CN104928794A - Feather fiber textile composite material with high firmness - Google Patents
Feather fiber textile composite material with high firmness Download PDFInfo
- Publication number
- CN104928794A CN104928794A CN201510372588.8A CN201510372588A CN104928794A CN 104928794 A CN104928794 A CN 104928794A CN 201510372588 A CN201510372588 A CN 201510372588A CN 104928794 A CN104928794 A CN 104928794A
- Authority
- CN
- China
- Prior art keywords
- feather
- parts
- solution
- composite material
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The invention discloses a feather fiber textile composite material with high firmness. The composite material is characterized by adopting the raw materials including, by weights: 70 to 100 parts of poultry feathers, 13 to 15 parts of goose down, 30 to 50 parts of ramie fiber, 7 to 10 parts of silane coupling agent kh590, 5 to 7 parts of urea, 0.2 to 0.4 part of potassium metabisulfite, 0.1 to 0.3 part of lauryl sodium sulfate, 1 to 3 parts of betaine, 3 to 5 parts of bamboo fiber spinning liquid, 1 to 2 parts of expanded perlite powder, 0.4 to 1 part of polydimethylsiloxane and the appropriate amount of water. Compared with a single feather fiber, the composite feather fiber has the advantages of better performance, the heat insulation, textile performance, air permeability and firmness are improved, the manufacture process is simple, the application prospect is promised, and promotion is benefited.
Description
Technical field
The present invention relates to textile material technical field, be specifically related to good feather fibre textide composite material of a kind of firmness and preparation method thereof.
Background technology
along with to the attention of environmental protection and the raising of consumer demand, the research and development of the tencel of environmental beneficial are more and more received publicity, some discarded textile raw materials are as wool, eider down, silk etc. belong to high-quality natural protein material, there is health, environmental friendliness, reproducible feature, China is bird big producing country, a large amount of filoplumes is difficult to direct utilization because of the restriction of itself structure, warming packing material is used as or as except reinforcing material except a small amount of, mostly just simply be processed into feed even directly to abandon, the lower occurring in nature keratin of value-added content of product extensively exists, only China discards poultry feather year just more than 70 ten thousand tons, therefore the regenerated protein obtained in discarded object or byproduct should give consideration.Protein content in feather can reach 85-89%, and present keratin is widely used in biological medicine industry, textile industry and animal feed industries etc.For the characteristic of spun protein, keratin as natural polymer meets completely, but because keratin is the protein being rich in disulfide bond, show again the characteristic different from other protein, wherein the degree of cross linking is large, be not easy dissolve, so utilization rate is low, can not be good given play to due characteristic.By feather, to make keratin solution and other material copolymerization be means through modified in the present invention, by wet spinning processing method, the shortcomings such as when solving keratin independent spinning, bad mechanical property, firmness are strong, tensile strength is low, and feather stem is also utilized, greatly strengthen utilization ratio.Keratin, as the broad-spectrum biomaterial of one, contains infinite commercial opportunities and fine development prospect, promotes the development and utilization of new resources, is worthy to be popularized.
Summary of the invention
The object of this invention is to provide good feather fibre textide composite material of a kind of firmness and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the invention is to be realized by following technological means:
The feather fibre textide composite material that a kind of firmness is good, it is characterized in that, be made up of the raw material of following weight portion: poultry feather 70-100, goose down 13-15, ramee 30-50, silane coupler kh5907-10, urea 5-7, potassium metabisulfite 0.2-0.4, lauryl sodium sulfate 0.1-0.3, betaine 1-3, bamboo filament fibre spinning solution 3-5, swelling perlite powder 1-2, dimethyl silicone polymer 0.4-1, water are appropriate;
The feather fibre textide composite material that a kind of firmness of the present invention is good, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 100-200 ° of C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) dissolved by the silane coupler kh590 acetone soln of 10-15 times amount, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 ° C constant temperature keeps 1h, then heating is back to except desolventizing, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20-25min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add bamboo filament fibre spinning solution, swelling perlite powder, dimethyl silicone polymer mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
Advantage of the present invention is: the present invention is by feather and feather stem sterilizing, deodorizing, by silane coupler modified after ungrease treatment, mixing feather powder is had excellent hydrophobic, the performance of moisture absorption, the protein degradation liquid that recycling suitable proportion obtains makes feather powder dissolution obtain viscosity, the good keratin solution of rheological characteristic, by keratin solution with mix through the ramee lysate of modification and carry out spinning, enhance the toughness of feather fiber greatly, tensile strength, fragility, ABRASION RESISTANCE, the characteristics such as spinnability, improve productive value and social benefit, eider down composite fibre prepared by the present invention has good performance compared with independent feather fiber, its warmth retention property, textile, gas permeability, firmness all has greatly improved, and preparation technology is simple, have a good application prospect, be worthy to be popularized.
Detailed description of the invention
The feather fibre textide composite material that a kind of firmness is good, it is characterized in that, be made up of the raw material of following weight portion (kilogram): poultry feather 94, goose down 13, ramee 43, silane coupler kh5909, urea 7, potassium metabisulfite 0.3, lauryl sodium sulfate 0.2, betaine 2, bamboo filament fibre spinning solution 4, swelling perlite powder 2, dimethyl silicone polymer 0.6, water are appropriate;
The feather fibre textide composite material that a kind of firmness of the present invention is good, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 150 ° of C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) dissolved by the silane coupler kh590 acetone soln of 13 times amount, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 ° C constant temperature keeps 1h, then heating is back to except desolventizing, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add bamboo filament fibre spinning solution, swelling perlite powder, dimethyl silicone polymer mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
The eider down composite fibre performance indications parameter using the present invention to prepare is as follows:
Hydroscopicity (%): 11.7;
Regain (%): 5.2;
Extensibility (%): 28.3;
Tensile break strength (N): 5.2.
Claims (2)
1. the feather fibre textide composite material that a firmness is good, it is characterized in that, be made up of the raw material of following weight portion: poultry feather 70-100, goose down 13-15, ramee 30-50, silane coupler kh5907-10, urea 5-7, potassium metabisulfite 0.2-0.4, lauryl sodium sulfate 0.1-0.3, betaine 1-3, bamboo filament fibre spinning solution 3-5, swelling perlite powder 1-2, dimethyl silicone polymer 0.4-1, water are appropriate.
2. the feather fibre textide composite material that a kind of firmness is good according to claim 1, is characterized in that, is made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization at 100-200 DEG C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) the silane coupler kh590 acetone soln of 10-15 times amount is dissolved, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 DEG C constant temperature keeps 1h, heating is back to except desolventizing again, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20-25min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add bamboo filament fibre spinning solution, swelling perlite powder, dimethyl silicone polymer mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510372588.8A CN104928794A (en) | 2015-06-26 | 2015-06-26 | Feather fiber textile composite material with high firmness |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510372588.8A CN104928794A (en) | 2015-06-26 | 2015-06-26 | Feather fiber textile composite material with high firmness |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104928794A true CN104928794A (en) | 2015-09-23 |
Family
ID=54116211
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510372588.8A Pending CN104928794A (en) | 2015-06-26 | 2015-06-26 | Feather fiber textile composite material with high firmness |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104928794A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019006942A1 (en) * | 2017-07-07 | 2019-01-10 | 苏州市晨彩纺织研发有限公司 | Textile material added with perlite powder and preparation method therefor |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1271743A (en) * | 2000-06-02 | 2000-11-01 | 奚柏君 | Process for preparing regenerated raw protein liquid and regenerated azelon and its products |
| CN1435516A (en) * | 2002-12-12 | 2003-08-13 | 内蒙古鄂尔多斯羊绒集团有限责任公司 | Technique for processing regenerated keratin functional fibre |
| CN102733001A (en) * | 2012-07-11 | 2012-10-17 | 成都起点投资有限公司 | Feather protein fiber and method for preparing same |
| CN103835020A (en) * | 2014-02-25 | 2014-06-04 | 浙江慧德新材料有限公司 | Novel healthcare fiber with multiple functional elements |
-
2015
- 2015-06-26 CN CN201510372588.8A patent/CN104928794A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1271743A (en) * | 2000-06-02 | 2000-11-01 | 奚柏君 | Process for preparing regenerated raw protein liquid and regenerated azelon and its products |
| CN1435516A (en) * | 2002-12-12 | 2003-08-13 | 内蒙古鄂尔多斯羊绒集团有限责任公司 | Technique for processing regenerated keratin functional fibre |
| CN102733001A (en) * | 2012-07-11 | 2012-10-17 | 成都起点投资有限公司 | Feather protein fiber and method for preparing same |
| CN103835020A (en) * | 2014-02-25 | 2014-06-04 | 浙江慧德新材料有限公司 | Novel healthcare fiber with multiple functional elements |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2019006942A1 (en) * | 2017-07-07 | 2019-01-10 | 苏州市晨彩纺织研发有限公司 | Textile material added with perlite powder and preparation method therefor |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104928792A (en) | Antistatic down composite fiber | |
| CN105088404A (en) | Washable wrinkle-proof compound silk floss material | |
| CN104947242A (en) | Down feather composite fiber having good flame-retardant effect | |
| CN105088398A (en) | Feather composite fibers added with negative ion polyester short fibers | |
| CN104674375B (en) | A kind of preparation method of wig composite fibre | |
| CN104928795A (en) | Down composite fiber with self-cleaning function | |
| CN104963020A (en) | Down feather complex fiber with good breathability | |
| CN104928794A (en) | Feather fiber textile composite material with high firmness | |
| CN104947240A (en) | Feather composite fiber textile material having health care function | |
| CN104928796A (en) | Down composite fiber with warmth retention and wind breaking functions | |
| CN104947237A (en) | Composite fiber capable of saving cost and increasing down feather weight | |
| CN104928793A (en) | Cool and moisture absorbent composite down fiber | |
| CN104911739A (en) | Textile feather composite fiber light in weight and good in comfort | |
| CN104947241A (en) | Soft antibacterial composite down feather fiber | |
| CN105133056A (en) | Novel composite fiber textile with good sound and thermal insulation properties | |
| CN105088397A (en) | High-extension-strength textile feather composite fiber | |
| CN110499545A (en) | Natural feather composite fibre with self-cleaning function | |
| CN104947238A (en) | Down feather composite fiber having good fluffy and antibacterial effects | |
| CN105088406A (en) | Polypropylene modified feather composite fibers and preparation method thereof | |
| CN104947236A (en) | Composite down feather fiber having good ultraviolet resistance | |
| CN105088401A (en) | Chinese herbal medicine anti-bacterial health care composite down fiber textile material | |
| CN105088399A (en) | Composite feather textile material with fresh scent | |
| CN105155029A (en) | Novel waterproof and breathable composite fiber textile material | |
| CN104894683A (en) | Washing-resistant feather-down composite fiber | |
| CN104911741A (en) | Down feather composite fiber with good dyeing degree |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150923 |
|
| RJ01 | Rejection of invention patent application after publication |