CN104973845A - Mine tailing filling gel powder and preparation method thereof - Google Patents
Mine tailing filling gel powder and preparation method thereof Download PDFInfo
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- CN104973845A CN104973845A CN201510274675.XA CN201510274675A CN104973845A CN 104973845 A CN104973845 A CN 104973845A CN 201510274675 A CN201510274675 A CN 201510274675A CN 104973845 A CN104973845 A CN 104973845A
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- China
- Prior art keywords
- mine tailing
- furnace slag
- gel powder
- granulated blast
- filling gel
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
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- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention discloses mine tailing filling gel powder and a preparation method thereof, and relates to the technical field of building materials. The mine tailing filling gel powder is prepared from raw materials of clinker, gypsum, mine tailing, granulated blast furnace slag and porcelain clay, and a chemical activator. The mass percentages of the raw materials are: clinker 15-35%, gypsum 3-10%, mine tailing 20-40%, granulated blast furnace slag 25-50%, and porcelain clay 5-20%. The dose of the chemical activator accounts for 0.05-0.15% of the total amount of the raw materials. According to the invention, the mine tailing, granulated blast furnace slag and porcelain clay are utilized; and through scientific content correction and complementation, potential activities of the mine tailing, granulated blast furnace slag and porcelain are stimulated, and wear-resistance coefficient is improved. With the method, raw resources are saved and replaced; circular economy development can be promoted; pollution can be reduced; and the ecological environment can be protected. Further pollution to the environment is not caused during a production process.
Description
Technical field
The present invention relates to gel powder preparing technical field, specifically a kind of mine tailing filling gel powder and preparation method thereof.
Background technology
Along with the process of modernization industry, human society more and more pays close attention to the research and development of Resources.The requirement of development to ecotope of society is more and more paid attention to.Backfill after mining utilizes novel material meet fortune and give birth to.
Summary of the invention
For the problems referred to above, the invention provides a kind of mine tailing filling gel powder and preparation method thereof, the gel powder that can effectively utilize a large amount of mine tailings, granulated blast-furnace slag, china clay to make is widely used in the backfill in mine.
The present invention realizes with following technical scheme: a kind of mine tailing filling gel powder, and it is that raw material adds chemical activator and makes by grog, gypsum, mine tailing, granulated blast-furnace slag, china clay, the mass percent of described each raw material
Described chemical activator raw material mass mixture ratio is:
Auxiliary agent raw material mass mixture ratio in chemical activator is:
It is further: the refuse that described mine tailing is remaining after being exploitation mineral products; Described granulated blast-furnace slag is Large Scale BF grain slag; Described china clay is china clay mineral products.
Above-mentioned gel powder specific surface area>=500m
2/ ㎏.
The making method of above-mentioned mine tailing filling gel powder, concrete steps are as follows:
(1), raw material is taken in proportion;
(2) grog, gypsum, mine tailing, granulated blast-furnace slag, china clay crusher are crushed to granularity≤10mm;
(3) iron tailings of step (2), granulated blast-furnace slag are dried to water ratio≤2%;
(4) with twin rollers, the raw material after drying is extruded further and is crushed to specific surface area>=250m
2/ ㎏;
(5) add chemical activator and be mixed into ball mill;
(6) grinding machine grinding homogenizing is to specific surface area>=500m
2/ ㎏; Be finished product.
The invention has the beneficial effects as follows: utilize mine tailing, granulated blast-furnace slag, china clay, the composition through science corrects complementary, excites the lateral reactivity of mine tailing, granulated blast-furnace slag, china clay.Improve wearing coefficient.The alternative Resources of saving, is conducive to promotion recycling economy development and decreasing pollution is preserved the ecological environment.The further pollution to environment is not produced in production process.
Embodiment
The present invention and effect is further illustrated below in conjunction with embodiment.
Embodiment 1:
Take raw material grog 20 ㎏, gypsum 3 ㎏, mine tailing 30 ㎏, granulated blast-furnace slag 40 ㎏, china clay 7 ㎏ by weight ratio, mix exciting agent 50mg outward.By grog 20 ㎏, gypsum 3 ㎏, mine tailing 30 ㎏, granulated blast-furnace slag 40 ㎏, china clay 7 ㎏, first by crusher in crushing to the particle of median size≤10mm; oven dry to water ratio is less than 2%; granulated blast-furnace slag 40 ㎏, mine tailing 30 ㎏, china clay 7 ㎏ use twin rollers grinding 50min again, mix chemical activator and are continued after grinding 25min to specific surface area>=500m by ball mill
2/ ㎏, product.
Embodiment 2:
Take raw material grog 30 ㎏, gypsum 5 ㎏, mine tailing 25 ㎏, granulated blast-furnace slag 35 ㎏, china clay 5 ㎏ by weight ratio, mix exciting agent 100mg outward.By grog 30 ㎏, gypsum 5 ㎏, mine tailing 25 ㎏, granulated blast-furnace slag 35 ㎏, china clay 5 ㎏ first by crusher in crushing to the particle of median size≤10mm; oven dry to water ratio is less than 2%; granulated blast-furnace slag 35 ㎏, mine tailing 25 ㎏, china clay 5 ㎏ use twin rollers grinding 50min again, mix chemical activator and are continued after grinding 25min to specific surface area>=500m by ball mill
2/ ㎏, product.
The product that above-mentioned 2 embodiments make, performance and technical requirements are better than GB/T3183-2003 " masonry cement " and JC/T1090-2008 " steel slag masonry cement " after testing.
Concrete outcome is in table 1, table 2.
Embodiment 1 stability 0.5mm; Sulfur trioxide content 3.01; 7 days anti-folding 4.0Mpa of embodiment 1,28 days anti-folding 6.5Mpa, 7 days resistance to compression 18.0Mpa, 28 days resistance to compression 30.8Mpa.
Embodiment 2 stability 0.56mm; Sulfur trioxide content 3.5; 7 days anti-folding 5.0Mpa of embodiment 2,28 days anti-folding 7.8Mpa, 7 days resistance to compression 19.0Mpa, 28 days resistance to compression 32.5Mpa.
The each grade strength of table 1 masonry cement and chemical index unit: Mpa
The each grade strength of table 2 steel slag masonry cement and chemical index unit: Mpa
The specific surface area produced under the power effect that Mechanical Crushing, extruding, grinding are different, granule-morphology, size distribution reach higher unification.Fiting chemical exciting agent, makes material combination material activity be not fully exerted.The activity of product and technical indicator are better than GB/T3183-2003 " masonry cement " and JC/T1090-2008 " steel slag masonry cement ".Mine tailing filling gel powder in the present invention is widely used in the backfilling material filling down-hole after replacing cement to do mineral exploration and exploitation, and alternative GB/T3183-2003 " masonry cement " and JC/T1090-2008 " steel slag masonry cement " is for masonry mortar, motar and blinding concrete, but be not suitable for structural concrete.Constant product quality of the present invention; intensity is higher than GB/T3183-2003 " masonry cement " and JC/T1090-2008 " steel slag masonry cement "; Save Resource Protect Environment, for the waste resources such as digestion process mine tailing provide wide channel, has higher technical economic benefit and social benefit.
Claims (4)
1. a mine tailing filling gel powder, is characterized in that: it is that raw material adds chemical activator and makes by a certain proportion of grog, gypsum, mine tailing, granulated blast-furnace slag, china clay, and the mass percent of above-mentioned each raw material is:
Described chemical activator raw materials quality and proportioning are:
Auxiliary agent raw materials quality in chemical activator and proportioning are:
2. a kind of mine tailing filling gel powder according to claim 1, is characterized in that: the refuse that described mine tailing is remaining after being exploitation mineral products; Described granulated blast-furnace slag is Large Scale BF grain slag; Described china clay is china clay mineral products.
3. a kind of mine tailing filling gel powder according to claim 1 and 2, is characterized in that: the specific surface area >=500 ㎡/㎏ of described mine tailing filling gel powder.
4. a making method for mine tailing filling gel powder, is characterized in that: concrete steps are as follows:
(1) raw material in claim 1 is taken in proportion;
(2) grog, gypsum, mine tailing, granulated blast-furnace slag, china clay crusher are crushed to granularity≤10mm;
(3) iron tailings of step (2), granulated blast-furnace slag are dried to water ratio≤2%;
(4) with twin rollers, the raw material after drying is extruded further and is crushed to specific surface area >=250 ㎡/㎏;
(5) add chemical activator and be mixed into ball mill;
(6) grinding machine grinding homogenizing is to specific surface area >=500 ㎡/㎏; Be finished product.
Priority Applications (1)
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CN201510274675.XA CN104973845A (en) | 2015-05-26 | 2015-05-26 | Mine tailing filling gel powder and preparation method thereof |
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CN201510274675.XA CN104973845A (en) | 2015-05-26 | 2015-05-26 | Mine tailing filling gel powder and preparation method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105541255A (en) * | 2016-01-11 | 2016-05-04 | 福州大学 | Copper slag-base low silicon iron tailing filling material and preparation technology thereof |
CN109534705A (en) * | 2019-01-25 | 2019-03-29 | 昌都龙者高新材料股份有限公司 | Fine fraction metal tailings consolidated fill eco-cement and preparation method thereof |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1218777A (en) * | 1997-12-02 | 1999-06-09 | 王品伦 | Activating agent for mortar |
JP2004075454A (en) * | 2002-08-16 | 2004-03-11 | Tetsugen Corp | Blast furnace granulated slag fine aggregate and method of preventing caking of blast furnace granulated slag |
KR20110053833A (en) * | 2009-11-16 | 2011-05-24 | 한국지질자원연구원 | Blast furnace slag cement synthetic method and blast furnace slag cement produced by this method |
CN104193201A (en) * | 2014-07-30 | 2014-12-10 | 南宁盈益环保建材科技有限公司 | Environment-friendly and energy-saving masonry cement |
CN104529198A (en) * | 2014-12-26 | 2015-04-22 | 徐州市宇鑫环保建材有限公司 | Silicate cement prepared from solid wastes and preparation method of silicate cement |
-
2015
- 2015-05-26 CN CN201510274675.XA patent/CN104973845A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1218777A (en) * | 1997-12-02 | 1999-06-09 | 王品伦 | Activating agent for mortar |
JP2004075454A (en) * | 2002-08-16 | 2004-03-11 | Tetsugen Corp | Blast furnace granulated slag fine aggregate and method of preventing caking of blast furnace granulated slag |
KR20110053833A (en) * | 2009-11-16 | 2011-05-24 | 한국지질자원연구원 | Blast furnace slag cement synthetic method and blast furnace slag cement produced by this method |
CN104193201A (en) * | 2014-07-30 | 2014-12-10 | 南宁盈益环保建材科技有限公司 | Environment-friendly and energy-saving masonry cement |
CN104529198A (en) * | 2014-12-26 | 2015-04-22 | 徐州市宇鑫环保建材有限公司 | Silicate cement prepared from solid wastes and preparation method of silicate cement |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105541255A (en) * | 2016-01-11 | 2016-05-04 | 福州大学 | Copper slag-base low silicon iron tailing filling material and preparation technology thereof |
CN105541255B (en) * | 2016-01-11 | 2017-09-22 | 福州大学 | Copper ashes base Low-silica iron ore tailings filler and its preparation technology |
CN109534705A (en) * | 2019-01-25 | 2019-03-29 | 昌都龙者高新材料股份有限公司 | Fine fraction metal tailings consolidated fill eco-cement and preparation method thereof |
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