CN105014691A - Integrated glove box - Google Patents

Integrated glove box Download PDF

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Publication number
CN105014691A
CN105014691A CN201510397246.1A CN201510397246A CN105014691A CN 105014691 A CN105014691 A CN 105014691A CN 201510397246 A CN201510397246 A CN 201510397246A CN 105014691 A CN105014691 A CN 105014691A
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Prior art keywords
glove box
purification
unit
integrated
catalyst
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CN201510397246.1A
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CN105014691B (en
Inventor
张德龙
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Weige Technology Suzhou Co ltd
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Zweig Gas Purification Technology (suzhou) Ltd By Share Ltd
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Abstract

The invention discloses an integrated glove box. The integrated glove box comprises a box body and a transition bin, and further comprises a renewable gas purification system arranged on the box body, wherein the renewable gas purification system comprises a circulating fan and a purification and deoxidization unit filled with a deoxidization material; the circulating fan is used for feeding a recycle gas into the box body; and oxygen in the gas is removed by the deoxidization material in the purification and the deoxidization unit. According to the integrated glove box, as the renewable gas purification system is adopted, a purification system, a circulating fan cabinet and the like at the lower part of the box body are omitted, the circulating fan does not need to be independently closed, and accordingly, the glove box is simple in structure; and the circulating fan and the purification and deoxidization unit which are compact and moderate in size are preferably selected and directly utilized on the side surface, the top surface or the back side of the box body, so that the space occupied by the whole glove box is reduced.

Description

A kind of integrated glove box
Technical field
The invention belongs to technical field of experiment equipment, relate to a kind of glove box, be specifically related to a kind of integrated glove box.
Background technology
Glove box is widely used in medical science, biology, chemical, nuclear energy, lithium electricity, and in the high-tech research field such as machining and manufacturing process.Glove box not only can provide anhydrous for various research and production, the experimental situation of anaerobic, and researcher can also be given with security protection, and such as medical biological fungi-proofing diseases prevention, nuclear energy radiation proof anti-leak, also have anti-toxic gas of chemical etc. simultaneously.
Current glove box mainly comprises casing, purification deoxygenation unit, purification except water unit, cycling element, and control unit etc., some is also containing other impurity clean units (such as organic gas).Principle is exactly that control unit controlled circulation unit is opened, in drive case, gas continues to flow through purification deoxygenation and purifies except water unit, the purification deoxygenation unit that dewaters constantly removes casing and to reveal or scientific research, production operation cause the oxygen that increases and water, makes oxygen and water management in certain limit to meet the requirement of user.
Purification deoxygenation unit, the purification of current glove box remove water unit, cycling element, and other impurity clean units are all functional modules independently, or the deoxygenation collection that dewaters is more together, or the organic gas purification unit dewatered in deoxygenation unit integrates, be then placed in a cupboard with cycling element unification.Make glove box volume become both bulk like this, give transport and use and safeguard and cause a lot of inconvenience.
Summary of the invention
For solving the problems of the technologies described above, the object of the present invention is to provide a kind of integrated glove box, can make that glove box volume is more portable and smart, structural design is simple, it is simply easy to use to control, transport, operation and maintenance are also convenient.
For achieving the above object, technical scheme of the present invention is as follows:
The invention provides a kind of integrated glove box, comprise casing and transitional storehouse, also comprise the renewable gas purge system be arranged on described casing, described renewable gas purge system comprises circulating fan and purification deoxygenation unit, oxygen scavenging material is filled with in described purification deoxygenation unit, described circulating fan is used for recyclegas to deliver in casing, and the oxygen in described gas is removed by the oxygen scavenging material in purification deoxygenation unit by described gas.
Integrated glove box of the present invention, adopts renewable gas purge system, uses glove box reproduction operation station to regenerate described renewable gas purge system after using; Can cancel the cleaning system of lower box, circulating fan cupboard etc., circulating fan does not need to be closed separately yet, thus makes the structure of glove box simple; Thus can optimum option compact and moderate cycling element and purification deoxygenation unit, these structures directly can be utilized at body side or end face or the back side, reduce whole glove box and taken up space.
On the basis of technique scheme, the present invention can also make following improvement:
As preferred scheme, described oxygen scavenging material is palladium catalyst or catalyst catalyst.
As preferred scheme, described oxygen scavenging material is palladium catalyst.
Adopt above-mentioned preferred scheme, make oxygen and hydrogen reaction by filling palladium catalyst in purification deoxygenation unit, palladium catalyst itself does not participate in reaction, does not thus need to arrange regenerative system, do not need cleaning system to regenerate, thus make the structure of glove box simple yet; And can optimum option compact and moderate cycling element and purification deoxygenation unit, make these structures can directly utilize in body side or a small amount of space of end face or the back side; In addition, the oxygen content in glove box can be made to maintain < 1ppm by palladium catalyst deoxygenation, further illustrate its excellent effect.
As preferred scheme, when described oxygen scavenging material is catalyst catalyst, described catalyst catalyst is copper catalyst catalyst and/or manganese catalyst catalyst.
As preferred scheme, described renewable gas purge system is integrated on described casing by integrated interface.
Adopt above-mentioned preferred scheme, through optimization integrated after, casing can not need independent cupboard to place those independently unit and supports, becomes structure simple, compact, uses convenient transportation.
As preferred scheme, described renewable gas purge system also comprises purification except water unit and purification and impurity removal matter unit, described circulating fan, purification deoxygenation unit, purification are all integrated on described casing by integrated interface except water unit and purification and impurity removal matter unit, and described circulating fan, purification deoxygenation unit, purification are connected with purification and impurity removal matter unit successively except water unit.
Adopt above-mentioned preferred scheme, purification can be optimized and to dewater cellular construction, optimize purification and impurity removal matter cellular construction, make the structure of glove box more simple.
As preferred scheme, described casing is also provided with the oxygen sensor for controlling oxygen content and the moisture transducer for controlling moisture.
Adopt above-mentioned preferred scheme, effectively can control the content of moisture and oxygen in glove box.
As preferred scheme, described renewable gas purge system is integrated in described casing side by integrated interface.
Adopt above-mentioned preferred scheme, make the structure of glove box more simple, volume is less, and it is more convenient to use.
As preferred scheme, described filtering cabin is arranged on described casing opposite side, comprises large filtering cabin and little filtering cabin.
As preferred scheme, described casing is also provided with gloves.
On the other hand, the present invention also provides a kind of energy-conserving and environment-protective glove box work station, for regenerating the renewable gas purification units in glove box of the present invention, described work station comprises work station body, also comprise workstation control unit, described work station body is provided with thermal regeneration element, described thermal regeneration element comprises multiple clean unit rest area, described clean unit rest area is for placing the clean unit of glove box, and described thermal regeneration element makes the clean unit of the glove box in clean unit rest area regenerate under the effect of described workstation control unit.
The present invention devise a set of have can regenerate simultaneously many covers new simplify glove box purification deoxygenation, except water unit glove box purification deoxygenation, dewater regeneration unit work station.Reproduction operation station can help all users regenerate use saturated after brand-new design simplify glove box purification deoxygenation, except water unit.Such glove box just does not need to be with renewable purification deoxygenation, except water unit, reduce purchase use cost, the social resources saved, client does not need the regeneration such as purchase hydrogen to save maintenance cost simultaneously, repetition and waste is avoided by reproduction operation station unified configuration regenerated resources, reduce glove box operation and maintenance cost, save the energy, reasonable disposition social resources.
On the basis of technique scheme, the present invention also can make following improvement:
As preferred scheme, described workstation control unit controls the temperature of thermal regeneration element, pressure and air-flow, thus described clean unit is regenerated.
Adopting above-mentioned preferred scheme, by controlling thermal regeneration element suitable temperature, pressure and air-flow, realizing the regeneration of clean unit.
As preferred scheme, described workstation control unit also comprises flow control switch, pressure elements and temperature element (TE, described workstation control unit controls the air-flow of described thermal regeneration element by described flow control switch; Described workstation control unit controls the pressure of described thermal regeneration element by pressure elements, and gives described workstation control unit by described pressure elements by the pressure feedback of described thermal regeneration element; Described workstation control unit controls the temperature of described thermal regeneration element by temperature element (TE, and gives described workstation control unit by described temperature element (TE by the temperature feedback of described thermal regeneration element, thus described clean unit is regenerated.
Adopt above-mentioned preferred scheme, control thermal regeneration element suitable temperature, pressure and air-flow by control element, be easy to control, realize.
As preferred scheme, described thermal regeneration element is also provided with the vacuum control valve, aeration valve and the air bleeding valve that are connected with flow control switch.
Again on the one hand, the present invention also provides a kind of energy-conserving and environment-protective glove box workstation system, for regenerating the renewable gas purification units in glove box of the present invention, described workstation system comprises energy-conserving and environment-protective glove box work station of the present invention, also comprises glove box.
Also on the one hand, the present invention also provides a kind of energy-conserving and environment-protective glove box work station of the present invention for the method for the renewable gas purification units of Regenerated hand casing, comprises the following steps:
1) the renewable gas purification units of the glove box after use is positioned in clean unit rest area;
2) after described workstation control unit senses renewable clean unit, described thermal regeneration element starts, under the control of described control unit, to described thermal regeneration element heating, pressurization or decompression, and control the air-flow entering described thermal regeneration element, thus make described renewable clean unit regeneration.
The method of Regenerated hand casing clean unit of the present invention, by reproduction operation station, regenerate the new glove box simplified of many covers simultaneously and purify deoxygenation, except the glove box purification deoxygenation of water unit, except water unit, reduce purchase use cost, the social resources saved, client does not need the regeneration such as purchase hydrogen to save maintenance cost simultaneously.
Accompanying drawing explanation
Fig. 1 is the front view of integrated glove box of the present invention;
Fig. 2 is the top view of integrated glove box of the present invention;
Fig. 3 is the structural representation of the energy-conserving and environment-protective glove box work station that the gas purification units in integrated glove box of the present invention carries out regenerating;
Fig. 4 is the structured flowchart of the energy-conserving and environment-protective glove box work station that the gas purification units in integrated glove box of the present invention carries out regenerating;
Wherein:
1. oxygen sensor, 2. moisture transducer, 3. casing, 4. great transition storehouse, 5. little transitional storehouse, 6. gloves, 7. circulating fan, 8. purification is except water unit, 9. purifies deoxygenation unit, 10. purification and impurity removal matter unit, 11. integrated interfaces, 12. work station bodies, 13. workstation control unit, 1301. flow control switch, 1302. pressure elements, 1303. temperature element (TEs, 14. thermal regeneration elements, 15. clean unit rest areas, 16. renewable gas purification units.
Detailed description of the invention
The preferred embodiment of the present invention is described in detail below in conjunction with accompanying drawing.
In order to reach object of the present invention, in certain embodiments, as shown in Figure 1-2, integrated glove box of the present invention, comprises casing 3 and transitional storehouse, also comprises the renewable gas purge system be arranged on described casing 3, described renewable gas purge system comprises circulating fan 7 and purification deoxygenation unit 9, be filled with oxygen scavenging material in described purification deoxygenation unit 9, described circulating fan 7 is for delivering in casing 3 by gas, the oxygen in described gas is removed by purification deoxygenation unit 9 by described gas.Integrated glove box of the present invention, adopts renewable gas purge system, uses glove box reproduction operation station to regenerate described renewable gas purge system after using; Can cancel the cleaning system of lower box, circulating fan cupboard etc., circulating fan does not need to be closed separately yet, thus makes the structure of glove box simple; Thus can optimum option compact and moderate cycling element and purification deoxygenation unit, these structures directly can be utilized at body side or end face or the back side, reduce whole glove box and taken up space.
In order to optimize implementation result of the present invention further, described oxygen scavenging material is palladium catalyst or catalyst catalyst.
In order to optimize implementation result of the present invention further, described oxygen scavenging material is palladium catalyst.Make oxygen and hydrogen reaction by filling palladium catalyst in purification deoxygenation unit, palladium catalyst itself does not participate in reaction, does not thus need to arrange regenerative system, does not need cleaning system to regenerate yet, thus make the structure of glove box simple; And can optimum option compact and moderate cycling element and purification deoxygenation unit, make these structures can directly utilize in body side or a small amount of space of end face or the back side; In addition, the oxygen content in glove box can be made to maintain < 1ppm by palladium catalyst deoxygenation, further illustrate its excellent effect.
In order to optimize implementation result of the present invention further, when described oxygen scavenging material is catalyst catalyst, described catalyst catalyst is copper catalyst catalyst and/or manganese catalyst catalyst.
In order to optimize implementation result of the present invention further, described renewable gas purge system is integrated on described casing 3 by integrated interface 11.Through optimization integrated after, casing can not need independent cupboard to place those independently unit and supports, becomes structure simple, compact, uses convenient transportation.
In order to optimize implementation result of the present invention further, described renewable gas purge system also comprises purification except water unit 8 and purification and impurity removal matter unit 10, described circulating fan 7, purification deoxygenation unit 9, purification are all integrated on described casing 3 by integrated interface 11 except water unit 8 and purification and impurity removal matter unit 10, and described circulating fan 7, purification deoxygenation unit 9, purification are connected with purification and impurity removal matter unit 10 successively except water unit 8.Optimize purification to dewater cellular construction, optimize purification and impurity removal matter cellular construction, make the structure of glove box more simple.
In order to optimize implementation result of the present invention further, described casing 3 is also provided with the oxygen sensor 1 for controlling oxygen content and the moisture transducer 2 for controlling moisture, thus effectively can controls the content of moisture and oxygen in glove box.
In order to optimize implementation result of the present invention further, described filtering cabin is arranged on described casing 3 opposite side, comprises large filtering cabin 4 and little filtering cabin 5.
In order to optimize implementation result of the present invention further, described casing 3 is also provided with gloves 6.
In order to reach object of the present invention, in certain embodiments, as shown in Figure 3-4, energy-conserving and environment-protective glove box work station of the present invention, comprise work station body 12, also comprise workstation control unit 13, described work station body 12 is provided with thermal regeneration element 14, described thermal regeneration element 14 comprises multiple renewable gas purification units rest area 15, described clean unit rest area 15 is for placing the renewable gas purification units 16 of glove box, described thermal regeneration element 14 makes the renewable gas purification units 16 of the glove box in clean unit rest area 15 regenerate under the effect of described workstation control unit 13.The reproduction operation station that the present invention designs has the glove box that simultaneously can regenerate the new simplification of many covers and purifies deoxygenation, except the glove box purification deoxygenation of water unit, except water unit; Can help all users regenerate use saturated after brand-new design simplify glove box purification deoxygenation, except water unit.Such glove box just does not need to be with renewable purification deoxygenation, except water unit, reduce purchase use cost, the social resources saved, client does not need the regeneration such as purchase hydrogen to save maintenance cost simultaneously, repetition and waste is avoided by reproduction operation station unified configuration regenerated resources, reduce glove box operation and maintenance cost, save the energy, reasonable disposition social resources.
In order to optimize implementation result of the present invention further, described workstation control unit 13 controls the temperature of thermal regeneration element 12, pressure and air-flow, thus described clean unit 14 is regenerated.By controlling thermal regeneration element suitable temperature, pressure and air-flow, realize the regeneration of clean unit.
In order to optimize implementation result of the present invention further, described workstation control unit 13 also comprises flow control switch 1301, pressure elements 1302 and temperature element (TE 1303, described workstation control unit 13 controls the air-flow of described thermal regeneration element 14 by described flow control switch 1301, described workstation control unit 13 controls the pressure of described thermal regeneration element 14 by pressure elements 1302, and gives described workstation control unit 13 by described pressure elements by the pressure feedback of described thermal regeneration element 14; Described workstation control unit 13 controls the temperature of described thermal regeneration element 14 by temperature element (TE 1303, and give described workstation control unit 13 by described temperature element (TE 1303 by the temperature feedback of described thermal regeneration element 14, thus described renewable gas purification units 16 is regenerated, described pressure elements 1302 can be pressure sensor, and described temperature element (TE 1303 is temperature sensor.Control thermal regeneration element suitable temperature, pressure and air-flow by control element, be easy to control, realize.
In order to optimize implementation result of the present invention further, described workstation control unit 13 controls the temperature of described thermal regeneration element 14 by temperature element (TE 1303.
In order to optimize implementation result of the present invention further, described thermal regeneration element 14 is also provided with the vacuum control valve, aeration valve and the air bleeding valve that are connected with flow control switch 1301.
In order to reach object of the present invention, in some embodiments, energy-conserving and environment-protective glove box workstation system of the present invention, comprises energy-conserving and environment-protective glove box work station of the present invention, also comprises glove box.
In order to reach object of the present invention, in some embodiments, energy-conserving and environment-protective glove box work station of the present invention is used for the method for Regenerated hand casing clean unit, comprises the following steps:
1) the renewable gas purification units of the glove box after use is positioned in clean unit rest area;
2) after described workstation control unit senses renewable gas purification units, described thermal regeneration element starts, under the control of described control unit, to described thermal regeneration element heating, pressurization or decompression, and control the air-flow entering described thermal regeneration element, thus make described renewable clean unit regeneration.
Above-described is only the preferred embodiment of the present invention, it should be pointed out that for the person of ordinary skill of the art, and without departing from the concept of the premise of the invention, can also make some distortion and improvement, these all belong to protection scope of the present invention.

Claims (10)

1. an integrated glove box, comprise casing and transitional storehouse, it is characterized in that, also comprise the renewable gas purge system be arranged on described casing, described renewable gas purge system comprises circulating fan and purification deoxygenation unit, be filled with oxygen scavenging material in described purification deoxygenation unit, described circulating fan is used for recyclegas to deliver in casing, and the oxygen in described gas is removed by the oxygen scavenging material in described purification deoxygenation unit by described gas.
2. integrated glove box according to claim 1, is characterized in that, described oxygen scavenging material is palladium catalyst or catalyst catalyst.
3. integrated glove box according to claim 2, is characterized in that, described oxygen scavenging material is palladium catalyst.
4. integrated glove box according to claim 2, is characterized in that, when described oxygen scavenging material is catalyst catalyst, described catalyst catalyst is copper catalyst catalyst and/or manganese catalyst catalyst.
5. integrated glove box according to claim 2, is characterized in that, described gas purge system is integrated on described casing by integrated interface.
6. integrated glove box according to claim 5, it is characterized in that, described renewable gas purge system also comprises purification except water unit and purification and impurity removal matter unit, described circulating fan, purification deoxygenation unit, purification are all integrated on described casing by integrated interface except water unit and purification and impurity removal matter unit, and described circulating fan, purification deoxygenation unit, purification are connected with purification and impurity removal matter unit successively except water unit.
7. integrated glove box according to any one of claim 1 to 6, is characterized in that, described casing is also provided with the oxygen sensor for controlling oxygen content and the moisture transducer for controlling moisture.
8. the integrated glove box according to any one of claim 2 to 6, is characterized in that, described renewable gas purge system is integrated in described casing side by integrated interface.
9. integrated glove box according to claim 8, is characterized in that, described transitional storehouse is arranged on described casing opposite side, comprises great transition storehouse and little transitional storehouse.
10. integrated glove box according to any one of claim 1 to 6, is characterized in that, described casing is also provided with gloves.
CN201510397246.1A 2015-07-08 2015-07-08 A kind of integrated glove box Active CN105014691B (en)

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CN105014691B CN105014691B (en) 2017-06-06

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107170124A (en) * 2017-06-23 2017-09-15 威格气体纯化科技(苏州)股份有限公司 A kind of Internet of Things glove box service system
CN114622271A (en) * 2022-02-10 2022-06-14 合肥科晶材料技术有限公司 Water-removing and oxygen-removing system of small-sized tube furnace

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0411794A1 (en) * 1989-07-20 1991-02-06 William Joseph Foster Anaerobic cabinet
GB2290044A (en) * 1994-06-07 1995-12-13 Peter Bernard Miller Glove boxes
CN2693437Y (en) * 2004-03-10 2005-04-20 赵明华 Vacuum glove experiment box
CN203003907U (en) * 2012-11-09 2013-06-19 上海米开罗那机电技术有限公司 Glove box capable of ensuring water oxygen index to be always below 1ppm in process of use
CN203665550U (en) * 2013-10-22 2014-06-25 甘肃大象能源科技有限公司 Glove box with steam medium regeneration function
CN203973569U (en) * 2014-06-19 2014-12-03 袁洪林 A kind of glove box that can realize automatic control
CN104175333A (en) * 2014-07-22 2014-12-03 张德龙 Multifunctional glovebox purification device

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0411794A1 (en) * 1989-07-20 1991-02-06 William Joseph Foster Anaerobic cabinet
GB2290044A (en) * 1994-06-07 1995-12-13 Peter Bernard Miller Glove boxes
CN2693437Y (en) * 2004-03-10 2005-04-20 赵明华 Vacuum glove experiment box
CN203003907U (en) * 2012-11-09 2013-06-19 上海米开罗那机电技术有限公司 Glove box capable of ensuring water oxygen index to be always below 1ppm in process of use
CN203665550U (en) * 2013-10-22 2014-06-25 甘肃大象能源科技有限公司 Glove box with steam medium regeneration function
CN203973569U (en) * 2014-06-19 2014-12-03 袁洪林 A kind of glove box that can realize automatic control
CN104175333A (en) * 2014-07-22 2014-12-03 张德龙 Multifunctional glovebox purification device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107170124A (en) * 2017-06-23 2017-09-15 威格气体纯化科技(苏州)股份有限公司 A kind of Internet of Things glove box service system
CN114622271A (en) * 2022-02-10 2022-06-14 合肥科晶材料技术有限公司 Water-removing and oxygen-removing system of small-sized tube furnace

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Address after: No. 58, Tingtao Road, Suzhou Industrial Park, Jiangsu 215000

Patentee after: Weige Technology (Suzhou) Co.,Ltd.

Address before: 215026 No.2 workshop, Xinxing Industrial Park, 78 Xinglin street, Suzhou Industrial Park, Jiangsu Province

Patentee before: VIGOR GAS PURIFICATION TECHNOLIGIES, Inc.