CN104997684A - Traditional Chinese medicine antibacterial hand washing solution and preparation method thereof - Google Patents
Traditional Chinese medicine antibacterial hand washing solution and preparation method thereof Download PDFInfo
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Abstract
The present invention discloses a traditional Chinese medicine antibacterial hand washing solution and a preparation method thereof, wherein the traditional Chinese medicine antibacterial hand washing solution comprises 4-10 parts of a caulis akebiae ethanol extract, 3-7 parts of a radix paeoniae rubra ethanol extract, 4-9 parts of flos hibisci water extract, 3-6 parts of rhizoma acori calami ethyl acetate extract, 5-10 parts of coconut diethanolamide, 4-8 parts of cetearyl alcohol polyoxyethylene ether, 6-12 parts of glycerin, 5-10 parts of gum arabic, and 300-500 parts of water. The preparation method comprises: (1) preparing a caulis akebiae ethanol extract and a radix paeoniae rubra ethanol extract; (2) preparing a flos hibisci water extract; (3) preparing a rhizoma acori calami ethyl acetate extract; and (4) uniformly mixing the components according to the weight ratio so as to obtain the traditional Chinese medicine antibacterial hand washing solution.
Description
Technical field
The invention belongs to handwashing liquid field, relate to a kind of handwashing liquid and preparation method thereof, particularly relate to a kind of Traditional Chinese medicine bacteriostatic handwashing liquid and preparation method thereof.
Background technology
Handwashing liquid is divided into two classes, and a class is common handwashing liquid, a generic sterile products, and a special class belongs to the dirty handwashing liquid of heavy oil in addition.The former plays the effect of clean decontamination, and the latter is just containing effective ingredient that is antibacterial, antibacterial or sterilization.The dirty handwashing liquid of heavy oil is then used for the cleaning of industrial class greasy dirt (such as machine oil, gasoline, butter, diesel oil etc.) and stain.Different handwashing liquid has respectively in outer package, and common handwashing liquid is generally " accurate font size ", and disinfection hand cleanser mostly then is " disappear font size ".Handwashing liquid is without phosphorus, the composition such as aluminum, alkali, sodium alkyl benzene sulfonate generally, adopts the principle of gentle decontamination, is easily accepted by skin.
In order to improve the anti-microbial property of handwashing liquid, needing to improve the antimicrobial component in handwashing liquid, adding Chinese medicine extract, effectively can improve the anti-microbial property of handwashing liquid.
Summary of the invention
The technical problem solved: common bacteriostatic hand sanitizer antipathogenic composition mostly wherein is organic chemical composition, it is larger to the injury of hand skin, and the fungistatic effect of the Traditional Chinese medicine bacteriostatic handwashing liquid of routine is poor, the object of the invention is openly a kind of Traditional Chinese medicine bacteriostatic handwashing liquid with good fungistatic effect and preparation method thereof.
Technical scheme: in order to solve the problem, the invention discloses a kind of Traditional Chinese medicine bacteriostatic handwashing liquid and preparation method thereof, and described Traditional Chinese medicine bacteriostatic handwashing liquid comprises the composition of following weight portion:
Caulis Clematidis pseudopogonandrae ethanol extraction 4-10 part,
Radix Paeoniae Rubra ethanol extraction 3-7 part,
Flos Hibisci water extract 4-9 part,
Rhizoma Acori Calami ethyl acetate extract 3-6 part,
Cocos nucifera oil acyl diethanolamine 5-10 part,
Cetearyl alcohol polyoxyethylenated alcohol 4-8 part,
Glycerol 6-12 part,
Arabic gum 5-10 part,
Water 300-500 part.
Further, described a kind of Traditional Chinese medicine bacteriostatic handwashing liquid, comprises the composition of following weight portion:
Caulis Clematidis pseudopogonandrae ethanol extraction 5-9 part,
Radix Paeoniae Rubra ethanol extraction 4-6 part,
Flos Hibisci water extract 5-8 part,
Rhizoma Acori Calami ethyl acetate extract 4-5 part,
Cocos nucifera oil acyl diethanolamine 7-9 part,
Cetearyl alcohol polyoxyethylenated alcohol 5-7 part,
Glycerol 7-10 part,
Arabic gum 6-9 part,
Water 350-450 part.
The preparation method of described a kind of Traditional Chinese medicine bacteriostatic handwashing liquid, comprises the following steps:
(1) drying in vacuum drying oven by Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra, after drying, Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra pulverizer are pulverized, lixiviate is carried out with dehydrated alcohol respectively after pulverizing, filter after lixiviate, filtering and collecting filter liquid, filtrate is carried out vacuum evaporation with Rotary Evaporators, is prepared as Caulis Clematidis pseudopogonandrae ethanol extraction and Radix Paeoniae Rubra ethanol extraction;
(2) Flos Hibisci is smashed to pieces rear use hot water extraction, centrifugalize after hot water extraction, concentrates supernatant again, and concentrating dry is Flos Hibisci water extract afterwards;
(3) Rhizoma Acori Calami is dry in vacuum drying oven, carrying out heated and stirred lixiviate by ethyl acetate after drying, centrifugalize after stirring and leaching, by supernatant vacuum concentration again, is Rhizoma Acori Calami ethyl acetate extract;
(4) Caulis Clematidis pseudopogonandrae ethanol extraction 4-10 part, Radix Paeoniae Rubra ethanol extraction 3-7 part, Flos Hibisci water extract 4-9 part, Rhizoma Acori Calami ethyl acetate extract 3-6 part, cocos nucifera oil acyl diethanolamine 5-10 part, cetearyl alcohol polyoxyethylenated alcohol 4-8 part, glycerol 6-12 part, arabic gum 5-10 part, water 300-500 part is got by weight respectively, by above-mentioned various composition mix homogeneously, it is Traditional Chinese medicine bacteriostatic handwashing liquid.
Further, the preparation method of described a kind of Traditional Chinese medicine bacteriostatic handwashing liquid, in described step (1), extraction temperature is 45-60 DEG C, and extraction time is 2-6h, and feed liquid weight ratio is 1:5-1:15.
Further, the preparation method of described a kind of Traditional Chinese medicine bacteriostatic handwashing liquid, in described step (2), extraction temperature is 55-75 DEG C, and extraction time is 1-4h, and feed liquid weight ratio is 1:4-1:10.
Further, the preparation method of described a kind of Traditional Chinese medicine bacteriostatic handwashing liquid, in described step (3), extraction temperature is 40-50 DEG C, and extraction time is 2-4h, and feed liquid weight ratio is 1:7-1:11.
Further, the preparation method of described a kind of Traditional Chinese medicine bacteriostatic handwashing liquid, in described step (1), vacuum drying temperature is 50-60 DEG C.
Further, the preparation method of described a kind of Traditional Chinese medicine bacteriostatic handwashing liquid, in described step (2), thickening temperature is 50-60 DEG C.
Beneficial effect: Traditional Chinese medicine bacteriostatic handwashing liquid disclosed by the invention effectively solves existing Traditional Chinese medicinal hand lotion to staphylococcus aureus, problem that escherichia coli suppression ratio is low, Traditional Chinese medicine bacteriostatic handwashing liquid of the present invention has good stability, feature that fungistatic effect is strong, and traditional Chinese medicine extraction component wherein improves its fungistatic effect significantly.
Detailed description of the invention
Embodiment 1
(1) drying in vacuum drying oven by Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra, after drying, Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra pulverizer are pulverized, lixiviate is carried out with dehydrated alcohol respectively after pulverizing, extraction temperature is 60 DEG C, and extraction time is 2h, and feed liquid weight ratio is 1:15, filter after lixiviate, filtering and collecting filter liquid, carries out vacuum evaporation filtrate with Rotary Evaporators, is prepared as Caulis Clematidis pseudopogonandrae ethanol extraction and Radix Paeoniae Rubra ethanol extraction; (2) Flos Hibisci is smashed to pieces rear use hot water extraction, extraction temperature is 75 DEG C, and extraction time is 4h, and feed liquid weight ratio is 1:4, and centrifugalize after hot water extraction, concentrates supernatant again, and concentrating dry is Flos Hibisci water extract afterwards; (3) Rhizoma Acori Calami is dry in vacuum drying oven, carry out heated and stirred lixiviate by ethyl acetate after drying, extraction temperature is 50 DEG C, extraction time is 2h, and feed liquid weight ratio is 1:11, centrifugalize after stirring and leaching, by supernatant vacuum concentration again, it is Rhizoma Acori Calami ethyl acetate extract; (4) Caulis Clematidis pseudopogonandrae ethanol extraction 10 parts, Radix Paeoniae Rubra ethanol extraction 3 parts, Flos Hibisci water extract 9 parts, Rhizoma Acori Calami ethyl acetate extract 6 parts, cocos nucifera oil acyl diethanolamine 10 parts, cetearyl alcohol polyoxyethylenated alcohol 4 parts, glycerol 12 parts, arabic gum 5 parts, 300 parts, water is got by weight respectively, by above-mentioned various composition mix homogeneously, it is Traditional Chinese medicine bacteriostatic handwashing liquid.
Embodiment 2
(1) drying in vacuum drying oven by Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra, after drying, Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra pulverizer are pulverized, lixiviate is carried out with dehydrated alcohol respectively after pulverizing, extraction temperature is 45 DEG C, and extraction time is 6h, and feed liquid weight ratio is 1:5, filter after lixiviate, filtering and collecting filter liquid, carries out vacuum evaporation filtrate with Rotary Evaporators, is prepared as Caulis Clematidis pseudopogonandrae ethanol extraction and Radix Paeoniae Rubra ethanol extraction; (2) Flos Hibisci is smashed to pieces rear use hot water extraction, extraction temperature is 55 DEG C, and extraction time is 1h, and feed liquid weight ratio is 1:10, and centrifugalize after hot water extraction, concentrates supernatant again, and concentrating dry is Flos Hibisci water extract afterwards; (3) Rhizoma Acori Calami is dry in vacuum drying oven, carry out heated and stirred lixiviate by ethyl acetate after drying, extraction temperature is 40 DEG C, extraction time is 4h, and feed liquid weight ratio is 1:7, centrifugalize after stirring and leaching, by supernatant vacuum concentration again, it is Rhizoma Acori Calami ethyl acetate extract; (4) Caulis Clematidis pseudopogonandrae ethanol extraction 4 parts, Radix Paeoniae Rubra ethanol extraction 7 parts, Flos Hibisci water extract 4 parts, Rhizoma Acori Calami ethyl acetate extract 3 parts, cocos nucifera oil acyl diethanolamine 5 parts, cetearyl alcohol polyoxyethylenated alcohol 8 parts, glycerol 6 parts, arabic gum 10 parts, 500 parts, water is got by weight respectively, by above-mentioned various composition mix homogeneously, it is Traditional Chinese medicine bacteriostatic handwashing liquid.
Embodiment 3
(1) drying in vacuum drying oven by Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra, after drying, Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra pulverizer are pulverized, lixiviate is carried out with dehydrated alcohol respectively after pulverizing, extraction temperature is 60 DEG C, and extraction time is 2h, and feed liquid weight ratio is 1:15, filter after lixiviate, filtering and collecting filter liquid, carries out vacuum evaporation filtrate with Rotary Evaporators, is prepared as Caulis Clematidis pseudopogonandrae ethanol extraction and Radix Paeoniae Rubra ethanol extraction; (2) Flos Hibisci is smashed to pieces rear use hot water extraction, extraction temperature is 75 DEG C, and extraction time is 4h, and feed liquid weight ratio is 1:4, and centrifugalize after hot water extraction, concentrates supernatant again, and concentrating dry is Flos Hibisci water extract afterwards; (3) Rhizoma Acori Calami is dry in vacuum drying oven, carry out heated and stirred lixiviate by ethyl acetate after drying, extraction temperature is 50 DEG C, extraction time is 2h, and feed liquid weight ratio is 1:11, centrifugalize after stirring and leaching, by supernatant vacuum concentration again, it is Rhizoma Acori Calami ethyl acetate extract; (4) Caulis Clematidis pseudopogonandrae ethanol extraction 5 parts, Radix Paeoniae Rubra ethanol extraction 6 parts, Flos Hibisci water extract 5 parts, Rhizoma Acori Calami ethyl acetate extract 5 parts, cocos nucifera oil acyl diethanolamine 9 parts, cetearyl alcohol polyoxyethylenated alcohol 5 parts, glycerol 10 parts, arabic gum 9 parts, 350 parts, water is got by weight respectively, by above-mentioned various composition mix homogeneously, it is Traditional Chinese medicine bacteriostatic handwashing liquid.
Embodiment 4
(1) drying in vacuum drying oven by Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra, after drying, Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra pulverizer are pulverized, lixiviate is carried out with dehydrated alcohol respectively after pulverizing, extraction temperature is 45 DEG C, and extraction time is 6h, and feed liquid weight ratio is 1:5, filter after lixiviate, filtering and collecting filter liquid, carries out vacuum evaporation filtrate with Rotary Evaporators, is prepared as Caulis Clematidis pseudopogonandrae ethanol extraction and Radix Paeoniae Rubra ethanol extraction; (2) Flos Hibisci is smashed to pieces rear use hot water extraction, extraction temperature is 55 DEG C, and extraction time is 1h, and feed liquid weight ratio is 1:10, and centrifugalize after hot water extraction, concentrates supernatant again, and concentrating dry is Flos Hibisci water extract afterwards; (3) Rhizoma Acori Calami is dry in vacuum drying oven, carry out heated and stirred lixiviate by ethyl acetate after drying, extraction temperature is 40 DEG C, extraction time is 4h, and feed liquid weight ratio is 1:7, centrifugalize after stirring and leaching, by supernatant vacuum concentration again, it is Rhizoma Acori Calami ethyl acetate extract; (4) Caulis Clematidis pseudopogonandrae ethanol extraction 9 parts, Radix Paeoniae Rubra ethanol extraction 4 parts, Flos Hibisci water extract 8 parts, Rhizoma Acori Calami ethyl acetate extract 4 parts, cocos nucifera oil acyl diethanolamine 7 parts, cetearyl alcohol polyoxyethylenated alcohol 7 parts, glycerol 7 parts, arabic gum 6 parts, 450 parts, water is got by weight respectively, by above-mentioned various composition mix homogeneously, it is Traditional Chinese medicine bacteriostatic handwashing liquid.
Embodiment 5
(1) drying in vacuum drying oven by Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra, after drying, Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra pulverizer are pulverized, lixiviate is carried out with dehydrated alcohol respectively after pulverizing, extraction temperature is 50 DEG C, and extraction time is 4h, and feed liquid weight ratio is 1:10, filter after lixiviate, filtering and collecting filter liquid, carries out vacuum evaporation filtrate with Rotary Evaporators, is prepared as Caulis Clematidis pseudopogonandrae ethanol extraction and Radix Paeoniae Rubra ethanol extraction; (2) Flos Hibisci is smashed to pieces rear use hot water extraction, extraction temperature is 65 DEG C, and extraction time is 3h, and feed liquid weight ratio is 1:7, and centrifugalize after hot water extraction, concentrates supernatant again, and concentrating dry is Flos Hibisci water extract afterwards; (3) Rhizoma Acori Calami is dry in vacuum drying oven, carry out heated and stirred lixiviate by ethyl acetate after drying, extraction temperature is 55 DEG C, extraction time is 3h, and feed liquid weight ratio is 1:9, centrifugalize after stirring and leaching, by supernatant vacuum concentration again, it is Rhizoma Acori Calami ethyl acetate extract; (4) Caulis Clematidis pseudopogonandrae ethanol extraction 7 parts, Radix Paeoniae Rubra ethanol extraction 5 parts, Flos Hibisci water extract 6 parts, Rhizoma Acori Calami ethyl acetate extract 4 parts, cocos nucifera oil acyl diethanolamine 8 parts, cetearyl alcohol polyoxyethylenated alcohol 6 parts, glycerol 8 parts, arabic gum 7 parts, 400 parts, water is got by weight respectively, by above-mentioned various composition mix homogeneously, it is Traditional Chinese medicine bacteriostatic handwashing liquid.
Comparative example 1
(1) drying in vacuum drying oven by Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra, after drying, Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra pulverizer are pulverized, lixiviate is carried out with dehydrated alcohol respectively after pulverizing, extraction temperature is 60 DEG C, and extraction time is 2h, and feed liquid weight ratio is 1:15, filter after lixiviate, filtering and collecting filter liquid, carries out vacuum evaporation filtrate with Rotary Evaporators, is prepared as Caulis Clematidis pseudopogonandrae ethanol extraction and Radix Paeoniae Rubra ethanol extraction; (2) Caulis Clematidis pseudopogonandrae ethanol extraction 10 parts, Radix Paeoniae Rubra ethanol extraction 3 parts, cocos nucifera oil acyl diethanolamine 10 parts, cetearyl alcohol polyoxyethylenated alcohol 4 parts, glycerol 12 parts, arabic gum 5 parts, 300 parts, water is got by weight respectively, by above-mentioned various composition mix homogeneously, it is Traditional Chinese medicine bacteriostatic handwashing liquid.
The Traditional Chinese medicine bacteriostatic handwashing liquid of embodiment and comparative example to staphylococcus aureus and colibacillary bacteriostasis rate as follows:
Staphylococcus aureus bacteriostasis rate (%) | Escherichia coli bacteriostasis rate (%) | |
Embodiment 1 | 87 | 89 |
Embodiment 2 | 86 | 88 |
Embodiment 3 | 90 | 92 |
Embodiment 4 | 91 | 91 |
Embodiment 5 | 95 | 96 |
Comparative example 1 | 72 | 71 |
Claims (8)
1. a Traditional Chinese medicine bacteriostatic handwashing liquid, is characterized in that, described Traditional Chinese medicine bacteriostatic handwashing liquid comprises the composition of following weight portion:
Caulis Clematidis pseudopogonandrae ethanol extraction 4-10 part,
Radix Paeoniae Rubra ethanol extraction 3-7 part,
Flos Hibisci water extract 4-9 part,
Rhizoma Acori Calami ethyl acetate extract 3-6 part,
Cocos nucifera oil acyl diethanolamine 5-10 part,
Cetearyl alcohol polyoxyethylenated alcohol 4-8 part,
Glycerol 6-12 part,
Arabic gum 5-10 part,
Water 300-500 part.
2. a kind of Traditional Chinese medicine bacteriostatic handwashing liquid according to claim 1, is characterized in that, described Traditional Chinese medicine bacteriostatic handwashing liquid comprises the composition of following weight portion:
Caulis Clematidis pseudopogonandrae ethanol extraction 5-9 part,
Radix Paeoniae Rubra ethanol extraction 4-6 part,
Flos Hibisci water extract 5-8 part,
Rhizoma Acori Calami ethyl acetate extract 4-5 part,
Cocos nucifera oil acyl diethanolamine 7-9 part,
Cetearyl alcohol polyoxyethylenated alcohol 5-7 part,
Glycerol 7-10 part,
Arabic gum 6-9 part,
Water 350-450 part.
3. the preparation method of a kind of Traditional Chinese medicine bacteriostatic handwashing liquid according to claim 1, it is characterized in that, described preparation method comprises the following steps:
(1) drying in vacuum drying oven by Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra, after drying, Caulis Clematidis pseudopogonandrae and Radix Paeoniae Rubra pulverizer are pulverized, lixiviate is carried out with dehydrated alcohol respectively after pulverizing, filter after lixiviate, filtering and collecting filter liquid, filtrate is carried out vacuum evaporation with Rotary Evaporators, is prepared as Caulis Clematidis pseudopogonandrae ethanol extraction and Radix Paeoniae Rubra ethanol extraction;
(2) Flos Hibisci is smashed to pieces rear use hot water extraction, centrifugalize after hot water extraction, concentrates supernatant again, and concentrating dry is Flos Hibisci water extract afterwards;
(3) Rhizoma Acori Calami is dry in vacuum drying oven, carrying out heated and stirred lixiviate by ethyl acetate after drying, centrifugalize after stirring and leaching, by supernatant vacuum concentration again, is Rhizoma Acori Calami ethyl acetate extract;
(4) Caulis Clematidis pseudopogonandrae ethanol extraction 4-10 part, Radix Paeoniae Rubra ethanol extraction 3-7 part, Flos Hibisci water extract 4-9 part, Rhizoma Acori Calami ethyl acetate extract 3-6 part, cocos nucifera oil acyl diethanolamine 5-10 part, cetearyl alcohol polyoxyethylenated alcohol 4-8 part, glycerol 6-12 part, arabic gum 5-10 part, water 300-500 part is got by weight respectively, by above-mentioned various composition mix homogeneously, it is Traditional Chinese medicine bacteriostatic handwashing liquid.
4. the preparation method of a kind of Traditional Chinese medicine bacteriostatic handwashing liquid according to claim 3, is characterized in that, in described step (1), extraction temperature is 45-60 DEG C, and extraction time is 2-6h, and feed liquid weight ratio is 1:5-1:15.
5. the preparation method of a kind of Traditional Chinese medicine bacteriostatic handwashing liquid according to claim 3, is characterized in that, in described step (2), extraction temperature is 55-75 DEG C, and extraction time is 1-4h, and feed liquid weight ratio is 1:4-1:10.
6. the preparation method of a kind of Traditional Chinese medicine bacteriostatic handwashing liquid according to claim 3, is characterized in that, in described step (3), extraction temperature is 40-50 DEG C, and extraction time is 2-4h, and feed liquid weight ratio is 1:7-1:11.
7. the preparation method of a kind of Traditional Chinese medicine bacteriostatic handwashing liquid according to claim 3, is characterized in that, in described step (1), vacuum drying temperature is 50-60 DEG C.
8. the preparation method of a kind of Traditional Chinese medicine bacteriostatic handwashing liquid according to claim 3, is characterized in that, in described step (2), thickening temperature is 50-60 DEG C.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN114099399A (en) * | 2021-10-18 | 2022-03-01 | 江苏今日卫生用品有限公司 | Chinese herbal medicine bacteriostatic hand sanitizer and preparation method thereof |
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2015
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CN1089499A (en) * | 1993-01-13 | 1994-07-20 | 张振祥 | Skin-cleaning liquid and preparation method |
CN103550116A (en) * | 2013-10-17 | 2014-02-05 | 苏州威尔德工贸有限公司 | Odor purifying and skin protection infant wet wipe |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN114099399A (en) * | 2021-10-18 | 2022-03-01 | 江苏今日卫生用品有限公司 | Chinese herbal medicine bacteriostatic hand sanitizer and preparation method thereof |
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