CN104175333B - A kind of multifunctional hand casing purifier - Google Patents
A kind of multifunctional hand casing purifier Download PDFInfo
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- CN104175333B CN104175333B CN201410350891.3A CN201410350891A CN104175333B CN 104175333 B CN104175333 B CN 104175333B CN 201410350891 A CN201410350891 A CN 201410350891A CN 104175333 B CN104175333 B CN 104175333B
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Abstract
The present invention relates to a kind of multifunctional hand casing purifier, comprise cylinder, described column body is disposed with the first chamber, the second chamber and the 3rd chamber that are connected along work gas airintake direction, organic solvent adsorbing material is filled in described first chamber, oxygen scavenging material is filled in described second chamber, fill the material that dewaters in described 3rd chamber, described first chamber is provided with work gas air inlet and vacuum orifice, described 3rd chamber is provided with work gas gas outlet.In the present invention, working gas enters from air inlet, and successively through the first chamber, second chamber and the 3rd chamber, finally discharge from work gas gas outlet, gas is purified, three chambers reach absorbing organic solvent successively, deoxygenation, the effect dewatered, compared to prior art, influence each other when cannot solve three kinds of packing material regeneration interference, and be forced to realize except organic solvent and water respectively with two pillars, oxygen, pipeline is complicated and take up space, the present invention can realize multiple purification function in same cylinder, same post internal regeneration, and structure is simple, leakage probability reduces, space availability ratio is high, also improve operating efficiency simultaneously.
Description
Technical field
The invention belongs to glove box field, particularly relate to a kind of multifunctional hand casing purifier.
Background technology
Glove box is filled with in casing by high purity inert gas, and be circulated throughout the laboratory equipment of moisture and the oxygen filtered wherein.Glove box can provide the atmosphere of inert gases closed of anhydrous and oxygen-free, both can prevent from occurring rotten to the material of water and oxygen sensitive, and harmful substance can be avoided again to be exposed in air.Glove box comprises main box and transfer chamber.In order to drop to minimum by the oxygen in glove box main box and moisture, need supporting decontaminating column, external work gas first be passed into casing again by decontaminating column, and need when glove box works the gas in casing to be circulated by decontaminating column.
In conventional art, decontaminating column, built with molecular sieve and copper catalyst, can play the function dewatered with deoxygenation respectively.But user is when using glove box; usually can use a large amount of organic solvents, these organic solvents can volatilize, be diffused in glove box body and pipeline, not only can pollute the operating environment in casing; more copper catalyst poisoning be can make, water oxygen probe, vavuum pump and magnetic valve damaged.When opening transfer chamber, the organic solvent in casing can be diffused in the air outside glove box, and grievous injury operating personnel's is healthy.In order to absorbing organic solvent, traditional flat case generally adopts extra decontaminating column, and needs to change sorbing material after sorbing material absorption is saturated, both adds cost, and easily causes again glove box to leak, more can reduce operating efficiency.
Therefore, a kind of glove box purifier integrating the functions such as absorbing organic solvent, adsorbed water, deoxygenation is needed badly.
Summary of the invention
The object of the invention is to overcome the defect that prior art exists, provide a kind of have dewater, deoxygenation, absorbing organic solvent multifunctional hand casing purifier.
The technical scheme realizing the object of the invention is: a kind of multifunctional hand casing purifier, comprise cylinder, described column body is disposed with the first chamber, the second chamber and the 3rd chamber that are connected along work gas airintake direction, organic solvent adsorbing material is filled in described first chamber, oxygen scavenging material is filled in described second chamber, the material that dewaters is filled in described 3rd chamber, described first chamber is provided with work gas air inlet and vacuum orifice, described 3rd chamber is provided with work gas gas outlet.
Further, the connectivity part of described first chamber, the second chamber and the 3rd chamber is provided with demarcation strip.
Further, described demarcation strip is porous or netted ventilating structure.
Further, described column body is also provided with heating and temperature controlling device.
Further, described 3rd chamber is also provided with regeneration gas air inlet and regeneration gas exhaust outlet, described regeneration gas import is extended in described second chamber by the wall body of described 3rd chamber.
The present invention has positive effect: in the present invention, working gas enters from work gas air inlet, and successively through the first chamber, second chamber and the 3rd chamber, finally discharge from work gas gas outlet, first chamber, organic solvent adsorbing material is filled successively in second chamber and the 3rd chamber, oxygen scavenging material and the material that dewaters, gas is purified, reach absorbing organic solvent successively, deoxygenation, the effect dewatered, compared to prior art, influence each other when cannot solve three kinds of packing material regeneration interference, and be forced to realize except organic solvent and water respectively with two pillars, oxygen, pipeline is complicated and take up space, the present invention can realize multiple purification function in same cylinder, same post internal regeneration, and structure is simple, leakage probability reduces, space availability ratio is high, also improve operating efficiency simultaneously.
Accompanying drawing explanation
In order to make content of the present invention more easily be clearly understood, below according to specific embodiment also by reference to the accompanying drawings, the present invention is further detailed explanation, wherein:
Fig. 1 is the structural representation of first embodiment of the invention;
Wherein: 1, cylinder, the 2, first chamber, the 3, the 3rd chamber, the 4, second chamber, 5, buffer chamber, 6, heating and temperature controlling device, 7, demarcation strip, 8, vacuum orifice, 9, work gas air inlet, 10, regeneration gas air inlet, 11, work gas gas outlet, 12, regeneration gas exhaust outlet.
Detailed description of the invention
The present invention, a kind of multifunctional hand casing purifier, some of them embodiment, comprise cylinder, column body is disposed with the first chamber, the second chamber and the 3rd chamber that are connected along work gas airintake direction, fills organic solvent adsorbing material in the first chamber, oxygen scavenging material is filled in second chamber, fill the material that dewaters in 3rd chamber, the first chamber is provided with work gas air inlet and vacuum orifice, the 3rd chamber is provided with work gas gas outlet.
Beneficial effect of the present invention: working gas enters from air inlet, and successively through the first chamber, the second chamber and the 3rd chamber, finally discharge from work gas outlet, organic solvent adsorbing material, oxygen scavenging material and the material that dewaters is filled successively in first chamber, the second chamber and the 3rd chamber, gas is purified, reach absorbing organic solvent, deoxygenation, the effect that dewaters successively, compared to prior art, multiple purification function can be realized in one.
As shown in Figure 1, present embodiment provides a kind of multifunctional hand casing purifier, comprising: cylinder 1, and cylinder 1 is divided into the first chamber 2 and the second chamber 4, the 3rd chamber 3 by demarcation strip 7, and the buffer chamber 5 of bottom.Organic solvent adsorbing material is filled in first chamber 2, oxygen scavenging material is filled in second chamber 4, the material that dewaters is filled in 3rd chamber 3, first chamber 2 is provided with on work gas air inlet 9 and vacuum orifice the 8, three chamber 3 and is provided with work gas gas outlet 11, regeneration gas air inlet 10 and regeneration gas exhaust outlet 12.According to the actual requirements, organic solvent adsorbing material is modified activated carbon, and oxygen scavenging material is copper catalyst, and adsorbed water material is molecular sieve.
Present embodiment, when normal circulation duty, the working gas that in Glove box body, water oxygen is higher enters purifier from work gas air inlet 9, through the first chamber 2 and buffer chamber 5, again through the second chamber 4 and the 3rd chamber 3, finally discharge, by gas purification from work gas gas outlet 11, clean work gas enters Glove box body again and uses, and so circulates.Three chambers reach absorbing organic solvent successively, dewater and the effect of deoxygenation, buffer chamber reaches airflow function of releiving, compared to prior art, influence each other when cannot solve three kinds of packing material regeneration interference, and be forced to realize except organic solvent and water, oxygen respectively with two pillars, pipeline is complicated and take up space, the present invention can realize multiple purification function, same post internal regeneration in same cylinder, and structure is simple, leakage probability reduces, space availability ratio is high, also improves operating efficiency simultaneously.
Present embodiment, when the decline of decontaminating column detergent power to a certain degree needs to start reproduced state, start heater, regeneration gas is passed into decontaminating column from regeneration gas air inlet 9, through the second chamber 4 and the 3rd chamber 3, finally discharge from regeneration gas gas outlet 12, the oxygen scavenging material regeneration that second chamber is filled, then regeneration gas air inlet and regeneration gas exhaust outlet is closed, vacuumize from vacuum orifice 8, by dewater material and the organic solvent adsorbing material regeneration of the first chamber and the 3rd chamber, so be circulated to regeneration effect the best, then decontaminating column normal circulation duty is continued, reach the object that circular regeneration uses.
Above-described specific embodiment; object of the present invention, technical scheme and beneficial effect are further described; be understood that; the foregoing is only specific embodiments of the invention; be not limited to the present invention; within the spirit and principles in the present invention all, any amendment made, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. a multifunctional hand casing purifier, it is characterized in that, comprise cylinder, described column body is disposed with the first chamber be connected along work gas airintake direction, second chamber and the 3rd chamber, organic solvent adsorbing material is filled in described first chamber, oxygen scavenging material is filled in described second chamber, the material that dewaters is filled in described 3rd chamber, described first chamber is provided with work gas air inlet and vacuum orifice, described 3rd chamber is provided with work gas gas outlet, described 3rd chamber is also provided with regeneration gas air inlet and regeneration gas exhaust outlet, described regeneration gas air inlet is extended in described second chamber by the wall body of described 3rd chamber.
2. multifunctional hand casing purifier according to claim 1, is characterized in that, described first chamber, also passes through divides between described second chamber and described 3rd chamber.
3. multifunctional hand casing purifier according to claim 2, is characterized in that, described demarcation strip is porous or netted ventilating structure.
4. multifunctional hand casing purifier according to claim 1, it is characterized in that, described column body is also provided with heating and temperature controlling device.
5. multifunctional hand casing purifier according to claim 1, it is characterized in that, described column body is also provided with buffer chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410350891.3A CN104175333B (en) | 2014-07-22 | 2014-07-22 | A kind of multifunctional hand casing purifier |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410350891.3A CN104175333B (en) | 2014-07-22 | 2014-07-22 | A kind of multifunctional hand casing purifier |
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| Publication Number | Publication Date |
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| CN104175333A CN104175333A (en) | 2014-12-03 |
| CN104175333B true CN104175333B (en) | 2016-04-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410350891.3A Active CN104175333B (en) | 2014-07-22 | 2014-07-22 | A kind of multifunctional hand casing purifier |
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Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105014691B (en) * | 2015-07-08 | 2017-06-06 | 威格气体纯化科技（苏州）股份有限公司 | A kind of integrated glove box |
| CN105013324A (en) * | 2015-07-08 | 2015-11-04 | 威格气体纯化科技（苏州）股份有限公司 | Oxygen removal method for glove box |
| CN104999481B (en) * | 2015-07-08 | 2017-05-10 | 威格气体纯化科技（苏州）股份有限公司 | Energy-saving and environment-friendly glove box workstation and method for regeneration of glove box purification unit |
| CN105583519A (en) * | 2016-03-16 | 2016-05-18 | 苏州北工激光技术有限公司 | Gas-shield laser forming repairing device |
| CN105666528B (en) * | 2016-03-29 | 2018-12-07 | 威格气体纯化科技（苏州）股份有限公司 | Dust free room circulation filter, dust free room and glove box |
| CN105688594A (en) * | 2016-03-29 | 2016-06-22 | 威格气体纯化科技（苏州）股份有限公司 | Carbon dioxide removal purifying column and glove box |
| CN105664661A (en) * | 2016-03-29 | 2016-06-15 | 威格气体纯化科技（苏州）股份有限公司 | Nitrogen-removing purification column and glove box |
| CN105688595A (en) * | 2016-03-29 | 2016-06-22 | 威格气体纯化科技（苏州）股份有限公司 | Ozone removal purifying column and glove box |
| CN108015811A (en) * | 2018-01-10 | 2018-05-11 | 南通荣诚手套有限公司 | It is a kind of that there is water removal, the multifunctional gloves cleaning equipment of deoxygenation |
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| CN2263573Y (en) * | 1996-09-10 | 1997-10-01 | 中国科学院空间科学与应用研究中心 | Simple air-injection and air-bleed type no-polution gloves box |
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| CN102962851A (en) * | 2012-12-11 | 2013-03-13 | 哈尔滨商业大学 | Multi-purpose glove box |
| CN103337269A (en) * | 2013-07-05 | 2013-10-02 | 中国原子能科学研究院 | Glove box for dry method post processing |
| CN203622453U (en) * | 2013-08-30 | 2014-06-04 | 上海储融检测技术有限公司 | Lithium ion battery disassembling glove box |
| CN203665550U (en) * | 2013-10-22 | 2014-06-25 | 甘肃大象能源科技有限公司 | Glove box with steam medium regeneration function |
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| AT412264B (en) * | 2002-09-16 | 2004-12-27 | Konstantin Technologies Gmbh | METHOD FOR FULLY FILLING THE GLOVE BOX WITH A GAS AND GLOVE BOX |
| JP5007877B2 (en) * | 2006-11-16 | 2012-08-22 | 大亜真空株式会社 | Gas circulation purification equipment |
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| CN2263573Y (en) * | 1996-09-10 | 1997-10-01 | 中国科学院空间科学与应用研究中心 | Simple air-injection and air-bleed type no-polution gloves box |
| CN1751775A (en) * | 2004-09-23 | 2006-03-29 | 中国科学院大连化学物理研究所 | Gas separation membrane air purification equipment and preparation method |
| CN102962851A (en) * | 2012-12-11 | 2013-03-13 | 哈尔滨商业大学 | Multi-purpose glove box |
| CN103337269A (en) * | 2013-07-05 | 2013-10-02 | 中国原子能科学研究院 | Glove box for dry method post processing |
| CN203622453U (en) * | 2013-08-30 | 2014-06-04 | 上海储融检测技术有限公司 | Lithium ion battery disassembling glove box |
| CN203665550U (en) * | 2013-10-22 | 2014-06-25 | 甘肃大象能源科技有限公司 | Glove box with steam medium regeneration function |
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| Publication number | Publication date |
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| CN104175333A (en) | 2014-12-03 |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| ASS | Succession or assignment of patent right |
Owner name: VIGOR GAS PURIFICATION EQUIPMENT TECHNOLOGIES (SUZ Free format text: FORMER OWNER: ZHANG DELONG Effective date: 20141114 |
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| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; TO: 215123 SUZHOU, JIANGSU PROVINCE |
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| TA01 | Transfer of patent application right |
Effective date of registration: 20141114 Address after: Suzhou Industrial Park Suzhou city Jiangsu province 215123 Xinglin Street No. 78 emerging industrial square No. 2 Factory Applicant after: Vigor Gas Purification Equipment Technologies (Suzhou Industrial Park) Co.,Ltd. Address before: The United States of New York, Ilha Grande Forest Road No. 280 Applicant before: Zhang Delong |
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| C10 | Entry into substantive examination | ||
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| C53 | Correction of patent of invention or patent application | ||
| CB02 | Change of applicant information |
Address after: Suzhou Industrial Park Suzhou city Jiangsu province 215123 Xinglin Street No. 78 emerging industrial square No. 2 Factory Applicant after: VIGOR GAS PURIFICATION TECHNOLIGIES, Inc. Address before: Suzhou Industrial Park Suzhou city Jiangsu province 215123 Xinglin Street No. 78 emerging industrial square No. 2 Factory Applicant before: Vigor Gas Purification Equipment Technologies (Suzhou Industrial Park) Co.,Ltd. |
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| COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: VIGOR GAS PURIFICATION EQUIPMENT TECHNOLOGIES (SUZHOU INDUSTRIAL PARK) CO., LTD. TO: VIGOR GAS PURIFICATION TECHNOLOGY (SUZHOU) CO., LTD. |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: No. 58, Tingtao Road, Suzhou Industrial Park, Jiangsu 215000 Patentee after: Weige Technology (Suzhou) Co.,Ltd. Address before: 215123 plant 2, Xinxing Industrial Building, No. 78 Xinglin street, Suzhou Industrial Park, Suzhou, Jiangsu Province Patentee before: VIGOR GAS PURIFICATION TECHNOLIGIES, Inc. |
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| CP03 | Change of name, title or address |