CN104997689A - Herbal mosquito-repellent lotion and preparation method thereof - Google Patents

Herbal mosquito-repellent lotion and preparation method thereof Download PDF

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CN104997689A
CN104997689A CN201510453085.3A CN201510453085A CN104997689A CN 104997689 A CN104997689 A CN 104997689A CN 201510453085 A CN201510453085 A CN 201510453085A CN 104997689 A CN104997689 A CN 104997689A
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parts
extract
mosquito
ethanol
repellent perfume
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吴克
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Abstract

The invention relates to herbal mosquito-repellent lotion and a preparation method thereof. The mosquito-repellent lotion comprises, by weight, the traditional Chinese medicinal materials of 10-18 parts of sweet flag aqueous extract, 3-7 parts of ocimum gratissimum ethyl acetate extract, 8-15 parts of wild chrysanthemum ethanol extract, 2-6 parts of mirabilis jalapa ethanol extract, 3-10 parts of campsis grandiflora ethanol extract, 20-30 parts of water, 100-300 parts of ethanol and 4-9 parts of mint aqueous extract. The obtained mosquito-repellent lotion is prepared by pure traditional Chinese medicine, damage to skins does not exist, and the mosquito-repellent and itching-relieving effects are good.

Description

A kind of draft mosquito-repellent perfume and preparation method thereof
Technical field
The present invention relates to filed of daily-use chemical industry, be specifically related to a kind of draft mosquito-repellent perfume and preparation method thereof.
Background technology
Floral water is oily as main body spice with liquid distilled from honeysuckle flowers or lotus leaves, is equipped with a kind of perfume series products that ethanol is made.The primary efficacy of floral water is decontamination, sterilization, anti-miliaria, antipruritic, meanwhile, is also the good summertime hygienic article of one of dispelling fetid sweat.
Mosquito-repellent perfume is on the basis of common floral water, is equipped with a kind of perfume series products that appropriate anophelifuge is made.Because of easy to carry can at any time anophelifuge, fragrant, simultaneously skinfeel refrigerant pleasant, also have floral water concurrently and to dispel the antipruritic effect of miliaria, be loved by the people.But general containing the household pesticides composition such as micro-diethyltoluamide or dimethyl phthalate in mosquito-repellent perfume, belong to micro-malicious product.
Conventional mosquito-repellent perfume all realizes repelling effect by dimethyl phthalate, and dimethyl phthalate has stable chemical nature, have high heat stability and high absorption of perspiration, and mosquito repellent time is long.But dimethyl phthalate has toxicity and zest, easy damaged is caused to be grown up the skin of particularly infant.
License publication number a kind of mosquito-repellent perfume that has been the disclosure of the invention of CN101711725A and preparation method thereof, composition comprises diethyltoluamide, emulsifying agent, cycloheptaamylose, methyl parahydroxybenzoate, spice, glycerol, second alcohol and water.Its invention selection is simple, has anophelifuge, sterilization, anti-miliaria, antipruritic effect, but employ part industrial chemicals injured skin and the DeGrain played and the persistent period short.
Summary of the invention
The object of the invention is to provide a kind of draft mosquito-repellent perfume and preparation method thereof to overcome above the deficiencies in the prior art.
Technical scheme: the invention discloses a kind of draft mosquito-repellent perfume, described mosquito-repellent perfume comprises following composition by weight: calamus water extract 10 ~ 18 parts, Ocimum Basilicum ethyl acetate extract 3 ~ 7 parts, chrysanthemum indicum extract 8 ~ 15 parts, Mirabilis jalapa ethanol extraction 2 ~ 6 parts, Flos Campsis ethanol extraction 3 ~ 10 parts, 20 ~ 30 parts, water and ethanol 100 ~ 300 parts.
Preferably, described a kind of draft mosquito-repellent perfume, the Chinese crude drug in floral water comprises following composition by weight: calamus water extract 10 ~ 18 parts, Ocimum Basilicum ethyl acetate extract 3 ~ 7 parts, chrysanthemum indicum extract 8 ~ 15 parts, Mirabilis jalapa ethanol extraction 2 ~ 6 parts, Flos Campsis ethanol extraction 3 ~ 10 parts, 20 ~ 30 parts, water, ethanol 100 ~ 300 parts and aqua methnae extract 4 ~ 9 parts.
Preferably, described a kind of draft mosquito-repellent perfume, the Chinese crude drug in floral water comprises following composition by weight: calamus water extract 15 parts, Ocimum Basilicum ethyl acetate extract 5 parts, chrysanthemum indicum extract 11 parts, Mirabilis jalapa ethanol extraction 4 parts, Flos Campsis ethanol extraction 6 parts, 25 parts, water, ethanol 200 parts and aqua methnae extract 7 parts.
A preparation method for draft mosquito-repellent perfume and preparation method thereof, comprises the steps:
Step one, by calamus and Herba Menthae respectively baking the affected part after applying some drugs do, pulverize respectively after baking the affected part after applying some drugs is dry last distilled water immersion, heating decocts, and filters rear medicinal residues adding distil water again, soak with method, decoct, filter, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract and aqua methnae extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol after pulverizing respectively and carry out lixiviate, after lixiviate, lixiviating solution is separated with filtering residue, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, carries out baking the affected part after applying some drugs by Ocimum Basilicum and does, and last ethyl acetate of pulverizing respectively after baking the affected part after applying some drugs is dry is soaked, and is separated by lixiviating solution, is concentrated by lixiviating solution after separation, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract after lixiviate with filtering residue;
Step 4, get calamus water extract 10 ~ 18 parts, Ocimum Basilicum ethyl acetate extract 3 ~ 7 parts, chrysanthemum indicum extract 8 ~ 15 parts, Mirabilis jalapa ethanol extraction 2 ~ 6 parts, Flos Campsis ethanol extraction 3 ~ 10 parts and aqua methnae extract 4 ~ 9 parts by weight, add 20 ~ 30 parts, water and ethanol 100 ~ 300 parts, after stirring, be draft mosquito-repellent perfume.
Preferably, the preparation method of described draft mosquito-repellent perfume and preparation method thereof, comprises the following steps:
Step one, by calamus and Herba Menthae respectively baking the affected part after applying some drugs do, hot bake out temperature is 60 DEG C, grinds to form respectively after 100 order powder with distilled water immersion 3 hours after baking the affected part after applying some drugs is dry, 100 DEG C of heating decoct, medicinal residues adding distil water again after filtering, soaks with method, decocts, filters, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract and aqua methnae extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol respectively after being ground into 100 order powder and carry out lixiviate, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, Ocimum Basilicum is carried out baking the affected part after applying some drugs do, hot bake out temperature is 70 DEG C, soak by ethyl acetate after grinding to form 100 order powder respectively after baking the affected part after applying some drugs is dry, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract;
Step 4, get calamus water extract 10 ~ 18 parts, Ocimum Basilicum ethyl acetate extract 3 ~ 7 parts, chrysanthemum indicum extract 8 ~ 15 parts, Mirabilis jalapa ethanol extraction 2 ~ 6 parts, Flos Campsis ethanol extraction 3 ~ 10 parts and aqua methnae extract 4 ~ 9 parts by weight, add 20 ~ 30 parts, water and ethanol 100 ~ 300 parts, after stirring, be draft mosquito-repellent perfume.
Beneficial effect: floral water is as the necessary article of daily life, and the effect of its antipruritic anophelifuge is valued by people, simultaneously for infant and skin allergy person, its damage caused skin is also particularly important.The present invention is as pure Chinese drug preparation gained, and to skin zero damage, and mosquito-expelling and antipruritic is effective.When calamus water extract 15 parts, Ocimum Basilicum ethyl acetate extract 5 parts, Mirabilis jalapa ethanol extraction 4 parts, chrysanthemum indicum extract 11 parts, Flos Campsis ethanol extraction 6 parts, 25 parts, water, ethanol 200 parts and aqua methnae extract 7 parts, the best results of floral water.
Detailed description of the invention
Embodiment 1
Step one, by calamus and Herba Menthae respectively baking the affected part after applying some drugs do, hot bake out temperature is 60 DEG C, grinds to form respectively after 100 order powder with distilled water immersion 3 hours after baking the affected part after applying some drugs is dry, 100 DEG C of heating decoct, medicinal residues adding distil water again after filtering, soaks with method, decocts, filters, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract and aqua methnae extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol respectively after being ground into 100 order powder and carry out lixiviate, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, Ocimum Basilicum is carried out baking the affected part after applying some drugs do, hot bake out temperature is 70 DEG C, soak by ethyl acetate after grinding to form 100 order powder respectively after baking the affected part after applying some drugs is dry, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract;
Step 4, get calamus water extract 10 parts, Ocimum Basilicum ethyl acetate extract 7 parts, chrysanthemum indicum extract 8 parts, Mirabilis jalapa ethanol extraction 6 parts, Flos Campsis ethanol extraction 3 parts and aqua methnae extract 9 parts by weight, add 20 parts, water and ethanol 300 parts, after stirring, be draft mosquito-repellent perfume.
Embodiment 2
Step one, by calamus and Herba Menthae respectively baking the affected part after applying some drugs do, hot bake out temperature is 60 DEG C, grinds to form respectively after 100 order powder with distilled water immersion 3 hours after baking the affected part after applying some drugs is dry, 100 DEG C of heating decoct, medicinal residues adding distil water again after filtering, soaks with method, decocts, filters, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract and aqua methnae extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol respectively after being ground into 100 order powder and carry out lixiviate, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, Ocimum Basilicum is carried out baking the affected part after applying some drugs do, hot bake out temperature is 70 DEG C, soak by ethyl acetate after grinding to form 100 order powder respectively after baking the affected part after applying some drugs is dry, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract;
Step 4, get calamus water extract 18 parts, Ocimum Basilicum ethyl acetate extract 3 parts, chrysanthemum indicum extract 15 parts, Mirabilis jalapa ethanol extraction 2 parts, Flos Campsis ethanol extraction 10 parts and aqua methnae extract 4 parts by weight, add 30 parts, water and ethanol 100 parts, after stirring, be draft mosquito-repellent perfume.
Embodiment 3
Step one, by calamus respectively baking the affected part after applying some drugs do, hot bake out temperature is 60 DEG C, grinds to form respectively after 100 order powder with distilled water immersion 3 hours after baking the affected part after applying some drugs is dry, 100 DEG C of heating decoct, medicinal residues adding distil water again after filtering, soaks with method, decocts, filters, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol respectively after being ground into 100 order powder and carry out lixiviate, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, Ocimum Basilicum is carried out baking the affected part after applying some drugs do, hot bake out temperature is 70 DEG C, soak by ethyl acetate after grinding to form 100 order powder respectively after baking the affected part after applying some drugs is dry, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract;
Step 4, get calamus water extract 18 parts, Ocimum Basilicum ethyl acetate extract 7 parts, chrysanthemum indicum extract 8 parts, Mirabilis jalapa ethanol extraction 2 parts and Flos Campsis ethanol extraction 10 parts by weight, add 20 parts, water and ethanol 100 parts, after stirring, be draft mosquito-repellent perfume.
Embodiment 4
Step one, by calamus respectively baking the affected part after applying some drugs do, hot bake out temperature is 60 DEG C, grinds to form respectively after 100 order powder with distilled water immersion 3 hours after baking the affected part after applying some drugs is dry, 100 DEG C of heating decoct, medicinal residues adding distil water again after filtering, soaks with method, decocts, filters, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol respectively after being ground into 100 order powder and carry out lixiviate, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, Ocimum Basilicum is carried out baking the affected part after applying some drugs do, hot bake out temperature is 70 DEG C, soak by ethyl acetate after grinding to form 100 order powder respectively after baking the affected part after applying some drugs is dry, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract;
Step 4, get calamus water extract 10 parts, Ocimum Basilicum ethyl acetate extract 3 parts, chrysanthemum indicum extract 15 parts, Mirabilis jalapa ethanol extraction 6 parts and Flos Campsis ethanol extraction 3 parts by weight, add 30 parts, water and ethanol 300 parts, after stirring, be draft mosquito-repellent perfume.
Embodiment 5
Step one, by calamus and Herba Menthae respectively baking the affected part after applying some drugs do, hot bake out temperature is 60 DEG C, grinds to form respectively after 100 order powder with distilled water immersion 3 hours after baking the affected part after applying some drugs is dry, 100 DEG C of heating decoct, medicinal residues adding distil water again after filtering, soaks with method, decocts, filters, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract and aqua methnae extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol respectively after being ground into 100 order powder and carry out lixiviate, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, Ocimum Basilicum is carried out baking the affected part after applying some drugs do, hot bake out temperature is 70 DEG C, soak by ethyl acetate after grinding to form 100 order powder respectively after baking the affected part after applying some drugs is dry, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract;
Step 4, get calamus water extract 15 parts, Ocimum Basilicum ethyl acetate extract 5 parts, chrysanthemum indicum extract 11 parts, Mirabilis jalapa ethanol extraction 4 parts, Flos Campsis ethanol extraction 6 parts and aqua methnae extract 7 parts by weight, add 25 parts, water and ethanol 200 parts, after stirring, be draft mosquito-repellent perfume.
Comparative example
The invention formula being CN101711725A according to license publication number makes a kind of mosquito-repellent perfume and preparation method thereof, get Flos Campsis 6g, Flos Chrysanthemi Indici 11g, Herba Pogostemonis 3g, Flos Chrysanthemi Indici 8g, Radix Salviae Miltiorrhizae 5g, Flos Campsis 6g and Radix Glycyrrhizae 8g to mix, add the ethanol of 1400mL, 50 DEG C, carry out ultrasonic extraction under 50KHz condition, extract 30 minutes, filter, filtrate concentrates, be Chinese medicine extract, get Chinese medicine extract 5%, ethanol 75%, Herba Menthae derivant 2%, deionized water surplus, preparation obtains mosquito-repellent perfume.
The floral water that the floral water prepare embodiment 1 to 5 and comparative example prepare uses to respectively skin sensitivity person, and number is 50 people, and observe the effect after using, result is as following table:
Table 1 embodiment 1-5 and comparative example are to the Contrast on effect used Yu do not use
Sample Use rear irritated number The earliest by the time bitten after using Time the most antipruritic after using
Embodiment 1 0 3h Be less than 1min
Embodiment 2 0 4h Be less than 1min
Embodiment 3 0 2h Be less than 1min
Embodiment 4 0 2h Be less than 1min
Embodiment 5 0 5h Be less than 1min
Comparative example 3 1h 2min
As known from Table 1, license publication number is that mosquito-repellent perfume prepared by the invention of CN101711725A has certain mosquito-expelling and antipruritic effect, the floral water that the present invention prepares by comparison effect has greatly improved, and the present invention be pure Chinese medicine obtain, without allergic phenomena.

Claims (10)

1. a draft mosquito-repellent perfume, it is characterized in that, described draft mosquito-repellent perfume comprises following composition by weight: calamus water extract 10 ~ 18 parts, Ocimum Basilicum ethyl acetate extract 3 ~ 7 parts, chrysanthemum indicum extract 8 ~ 15 parts, Mirabilis jalapa ethanol extraction 2 ~ 6 parts, Flos Campsis ethanol extraction 3 ~ 10 parts, 20 ~ 30 parts, water and ethanol 100 ~ 300 parts.
2. a kind of draft mosquito-repellent perfume according to claim 1, it is characterized in that, described draft mosquito-repellent perfume comprises following composition by weight: calamus water extract 10 ~ 18 parts, Ocimum Basilicum ethyl acetate extract 3 ~ 7 parts, chrysanthemum indicum extract 8 ~ 15 parts, Mirabilis jalapa ethanol extraction 2 ~ 6 parts, Flos Campsis ethanol extraction 3 ~ 10 parts, 20 ~ 30 parts, water, ethanol 100 ~ 300 parts and aqua methnae extract 4 ~ 9 parts.
3. a kind of draft mosquito-repellent perfume according to claim 2, is characterized in that, in described draft mosquito-repellent perfume, calamus water extract is 15 parts.
4. a kind of draft mosquito-repellent perfume according to claim 2, is characterized in that, in described draft mosquito-repellent perfume, Ocimum Basilicum ethyl acetate extract is 5 parts.
5. a kind of draft mosquito-repellent perfume according to claim 2, is characterized in that, in described draft mosquito-repellent perfume, Mirabilis jalapa ethanol extraction is 4 parts, chrysanthemum indicum extract 11 parts.
6. a kind of draft mosquito-repellent perfume according to claim 2, is characterized in that, in described draft mosquito-repellent perfume, Flos Campsis ethanol extraction is 6 parts.
7. a kind of draft mosquito-repellent perfume according to claim 2, is characterized in that, in described draft mosquito-repellent perfume, aqua methnae extract is 7 parts.
8. a kind of draft mosquito-repellent perfume according to claim 2, is characterized in that, in described draft mosquito-repellent perfume, water is 25 parts, and ethanol is 200 parts.
9. the preparation method of a kind of draft mosquito-repellent perfume according to claim 2, it is characterized in that, described preparation method comprises the steps:
Step one, by calamus and Herba Menthae respectively baking the affected part after applying some drugs do, pulverize respectively after baking the affected part after applying some drugs is dry last distilled water immersion, heating decocts, and filters rear medicinal residues adding distil water again, soak with method, decoct, filter, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract and aqua methnae extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol after pulverizing respectively and carry out lixiviate, after lixiviate, lixiviating solution is separated with filtering residue, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, carries out baking the affected part after applying some drugs by Ocimum Basilicum and does, and last ethyl acetate of pulverizing respectively after baking the affected part after applying some drugs is dry is soaked, and is separated by lixiviating solution, is concentrated by lixiviating solution after separation, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract after lixiviate with filtering residue;
Step 4, get calamus water extract 10 ~ 18 parts, Ocimum Basilicum ethyl acetate extract 3 ~ 7 parts, chrysanthemum indicum extract 8 ~ 15 parts, Mirabilis jalapa ethanol extraction 2 ~ 6 parts, Flos Campsis ethanol extraction 3 ~ 10 parts and aqua methnae extract 4 ~ 9 parts by weight, add 20 ~ 30 parts, water and ethanol 100 ~ 300 parts, after stirring, be draft mosquito-repellent perfume.
10. the preparation method of a kind of draft mosquito-repellent perfume according to claim 9, it is characterized in that, described preparation method comprises the steps:
Step one, by calamus and Herba Menthae respectively baking the affected part after applying some drugs do, hot bake out temperature is 60 DEG C, grinds to form respectively after 100 order powder with distilled water immersion 3 hours after baking the affected part after applying some drugs is dry, 100 DEG C of heating decoct, medicinal residues adding distil water again after filtering, soaks with method, decocts, filters, by twice filtrate mixing, heating is concentrated into small size, ultrafiltration membrance filter, drying under reduced pressure, obtains calamus water extract and aqua methnae extract;
Step 2, pulverize after Flos Campsis, Mirabilis jalapa and Flos Chrysanthemi Indici are carried out lyophilization respectively, add ethanol respectively after being ground into 100 order powder and carry out lixiviate, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, being concentrated into no solvent residue, is Mirabilis jalapa ethanol extraction, Flos Campsis ethanol extraction and chrysanthemum indicum extract;
Step 3, Ocimum Basilicum is carried out baking the affected part after applying some drugs do, hot bake out temperature is 70 DEG C, soak by ethyl acetate after grinding to form 100 order powder respectively after baking the affected part after applying some drugs is dry, lixiviating solution was separated with filtering residue after 2 hours by lixiviate, after separation, lixiviating solution is concentrated, be concentrated into no solvent residue and obtain Ocimum Basilicum ethyl acetate extract;
Step 4, get calamus water extract 10 ~ 18 parts, Ocimum Basilicum ethyl acetate extract 3 ~ 7 parts, chrysanthemum indicum extract 8 ~ 15 parts, Mirabilis jalapa ethanol extraction 2 ~ 6 parts, Flos Campsis ethanol extraction 3 ~ 10 parts and aqua methnae extract 4 ~ 9 parts by weight, add 20 ~ 30 parts, water and ethanol 100 ~ 300 parts, after stirring, be draft mosquito-repellent perfume.
CN201510453085.3A 2015-07-29 2015-07-29 Herbal mosquito-repellent lotion and preparation method thereof Pending CN104997689A (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
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Publication number Priority date Publication date Assignee Title
CN102885718A (en) * 2011-07-21 2013-01-23 新乡博凯生物技术有限公司 Honeysuckle flower compound mosquito repellent and preparation method thereof
CN103655245A (en) * 2012-08-31 2014-03-26 郭心仪 Mosquito repelling flora water
CN103798308A (en) * 2014-02-28 2014-05-21 曹以鉴 Natural traditional Chinese medicine mosquito-repellent incense
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CN104758221A (en) * 2015-01-08 2015-07-08 海南蛛王药业有限公司 Spider freeze-dried powder mosquito repellent liquid and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107233247A (en) * 2017-06-13 2017-10-10 朱洁 A kind of mosquito repellent formula and preparation method thereof

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Application publication date: 20151028