CN104946212A - Clean anti-freezing solution for automobiles and preparation method thereof - Google Patents
Clean anti-freezing solution for automobiles and preparation method thereof Download PDFInfo
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- CN104946212A CN104946212A CN201510323949.XA CN201510323949A CN104946212A CN 104946212 A CN104946212 A CN 104946212A CN 201510323949 A CN201510323949 A CN 201510323949A CN 104946212 A CN104946212 A CN 104946212A
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- parts
- decarbonizer
- silicate
- deicing fluid
- cleaning vehicle
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
- C09K5/20—Antifreeze additives therefor, e.g. for radiator liquids
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- Chemical & Material Sciences (AREA)
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- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Thermal Sciences (AREA)
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- Organic Chemistry (AREA)
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Abstract
The invention discloses a clean anti-freezing solution for automobiles, and belongs to the technical field of anti-freezing solutions. The anti-freezing solution is obtained from reacting the following components in parts by weight: 80-90 parts of propylene glycol, 10-30 parts of deionized water, 2-3 parts of a decarbonizer, 10-20 parts of a corrosion inhibiter, 5-10 parts of silicate, 6-8 parts of a silicate stabilizer, 1-3 parts of a defoamer and 1-5 parts of a colorant, wherein the decarbonizer is prepared from the following raw materials by weight proportion: 90% of deionized water, 5% of triethanolamine, 1% of a surfactant and 4% of a foaming agent; the corrosion inhibiter adopts triethanolamine. The invention also discloses a preparation method of the anti-freezing solution. The clean anti-freezing solution for automobiles provided by the invention can provide long-acting corrosion protection through the homemade decarbonizer, is low in cost, environment-friendly and free of pollution, and avoids gel deposition and scale formation; the preparation method of the clean anti-freezing solution for automobiles is simple and environment-friendly in steps and easy to operate.
Description
Technical field
The invention belongs to deicing fluid technical field, be specifically related to a kind of cleaning vehicle deicing fluid and preparation method thereof.
Background technology
The full name of deicing fluid should be anti-freeze cooling liquid, means the cooling fluid of antifreeze function, and deicing fluid is internal combustion
The heat-eliminating medium of machine circulating cooling system, and the working order of cooling system directly affect vehicle normal operation and
In the work-ing life of vehicle, deicing fluid is not only winter, and it should use in the whole year.
Traditional deicing fluid process contamination is serious, and very easily adsorbing contaminant, causes secondary pollution.
Summary of the invention
Goal of the invention: the object of the present invention is to provide a kind of cleaning vehicle deicing fluid deicing fluid, make its cleanliness without any pollution, and precipitation and fouling can not be produced; Another object of the present invention is to provide the preparation method of this cleaning vehicle deicing fluid.
Technical scheme: for achieving the above object, the present invention adopts following technical scheme:
A kind of cleaning vehicle deicing fluid, by being obtained by reacting of following component: 80 ~ 90 parts of propylene glycol, 10 ~ 30 parts of deionized waters, decarbonizer 2 ~ 3 parts, inhibiter 10 ~ 20 parts, silicate 5 ~ 10 parts, silicate stabilizers 6 ~ 8 parts, defoamer 1 ~ 3 part and tinting materials 1 ~ 5 part; Described decarbonizer is made up of the raw material of following weight proportion: the deionized water of 90%, the trolamine of 5%, the tensio-active agent of 1% and the whipping agent of 4%; Described inhibiter is trolamine.
Described silicate stabilizers is Si
2n and Si
2the compound of P.
Described defoamer is silicone or glycidyl ether.
Described tinting material is any one in blue, the phenol red or methyl red of bromine first.
Prepare the method for cleaning vehicle deicing fluid, comprise the following steps:
(1) frostproofer is mixed
At normal temperatures, 80 ~ 90 parts of propylene glycol, 10 ~ 30 parts of deionized waters are uniformly mixed in reaction container, stirring velocity controls at 40 ~ 60 revs/min, stirs 20 ~ 30 minutes, obtains mixed frostproofer;
(2) auxiliary agent is added
Inhibiter 10 ~ 20 parts, silicate 5 ~ 10 parts, decarbonizer 2 ~ 3 parts, silicate stabilizers 6 ~ 8 parts, defoamer 1 ~ 3 part and tinting material 1 ~ 5 part are progressively added in mixed frostproofer, returns to normal temperature after continuing stirring 1 ~ 2h and namely obtain work in-process;
(3) packaging is left standstill
After work in-process are left standstill ten minutes, the particulate state leached in reaction container is not tolerant, and after adjust ph, continuation stirring can be shut down and is packaged to be finished product for ten minutes.
Beneficial effect: compared with prior art, cleaning vehicle deicing fluid of the present invention, by homemade decarbonizer, can not only provide long life anti corrosion, cheap, environment friendly and pollution-free, and can not produce, gel precipitation and fouling; The preparation method of this cleaning vehicle deicing fluid, the simple environmental protection of step, easy to implement.
Embodiment
Below in conjunction with specific embodiment, the present invention is described further.
Embodiment 1
A kind of cleaning vehicle deicing fluid, by being obtained by reacting of following component: 80 parts of propylene glycol, 10 parts of deionized waters, decarbonizer 2 parts, inhibiter 10 parts, silicate 5 parts, silicate stabilizers 6 parts, defoamer 1 part and tinting materials 1 part; Described decarbonizer is made up of the raw material of following weight proportion: the deionized water of 90%, the trolamine of 5%, the tensio-active agent of 1% and the whipping agent of 4%; Described inhibiter is trolamine.Silicate stabilizers is Si
2n and Si
2the compound of P.Defoamer is silicone or glycidyl ether.Tinting material is any one in blue, the phenol red or methyl red of bromine first.
Prepare the method for cleaning vehicle deicing fluid, comprise the following steps:
(1) frostproofer is mixed
At normal temperatures, 80 parts of propylene glycol, 10 parts of deionized waters are uniformly mixed in reaction container, stirring velocity controls at 40 revs/min, stirs 20 minutes, obtains mixed frostproofer;
(2) auxiliary agent is added
Inhibiter 10 parts, silicate 5 parts, decarbonizer 2 parts, silicate stabilizers 6 parts, defoamer 1 part and tinting material 1 part are progressively added in mixed frostproofer, returns to normal temperature after continuing to stir 1h and namely obtain work in-process;
(3) packaging is left standstill
After work in-process are left standstill ten minutes, the particulate state leached in reaction container is not tolerant, and after adjust ph, continuation stirring can be shut down and is packaged to be finished product 1 for ten minutes.
Embodiment 2
A kind of cleaning vehicle deicing fluid, by being obtained by reacting of following component: 90 parts of propylene glycol, 30 parts of deionized waters, decarbonizer 3 parts, inhibiter 20 parts, silicate 10 parts, silicate stabilizers 8 parts, defoamer 3 parts and tinting materials 5 parts; Described decarbonizer is made up of the raw material of following weight proportion: the deionized water of 90%, the trolamine of 5%, the tensio-active agent of 1% and the whipping agent of 4%; Described inhibiter is trolamine.Silicate stabilizers is Si
2n and Si
2the compound of P.Defoamer is silicone or glycidyl ether.Tinting material is any one in blue, the phenol red or methyl red of bromine first.
Prepare the method for cleaning vehicle deicing fluid, comprise the following steps:
(1) frostproofer is mixed
At normal temperatures, 90 parts of propylene glycol, 30 parts of deionized waters are uniformly mixed in reaction container, stirring velocity controls at 60 revs/min, stirs 30 minutes, obtains mixed frostproofer;
(2) auxiliary agent is added
Inhibiter 20 parts, silicate 10 parts, decarbonizer 3 parts, silicate stabilizers 8 parts, defoamer 3 parts and tinting material 5 parts are progressively added in mixed frostproofer, returns to normal temperature after continuing to stir 2h and namely obtain work in-process;
(3) packaging is left standstill
After work in-process are left standstill ten minutes, the particulate state leached in reaction container is not tolerant, and after adjust ph, continuation stirring can be shut down and is packaged to be finished product 2 for ten minutes.
Embodiment 3 inspection after construction
Finished product 1 ~ 2 sampling detected, gained finished product 1 ~ 2 reaches following technical indicator: reserve alkalinity: 16.92ml; Lather volume :≤20ml; Foam vanishing time :≤1.4s; Artificial corrosion tests: 1000h hour unchanged.
Claims (5)
1. a cleaning vehicle deicing fluid, is characterized in that: by being obtained by reacting of following component: 80 ~ 90 parts of propylene glycol, 10 ~ 30 parts of deionized waters, decarbonizer 2 ~ 3 parts, inhibiter 10 ~ 20 parts, silicate 5 ~ 10 parts, silicate stabilizers 6 ~ 8 parts, defoamer 1 ~ 3 part and tinting materials 1 ~ 5 part; Described decarbonizer is made up of the raw material of following weight proportion: the deionized water of 90%, the trolamine of 5%, the tensio-active agent of 1% and the whipping agent of 4%; Described inhibiter is trolamine.
2. cleaning vehicle deicing fluid according to claim 1, is characterized in that: described silicate stabilizers is Si
2n and Si
2the compound of P.
3. cleaning vehicle deicing fluid according to claim 1, is characterized in that: described defoamer is silicone or glycidyl ether.
4. cleaning vehicle deicing fluid according to claim 1, is characterized in that: described tinting material is any one in blue, the phenol red or methyl red of bromine first.
5. prepare the method for the cleaning vehicle deicing fluid in claim 1 ~ 5 described in any one, comprise the following steps:
(1) frostproofer is mixed
At normal temperatures, 80 ~ 90 parts of propylene glycol, 10 ~ 30 parts of deionized waters are uniformly mixed in reaction container, stirring velocity controls at 40 ~ 60 revs/min, stirs 20 ~ 30 minutes, obtains mixed frostproofer;
(2) auxiliary agent is added
Inhibiter 10 ~ 20 parts, silicate 5 ~ 10 parts, decarbonizer 2 ~ 3 parts, silicate stabilizers 6 ~ 8 parts, defoamer 1 ~ 3 part and tinting material 1 ~ 5 part are progressively added in mixed frostproofer, returns to normal temperature after continuing stirring 1 ~ 2h and namely obtain work in-process;
(3) packaging is left standstill
After work in-process are left standstill ten minutes, the particulate state leached in reaction container is not tolerant, and after adjust ph, continuation stirring can be shut down and is packaged to be finished product for ten minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510323949.XA CN104946212A (en) | 2015-06-15 | 2015-06-15 | Clean anti-freezing solution for automobiles and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510323949.XA CN104946212A (en) | 2015-06-15 | 2015-06-15 | Clean anti-freezing solution for automobiles and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104946212A true CN104946212A (en) | 2015-09-30 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510323949.XA Pending CN104946212A (en) | 2015-06-15 | 2015-06-15 | Clean anti-freezing solution for automobiles and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107151550A (en) * | 2016-03-04 | 2017-09-12 | 雅孚顿（天津）石化产品有限公司 | A kind of multifunction long-acting anti-freeze solution and its preparation technology |
| CN113234423A (en) * | 2021-06-07 | 2021-08-10 | 温州大学激光与光电智能制造研究院 | Cooling liquid and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102618397A (en) * | 2012-02-21 | 2012-08-01 | 上海约锐克实业有限公司 | Foam-type decarbonizer for combustion chamber |
| CN104130755A (en) * | 2014-07-02 | 2014-11-05 | 宝捷润滑油镇江有限公司 | Anticorrosion and environmental protection automobile antifreeze fluid and preparation method thereof |
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2015
- 2015-06-15 CN CN201510323949.XA patent/CN104946212A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102618397A (en) * | 2012-02-21 | 2012-08-01 | 上海约锐克实业有限公司 | Foam-type decarbonizer for combustion chamber |
| CN104130755A (en) * | 2014-07-02 | 2014-11-05 | 宝捷润滑油镇江有限公司 | Anticorrosion and environmental protection automobile antifreeze fluid and preparation method thereof |
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| 王晓波等: "车用防冻液概述", 《化工科技》 * |
| 贾睿等: "汽车燃油清洗剂的发展及展望", 《清洗世界》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107151550A (en) * | 2016-03-04 | 2017-09-12 | 雅孚顿（天津）石化产品有限公司 | A kind of multifunction long-acting anti-freeze solution and its preparation technology |
| CN113234423A (en) * | 2021-06-07 | 2021-08-10 | 温州大学激光与光电智能制造研究院 | Cooling liquid and preparation method thereof |
| CN113234423B (en) * | 2021-06-07 | 2022-01-14 | 富地润滑科技股份有限公司 | Cooling liquid and preparation method thereof |
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Application publication date: 20150930 |
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