CN104946401A - Tobacco pineapple spice preparation method - Google Patents
Tobacco pineapple spice preparation method Download PDFInfo
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- CN104946401A CN104946401A CN201510403824.8A CN201510403824A CN104946401A CN 104946401 A CN104946401 A CN 104946401A CN 201510403824 A CN201510403824 A CN 201510403824A CN 104946401 A CN104946401 A CN 104946401A
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- 244000099147 Ananas comosus Species 0.000 title 1
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 241000234671 Ananas Species 0.000 claims abstract description 102
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 55
- 239000012528 membrane Substances 0.000 claims abstract description 41
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 26
- 238000001914 filtration Methods 0.000 claims abstract description 19
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- 238000000034 method Methods 0.000 claims abstract description 9
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
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- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
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Abstract
The invention discloses a tobacco pineapple spice preparation method. The tobacco pineapple spice preparation method comprises the following steps that fresh pineapples are washed and dried; juice squeezing processing is conducted on the pineapples at room temperature to squeeze the pineapple into heavy paste; the heavy paste pineapples are placed at 2-15 DEG C for 6-24 hours, separation is conducted, and pineapple supernatant liquid is obtained; the obtained pineapple supernatant liquid is subjected to circulating filtration at the pressure ranging from 0.05-0.35 Mpa and the temperature ranging from 12 DEG C to 40 DEG C by using an ultra-filtration membrane with the membrane pore size ranging from 20000 to 30000, and the obtained supernatant liquid is pineapple supernatant liquid; the obtained pineapple supernatant liquid is subjected to circulating filtration at the pressure ranging from 0.30 Mpa to 1.25 Mpa and the temperature ranging from 12 DEG C to 40 DEG C by using an ultra-filtration membrane with the membrane pore size ranging from 1000 to 3000, and then the concentrated solution withheld is the tobacco pineapple spice. The tobacco pineapple spice preparation method has the advantages that the tobacco pineapple spice prepared by the method is real in fragrance and clear and transparent in appearance, when the tobacco pineapple spice is added into cigarettes, the fragrance of the cigarettes can be improved, the stimulation can be reduced, the smoke can be softened, and salivation promotion and sweet back flow are achieved.
Description
Technical field
The present invention relates to the preparation method of essence spice for cigarette, specifically refer to a kind of preparation method of cigarette pineapple flavors.Adopt ultrafiltration membrane technique separation and Extraction cigarette pineapple flavors from pineapple extracting solution specifically.
Background technology
Pineapple property is put down, sweet, the micro-acid of taste, micro-puckery, cold nature, have that heat clearly quenches one's thirst, the antidiarrheal that helps digestion, tonifying the spleen and stomach, reinforcing premodial qi, replenishing QI and blood, help digestion, clearing damp, the effect such as beauty treatment weight reducing.Pineapple fruit is best in quality, nutritious, containing a large amount of fructose, glucose, vitamins B, C, and the materials such as phosphorus, citric acid and proteolytic enzyme.
Pineapple contains a kind of material being " pineapple proteinase ", and its energy decomposing protein, helps digest, and dissolves the scleroproein and blood clot that block in tissue, improves the blood circulation of local, dilute blood fat, diminish inflammation and oedema, promote circulation of blood.
Bromeline can effectively decompose protein in food, increases enterogastric peristalsis.This enzyme is decomposable asymmetric choice net protein under one's belt, supplements the deficiency of the digested enzyme of human body.In addition, sugar contained in pineapple, enzyme have certain diuretic properties, to ephritis and hyperpietic useful, also have auxiliary curative effect to bronchitis.Due to cellulosic effect, also there is certain curative effect to constipation therapy.In addition, pineapple rich vitamin B1, can enhance metabolism, banish the feeling of languor.
Pineapple juice has the effect of cooling, and effectively can prevent bronchitis, but fever had better not eat.Through medical research, since ancient times, mankind's symptom of just usually relying on the bromeline contained in pineapple to carry out mitigation to have a sore throat and cough.Be rich in Traumanase in pineapple peel, have abundant pharmaceutical use, according to external expert experiment in more than 20 year, for a long time edible pineapple peel, cardiovascular and cerebrovascular, onset diabetes rate significantly reduces, and has certain anticancer effect.Still containing a kind of ferment, can decomposing protein.
Ultra-filtration membrane screening process, with the pressure difference of film both sides for motivating force, take ultra-filtration membrane as filtration medium, under pressure, when stoste flows through film surface, the many tiny micropore that ultrafiltration membrane surface gathers only allows water and small-molecule substance pass through and become permeate, and the material that in stoste, volume is greater than film surface micropore footpath is then trapped within the liquid feeding side of film, become concentrated solution, thus realize the object of the purification to stoste, isolation and identification.Ultra-filtration technique can utilize the film of different pore size to realize classification to macromolecular substance and collect, and sepn process is simple to operate, without phase transformation, solvent-free pollution, easily keeps biomolecule activity, has obtained increasing practical application.
Because the active skull cap components major part in pineapple belongs to heat-sensitive material, high temperature extraction concentrates, and can destroy active substance wherein, causes and loses normal nourishing function; The flavoring pineapple essence composition simultaneously obtained by chemical synthesis process is single, and raw material is residual serious, all brings threat to physical environment and HUMAN HEALTH.And the rarely seen report of the use of pineapple in essence spice for cigarette.Therefore the preparation method inventing a kind of cigarette pineapple flavors effectively can fill up the blank in essence spice for cigarette field.
Summary of the invention
The object of the invention is exactly the blank for prior art, provides a kind of preparation method of cigarette pineapple flavors.The cigarette pineapple flavors fragrance that the present invention prepares is true to nature, and outward appearance is transparent.This cigarette pineapple flavors adds in cigarette, can improve cigarette flavor, reduce stimulation, soft flue gas, promote the production of body fluid Hui Tian.
For achieving the above object, technical scheme of the present invention is achieved in that the present invention can obtain a kind of extract adopting ultrafiltration membrane technique to extract from pineapple.
A preparation method for cigarette pineapple flavors, is characterized in that, comprises the following steps:
(1) get the raw materials ready: fresh pineapple is cleaned, dries, for subsequent use.
(2) squeeze: at room temperature, above-mentioned pineapple is carried out process of squeezing the juice, is squeezed into thick paste.
(3) freeze and analyse: the thick paste pineapple of gained is under freezing conditions placed 6 ~ 24h, be separated and obtain pineapple supernatant liquor.
(4) filter: by the pineapple supernatant liquor of gained, be 0.05 ~ 0.35Mpa with ultra-filtration membrane at pressure, temperature is carry out circulating filtration under the condition of 12 ~ 40 DEG C, and gained cleaner liquid is pineapple filtrate.Current filtration affects the impurity of cigarette taste in order to remove pigment, pectin, tannin, protein and most of polysaccharide etc., reduce cigarette to the stimulation of smoker.
(5) concentrated: by the pineapple filtrate of gained, be 0.30 ~ 1.25Mpa with ultra-filtration membrane at pressure, temperature is again carry out circulating filtration under the condition of 12 ~ 40 DEG C, and the concentrated solution retained is cigarette pineapple flavors.Current filtration, in order to filter most water, a small amount of monose, amino acid etc., retains the effective constituent of pineapple flavors.
As preferably, the freezing temp in described step (3) is 2 ~ 15 DEG C.
As preferably, the membrane pore size of the ultra-filtration membrane in described step (4) is 20000 ~ 30000.
As preferably, the membrane pore size of the ultra-filtration membrane in described step (5) is 1000 ~ 3000.
The invention has the advantages that:
1, extraction and concentration involved in the present invention all carries out at low temperatures, effectively prevents oxidation and the loss of heat-sensitive substance, very effective to the activeconstituents kept in pineapple.
2, the cigarette pineapple flavors that obtains of the present invention is not containing impurity components such as pigment, pectin, tannin, protein and most of polysaccharide, this cigarette pineapple flavors to be applied in cigarette improving mouthfeel, reduce stimulate, to reduce oral cavity residual all helpful.
3, the cigarette pineapple flavors fragrance that obtains of the present invention is true to nature, and outward appearance is transparent.This cigarette pineapple flavors is sprayed on pipe tobacco and makes cigarette, the effect improving cigarette flavor, soft flue gas, the Hui Tian that promotes the production of body fluid can be played.
4, the present invention does not relate to the use of organic solvent, health environment-friendly, and cost is low, and technique is simple, is conducive to carrying out suitability for industrialized production.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail.
Embodiment 1
Take clean fresh pineapple 600 grams, be squeezed into thick paste with juice extractor, under 2 DEG C of conditions, leave standstill 8 hours, be separated and obtain pineapple supernatant liquor.Gained pineapple supernatant liquor is first adopted membrane pore size be 30000 ultra-filtration membrane be 0.05Mpa at pressure, temperature is carry out circulating filtration under the condition of 12 DEG C, and gained cleaner liquid is pineapple filtrate.Gained pineapple filtrate is adopted again membrane pore size be 1000 ultra-filtration membrane be 1.25Mpa at pressure, temperature is carry out circulating filtration under the condition of 12 DEG C, and the concentrated solution retained is cigarette pineapple flavors.
This cigarette pineapple flavors fragrance is true to nature, and outward appearance is transparent.This cigarette pineapple flavors is sprayed on pipe tobacco and makes cigarette, cigarette flavor can be improved, reduce stimulation, soft flue gas, promote the production of body fluid Hui Tian.
Embodiment 2
Take clean fresh pineapple 800 grams, be squeezed into thick paste with juice extractor, under 9 DEG C of conditions, leave standstill 12 hours, be separated and obtain pineapple supernatant liquor.Gained pineapple supernatant liquor is first adopted membrane pore size be 20000 ultra-filtration membrane be 0.1Mpa at pressure, temperature is carry out circulating filtration under the condition of 12 DEG C, and gained cleaner liquid is pineapple filtrate.Gained pineapple filtrate is adopted again membrane pore size be the ultra-filtration membrane of 1000 at pressure 1.0Mpa, carry out circulating filtration under the condition that temperature is 15 DEG C, the concentrated solution retained is cigarette pineapple flavors.
This cigarette pineapple flavors fragrance is true to nature, and outward appearance is transparent.This cigarette pineapple flavors is sprayed on pipe tobacco and makes cigarette, cigarette flavor can be improved, reduce stimulation, soft flue gas, promote the production of body fluid Hui Tian.
Embodiment 3
Take clean fresh pineapple 960 grams, be squeezed into thick paste with juice extractor, under 12 DEG C of conditions, leave standstill 18 hours, be separated and obtain pineapple supernatant liquor.Gained pineapple supernatant liquor is first adopted membrane pore size be 20000 ultra-filtration membrane be 0.35Mpa at pressure, temperature is carry out circulating filtration under the condition of 20 DEG C, and gained cleaner liquid is pineapple filtrate.Gained pineapple filtrate is adopted again membrane pore size be 2000 ultra-filtration membrane be 0.80Mpa at pressure, temperature is carry out circulating filtration under the condition of 15 DEG C, and the concentrated solution retained is cigarette pineapple flavors.
This cigarette pineapple flavors fragrance is true to nature, and outward appearance is transparent.This cigarette pineapple flavors is sprayed on pipe tobacco and makes cigarette, cigarette flavor can be improved, reduce stimulation, soft flue gas, promote the production of body fluid Hui Tian.
Embodiment 4
Take clean fresh pineapple 1200 grams, be squeezed into thick paste with juice extractor, under 15 DEG C of conditions, leave standstill 20 hours, be separated and obtain pineapple supernatant liquor.Gained pineapple supernatant liquor is first adopted membrane pore size be 30000 ultra-filtration membrane be 0.18Mpa at pressure, temperature is carry out circulating filtration under the condition of 30 DEG C, and gained cleaner liquid is pineapple filtrate.Gained pineapple filtrate is adopted again membrane pore size be 3000 ultra-filtration membrane be 0.30Mpa at pressure, temperature is carry out circulating filtration under the condition of 40 DEG C, and the concentrated solution retained is cigarette pineapple flavors.
This cigarette pineapple flavors fragrance is true to nature, and outward appearance is transparent.This cigarette pineapple flavors is sprayed on pipe tobacco and makes cigarette, cigarette flavor can be improved, reduce stimulation, soft flue gas, promote the production of body fluid Hui Tian.
Embodiment 5
Take clean fresh pineapple 1500 grams, be squeezed into thick paste with juice extractor, under 15 DEG C of conditions, leave standstill 24 hours, be separated and obtain pineapple supernatant liquor.Gained pineapple supernatant liquor is first adopted membrane pore size be 25000 ultra-filtration membrane be 0.25Mpa at pressure, temperature is carry out circulating filtration under the condition of 40 DEG C, and gained cleaner liquid is pineapple filtrate.Gained pineapple filtrate is adopted again membrane pore size be 3000 ultra-filtration membrane be 0.55Mpa at pressure, temperature is carry out circulating filtration under the condition of 30 DEG C, and the concentrated solution retained is cigarette pineapple flavors.
This cigarette pineapple flavors fragrance is true to nature, and outward appearance is transparent.This cigarette pineapple flavors is sprayed on pipe tobacco and makes cigarette, cigarette flavor can be improved, reduce stimulation, soft flue gas, promote the production of body fluid Hui Tian.
The above, be the specific embodiment of the present invention.It should be pointed out that the change or replacement that can expect easily in the technical scope disclosed by the present invention, all should be encompassed within protection scope of the present invention.
Claims (4)
1. a preparation method for cigarette pineapple flavors, is characterized in that, comprises the following steps:
(1) get the raw materials ready: fresh pineapple is cleaned, dries, for subsequent use;
(2) squeeze: at room temperature, above-mentioned pineapple is carried out process of squeezing the juice, is squeezed into thick paste;
(3) freeze and analyse: the thick paste pineapple of gained is under freezing conditions placed 6 ~ 24h, be separated and obtain pineapple supernatant liquor;
(4) filter: by the pineapple supernatant liquor of gained, be 0.05 ~ 0.35Mpa with ultra-filtration membrane at pressure, temperature is carry out circulating filtration under the condition of 12 ~ 40 DEG C, and gained cleaner liquid is pineapple filtrate;
(5) concentrated: by the pineapple filtrate of gained, be 0.30 ~ 1.25Mpa with ultra-filtration membrane at pressure, temperature is again carry out circulating filtration under the condition of 12 ~ 40 DEG C, and the concentrated solution retained is cigarette pineapple flavors.
2. the preparation method of a kind of cigarette pineapple flavors according to claim 1, is characterized in that: the freezing temp in described step (3) is 2 ~ 15 DEG C.
3. the preparation method of a kind of cigarette pineapple flavors according to claim 1, is characterized in that: the membrane pore size of the ultra-filtration membrane in described step (4) is 20000 ~ 30000.
4. the preparation method of a kind of cigarette pineapple flavors according to claim 1, is characterized in that: the membrane pore size of the ultra-filtration membrane in described step (5) is 1000 ~ 3000.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510403824.8A CN104946401A (en) | 2015-07-10 | 2015-07-10 | Tobacco pineapple spice preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510403824.8A CN104946401A (en) | 2015-07-10 | 2015-07-10 | Tobacco pineapple spice preparation method |
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| CN104946401A true CN104946401A (en) | 2015-09-30 |
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| CN201510403824.8A Pending CN104946401A (en) | 2015-07-10 | 2015-07-10 | Tobacco pineapple spice preparation method |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101744324A (en) * | 2010-01-12 | 2010-06-23 | 东莞市美福乐商贸有限公司 | Method for producing clear pineapple juice |
| CN102178297A (en) * | 2011-04-13 | 2011-09-14 | 北海田野食品有限公司 | Method for preparing concentrated pineapple juice |
| CN102423116A (en) * | 2011-11-07 | 2012-04-25 | 上海聚华科技股份有限公司 | Preparation method for pineapple spice for cigarette |
| CN103865645A (en) * | 2012-12-11 | 2014-06-18 | 爱普香料集团股份有限公司 | Preparation method of fruit concentrate Maillard reaction product, and application of product in tobacco perfuming |
| CN103865651A (en) * | 2014-03-26 | 2014-06-18 | 安徽中烟工业有限责任公司 | Preparation method of melon and fruit perfume for cigarettes |
-
2015
- 2015-07-10 CN CN201510403824.8A patent/CN104946401A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101744324A (en) * | 2010-01-12 | 2010-06-23 | 东莞市美福乐商贸有限公司 | Method for producing clear pineapple juice |
| CN102178297A (en) * | 2011-04-13 | 2011-09-14 | 北海田野食品有限公司 | Method for preparing concentrated pineapple juice |
| CN102423116A (en) * | 2011-11-07 | 2012-04-25 | 上海聚华科技股份有限公司 | Preparation method for pineapple spice for cigarette |
| CN103865645A (en) * | 2012-12-11 | 2014-06-18 | 爱普香料集团股份有限公司 | Preparation method of fruit concentrate Maillard reaction product, and application of product in tobacco perfuming |
| CN103865651A (en) * | 2014-03-26 | 2014-06-18 | 安徽中烟工业有限责任公司 | Preparation method of melon and fruit perfume for cigarettes |
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Application publication date: 20150930 |
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