment protection coating；It is applicable on the small household electrical appliances such as the interior painting of cooker non-stick pan, and coffee pot, thermos cup.
Description
Technical field
The present invention relates to kitchen tools technical field of coatings, more particularly, to a kind of ceramic coating with antibacterial functions and its system
Preparation Method.
Background technology
Nano material is used for anti-biotic material mainly due to the reduction of agent particle size, and specific surface area is greatly increased, grain
The particle of footpath 5nm, the percentage by volume on surface is 50%, and during particle diameter 2nm, the percentage by volume on surface increases to 80%.It is huge
Specific surface, be good for state severe mismatch, there are many activated centres, make nano material that there is extremely strong adsorption capacity.This causes to receive
Rice corpuscles still produces alkane quasi-molecule of other peculiar smell etc. for the oxygen atom, the oxygen radical that either promote material corrupt,
Be respectively provided with it is extremely strong grab prisoner's ability, make it have anti-corrosive antibacterial function.
With the development of society, anti-biotic material is in daily fiber garment, household electrical appliance, sanitary ware, food bag
It is filled with and steel plate for building, the field such as coating obtains and is increasingly widely applied, wherein in household articles, family's fiber system
Product, electrical home appliances and field of medical products are applied.As cooker non-viscous paint, because it is directly contacted with food, except
Need with good non-adhesion behavior and security, in order to further improve the environmental quality in people's live and work space, need
Develop the coating with antibacterial functions.But there is no in the market any a suitable for applying coating in cooker while having
Non-adhesion behavior, security performance and the coating with antibacterial functions.
The content of the invention
In view of the above-mentioned problems existing in the prior art, the applicant provide a kind of ceramic coating with antibacterial functions and
Its preparation method.Without hazardous decomposition products in coating process of the present invention, VOC emission is extremely low, meets the environmental requirement of RoHS, is one
Plant new green environment protection coating；It is applicable on the small household electrical appliances such as the interior painting of cooker non-stick pan, and coffee pot, thermos cup.
Technical scheme is as follows：
A kind of ceramic coating with antibacterial functions, is made up of priming paint and finish paint two parts, the priming paint and finish paint by
Component A hosts, component B curing agent and component C catalyst composition；
The component A of the priming paint and finish paint:Component B:Component C is by weight ratio:2-4:1-2:0.01-0.02；
The raw material weight percent of the primer composition A hosts is：
The raw material weight percent of the finish paint component A hosts is：
The particle diameter of the Ludox is 9-17nm；
The Nano-meter SiO_22Dispersion liquid is the SiO of particle diameter 100-120nm solids contents 20%2Aqueous dispersions；
The priming paint is with the raw material weight percent of finish paint component B curing agent：
MTMS 96-98%
Silicone oil 2-4；
The priming paint is with the raw material weight percent of finish paint component C catalyst：
Formic acid 100%.
The inorganic pigment is titanium dioxide.The pearl powder is Merck silvery white pearl essence Iriodin 153.
A kind of preparation method of the ceramic coating with antibacterial functions, concretely comprises the following steps：
(1) primer composition A hosts：
1. first by Ludox 200-300 mesh nylon net filters, and stirred with 600-800rpm/ minutes rotating speed；
2. uniform deionized water and butyl glycol ether mixture will be pre-mixed, in being added to Ludox in stirring；
3. in above-mentioned compound, under 600-800rpm/ minutes stirring, bentonite is added, and with 800-
The Rate Dispersion of 1000rpm/ minutes 5 minutes；
4. in above-mentioned compound, under 600-800rpm/ minutes stirring, add inorganic pigment and aluminum oxide wear-resisting
Powder, with Rate Dispersion 15-20 minutes of 800-1000rpm/ minutes；
5. after above-mentioned compound being ground into fineness less than 15 μm using basket sand machine, stirred with 600-800rpm/ minutes
Nano-meter SiO_2 is added under state2Dispersion liquid, and the finished product made after stirring 5-10 minutes；
The viscosity of the finished product is 12 ± 3 seconds, and the viscosity No. 4 cups of DIN are measured at a temperature of 23 DEG C；
(2) finish paint component A hosts：
1. first by Ludox 200-300 mesh nylon net filters, and stirred with 600-800rpm/ minutes rotating speed；
2. uniform deionized water and butyl glycol ether mixture will be pre-mixed, in being added to Ludox in stirring；
3. in above-mentioned compound, under 600-800rpm/ minutes stirring, pearl powder is added, and with 800-1000rpm/
The Rate Dispersion of minute 5 minutes；
The viscosity of the finished product is 8-12 seconds, and viscosity DIN4 cups are measured at a temperature of 23 DEG C；
(3) priming paint and finish paint component B curing agent：
MTMS, silicone oil is uniform in 100-120rpm/ minutes speed scroll；
(4) priming paint and finish paint component C catalyst：
Catalyst component C：Formic acid can be used directly without specially treated；
(5) finished product is after curing process is cured with priming and finish paint each component, the curing process is as follows：
Priming paint：Above-mentioned catalyst component C is proportionally added into curing agent B component, component A is all added after being well mixed
In, with after being mixed thoroughly and reacting and reach 30-40 DEG C to temperature, rolling speed 120- will be placed on after container good seal
In the rolling oil machine of 180rpm, curing 2-4h is rolled, the mixture after curing is removed from rolling oil machine, after it is cooled to room temperature
It is stand-by；
Finish paint：Above-mentioned catalyst component C is proportionally added into curing agent B component, component A is all added after being well mixed
In, will be mixed thoroughly after container good seal and reacted after reaching 30-40 DEG C to temperature, it is placed on rolling speed 120-
In the rolling oil machine of 180rpm, curing 20-24h is rolled, the mixture after curing is removed from rolling oil machine, treat that it is cooled to room temperature
It is stand-by afterwards；
(6) requirement of priming paint thickness is sprayed into 30-45um when using, and the requirement of finish paint thickness is sprayed into 3-10um.
The whole dispersion, stirring and temperature is not less than 10 DEG C and not higher than 35 DEG C in process of lapping.
The present invention is beneficial to be had technical effect that：
Weak point it is an object of the invention to make up existing product, develops a kind of ceramics painting with antibacterial functions
Material, using Ludox and 0.12 μm of SiO of particle diameter of safe particle diameter 11nm2The collocation of particle is used so that final paint film
Surface particle has great specific surface area, so that many activated centres occurs in paint film inside, makes it have extremely strong suction
Attached ability, so as to promoting the oxygen atom of material corruption, oxygen radical and producing alkane quasi-molecule of other peculiar smell etc., have
Have it is extremely strong grab prisoner's ability, make it have anti-corrosive antibacterial function.
Specific embodiment
With reference to embodiment, the present invention is specifically described.Its formula rate percentage：
Embodiment 1
First, priming paint：
(1) component A hosts：
1. first by Ludox 45% with 300 mesh nylon net filters, and stirred with 800rpm/ minutes rotating speed；
2. uniform deionized water 2% and the mixture of butyl glycol ether 1.5% will be pre-mixed, silicon be added in stirring molten
In glue；
3. in above-mentioned compound, under 800rpm/ minutes stirring, bentonite 0.3% is added, and with 1000rpm/ points
The Rate Dispersion of clock 5 minutes；
4. in above-mentioned compound, under 800rpm/ minutes stirring, titanium dioxide 30% and aluminum oxide abrasion-resistant powder are added
4%, with the Rate Dispersion 15 minutes of 1000rpm/ minutes；
5. above-mentioned compound is ground to fineness less than 10um using basket sand machine, with 800rpm/ minutes stirring
Add Nano-meter SiO_22Dispersion liquid 17.2%, and 1000rpm/ minutes stirring 10 minutes after make finished product.
The viscosity of priming paint finished product is 12 ± 3 seconds, and the viscosity No. 4 cups of DIN are measured at a temperature of 23 DEG C.
(2) component B curing agent：MTMS 98%, silicone oil 2% are rolled under 120rpm/ minutes speed
Uniformly.
(3) component C catalyst：Catalyst component C formic acid 100% can be used directly without specially treated.
2nd, finish paint：
(1) component A hosts：
1. first by Ludox 83% with 300 mesh nylon net filters, and stirred with 800rpm/ minutes rotating speed；
2. uniform deionized water 13.8% and the mixture of butyl glycol ether 2% will be pre-mixed, silicon will be added in stirring
In colloidal sol；
3. in above-mentioned compound, under 800rpm/ minutes stirring, pearl powder 1.2% is added, and with 1000rpm/ minutes
Rate Dispersion 5 minutes.
(2) component B curing agent：MTMS 98%, silicone oil 2% are rolled under 120rpm/ minutes speed
Uniformly.
(3) component C catalyst：Catalyst component C formic acid 100% can be used directly without specially treated.
3rd, finished product is after curing process curing, its curing process is as follows：
(1) priming paint：Above-mentioned catalyst component C is proportionally added into curing agent B component according to the weight proportion shown in table 1
In, rock in well mixed rear all additions component As, will firmly be rocked until each component is mixed thoroughly after container good seal
And after reaction reaches 40 DEG C to temperature, be placed in the rolling oil machine of rolling speed 180rpm, curing 2h is rolled, after curing
Mixture is removed from rolling oil machine, stand-by after it is cooled to room temperature；
(2) finish paint：Above-mentioned catalyst component C is proportionally added into curing agent B component according to the weight proportion shown in table 1
In, rock in well mixed rear all additions component As, will firmly be rocked until each component is mixed thoroughly after container good seal
And after reaction reaches 40 DEG C to temperature, be placed in the rolling oil machine of rolling speed 180rpm, curing 20h is rolled, after curing
Mixture from rolling oil machine on remove, it is stand-by after it is cooled to room temperature.
4th, film：Usage amount according to the priming paint shown in table 1 and finish paint carries out film, during film, the requirement spray of priming paint thickness
45um is applied to, the requirement of finish paint thickness is sprayed into 10um.
The priming paint of 1 embodiment of table 1 and finish paint each component and weight proportion
| Component (unit：Weight portion) | Priming paint | Finish paint |
| Component A | 3.435 | 2 |
| Component B | 1.55 | 1 |
| Component C | 0.015 | 0.01 |
The particle diameter of above-mentioned Ludox used is 10nm；Nano-meter SiO_2 used2Dispersion liquid is particle diameter 100nm solids contents 20%
SiO2Aqueous dispersions.
Embodiment 2
First, priming paint：
(1) component A hosts：
1. first by Ludox 52% with 200 mesh nylon net filters, and stirred with 600rpm/ minutes rotating speed；
2. uniform deionized water 1% and the mixture of butyl glycol ether 1% will be pre-mixed, Ludox will be added in stirring
In；
3. in above-mentioned compound, under 600rpm/ minutes stirring, bentonite 0.6% is added, and with 800rpm/ points
The Rate Dispersion of clock 5 minutes；
4. in above-mentioned compound, under 600rpm/ minutes stirring, titanium dioxide 25% and aluminum oxide abrasion-resistant powder are added
5%, with the Rate Dispersion 15 minutes of 800rpm/ minutes；
5. above-mentioned compound is ground to fineness less than 10um using basket sand machine, with 600rpm/ minutes stirring
Add Nano-meter SiO_22Dispersion liquid 15.4%, and 600rpm/ minutes stirring 10 minutes after make finished product.
The viscosity of priming paint finished product is 12 ± 3 seconds, and the viscosity No. 4 cups of DIN are measured at a temperature of 23 DEG C.
(2) component B curing agent：MTMS 96%, silicone oil 4% are rolled under 100rpm/ minutes speed
Uniformly.
(3) component C catalyst：Catalyst component C formic acid 100% can be used directly without specially treated.
2nd, finish paint：
(1) component A hosts：
1. first by Ludox 66% with 200 mesh nylon net filters, and stirred with 600rpm/ minutes rotating speed；
2. uniform deionized water 30% and the mixture of butyl glycol ether 4% will be pre-mixed, silicon be added in stirring molten
In glue；
(2) component B curing agent：MTMS 96%, silicone oil 4% are rolled under 100rpm/ minutes speed
Uniformly.
(3) component C catalyst：Catalyst component C formic acid 100% can be used directly without specially treated.
3rd, finished product is after curing process curing, its curing process is as follows：
(1) priming paint：Above-mentioned catalyst component C is proportionally added into curing agent B component according to the weight proportion shown in table 2
In, rock in well mixed rear all additions component As, will firmly be rocked until each component is mixed thoroughly after container good seal
And after reaction reaches 30 DEG C to temperature, be placed in the rolling oil machine of rolling speed 120rpm, curing 4h is rolled, after curing
Mixture is removed from rolling oil machine, stand-by after it is cooled to room temperature；
(2) finish paint：Above-mentioned catalyst component C is proportionally added into curing agent B component according to the weight proportion shown in table 2
In, rock in well mixed rear all additions component As, will firmly be rocked until each component is mixed thoroughly after container good seal
And after reaction reaches 30 DEG C to temperature, be placed in the rolling oil machine of rolling speed 120rpm, curing 24h is rolled, after curing
Mixture from rolling oil machine on remove, it is stand-by after it is cooled to room temperature.
4th, film：Usage amount according to the priming paint shown in table 2 and finish paint carries out film, during film, the requirement spray of priming paint thickness
30um is applied to, the requirement of finish paint thickness is sprayed into 3um.
The priming paint of 2 embodiment of table 2 and finish paint each component and weight proportion
| Component (unit：Weight portion) | Priming paint | Finish paint |
| Component A | 2 | 2 |
| Component B | 1 | 1.5 |
| Component C | 0.01 | 0.02 |
The particle diameter of above-mentioned Ludox used is 16nm；Nano-meter SiO_2 used2Dispersion liquid is particle diameter 120nm solids contents 20%
SiO2Aqueous dispersions.
Embodiment 3
First, priming paint：
(1) component A hosts：
1. first by Ludox 40% with 240 mesh nylon net filters, and stirred with 700rpm/ minutes rotating speed；
2. under 700rpm/ minutes stirring, bentonite 0.7% is added, and with the Rate Dispersion 5 of 900rpm/ minutes
Minute；
3. in above-mentioned compound, under 700rpm/ minutes stirring, titanium dioxide 32.3% and aluminum oxide abrasion-resistant powder are added
7%, with the Rate Dispersion 15 minutes of 900rpm/ minutes；
4. above-mentioned compound is ground to fineness less than 10um using basket sand machine, with 700rpm/ minutes stirring
Add Nano-meter SiO_22Dispersion liquid 20%, and with 700rpm/ minutes stirring 10 minutes after make finished product.
The viscosity of priming paint finished product is 12 ± 3 seconds, and the viscosity No. 4 cups of DIN are measured at a temperature of 23 DEG C.
(2) component B curing agent：MTMS 97%, silicone oil 3% are rolled under 110rpm/ minutes speed
Uniformly.
(3) component C catalyst：Catalyst component C formic acid 100% can be used directly without specially treated.
2nd, finish paint：
(1) component A hosts：
1. first by Ludox 74% with 240 mesh nylon net filters, and stirred with 700rpm/ minutes rotating speed；
2. uniform deionized water 20% and the mixture of butyl glycol ether 3% will be pre-mixed, silicon be added in stirring molten
In glue；
3. in above-mentioned compound, under 700rpm/ minutes stirring, pearl powder 3% is added, and with 900rpm/ minutes
Rate Dispersion 5 minutes.
(2) component B curing agent：MTMS 97%, silicone oil 3% are rolled under 110rpm/ minutes speed
Uniformly.
(3) component C catalyst：Catalyst component C formic acid 100% can be used directly without specially treated.
3rd, finished product is after curing process curing, its curing process is as follows：
(1) priming paint：Above-mentioned catalyst component C is proportionally added into curing agent B component according to the weight proportion shown in table 3
In, rock in well mixed rear all additions component As, will firmly be rocked until each component is mixed thoroughly after container good seal
And after reaction reaches 35 DEG C to temperature, be placed in the rolling oil machine of rolling speed 150rpm, curing 3h is rolled, after curing
Mixture is removed from rolling oil machine, stand-by after it is cooled to room temperature；
(2) finish paint：Above-mentioned catalyst component C is proportionally added into curing agent B component according to the weight proportion shown in table 3
In, rock in well mixed rear all additions component As, will firmly be rocked until each component is mixed thoroughly after container good seal
And after reaction reaches 35 DEG C to temperature, be placed in the rolling oil machine of rolling speed 150rpm, curing 22h is rolled, after curing
Mixture from rolling oil machine on remove, it is stand-by after it is cooled to room temperature.
4th, film：Usage amount according to the priming paint shown in table 3 and finish paint carries out film, during film, the requirement spray of priming paint thickness
40um is applied to, the requirement of finish paint thickness is sprayed into 6um.
The priming paint of 3 embodiment of table 3 and finish paint each component and weight proportion
| Component (unit：Weight portion) | Priming paint | Finish paint |
| Component A | 4 | 2 |
| Component B | 1.5 | 1 |
| Component C | 0.02 | 0.015 |
The particle diameter of above-mentioned Ludox used is 12nm；Nano-meter SiO_2 used2Dispersion liquid is particle diameter 110nm solids contents 20%
SiO2Aqueous dispersions.
Pearl powder used by embodiment 1~3 is that pearl powder is Merck silvery white pearl essence Iriodin 153.
Film performance is tested
The film performance test result that embodiment 1 is prepared is as shown in table 4.
The film performance of table 4 is tested
The above is only the preferred embodiment of the present invention, the invention is not restricted to above example.It is appreciated that ability
The oher improvements and changes that field technique personnel directly derive or associate without departing from the spirit and concept in the present invention,
It is considered as being included within protection scope of the present invention.
Claims (5)
1. a kind of ceramic coating with antibacterial functions, is made up of priming paint and finish paint two parts, it is characterised in that the priming paint and
Finish paint is constituted by component A hosts, component B curing agent and component C catalyst；
The component A of the priming paint and finish paint:Component B:Component C is by weight ratio:2-4:1-2:0.01-0.02；
The raw material weight percent of the primer composition A hosts is：
The raw material weight percent of the finish paint component A hosts is：
The particle diameter of the Ludox is 11nm；
The Nano-meter SiO_22Dispersion liquid is the SiO of particle diameter 120nm solids contents 20%2Aqueous dispersions；
The priming paint is with the raw material weight percent of finish paint component B curing agent：
MTMS 96-98%
Silicone oil 2-4；
The priming paint is with the raw material weight percent of finish paint component C catalyst：
Formic acid 100%.
2. the ceramic coating with antibacterial functions according to claim 1, it is characterised in that the inorganic pigment is titanium white
Powder.
3. the ceramic coating with antibacterial functions according to claim 1, it is characterised in that the pearl powder is Merck silvery white
Pearl essence Iriodin 153.
4. a kind of preparation method of the ceramic coating with antibacterial functions described in claim 1 or 2, it is characterised in that specific step
Suddenly it is：
(1) primer composition A hosts：
1. first by Ludox 200-300 mesh nylon net filters, and stirred with 600-800rpm/ minutes rotating speed；
2. uniform deionized water and butyl glycol ether mixture will be pre-mixed, in being added to Ludox in stirring；
3. in above-mentioned compound, under 600-800rpm/ minutes stirring, bentonite is added, and with 800-1000rpm/ points
The Rate Dispersion of clock 5 minutes；
4. in above-mentioned compound, under 600-800rpm/ minutes stirring, inorganic pigment and aluminum oxide abrasion-resistant powder are added, with
Rate Dispersion 15-20 minutes of 800-1000rpm/ minutes；
5. after above-mentioned compound being ground into fineness less than 15 μm using basket sand machine, with 600-800rpm/ minutes stirring
Lower addition Nano-meter SiO_22Dispersion liquid, and the finished product made after stirring 5-10 minutes；
The viscosity of the finished product is 12 ± 3 seconds, and the viscosity No. 4 cups of DIN are measured at a temperature of 23 DEG C；
(2) finish paint component A hosts：
1. first by Ludox 200-300 mesh nylon net filters, and stirred with 600-800rpm/ minutes rotating speed；
2. uniform deionized water and butyl glycol ether mixture will be pre-mixed, in being added to Ludox in stirring；
3. in above-mentioned compound, under 600-800rpm/ minutes stirring, pearl powder is added, and with 800-1000rpm/ minutes
Rate Dispersion 5 minutes；
The viscosity of the finished product is 8-12 seconds, and viscosity DIN4 cups are measured at a temperature of 23 DEG C；
(3) priming paint and finish paint component B curing agent：
MTMS, silicone oil is uniform in 100-120rpm/ minutes speed scroll；
(4) priming paint and finish paint component C catalyst：
Catalyst component C：Formic acid can be used directly without specially treated；
(5) finished product is after curing process is cured with priming and finish paint each component, the curing process is as follows：
Priming paint：Above-mentioned catalyst component C is proportionally added into curing agent B component, after being well mixed in whole addition component As,
, with after being mixed thoroughly and reacting and reach 30-40 DEG C to temperature, rolling speed 120- will be placed on after container good seal
In the rolling oil machine of 180rpm, curing 2-4h is rolled, the mixture after curing is removed from rolling oil machine, after it is cooled to room temperature
It is stand-by；
Finish paint：Above-mentioned catalyst component C is proportionally added into curing agent B component, after being well mixed in whole addition component As,
To be mixed thoroughly after container good seal and reacted after reaching 30-40 DEG C to temperature, be placed on rolling speed 120-
In the rolling oil machine of 180rpm, curing 20-24h is rolled, the mixture after curing is removed from rolling oil machine, treat that it is cooled to room temperature
It is stand-by afterwards；
(6) requirement of priming paint thickness is sprayed into 30-45 μm when using, and the requirement of finish paint thickness is sprayed into 3-10 μm.
5. preparation method according to claim 4, it is characterised in that the whole dispersion, stirring and temperature in process of lapping
It is not less than 10 DEG C and not higher than 35 DEG C.
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| CN105330200A (en) * | 2015-11-30 | 2016-02-17 | 无锡大塘复合材料有限公司 | Crack-resistant high-toughness non-stick paint |
| CN105331211A (en) * | 2015-11-30 | 2016-02-17 | 无锡大塘复合材料有限公司 | Hard antibacterial water-based non-stick coating |
| CN105295472A (en) * | 2015-11-30 | 2016-02-03 | 无锡大塘复合材料有限公司 | High-thermal-conductivity non-stick paint |
| CN105778575A (en) * | 2015-12-18 | 2016-07-20 | 广州卡秀堡辉涂料有限公司 | Aqueous ceramic non-stick coating material for kitchenware surfaces and preparation method for aqueous ceramic non-stick coating material |
| CN109536008A (en) * | 2017-08-11 | 2019-03-29 | 永康市悦味厨具有限公司 | A kind of titaniferous anti-bacteria ceramic coating and preparation method thereof |
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| CN110294947B (en) * | 2019-07-02 | 2021-12-03 | 中国科学院宁波材料技术与工程研究所 | High-temperature-resistant coating for metal surface and preparation method and application thereof |
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| CN111040482A (en) * | 2019-12-27 | 2020-04-21 | 广东四方英特宝新材料科技有限公司 | Curtain wall coating and preparation method thereof |
| JP7054586B1 (en) * | 2021-01-21 | 2022-04-14 | 日東電工株式会社 | Primer and anticorrosion structure |
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Address after: Lake town of Xishan District 214116 Jiangsu city of Wuxi province Yan Xiang Road No. 98 Patentee after: Caxiu Wanhui (Wuxi) high tech materials Co., Ltd Address before: Lake town of Xishan District 214116 Jiangsu city of Wuxi province Yan Xiang Road No. 98 Patentee before: CMW COATINGS (WUXI) Ltd. |