CN104947240A - Feather composite fiber textile material having health care function - Google Patents
Feather composite fiber textile material having health care function Download PDFInfo
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- CN104947240A CN104947240A CN201510368731.6A CN201510368731A CN104947240A CN 104947240 A CN104947240 A CN 104947240A CN 201510368731 A CN201510368731 A CN 201510368731A CN 104947240 A CN104947240 A CN 104947240A
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Abstract
The invention discloses a feather composite fiber textile material having a health care function. The feather composite fiber textile material is characterized by being prepared from the following raw materials in parts by weight: 70-100 parts of poultry feather, 13-15 parts of goose down, 30-50 parts of ramine fiber, 7-10 parts of silane coupling agent kh590, 5-7 parts of urea, 0.2-0.4 part of potassium metabisulphate, 0.1-0.3 part of sodium dodecyl sulfate, 1-3 part of betaine, 2-3 parts of tourmaline flour, 0.3-0.5 part of boron carbide, 0.2-0.4 part of zirconium sulfate and an appropriate amount of water; due to the synergistic effect of the tourmaline flour, boron carbide and zirconium sulfate added, the outside energy can be effectively absorbed in addition to the radiation of far infrared the same as human body bio-waves, and therefore, the health care functions of keeping warm, inhibiting bacteria and promoting blood circulation can be provided; the feather composite fiber textile material is simple in preparation method and wide in material source; besides, the feather is greatly utilized and the utilization rate of the feather is increased; in short, the feather composite fiber textile material is green, environmentally riendly and worthy of popularization.
Description
Technical field
The present invention relates to textile material technical field, be specifically related to a kind of feather composite fibre textile material with health care and preparation method thereof.
Background technology
along with to the attention of environmental protection and the raising of consumer demand, the research and development of the tencel of environmental beneficial are more and more received publicity, some discarded textile raw materials are as wool, eider down, silk etc. belong to high-quality natural protein material, there is health, environmental friendliness, reproducible feature, China is bird big producing country, a large amount of filoplumes is difficult to direct utilization because of the restriction of itself structure, warming packing material is used as or as except reinforcing material except a small amount of, mostly just simply be processed into feed even directly to abandon, the lower occurring in nature keratin of value-added content of product extensively exists, only China discards poultry feather year just more than 70 ten thousand tons, therefore the regenerated protein obtained in discarded object or byproduct should give consideration.Protein content in feather can reach 85-89%, and present keratin is widely used in biological medicine industry, textile industry and animal feed industries etc.For the characteristic of spun protein, keratin as natural polymer meets completely, but because keratin is the protein being rich in disulfide bond, show again the characteristic different from other protein, wherein the degree of cross linking is large, be not easy dissolve, so utilization rate is low, can not be good given play to due characteristic.By feather, to make keratin solution and other material copolymerization be means through modified in the present invention, by wet spinning processing method, the shortcomings such as when solving keratin independent spinning, bad mechanical property, firmness are strong, tensile strength is low, and feather stem is also utilized, greatly strengthen utilization ratio.Keratin, as the broad-spectrum biomaterial of one, contains infinite commercial opportunities and fine development prospect, promotes the development and utilization of new resources, is worthy to be popularized.
Summary of the invention
The object of this invention is to provide a kind of feather composite fibre textile material with health care and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the invention is to be realized by following technological means:
A kind of feather composite fibre textile material with health care, it is characterized in that, be made up of the raw material of following weight portion: poultry feather 70-100, goose down 13-15, ramee 30-50, silane coupler kh5907-10, urea 5-7, potassium metabisulfite 0.2-0.4, lauryl sodium sulfate 0.1-0.3, betaine 1-3, Tourmaline stone flour 2-3, boron carbide 0.3-0.5, zirconium sulfate 0.2-0.4, water are appropriate;
A kind of feather composite fibre textile material with health care of the present invention, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 100-200 ° of C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) dissolved by the silane coupler kh590 acetone soln of 10-15 times amount, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 ° C constant temperature keeps 1h, then heating is back to except desolventizing, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20-25min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add Tourmaline stone flour, boron carbide, zirconium sulfate mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
Advantage of the present invention is: the present invention is by feather and feather stem sterilizing, deodorizing, by silane coupler modified after ungrease treatment, mixing feather powder is had excellent hydrophobic, the performance of moisture absorption, the protein degradation liquid that recycling suitable proportion obtains makes feather powder dissolution obtain viscosity, the good keratin solution of rheological characteristic, by keratin solution with mix through the ramee lysate of modification and carry out spinning, enhance the toughness of feather fiber greatly, tensile strength, fragility, ABRASION RESISTANCE, the characteristics such as spinnability, improve productive value and social benefit, the Tourmaline stone flour added, boron carbide, zirconium sulfate three acts synergistically, effectively can absorb outside energy and the identical far infrared of radiation human body biological wave, there is insulation, antibacterial and stimulate circulation health care function, preparation method of the present invention is simple, material source is extensive, and make use of feather greatly, add the utilization rate of feather, environmental protection, be worthy to be popularized.
Detailed description of the invention
A kind of feather composite fibre textile material with health care, it is characterized in that, be made up of the raw material of following weight portion (kilogram): poultry feather 95, goose down 14, ramee 46, silane coupler kh5909, urea 6, potassium metabisulfite 0.3, lauryl sodium sulfate 0.3, betaine 3, Tourmaline stone flour 2, boron carbide 0.3, zirconium sulfate 0.4, water are appropriate;
A kind of feather composite fibre textile material with health care of the present invention, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 150 ° of C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol to soak 6 hours, then is neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) dissolved by the silane coupler kh590 acetone soln of 14 times amount, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 ° C constant temperature keeps 1h, then heating is back to except desolventizing, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add Tourmaline stone flour, boron carbide, zirconium sulfate mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
The eider down composite fibre performance indications parameter using the present invention to prepare is as follows:
Hydroscopicity (%): 12.6;
Regain (%): 5.5;
Extensibility (%): 33.2;
Tensile break strength (N): 6.3.
Claims (2)
1. one kind has the feather composite fibre textile material of health care, it is characterized in that, be made up of the raw material of following weight portion: poultry feather 70-100, goose down 13-15, ramee 30-50, silane coupler kh5907-10, urea 5-7, potassium metabisulfite 0.2-0.4, lauryl sodium sulfate 0.1-0.3, betaine 1-3, Tourmaline stone flour 2-3, boron carbide 0.3-0.5, zirconium sulfate 0.2-0.4, water are appropriate.
2. a kind of feather composite fibre textile material with health care according to claim 1, is characterized in that, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization at 100-200 DEG C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) dissolved by the silane coupler kh590 acetone soln of 10-15 times amount, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 DEG C constant temperature keeps 1h, then heating is back to except desolventizing, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20-25min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add Tourmaline stone flour, boron carbide, zirconium sulfate mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510368731.6A CN104947240A (en) | 2015-06-26 | 2015-06-26 | Feather composite fiber textile material having health care function |
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| CN201510368731.6A CN104947240A (en) | 2015-06-26 | 2015-06-26 | Feather composite fiber textile material having health care function |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106884222A (en) * | 2017-04-01 | 2017-06-23 | 百事基材料（青岛）股份有限公司 | A kind of preparation method of high accuracy far infrared wave spectrum polyester monofilament fiber |
| CN107034546A (en) * | 2017-04-19 | 2017-08-11 | 马志明 | A kind of composite fibre textile material and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1271743A (en) * | 2000-06-02 | 2000-11-01 | 奚柏君 | Process for preparing regenerated raw protein liquid and regenerated azelon and its products |
| CN1435516A (en) * | 2002-12-12 | 2003-08-13 | 内蒙古鄂尔多斯羊绒集团有限责任公司 | Technique for processing regenerated keratin functional fibre |
| CN102733001A (en) * | 2012-07-11 | 2012-10-17 | 成都起点投资有限公司 | Feather protein fiber and method for preparing same |
| CN103835020A (en) * | 2014-02-25 | 2014-06-04 | 浙江慧德新材料有限公司 | Novel healthcare fiber with multiple functional elements |
-
2015
- 2015-06-26 CN CN201510368731.6A patent/CN104947240A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1271743A (en) * | 2000-06-02 | 2000-11-01 | 奚柏君 | Process for preparing regenerated raw protein liquid and regenerated azelon and its products |
| CN1435516A (en) * | 2002-12-12 | 2003-08-13 | 内蒙古鄂尔多斯羊绒集团有限责任公司 | Technique for processing regenerated keratin functional fibre |
| CN102733001A (en) * | 2012-07-11 | 2012-10-17 | 成都起点投资有限公司 | Feather protein fiber and method for preparing same |
| CN103835020A (en) * | 2014-02-25 | 2014-06-04 | 浙江慧德新材料有限公司 | Novel healthcare fiber with multiple functional elements |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106884222A (en) * | 2017-04-01 | 2017-06-23 | 百事基材料（青岛）股份有限公司 | A kind of preparation method of high accuracy far infrared wave spectrum polyester monofilament fiber |
| CN107034546A (en) * | 2017-04-19 | 2017-08-11 | 马志明 | A kind of composite fibre textile material and preparation method thereof |
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