CN104175333A - Multifunctional glovebox purification device - Google Patents
Multifunctional glovebox purification device Download PDFInfo
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- CN104175333A CN104175333A CN201410350891.3A CN201410350891A CN104175333A CN 104175333 A CN104175333 A CN 104175333A CN 201410350891 A CN201410350891 A CN 201410350891A CN 104175333 A CN104175333 A CN 104175333A
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Abstract
The invention relates to a multifunctional glovebox purification device which comprises a column body, wherein a first cavity, a second cavity and a third cavity which are communicated are sequentially formed in the column body in a working gas inlet direction, wherein the first cavity is filled with an organic solvent adsorbing material, the second cavity is filled with a deoxidizing material, the third cavity is filled with a dewatering material, a working gas inlet and a vacuumizing port are formed in the first cavity, and a working gas outlet is formed in the third cavity. According to the device, the working gas enters from the inlet, passes through the first cavity, the second cavity and the third cavity sequentially and is discharged from the working gas outlet; gas is purified, the effects of organic solvent adsorbing, deoxidizing and dewatering are achieved in the three cavities sequentially, and compared with the prior art, the problems that two column bodies are required to be used for removing an organic solvent, oxygen and water respectively, the pipeline is complicated and space is occupied due to the fact that three filling materials influence and interfere each other during regeneration are solved; and multiple purification functions and regeneration are achieved in the same column body, the structure is simple, the leakage rate is reduced, the space utilization rate is high, and the working efficiency is increased simultaneously.
Description
Technical field
The invention belongs to glove box field, relate in particular to a kind of multifunctional hand casing purifier.
Background technology
Glove box is that high purity inert gas is filled with in casing, and is circulated throughout the moisture that filters wherein and the laboratory equipment of oxygen.Glove box can provide the atmosphere of inert gases of the sealing of anhydrous and oxygen-free, both can prevent the material of water and oxygen sensitive to occur to go bad, and can avoid again harmful substance to be exposed in air.Glove box comprises main box and transfer chamber.Minimum for the oxygen in glove box main box and moisture are dropped to, need supporting decontaminating column, external work gas is first passed into casing again by decontaminating column, and the gas in casing need to be circulated by decontaminating column when glove box is worked.
In conventional art, molecular sieve and copper catalyst are housed in decontaminating column, can play respectively the function dewatering with deoxygenation.But user is when using glove box; usually can use a large amount of organic solvents, these organic solvents can volatilize, be diffused in glove box body and pipeline, not only can pollute the operating environment in casing; more copper catalyst poisoning be can make, water oxygen probe, vavuum pump and magnetic valve damaged.When opening transfer chamber, the organic solvent in casing can be diffused in the air outside glove box, and grievous injury operating personnel's is healthy.In order to adsorb organic solvent, traditional glove box is general adopts extra decontaminating column, and needs to change sorbing material after sorbing material absorption is saturated, has both increased cost, easily causes again glove box to leak, more can reduce operating efficiency.
Therefore, need a kind of glove box purifier that integrates the functions such as absorption organic solvent, adsorbed water, deoxygenation badly.
Summary of the invention
The object of the invention is to overcome the defect that prior art exists, provide a kind of have dewater, the multifunctional hand casing purifier of deoxygenation, absorption organic solvent.
The technical scheme that realizes the object of the invention is: a kind of multifunctional hand casing purifier, comprise cylinder, described column body is disposed with along work gas airintake direction the first chamber, the second chamber and the 3rd chamber being connected, in described the first chamber, fill organic solvent adsorbing material, in described the second chamber, fill deoxygenation material, in described the 3rd chamber, fill the material that dewaters, on described the first chamber, be provided with work gas air inlet and vacuum orifice, on described the 3rd chamber, be provided with work gas gas outlet.
Further, the connectivity part of described the first chamber, the second chamber and the 3rd chamber is provided with demarcation strip.
Further, described demarcation strip is porous or netted ventilating structure.
Further, described column body is also provided with heating and temperature controlling device.
Further, on described the 3rd chamber, be also provided with regeneration gas air inlet and regeneration gas exhaust outlet, described regeneration gas import is extended setting by the wall body of described the 3rd chamber in described the second chamber.
The present invention has positive effect: in the present invention, working gas enters from work gas air inlet, and successively through the first chamber, the second chamber and the 3rd chamber, finally from work gas gas outlet, discharge, the first chamber, in the second chamber and the 3rd chamber, fill successively organic solvent adsorbing material, deoxygenation material and the material that dewaters, gas is purified, reach successively absorption organic solvent, deoxygenation, the effect dewatering, compared to prior art, interference influences each other in the time of cannot solving three kinds of packing material regeneration, and be forced to realize respectively except organic solvent and water with two pillars, oxygen, pipeline is complicated and take up space, the present invention can realize multiple purification function in same cylinder, same post internal regeneration, and simple in structure, leakage probability reduces, space availability ratio is high, also improved operating efficiency simultaneously.
Accompanying drawing explanation
For content of the present invention is more easily expressly understood, according to specific embodiment also by reference to the accompanying drawings, the present invention is further detailed explanation below, wherein:
Fig. 1 is the structural representation of first embodiment of the invention;
Wherein: 1, cylinder, the 2, first chamber, the 3, the 3rd chamber, the 4, second chamber, 5, buffer chamber, 6, heating and temperature controlling device, 7, demarcation strip, 8, vacuum orifice, 9, work gas air inlet, 10, regeneration gas air inlet, 11, work gas gas outlet, 12, regeneration gas exhaust outlet.
The specific embodiment
The present invention, a kind of multifunctional hand casing purifier, some of them embodiment, comprise cylinder, column body is disposed with along work gas airintake direction the first chamber, the second chamber and the 3rd chamber being connected, and fills organic solvent adsorbing material in the first chamber, in the second chamber, fill deoxygenation material, in the 3rd chamber, fill the material that dewaters, on the first chamber, be provided with work gas air inlet and vacuum orifice, on the 3rd chamber, be provided with work gas gas outlet.
Beneficial effect of the present invention: working gas enters from air inlet, and successively through the first chamber, the second chamber and the 3rd chamber, finally from work gas outlet, discharge, in the first chamber, the second chamber and the 3rd chamber, fill successively organic solvent adsorbing material, deoxygenation material and the material that dewaters, gas is purified, the effect that reach successively absorption organic solvent, deoxygenation, dewaters, compared to prior art, can realize multiple purification function in one.
As shown in Figure 1, present embodiment provides a kind of multifunctional hand casing purifier, comprising: cylinder 1, cylinder 1 is divided into the first chamber 2 and the second chamber 3, the 3rd chamber 4 by demarcation strip 7, and the buffer chamber 5 of bottom.The interior filling organic solvent adsorbing material of the first chamber 2, the interior filling deoxygenation of the second chamber 3 material, the interior filling of the 3rd chamber 4 material that dewaters, on the first chamber 2, be provided with on work gas air inlet 9 and vacuum orifice 8, the three chambers 4 and be provided with work gas gas outlet 11, regeneration gas air inlet 10 and regeneration gas exhaust outlet 12.According to the actual requirements, organic solvent adsorbing material is modified activated carbon, and deoxygenation material is copper catalyst, and adsorbed water material is molecular sieve.
Present embodiment, when normal circulation duty, the working gas that in glove box casing, water oxygen is higher enters purifier from work gas air inlet 9, through the first chamber 2 and buffer chamber 5, through the second chamber 3 and the 3rd chamber 4, finally from work gas gas outlet 11, discharge, by gas purification again, clean work gas enters glove box casing again and uses, so circulation.Three chambers reach absorption organic solvent successively, dewater and the effect of deoxygenation, buffer chamber reaches the airflow function of releiving, compared to prior art, interference influences each other in the time of cannot solving three kinds of packing material regeneration, and be forced to realize respectively except organic solvent and water, oxygen with two pillars, pipeline is complicated and take up space, the present invention can realize multiple purification function, same post internal regeneration in same cylinder, and simple in structure, leakage probability reduces, space availability ratio is high, has also improved operating efficiency simultaneously.
Present embodiment, when the decline of decontaminating column detergent power to a certain degree needs to start reproduced state, start heater, regeneration gas is passed into decontaminating column from regeneration gas air inlet 9, through the second chamber 2 and the 3rd chamber 4, finally 12 discharges from regeneration gas gas outlet, the deoxygenation material regeneration that the second chamber is filled, then close regeneration gas air inlet and regeneration gas exhaust outlet, from vacuum orifice 8, vacuumize, by dewater material and the organic solvent adsorbing material regeneration of the first chamber and the 3rd chamber, so be circulated to regeneration effect the best, then continue decontaminating column normal circulation duty, reach the object that circular regeneration is used.
Above-described specific embodiment; object of the present invention, technical scheme and beneficial effect are further described; institute is understood that; the foregoing is only specific embodiments of the invention; be not limited to the present invention; within the spirit and principles in the present invention all, any modification of making, be equal to replacement, improvement etc., within all should being included in protection scope of the present invention.
Claims (6)
1. a multifunctional hand casing purifier, it is characterized in that, comprise cylinder, described column body is disposed with along work gas airintake direction the first chamber, the second chamber and the 3rd chamber being connected, in described the first chamber, fill organic solvent adsorbing material, in described the second chamber, fill deoxygenation material, in described the 3rd chamber, fill the material that dewaters, on described the first chamber, be provided with work gas air inlet and vacuum orifice, on described the 3rd chamber, be provided with work gas gas outlet.
2. multifunctional hand casing purifier according to claim 1, is characterized in that, between described the first chamber, described the second chamber and described the 3rd chamber, also by demarcation strip, separates.
3. multifunctional hand casing purifier according to claim 2, is characterized in that, described demarcation strip is many empty or netted ventilating structures.
4. multifunctional hand casing purifier according to claim 1, is characterized in that, described column body is also provided with heating and temperature controlling device.
5. multifunctional hand casing purifier according to claim 1, it is characterized in that, on described the 3rd chamber, be also provided with regeneration gas air inlet and regeneration gas exhaust outlet, described regeneration gas air inlet extends setting by the wall body of described the 3rd chamber in described the second chamber.
6. multifunctional hand casing purifier according to claim 1, is characterized in that, described column body is also provided with buffer chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410350891.3A CN104175333B (en) | 2014-07-22 | 2014-07-22 | A kind of multifunctional hand casing purifier |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410350891.3A CN104175333B (en) | 2014-07-22 | 2014-07-22 | A kind of multifunctional hand casing purifier |
Publications (2)
| Publication Number | Publication Date |
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| CN104175333A true CN104175333A (en) | 2014-12-03 |
| CN104175333B CN104175333B (en) | 2016-04-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410350891.3A Active CN104175333B (en) | 2014-07-22 | 2014-07-22 | A kind of multifunctional hand casing purifier |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104999481A (en) * | 2015-07-08 | 2015-10-28 | 威格气体纯化科技（苏州）股份有限公司 | Energy-saving and environment-friendly glove box workstation and method for regeneration of glove box purification unit |
| CN105014691A (en) * | 2015-07-08 | 2015-11-04 | 威格气体纯化科技（苏州）股份有限公司 | Integrated glove box |
| CN105013324A (en) * | 2015-07-08 | 2015-11-04 | 威格气体纯化科技（苏州）股份有限公司 | Oxygen removal method for glove box |
| CN105583519A (en) * | 2016-03-16 | 2016-05-18 | 苏州北工激光技术有限公司 | Gas-shield laser forming repairing device |
| CN105666528A (en) * | 2016-03-29 | 2016-06-15 | 威格气体纯化科技（苏州）股份有限公司 | Circulating filtration device for clean room, clean room and glove box |
| CN105664661A (en) * | 2016-03-29 | 2016-06-15 | 威格气体纯化科技（苏州）股份有限公司 | Nitrogen-removing purification column and glove box |
| CN105688594A (en) * | 2016-03-29 | 2016-06-22 | 威格气体纯化科技（苏州）股份有限公司 | Carbon dioxide removal purifying column and glove box |
| CN105688595A (en) * | 2016-03-29 | 2016-06-22 | 威格气体纯化科技（苏州）股份有限公司 | Ozone removal purifying column and glove box |
| CN108015811A (en) * | 2018-01-10 | 2018-05-11 | 南通荣诚手套有限公司 | It is a kind of that there is water removal, the multifunctional gloves cleaning equipment of deoxygenation |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2263573Y (en) * | 1996-09-10 | 1997-10-01 | 中国科学院空间科学与应用研究中心 | Simple air-injection and air-bleed type no-polution gloves box |
| WO2004025667A1 (en) * | 2002-09-16 | 2004-03-25 | Konstantin Technologies Gmbh | Method for completely filling a glove box with a gas, and corresponding glove box |
| CN1751775A (en) * | 2004-09-23 | 2006-03-29 | 中国科学院大连化学物理研究所 | Gas separation membrane air purification equipment and preparation method |
| JP2008128224A (en) * | 2006-11-16 | 2008-06-05 | Dia Shinku Kk | Case storage type blower and gas circulation refining device |
| CN102962851A (en) * | 2012-12-11 | 2013-03-13 | 哈尔滨商业大学 | Multi-purpose glove box |
| CN103337269A (en) * | 2013-07-05 | 2013-10-02 | 中国原子能科学研究院 | Glove box for dry method post processing |
| CN203622453U (en) * | 2013-08-30 | 2014-06-04 | 上海储融检测技术有限公司 | Lithium ion battery disassembling glove box |
| CN203665550U (en) * | 2013-10-22 | 2014-06-25 | 甘肃大象能源科技有限公司 | Glove box with steam medium regeneration function |
-
2014
- 2014-07-22 CN CN201410350891.3A patent/CN104175333B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2263573Y (en) * | 1996-09-10 | 1997-10-01 | 中国科学院空间科学与应用研究中心 | Simple air-injection and air-bleed type no-polution gloves box |
| WO2004025667A1 (en) * | 2002-09-16 | 2004-03-25 | Konstantin Technologies Gmbh | Method for completely filling a glove box with a gas, and corresponding glove box |
| CN1751775A (en) * | 2004-09-23 | 2006-03-29 | 中国科学院大连化学物理研究所 | Gas separation membrane air purification equipment and preparation method |
| JP2008128224A (en) * | 2006-11-16 | 2008-06-05 | Dia Shinku Kk | Case storage type blower and gas circulation refining device |
| CN102962851A (en) * | 2012-12-11 | 2013-03-13 | 哈尔滨商业大学 | Multi-purpose glove box |
| CN103337269A (en) * | 2013-07-05 | 2013-10-02 | 中国原子能科学研究院 | Glove box for dry method post processing |
| CN203622453U (en) * | 2013-08-30 | 2014-06-04 | 上海储融检测技术有限公司 | Lithium ion battery disassembling glove box |
| CN203665550U (en) * | 2013-10-22 | 2014-06-25 | 甘肃大象能源科技有限公司 | Glove box with steam medium regeneration function |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104999481A (en) * | 2015-07-08 | 2015-10-28 | 威格气体纯化科技（苏州）股份有限公司 | Energy-saving and environment-friendly glove box workstation and method for regeneration of glove box purification unit |
| CN105014691A (en) * | 2015-07-08 | 2015-11-04 | 威格气体纯化科技（苏州）股份有限公司 | Integrated glove box |
| CN105013324A (en) * | 2015-07-08 | 2015-11-04 | 威格气体纯化科技（苏州）股份有限公司 | Oxygen removal method for glove box |
| CN105014691B (en) * | 2015-07-08 | 2017-06-06 | 威格气体纯化科技（苏州）股份有限公司 | A kind of integrated glove box |
| CN105583519A (en) * | 2016-03-16 | 2016-05-18 | 苏州北工激光技术有限公司 | Gas-shield laser forming repairing device |
| CN105666528A (en) * | 2016-03-29 | 2016-06-15 | 威格气体纯化科技（苏州）股份有限公司 | Circulating filtration device for clean room, clean room and glove box |
| CN105664661A (en) * | 2016-03-29 | 2016-06-15 | 威格气体纯化科技（苏州）股份有限公司 | Nitrogen-removing purification column and glove box |
| CN105688594A (en) * | 2016-03-29 | 2016-06-22 | 威格气体纯化科技（苏州）股份有限公司 | Carbon dioxide removal purifying column and glove box |
| CN105688595A (en) * | 2016-03-29 | 2016-06-22 | 威格气体纯化科技（苏州）股份有限公司 | Ozone removal purifying column and glove box |
| CN108015811A (en) * | 2018-01-10 | 2018-05-11 | 南通荣诚手套有限公司 | It is a kind of that there is water removal, the multifunctional gloves cleaning equipment of deoxygenation |
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| Publication number | Publication date |
|---|---|
| CN104175333B (en) | 2016-04-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| ASS | Succession or assignment of patent right |
Owner name: VIGOR GAS PURIFICATION EQUIPMENT TECHNOLOGIES (SUZ Free format text: FORMER OWNER: ZHANG DELONG Effective date: 20141114 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; TO: 215123 SUZHOU, JIANGSU PROVINCE |
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| TA01 | Transfer of patent application right |
Effective date of registration: 20141114 Address after: Suzhou Industrial Park Suzhou city Jiangsu province 215123 Xinglin Street No. 78 emerging industrial square No. 2 Factory Applicant after: Vigor Gas Purification Equipment Technologies (Suzhou Industrial Park) Co.,Ltd. Address before: The United States of New York, Ilha Grande Forest Road No. 280 Applicant before: Zhang Delong |
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| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C53 | Correction of patent of invention or patent application | ||
| CB02 | Change of applicant information |
Address after: Suzhou Industrial Park Suzhou city Jiangsu province 215123 Xinglin Street No. 78 emerging industrial square No. 2 Factory Applicant after: VIGOR GAS PURIFICATION TECHNOLIGIES, Inc. Address before: Suzhou Industrial Park Suzhou city Jiangsu province 215123 Xinglin Street No. 78 emerging industrial square No. 2 Factory Applicant before: Vigor Gas Purification Equipment Technologies (Suzhou Industrial Park) Co.,Ltd. |
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| COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: VIGOR GAS PURIFICATION EQUIPMENT TECHNOLOGIES (SUZHOU INDUSTRIAL PARK) CO., LTD. TO: VIGOR GAS PURIFICATION TECHNOLOGY (SUZHOU) CO., LTD. |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: No. 58, Tingtao Road, Suzhou Industrial Park, Jiangsu 215000 Patentee after: Weige Technology (Suzhou) Co.,Ltd. Address before: 215123 plant 2, Xinxing Industrial Building, No. 78 Xinglin street, Suzhou Industrial Park, Suzhou, Jiangsu Province Patentee before: VIGOR GAS PURIFICATION TECHNOLIGIES, Inc. |
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| CP03 | Change of name, title or address |