CN104961351A - Preparation method of anti-dazzle glass - Google Patents
Preparation method of anti-dazzle glass Download PDFInfo
- Publication number
- CN104961351A CN104961351A CN201510260771.9A CN201510260771A CN104961351A CN 104961351 A CN104961351 A CN 104961351A CN 201510260771 A CN201510260771 A CN 201510260771A CN 104961351 A CN104961351 A CN 104961351A
- Authority
- CN
- China
- Prior art keywords
- glass
- dry
- time
- temperature
- oven
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The invention discloses a preparation method of anti-dazzle glass. According to the preparation method, image forming on glass can be realized preferably by controlling developing time and developing temperature; glass cleaning performance can be improved by controlling acetone immersion time, and an excellent environment is provided for subsequent printing; adhesion performance of printing paste with the glass, and presswork glossiness can be improved by controlling the composition and ratio of the printing paste in printing; acid-base neutralization after sintering can be realized via acid corrosion treatment after sintering so as to ensure uniformity of surface ingredients of the anti-dazzle glass. The anti-dazzle glass prepared via the preparation method is excellent in transmittance and haze, and low in reflectivity; market potential is large; and prospect is promising.
Description
Technical field
The invention belongs to the preparation field of glass, more particularly, the present invention relates to a kind of preparation technology of anti-glare glass.
Background technology
Anti-glare glass, also known as non-reflecting glass or anti reflection glass, a kind of glass glass surface being carried out special processing " anti-glare glass is through special process process the single or double of high-quality original sheet glass; make it have lower reflectivity compared with simple glass; substantially do not affect light through, light reflectance is reduced to less than 4% by 8%.Glass curtain wall but becomes the major manufacturers of light pollution, under strong sunlight, the reflected light of city high-lager building glass curtain wall, belong to a kind of reflection coefficient comparatively strong, single visual environment is formed, dazzle containing stronger visible component is polluted, in this environment, the visual stimulus suffered by human eye is difficult to alleviate, and its sight function can be subject to very large suppression, thus cause the injury to eyes, urgently need a kind of anti-glare glass to change this present situation.
Summary of the invention
Problem to be solved by this invention is to provide a kind of preparation technology of anti-glare glass.
To achieve these goals, the technical scheme that the present invention takes is:
A preparation technology for anti-glare glass, comprises the steps:
(1) processing of silk screen plate
Select suitable nylon mesh as required, then clean, then carry out drying and processing, the temperature of oven dry is 60-70 DEG C
(2) gluing
Nylon mesh after drying is carried out gluing process by tackiness agent, and then put and dry in an oven, the temperature of oven dry is 50-60 DEG C;
(3) stretch tight net: be fixed on screen frame by the nylon mesh after gluing, and during development, temperature is 25-27 DEG C, and the time is 40-60min;
(4) exposure and development: coated by the nylon mesh on screen frame and expose agent and expose, the time shutter is 1-2h, then spray development agent on nylon mesh, development dry after formation silk screen printing forme;
(5) cutting, the edging of glass
As required by the size that ball mill will be chosen glass cutting and becomes suitable, then polished in its corner;
(6) clean
With tap water, glass sparge is clean, then soak with acetone mixture, then use washed with de-ionized water, finally put dry in an oven, the temperature of baking oven is 60-80 DEG C;
(7) print
Be fixed on screen printing table by dried screen printing forme and glass, by scraping impression material with scraper plate, the print material leaked down through silk screen plate forms pattern on glass;
(8) sinter
Sintered through burning stove by the glass of upper for printing assorted print material, the temperature of burning stove is 200-300 DEG C, and the time of sintering is 2-4h;
(9) cleaning, drying
By the glass washed with de-ionized water after sintering, then put dry in an oven, the temperature of baking oven is 50-60 DEG C, and the dry time is 1-2h.
Preferably, the time of described step (4) development post-drying is 2-3h, and after drying, moisture content is 1-3%.
Preferably, the time that in described step (6), acetone soaks is 1-3min.
Preferably, in described step (7), during printing, print is expected composition frosting pulvis, hydrochloric acid, thickening material and binder.
Preferably, the proportioning of described print material is frosting pulvis 1.5-2, hydrochloric acid 1-3, thickening material 0.5-0.7, binder 0.2-0.4.
Preferably, carry out acid corrosion process after sintering in described step (8), etching time is 10-20min.
Beneficial effect: the preparation technology that the invention provides a kind of anti-glare glass, the control of described development time and development temperature, can make glass forms image better, the control of acetone soak time, the cleaning dynamics of glass can be improved, for next step printing provides excellent environment, the composition of print material and the control of proportioning during printing, the attachment fastness of print material and glass can be made good, printing glossiness is good, acid corrosion process is carried out after sintering, the potential of hydrogen after calcining can be neutralized, ensure the homogeneity of anti-glare glass surface composition, it is high that the anti-glare glass adopting this kind of method to prepare has transmitance, large and the advantage that reflectivity is low of mist degree, market potential is huge, have a extensive future.
Embodiment
Embodiment 1:
A preparation technology for anti-glare glass, comprises the steps:
(1) processing of silk screen plate
Select suitable nylon mesh as required, then clean, then carry out drying and processing, the temperature of oven dry is 60 DEG C
(2) gluing
Nylon mesh after drying is carried out gluing process by tackiness agent, and then put and dry in an oven, the temperature of oven dry is 50 DEG C;
(3) stretch tight net: be fixed on screen frame by the nylon mesh after gluing, and during development, temperature is 25 DEG C, and the time is 40min;
(4) exposure and development: the nylon mesh on screen frame is coated and exposes agent and expose, time shutter is 1h, then spray development agent on nylon mesh, and development forms silk screen printing forme after drying, the time of development post-drying is 2h, and after drying, moisture content is 1%;
(5) cutting, the edging of glass
As required by the size that ball mill will be chosen glass cutting and becomes suitable, then polished in its corner;
(6) clean
With tap water, glass sparge is clean, then soak 1min with acetone mixture, then use washed with de-ionized water, finally put dry in an oven, the temperature of baking oven is 60 DEG C;
(7) print
Dried screen printing forme and glass are fixed on screen printing table, by scraping impression material with scraper plate, the print material leaked down through silk screen plate forms pattern on glass, the composition frosting pulvis that during printing, print is expected, hydrochloric acid, thickening material and binder, proportioning is frosting pulvis 1.5, hydrochloric acid 1, thickening material 0.5, binder 0.2;
(8) sinter
Sintered through burning stove by the glass of upper for printing assorted print material, the temperature of burning stove is 200 DEG C, and the time of sintering is 2h, carries out acid corrosion process after sintering, and etching time is 10min;
(9) cleaning, drying
By the glass washed with de-ionized water after sintering, then put dry in an oven, the temperature of baking oven is 50 DEG C, and the dry time is 1h.
Embodiment 2:
A preparation technology for anti-glare glass, comprises the steps:
(1) processing of silk screen plate
Select suitable nylon mesh as required, then clean, then carry out drying and processing, the temperature of oven dry is 65 DEG C
(2) gluing
Nylon mesh after drying is carried out gluing process by tackiness agent, and then put and dry in an oven, the temperature of oven dry is 55 DEG C;
(3) stretch tight net: be fixed on screen frame by the nylon mesh after gluing, and during development, temperature is 26 DEG C, and the time is 50min;
(4) exposure and development: the nylon mesh on screen frame is coated and exposes agent and expose, time shutter is 1.5h, then spray development agent on nylon mesh, and development forms silk screen printing forme after drying, the time of development post-drying is 2.5h, and after drying, moisture content is 2%;
(5) cutting, the edging of glass
As required by the size that ball mill will be chosen glass cutting and becomes suitable, then polished in its corner;
(6) clean
With tap water, glass sparge is clean, then soak 2min with acetone mixture, then use washed with de-ionized water, finally put dry in an oven, the temperature of baking oven is 70 DEG C;
(7) print
Dried screen printing forme and glass are fixed on screen printing table, by scraping impression material with scraper plate, the print material leaked down through silk screen plate forms pattern on glass, the composition frosting pulvis that during printing, print is expected, hydrochloric acid, thickening material and binder, proportioning is frosting pulvis 1.8, hydrochloric acid 2, thickening material 0.6, binder 0.3;
(8) sinter
Sintered through burning stove by the glass of upper for printing assorted print material, the temperature of burning stove is 250 DEG C, and the time of sintering is 3h, carries out acid corrosion process after sintering, and etching time is 15min;
(9) cleaning, drying
By the glass washed with de-ionized water after sintering, then put dry in an oven, the temperature of baking oven is 55 DEG C, and the dry time is 1.5h.
Embodiment 3:
A preparation technology for anti-glare glass, comprises the steps:
(1) processing of silk screen plate
Select suitable nylon mesh as required, then clean, then carry out drying and processing, the temperature of oven dry is 70 DEG C
(2) gluing
Nylon mesh after drying is carried out gluing process by tackiness agent, and then put and dry in an oven, the temperature of oven dry is 60 DEG C;
(3) stretch tight net: be fixed on screen frame by the nylon mesh after gluing, and during development, temperature is 27 DEG C, and the time is 60min;
(4) exposure and development: the nylon mesh on screen frame is coated and exposes agent and expose, time shutter is 2h, then spray development agent on nylon mesh, and development forms silk screen printing forme after drying, the time of development post-drying is 3h, and after drying, moisture content is 3%;
(5) cutting, the edging of glass
As required by the size that ball mill will be chosen glass cutting and becomes suitable, then polished in its corner;
(6) clean
With tap water, glass sparge is clean, then soak 3min with acetone mixture, then use washed with de-ionized water, finally put dry in an oven, the temperature of baking oven is 80 DEG C;
(7) print
Dried screen printing forme and glass are fixed on screen printing table, by scraping impression material with scraper plate, the print material leaked down through silk screen plate forms pattern on glass, the composition frosting pulvis that during printing, print is expected, hydrochloric acid, thickening material and binder, proportioning is frosting pulvis 2, hydrochloric acid 3, thickening material 0.7, binder 0.4;
(8) sinter
Sintered through burning stove by the glass of upper for printing assorted print material, the temperature of burning stove is 300 DEG C, and the time of sintering is 4h, carries out acid corrosion process after sintering, and etching time is 20min;
(9) cleaning, drying
By the glass washed with de-ionized water after sintering, then put dry in an oven, the temperature of baking oven is 60 DEG C, and the dry time is 2h.
After above art breading, take out sample respectively, measuring result is as follows:
Can draw according to above table data, the anti-glare glass transmitance that the anti-glare glass prepared when embodiment 2 parameter is prepared than prior art is high, mist degree is large and reflectivity is low, is now more conducive to the preparation of anti-glare glass.
The invention provides a kind of preparation technology of anti-glare glass, the control of described development time and development temperature, can make glass forms image better, the control of acetone soak time, the cleaning dynamics of glass can be improved, for next step printing provides excellent environment, the composition of print material and the control of proportioning during printing, the attachment fastness of print material and glass can be made good, printing glossiness is good, acid corrosion process is carried out after sintering, the potential of hydrogen after calcining can be neutralized, ensure the homogeneity of anti-glare glass surface composition, it is high that the anti-glare glass adopting this kind of method to prepare has transmitance, large and the advantage that reflectivity is low of mist degree, market potential is huge, have a extensive future.
The foregoing is only embodiments of the invention; not thereby the scope of the claims of the present invention is limited; every utilize description of the present invention to do equivalent structure or equivalent flow process conversion; or be directly or indirectly used in other relevant technical fields, be all in like manner included in scope of patent protection of the present invention.
Claims (6)
1. a preparation technology for anti-glare glass, is characterized in that, comprises the steps:
(1) processing of silk screen plate
Select suitable nylon mesh as required, then clean, then carry out drying and processing, the temperature of oven dry is 60-70 DEG C
(2) gluing
Nylon mesh after drying is carried out gluing process by tackiness agent, and then put and dry in an oven, the temperature of oven dry is 50-60 DEG C;
(3) stretch tight net: be fixed on screen frame by the nylon mesh after gluing, and during development, temperature is 25-27 DEG C, and the time is 40-60min;
(4) exposure and development: coated by the nylon mesh on screen frame and expose agent and expose, the time shutter is 1-2h, then spray development agent on nylon mesh, development dry after formation silk screen printing forme;
(5) cutting, the edging of glass
As required by the size that ball mill will be chosen glass cutting and becomes suitable, then polished in its corner;
(6) clean
With tap water, glass sparge is clean, then soak with acetone mixture, then use washed with de-ionized water, finally put dry in an oven, the temperature of baking oven is 60-80 DEG C;
(7) print
Be fixed on screen printing table by dried screen printing forme and glass, by scraping impression material with scraper plate, the print material leaked down through silk screen plate forms pattern on glass;
(8) sinter
Sintered through burning stove by the glass of upper for printing assorted print material, the temperature of burning stove is 200-300 DEG C, and the time of sintering is 2-4h;
(9) cleaning, drying
By the glass washed with de-ionized water after sintering, then put dry in an oven, the temperature of baking oven is 50-60 DEG C, and the dry time is 1-2h.
2. according to the preparation technology of a kind of anti-glare glass according to claim 1, it is characterized in that: the time of described step (4) development post-drying is 2-3h, and after drying, moisture content is 1-3%.
3. according to the preparation technology of a kind of anti-glare glass according to claim 1, it is characterized in that: the time that in described step (6), acetone soaks is 1-3min.
4. according to the preparation technology of a kind of anti-glare glass according to claim 1, it is characterized in that: the composition frosting pulvis that in described step (7), during printing, print is expected, hydrochloric acid, thickening material and binder.
5. according to the preparation technology of a kind of anti-glare glass according to claim 4, it is characterized in that: the proportioning of described print material is frosting pulvis 1.5-2, hydrochloric acid 1-3, thickening material 0.5-0.7, binder 0.2-0.4.
6. according to the preparation technology of a kind of anti-glare glass according to claim 1, it is characterized in that: carry out acid corrosion process after sintering in described step (8), etching time is 10-20min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510260771.9A CN104961351A (en) | 2015-05-20 | 2015-05-20 | Preparation method of anti-dazzle glass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510260771.9A CN104961351A (en) | 2015-05-20 | 2015-05-20 | Preparation method of anti-dazzle glass |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104961351A true CN104961351A (en) | 2015-10-07 |
Family
ID=54215481
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510260771.9A Pending CN104961351A (en) | 2015-05-20 | 2015-05-20 | Preparation method of anti-dazzle glass |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104961351A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107902918A (en) * | 2017-12-08 | 2018-04-13 | 福耀玻璃工业集团股份有限公司 | A kind of preparation method of anti-reflection antireflection film layer |
| CN109664628A (en) * | 2018-12-21 | 2019-04-23 | 东莞市银泰丰光学科技有限公司 | A kind of production method of novel dumb light anti-dazzle glas |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1098074A (en) * | 1993-07-28 | 1995-02-01 | 天津市华桂技术实业公司 | The working method of mat glass |
-
2015
- 2015-05-20 CN CN201510260771.9A patent/CN104961351A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1098074A (en) * | 1993-07-28 | 1995-02-01 | 天津市华桂技术实业公司 | The working method of mat glass |
Non-Patent Citations (1)
| Title |
|---|
| 王承遇等: "《玻璃表面装饰》", 31 January 2011, 国防工业出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107902918A (en) * | 2017-12-08 | 2018-04-13 | 福耀玻璃工业集团股份有限公司 | A kind of preparation method of anti-reflection antireflection film layer |
| CN107902918B (en) * | 2017-12-08 | 2020-03-31 | 福耀玻璃工业集团股份有限公司 | Preparation method of anti-reflection and anti-reflection film layer |
| CN109664628A (en) * | 2018-12-21 | 2019-04-23 | 东莞市银泰丰光学科技有限公司 | A kind of production method of novel dumb light anti-dazzle glas |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104961351A (en) | Preparation method of anti-dazzle glass | |
| CN101948640B (en) | Dark infrared reflective insulation material and preparation method thereof | |
| CN105316929A (en) | Preparation method of formaldehyde-removing cotton fabric | |
| WO2018210111A1 (en) | 3d decorative glass and manufacturing method thereof | |
| CN107747241B (en) | White-proof pulp for physical anti-printing of reactive dye and preparation method thereof | |
| CN104231683A (en) | Titanium dioxide-silicon dioxide composite photocatalytic coating and preparation method thereof | |
| CN107300150A (en) | Preparation method, the film and the projection lamp of the film | |
| CN104692671A (en) | Preparation method of super-hydrophobic self-cleaning glass based on ZnO nano array coating | |
| CN111454478B (en) | Shading film for aircraft porthole shading curtain | |
| CN101816506A (en) | Warp-knitted base sun shading material and preparation method thereof | |
| CN107522888A (en) | A kind of shielding of film surface is ultraviolet and water-mist-proof coating and preparation method thereof | |
| UA127121C2 (en) | Camera hole cover plate, camera hole cover plate processing method and mobile terminal | |
| CN114751651A (en) | Glass frosting liquid with AG effect and preparation and application thereof | |
| CN205787185U (en) | A kind of LCDs two-in-one plated film of anti-dazzle antireflective | |
| CN114213036A (en) | AG anti-glare glass and preparation method thereof | |
| CN104643756B (en) | Printed luminous woollen blanket, carpet and production technology thereof | |
| CN101279819A (en) | Preparation of red glass | |
| CN106189782A (en) | A kind of preparation method of light fixture glare proof glass coating | |
| CN110790511A (en) | Low-temperature environment-friendly black glass slurry with high optical density and preparation method thereof | |
| JPS58168019A (en) | Manufacture of partially colored polarizing film | |
| CN101377617A (en) | Surface treating method of cutting tool | |
| US20140272917A1 (en) | Glass non-glare marker board | |
| CN115028370A (en) | Textured glass panel, method of making and use thereof | |
| CN109023979B (en) | Manufacturing method of color glue silver-coated pleated curtain fabric | |
| CN204427427U (en) | Printed luminous woollen blanket, carpet |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20151007 |