Background technology
Along with to the continuous exploration and development of unconventional gas resources, the research for Unconventional forage reservoir is also deepening continuously.At present, when studying unconventional reservoir, particularly low hole, hypotonic shale reservoir, one of the spontaneous imbibition intensity of reservoir rock research becoming emphasis.
The sandstone of shale spontaneous imbibition energy force rate routine is stronger, this wherein greatly reason just depend on the matrix of shale.When fracturing liquid carries out pressure break to shale reservoir, due to powerful capillary force, make liquid from crack to matrix flow, enter in the gap of matrix and inside thereof.This process displacement can go out the adsorbed gas of its content and by its deep research, can obtain some physical propertys of reservoir rock, as parameters such as the imbibition intensity of rock, imbibition speed and throat distribution.
From engineering viewpoint, carrying out in frac job to compact reservoir, fracturing fluid recovery (backflow) rate is one of numerous emphasis parameters paid close attention in frac job.At low permeability gas reservoir reservoir, particularly in clay shale with low permeability gas reservoir, because blowhole venturi is narrow, hollow billet effect is obvious, and rock has super dryness, its water saturation is also lower than irreducible water saturation, even if do not have high pressure during pressure break, fracturing liquid also can be entered in rock by spontaneous imbibition effect.
Usually in the fracturing liquid work carrying out conventional reservoir, because the agency part fracturing liquids such as pore constriction trapping are trapped in rock, reservoir is caused to the injuries such as water lock, but in clay shale with low permeability gas reservoir, fracturing liquid is trapped in after in rock, can be spontaneous to imbibition in matrix, thus reduce even solution and dewater the fracturing liquids such as lock to the injury of reservoir.
In sum, how research evaluates the spontaneous imbibition of liquid enters this phenomenon of matrix, can provide basic research for the injury analysis of frac job to gas reservoir, also for the design of low permeability gas reservoir fracturing liquid provides guidance instruction.Therefore, need a kind of measurement mechanism of invention badly, so as fast, evaluate the spontaneous imbibition ability of shale gas reservoir rock matrix easily.
Imbibition measurement mechanism of the prior art is by being soaked in cylinder by rock core, and connects in one end of cylinder the glass tube that can be measured the height of water, monitors for liquid level in glass tube.By record liquid level falling head over time, calculate matrix and suck the quality of water over time.If if the spontaneous water absorbing capacity of matrix is little, the defect error of this device can be apparent, because the diameter of glass tube limits by manufacturing process, if diameter is too large, level change is not obvious, if diameter is too little, glass tube inherently can produce hollow billet effect, interference experiment data, affect experimental result.In addition, in water absorption course, the gas of rock interior can be arranged in the form of bubbles and displace, if can not ensure that bubble is discharged from thin glass tube, can have impact on the precision of experiment.
Summary of the invention
The present invention, for overcoming Problems existing in aforementioned means, realizes fast simultaneously, evaluates easily the spontaneous imbibition ability of shale gas reservoir rock matrix, propose a kind of matrix imbibition measurement mechanism.This device can measure the fracturing liquid quality relation over time that matrix sample sucks under constant temperature normal pressure, this matrix sample rate of water absorption, capillary force and water absorbing capacitys etc. are studied from spontaneous imbibition phenomena, thus can better be familiar with the character such as the throat distribution of rock, for the work of Optimum Fracturing liquid provides guidance and foundation.
For achieving the above object, the present invention proposes a kind of matrix imbibition measurement mechanism, comprising casing 1, in casing 1, be provided with test cabinet 2, in test cabinet 2, being provided with thermal insulation board 3 and Weighing module 4; Wherein, test cabinet 2 is divided into two spaces by thermal insulation board 3, the first heating and temperature controlling device 7 is provided with in first space 5, the temperature that the second heating and temperature controlling device 8, first heating and temperature controlling device 7 and the second heating and temperature controlling device 8 are respectively used in adjustment first space 5 and second space 6 is provided with in second space 6; Weighing module 4 comprises: stationary installation 9, matrix bag 10, imbibition pipe 11, catheter 12, closed container 13, strain gauge 14; Wherein, stationary installation 9, matrix bag 10, imbibition pipe 11 are arranged in the first space 5, and closed container 13, strain gauge 14 are arranged in second space 6; Closed container 13 is positioned on strain gauge 14, and inside fills experiment liquid, is full of experiment liquid in imbibition pipe 11 and catheter 12, and one end of catheter 12 is communicated with imbibition pipe 11, and the other end inserts in the experiment liquid in closed container 13; Matrix bag 10, built with matrix to be measured, is immersed in the experiment liquid in imbibition pipe 11; Stationary installation 9 is arranged in imbibition pipe 11, for fixing matrix bag 10, makes matrix bag 10 keep stable; After testing liquid described in the matrix imbibition to be measured in matrix bag 10, imbibition pipe 11 sucks the experiment liquid in closed container 13 by catheter 12, strain gauge 14 gathers the mass change of the experiment liquid in closed container 13, generate mass change Data Concurrent and deliver to computing machine 15, computing machine 15 generates imbibition measurement result and screen display by after described mass change data processing, so that the imbibition change of Real Time Observation matrix to be measured.
The matrix spontaneous imbibition measurement mechanism tool that the present invention proposes has the following advantages: 1, this device sets rock sample drying chamber, measuring chamber and signal output of one, can be implemented in situ of drilling well and constant temperature drying is carried out to detritus sample, be processed into required matrix, put into experiment liquid again to measure for its spontaneous imbibition process, entirety is body structure, convenient carrying, and shock attenuation device is arranged at bottom, situ of drilling well complex environment can be adapted to, ensure data precision.2, this device is lower to rock core shape need, relies on this device, only needs the matrix landwaste in drilling process being processed into required order number just can evaluate the spontaneous imbibition ability of reservoir, does not need down-hole to get core, saves testing cost.3, this device is simple to operate, utilize this device carry out spontaneous imbibition experiment time, can by signal output part by matrix quality over time data export computing machine to, realize automatic acquisition function.
Accompanying drawing explanation
Accompanying drawing described herein is used to provide a further understanding of the present invention, forms a application's part, does not form limitation of the invention.In the accompanying drawings:
Fig. 1 is the matrix imbibition measurement mechanism structural representation of one embodiment of the invention.
Fig. 2 is the Weighing module structural representation of one embodiment of the invention.
Accompanying drawing indicates and illustrates:
Casing 1, test cabinet 2, thermal insulation board 3, Weighing module 4, first space 5, second space 6, first heating and temperature controlling device 7, second heating and temperature controlling device 8, stationary installation 9, matrix bag 10, imbibition pipe 11, catheter 12, closed container 13, strain gauge 14, computing machine 15, first temperature sensor 16, first electro-heat equipment 17, first radiator valve 18, second temperature sensor 19, second electro-heat equipment 20, second radiator valve 21, vessel clamp 22, drying chamber 23, 3rd heating and temperature controlling device 24, bottom is provided with ventilating opening 25, three-temperature sensor 26, 3rd electro-heat equipment 27, 3rd radiator valve 28, shock attenuation device 29.
Embodiment
Below coordinating diagram and preferred embodiment of the present invention, setting forth the technological means that the present invention takes for reaching predetermined goal of the invention further.
Fig. 1 is the matrix imbibition measurement mechanism structural representation of one embodiment of the invention.As shown in Figure 1, this device comprises: casing 1, is provided with test cabinet 2 in casing 1, is provided with thermal insulation board 3 and Weighing module 4 in test cabinet 2.Wherein,
Test cabinet 2 is divided into two spaces by thermal insulation board 3, the first heating and temperature controlling device 7 is provided with in first space 5, the temperature that the second heating and temperature controlling device 8, first heating and temperature controlling device 7 and the second heating and temperature controlling device 8 are respectively used in adjustment first space 5 and second space 6 is provided with in second space 6.
Fig. 2 is the Weighing module structural representation of one embodiment of the invention.As shown in Figure 2, Weighing module 4 comprises: stationary installation 9, matrix bag 10, imbibition pipe 11, catheter 12, closed container 13, strain gauge 14.Wherein,
Stationary installation 9, matrix bag 10, imbibition pipe 11 are arranged in the first space 5, and closed container 13, strain gauge 14 are arranged in second space 6.
Closed container 13 is positioned on strain gauge 14, and inside fills experiment liquid, is full of experiment liquid in imbibition pipe 11 and catheter 12, and one end of catheter 12 is communicated with imbibition pipe 11, and the other end inserts in the experiment liquid in closed container 13.
Matrix bag 10, built with matrix to be measured, is immersed in the experiment liquid in imbibition pipe 11.In matrix bag 10, only have inner matrix to be measured to suck experiment liquid, and the bag of outside does not suck experiment liquid.
Stationary installation 9 is arranged in imbibition pipe 11, for fixing matrix bag 10, makes matrix bag 10 keep stable.
After testing liquid described in the matrix imbibition to be measured in matrix bag 10, imbibition pipe 11 sucks the experiment liquid in closed container 13 by catheter 12, strain gauge 14 gathers the mass change of the experiment liquid in closed container 13, generate mass change Data Concurrent and deliver to computing machine 15, computing machine 15 generates imbibition measurement result and screen display by after described mass change data processing, so that the imbibition change of Real Time Observation matrix to be measured.In experimentation, as long as ensure that matrix bag 10 is stablized, fluid injection simultaneously keeps slowly, there will not be bubble in imbibition pipe 11.
Preferably, the outer wall of test cabinet 2 can be heat-barrier material.
Preferably, bottom casing 1, shock attenuation device 29 can being set, stablizing, for whole experimental provision provides metastable working environment for making casing 1.
Preferably, Weighing module 4 can also comprise vessel clamp 22, for turning off or opening catheter 12.
Preferably, the measuring accuracy of strain gauge 14 can reach 0.1mg.
In the present embodiment, can also be provided with drying chamber 23 in casing 1, the outer wall of drying chamber 23 is heat-barrier material, and inside is provided with the 3rd heating and temperature controlling device 24, and bottom is provided with ventilating opening 25.
In the present embodiment, the first heating and temperature controlling device 7 comprises: the first temperature sensor 16, first electro-heat equipment 17, first radiator valve 18; First temperature sensor 16 and the first electro-heat equipment 17 are connected to the first radiator valve 18; Wherein, the first radiator valve 18 senses the temperature in the first space 5 by the first temperature sensor 16, and regulates the temperature in the first space 5 according to experimental temperature scope control first electro-heat equipment 17 preset.
Second heating and temperature controlling device 8 comprises: the second temperature sensor 19, second electro-heat equipment 20, second radiator valve 21; Second temperature sensor 19 and the second electro-heat equipment 20 are connected to the second radiator valve 21; Wherein, the second radiator valve 21 senses the temperature in second space 6 by the second temperature sensor 19, and regulates the temperature in second space 6 according to experimental temperature scope control second electro-heat equipment 20 preset.
3rd heating and temperature controlling device 24 comprises: three-temperature sensor 26, the 3rd electro-heat equipment 27, the 3rd radiator valve 28; Three-temperature sensor 26 and the 3rd electro-heat equipment 27 are connected to the 3rd radiator valve 28; Wherein, the 3rd radiator valve 28 senses the temperature in drying chamber 23 by three-temperature sensor 26, and regulates the temperature in drying chamber 23 according to experimental temperature scope control the 3rd electro-heat equipment 27 preset.
In order to more clearly explain above-mentioned matrix imbibition measurement mechanism, be described below in conjunction with a specific embodiment, but it should be noted that this embodiment is only to better the present invention is described, do not form and the present invention is limited improperly.
Below in conjunction with an application scenarios, reference also utilizes the matrix imbibition measurement mechanism described by Fig. 1, Fig. 2 to carry out on-the-spot matrix imbibition evaluation, and concrete steps are as follows:
Step 1, first, in the rock fragment gathered at the scene, selects sizeable fragment, and put into drying chamber 23 and dry, drying chamber temperature is set to 105 degrees Celsius.Drying time, depending on rock sample size, general dried quality after 10 hours and is no longer changed, and thinks rock drying.Rock after oven dry is processed into the matrix of required order number, puts into matrix bag 10.
Step 2, installs Weighing module 4 according to shown in Fig. 2, is full of experiment liquid (now, vessel clamp 22 is in off state), injects a certain amount of experiment liquid in closed container 13 in imbibition pipe 11 and catheter 12.The signal output part of strain gauge 14 is connected with computing machine 15, starts strain gauge 14 and computing machine 15, strain gauge 14 is reset, measures the weight of current closed container 13 as initial weight.
Step 3, opens heating and temperature controlling device, regulates the temperature in test cabinet to reach constant temperature, opens vessel clamp 22.
Step 4, utilizes the weight situation of change in time of computer recording closed container, and the data of record is converted to matrix imbibition quality data over time.By checking imbibition measurement result, analyzing parameters such as obtaining self-priming capillary force, liquid rate of water absorption, completing the spontaneous imbibition evaluation of this matrix.
The matrix spontaneous imbibition measurement mechanism tool that the present invention proposes has the following advantages: 1, this device sets rock sample drying chamber, measuring chamber and signal output of one, can be implemented in situ of drilling well and constant temperature drying is carried out to detritus sample, be processed into required matrix, then put into experiment liquid measure for its spontaneous imbibition process.This device entirety is body structure, convenient carrying, and shock attenuation device is arranged at bottom, can adapt to situ of drilling well complex environment, ensures data precision.2, this device is lower to rock core shape need, relies on this device, only needs the matrix landwaste in drilling process being processed into required order number just can evaluate the spontaneous imbibition ability of reservoir, does not need down-hole to get core, saves testing cost.3, this device is simple to operate, utilize this device carry out spontaneous imbibition experiment time, can by signal output part by matrix quality over time data export computing machine to, realize automatic acquisition function.
Above-described specific embodiment; object of the present invention, technical scheme and beneficial effect are further described; be understood that; the foregoing is only specific embodiments of the invention; the protection domain be not intended to limit the present invention; within the spirit and principles in the present invention all, any amendment made, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.