CN104946137A - Efficient diamond spray polishing agent - Google Patents
Efficient diamond spray polishing agent Download PDFInfo
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- CN104946137A CN104946137A CN201510250899.7A CN201510250899A CN104946137A CN 104946137 A CN104946137 A CN 104946137A CN 201510250899 A CN201510250899 A CN 201510250899A CN 104946137 A CN104946137 A CN 104946137A
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- nano
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- diamond
- polishing
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
The invention discloses a compounding method of an efficient diamond spray polishing agent. The efficient diamond spray polishing agent is synthesized from the following components in percentage by mass: 7-16% of nano diamond, 15-30% of solvent, 6-17% of nano attapulgite, 9-18% of bentonite, 8-14% of surfactant, 4-17% of dispersing agent, 0.2-6% of pH regulator and 2-50% of pressurized gas. According to the method disclosed by the invention, when the spray polishing agent prepared by adding the nano attapulgite and bentonite is adopted for polishing in cooperation with paper, the paper is not easily broken, thus the polishing paper does not need to be frequently changed, the paper waste is reduced, the time is greatly saved, the polishing efficiency is high, and the development of national economy is promoted.
Description
Technical field
The present invention relates to a kind of preparation method of rumbling compound of spraying, especially a kind of metallurgical polishing technical field.
Background technology
Diamond is the xln of carbon under high-temperature and high-pressure conditions, is the mineral that nature is the hardest, is a kind of rare, valuable nonmetallic minerals, has important effect in national economy, recently, producer is had to release the polishing medium of the other types such as paper using abroad, domestic have the producer's external a complete set of polissoir of import and various associated materials, and carry out the production domesticization of material, the side abroad provided is by being: with diamond polishing liquid and special paper with the use of carrying out polishing, problem has been there is when the spray abrasive for diamond produced with my company substitutes the polishing fluid of import, when spray abrasive for diamond is sprayed on and paper carries out polishing, paper is very easily damaged, careful use generally polishing three can only coil sample, a dish can fill six samples at that time, frequently must change polishing paper like this, a large amount of wastes of paper are not only caused to the more important thing is too much consuming time, seriously affect completing of testing, in order to save paper, reduce use cost, the minimizing time etc., invent a kind of high-efficiency diamond spraying rumbling compound adding nano-attapulgite and wilkinite and make, this rumbling compound with paper with the use of time, paper is cracky not, greatly reduce cost, polishing efficiency is high, facilitate the development of national economy.
Summary of the invention
The drawback such as the waste, the use cost that the present invention is directed to paper are high, short time consumption is long, polishing efficiency is low, provide a kind of high-efficiency diamond spraying rumbling compound, solve rumbling compound when carrying out polishing on paper, paper be very easily damaged, paper is wasted in a large number, the problem such as too much consuming time.
For solving the problems of the technologies described above, the present invention adopts technical scheme as described below: this spraying rumbling compound is synthesized by Nano diamond, solvent, nano-attapulgite, wilkinite, tensio-active agent, dispersion agent, pH adjusting agent, gas under pressure; By mass percentage, wherein Nano diamond 7% ~ 16%, solvent 15% ~ 30%, nano-attapulgite 6% ~ 17%, wilkinite 9% ~ 18%, tensio-active agent 8% ~ 14%, dispersion agent 4% ~ 17%, pH adjusting agent 0.2% ~ 6%, gas under pressure 2% ~ 50%; Described solvent is water or ethanol; Described tensio-active agent is in polyoxyethylenated alcohol sodium sulfate, fatty alcohol-polyoxyethylene ether, heavy alkylbenzene sulfonate two or three; Described dispersion agent is in methyl amyl alcohol, triethyl hexyl phosphoric acid, fatty acid polyglycol ester two or three; Described gas under pressure is nitrogen.
Described tensio-active agent forms by mass percentage, polyoxyethylenated alcohol sodium sulfate 25% ~ 60%, fatty alcohol-polyoxyethylene ether 20% ~ 40%, heavy alkylbenzene sulfonate 15% ~ 30%; Described dispersion agent forms by mass percentage, methyl amyl alcohol 10% ~ 35%, triethyl hexyl phosphoric acid 20% ~ 50%, fatty acid polyglycol ester 30% ~ 60%.
Described a kind of high-efficiency diamond spraying rumbling compound, is characterized in that concrete composite step is:
(1) first choose 7% ~ 16% Nano diamond, carry out secondary breaking, then carry out chemical purification and cleaning, then carry out drying, obtained Nano diamond powder;
(2) 6% ~ 17% nano-attapulgite and Nano diamond powder are mixed than row by certain, add 15% ~ 30% solvent, insert in Erlenmeyer flask, after being heated to 40 DEG C ~ 60 DEG C, slowly join in mixing solutions by 9% ~ 18% wilkinite, rising to temperature is 60 DEG C ~ 90 DEG C continuation reactions;
(3) 8% ~ 14% tensio-active agent, 4% ~ 17% dispersion agent is added again, with 0.2% ~ 6%pH conditioning agent, pH value is adjusted between 5 ~ 7, stir, be then ultrasonic emulsification 10 ~ 35 minutes under the condition of 25HZ ~ 55HZ in frequency by the mixing solutions of gained, join again in autoclave, be filled with 2% ~ 50% nitrogen.
The present invention is compared with additive method, and Advantageous Effects is:
(1) after adding nano-attapulgite and wilkinite, with paper with the use of, paper is cracky not;
(2) save paper, use cost reduces;
(3) consuming time short, polishing efficiency is high.
Concrete application: with diamond spraying rumbling compound and special paper with the use of carrying out polishing, be sprayed on when paper carrying out polishing, paper is cracky not, polishing ten can coil sample, one dish can fill ten samples, do not need so frequently to change polishing paper, polishing efficiency reaches 82%, not only saves use cost and also greatly reduces short time consumption.
Embodiment
The present invention is synthesized by Nano diamond, solvent, nano-attapulgite, wilkinite, tensio-active agent, dispersion agent, pH adjusting agent, gas under pressure; By mass percentage, wherein Nano diamond 7% ~ 16%, solvent 15% ~ 30%, nano-attapulgite 6% ~ 17%, wilkinite 9% ~ 18%, tensio-active agent 8% ~ 14%, dispersion agent 4% ~ 17%, pH adjusting agent 0.2% ~ 6%, gas under pressure 2% ~ 50%; Described solvent is water or ethanol; Described tensio-active agent is in polyoxyethylenated alcohol sodium sulfate, fatty alcohol-polyoxyethylene ether, heavy alkylbenzene sulfonate two or three; Described dispersion agent is in methyl amyl alcohol, triethyl hexyl phosphoric acid, fatty acid polyglycol ester two or three; Described gas under pressure is nitrogen.
Described tensio-active agent forms by mass percentage, polyoxyethylenated alcohol sodium sulfate 25% ~ 60%, fatty alcohol-polyoxyethylene ether 20% ~ 40%, heavy alkylbenzene sulfonate 15% ~ 30%; Described dispersion agent forms by mass percentage, methyl amyl alcohol 10% ~ 35%, triethyl hexyl phosphoric acid 20% ~ 50%, fatty acid polyglycol ester 30% ~ 60%.
First choose 7% ~ 16% Nano diamond, carry out secondary breaking, then carry out chemical purification and cleaning, then carry out drying, obtained Nano diamond powder; 6% ~ 17% nano-attapulgite and Nano diamond powder are mixed than row by certain, add 15% ~ 30% solvent, insert in Erlenmeyer flask, after being heated to 40 DEG C ~ 60 DEG C, slowly join in mixing solutions by 9% ~ 18% wilkinite, rising to temperature is 60 DEG C ~ 90 DEG C continuation reactions; Add 8% ~ 14% tensio-active agent, 4% ~ 17% dispersion agent again, with 0.2% ~ 6%pH conditioning agent, pH value is adjusted between 5 ~ 7, stir, be then ultrasonic emulsification 10 ~ 35 minutes under the condition of 25HZ ~ 55HZ in frequency by the mixing solutions of gained, join again in autoclave, be filled with 2% ~ 50% nitrogen.
Example 1
First choose 10% Nano diamond, carry out secondary breaking, then carry out chemical purification and cleaning, then carry out drying, obtained Nano diamond powder; 17% nano-attapulgite and Nano diamond powder are added 10% solvent, insert in Erlenmeyer flask by certain than row mixing, after being heated to 40 DEG C, slowly join in mixing solutions by 14% wilkinite, and rising to temperature is 60 DEG C of continuation reactions; Add 6% fatty alcohol-polyoxyethylene ether, 3.6% methyl amyl alcohol again, with 2%pH conditioning agent, pH value being adjusted to 6, stirring, is then ultrasonic emulsification 18 minutes under the condition of 30HZ in frequency by the mixing solutions of gained, join again in autoclave, be filled with 23% nitrogen; When the spraying rumbling compound paper that this method is obtained carries out polishing, paper is cracky not, the sample that energy polishing is over half, so does not just need frequently to change polishing paper, not only decrease the waste of paper but also greatly save the time, more can not affect completing of testing.
Example 2
First choose 14% Nano diamond, carry out secondary breaking, then carry out chemical purification and cleaning, then carry out drying, obtained Nano diamond powder; 15% nano-attapulgite and Nano diamond powder are added 8% solvent, insert in Erlenmeyer flask by certain than row mixing, after being heated to 50 DEG C, slowly join in mixing solutions by 16% wilkinite, and rising to temperature is 80 DEG C of continuation reactions; Add 3.2% polyoxyethylenated alcohol sodium sulfate, 2.5% triethyl hexyl phosphoric acid again, with 4%pH conditioning agent, pH value is adjusted to 5, stir, be then ultrasonic emulsification 22 minutes under the condition of 40HZ in frequency by the mixing solutions of gained, join again in autoclave, be filled with 30% nitrogen; When the spraying rumbling compound paper that this method is obtained carries out polishing, paper is cracky not, the sample that energy polishing is over half, so does not just need frequently to change polishing paper, not only decrease the waste of paper but also greatly save the time, more can not affect completing of testing; When the spraying rumbling compound paper that this method is obtained carries out polishing, paper is cracky not, the sample that energy polishing is over half, so does not just need frequently to change polishing paper, not only decrease the waste of paper but also greatly save the time, more can not affect completing of testing.
Example 3
First choose 8% Nano diamond, carry out secondary breaking, then carry out chemical purification and cleaning, then carry out drying, obtained Nano diamond powder; 9% nano-attapulgite and Nano diamond powder are added 8% solvent, insert in Erlenmeyer flask by certain than row mixing, after being heated to 60 DEG C, slowly join in mixing solutions by 10% wilkinite, and rising to temperature is 90 DEG C of continuation reactions; Add 3.6% heavy alkylbenzene sulfonate, 8.4% fatty acid polyglycol ester again, with 6%pH conditioning agent, pH value being adjusted to 7, stirring, is then ultrasonic emulsification 28 minutes under the condition of 40HZ in frequency by the mixing solutions of gained, join again in autoclave, be filled with 33% nitrogen; When the spraying rumbling compound paper that this method is obtained carries out polishing, paper is cracky not, the sample that energy polishing is over half, so does not just need frequently to change polishing paper, not only decrease the waste of paper but also greatly save the time, more can not affect completing of testing.
Claims (3)
1. a high-efficiency diamond spraying rumbling compound, is characterized in that: this spraying rumbling compound is synthesized by Nano diamond, solvent, nano-attapulgite, wilkinite, tensio-active agent, dispersion agent, pH adjusting agent, gas under pressure; By mass percentage, wherein Nano diamond 7% ~ 16%, solvent 15% ~ 30%, nano-attapulgite 6% ~ 17%, wilkinite 9% ~ 18%, tensio-active agent 8% ~ 14%, dispersion agent 4% ~ 17%, pH adjusting agent 0.2% ~ 6%, gas under pressure 2% ~ 50%; Described solvent is water or ethanol; Described tensio-active agent is in polyoxyethylenated alcohol sodium sulfate, fatty alcohol-polyoxyethylene ether, heavy alkylbenzene sulfonate two or three; Described dispersion agent is in methyl amyl alcohol, triethyl hexyl phosphoric acid, fatty acid polyglycol ester two or three; Described gas under pressure is nitrogen.
2. a kind of high-efficiency diamond spraying rumbling compound according to claim 1, it is characterized in that: described tensio-active agent forms by mass percentage, polyoxyethylenated alcohol sodium sulfate 25% ~ 60%, fatty alcohol-polyoxyethylene ether 20% ~ 40%, heavy alkylbenzene sulfonate 15% ~ 30%; Described dispersion agent forms by mass percentage, methyl amyl alcohol 10% ~ 35%, triethyl hexyl phosphoric acid 20% ~ 50%, fatty acid polyglycol ester 30% ~ 60%.
3. a kind of high-efficiency diamond spraying rumbling compound according to claim 1, is characterized in that concrete composite step is:
(1) first choose 7% ~ 16% Nano diamond, carry out secondary breaking, then carry out chemical purification and cleaning, then carry out drying, obtained Nano diamond powder;
(2) 6% ~ 17% nano-attapulgite and Nano diamond powder are mixed than row by certain, add 15% ~ 30% solvent, insert in Erlenmeyer flask, after being heated to 40 DEG C ~ 60 DEG C, slowly join in mixing solutions by 9% ~ 18% wilkinite, rising to temperature is 60 DEG C ~ 90 DEG C continuation reactions;
(3) 8% ~ 14% tensio-active agent, 4% ~ 17% dispersion agent is added again, with 0.2% ~ 6%pH conditioning agent, pH value is adjusted between 5 ~ 7, stir, be then ultrasonic emulsification 10 ~ 35 minutes under the condition of 25HZ ~ 55HZ in frequency by the mixing solutions of gained, join again in autoclave, be filled with 2% ~ 50% nitrogen.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510250899.7A CN104946137A (en) | 2015-05-12 | 2015-05-12 | Efficient diamond spray polishing agent |
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| CN201510250899.7A CN104946137A (en) | 2015-05-12 | 2015-05-12 | Efficient diamond spray polishing agent |
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| CN104946137A true CN104946137A (en) | 2015-09-30 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113265224A (en) * | 2021-04-29 | 2021-08-17 | 郑州磨料磨具磨削研究所有限公司 | Spray type diamond grinding fluid and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1064495A (en) * | 1992-03-12 | 1992-09-16 | 武汉工业大学 | Spray abrasive for diamond |
| CN101050339A (en) * | 2007-05-17 | 2007-10-10 | 中国地质大学（武汉） | Diamond polishing paste in high purity, and preparation method |
| CN103525314A (en) * | 2013-10-30 | 2014-01-22 | 湖北三翔超硬材料有限公司 | High-efficiency diamond lubricating cooling polishing solution and preparation method and application thereof |
| CN104031560A (en) * | 2013-03-07 | 2014-09-10 | 天津市乾宇超硬科技有限公司 | Water-based diamond polishing solution used for crystal processing |
-
2015
- 2015-05-12 CN CN201510250899.7A patent/CN104946137A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1064495A (en) * | 1992-03-12 | 1992-09-16 | 武汉工业大学 | Spray abrasive for diamond |
| CN101050339A (en) * | 2007-05-17 | 2007-10-10 | 中国地质大学（武汉） | Diamond polishing paste in high purity, and preparation method |
| CN104031560A (en) * | 2013-03-07 | 2014-09-10 | 天津市乾宇超硬科技有限公司 | Water-based diamond polishing solution used for crystal processing |
| CN103525314A (en) * | 2013-10-30 | 2014-01-22 | 湖北三翔超硬材料有限公司 | High-efficiency diamond lubricating cooling polishing solution and preparation method and application thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113265224A (en) * | 2021-04-29 | 2021-08-17 | 郑州磨料磨具磨削研究所有限公司 | Spray type diamond grinding fluid and preparation method thereof |
| CN113265224B (en) * | 2021-04-29 | 2021-11-30 | 郑州磨料磨具磨削研究所有限公司 | Spray type diamond grinding fluid and preparation method thereof |
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Application publication date: 20150930 |
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