CN104944913A - Production method for dry-joint sticking clay of Nixing pottery - Google Patents
Production method for dry-joint sticking clay of Nixing pottery Download PDFInfo
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- CN104944913A CN104944913A CN201510413223.5A CN201510413223A CN104944913A CN 104944913 A CN104944913 A CN 104944913A CN 201510413223 A CN201510413223 A CN 201510413223A CN 104944913 A CN104944913 A CN 104944913A
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Abstract
The invention provides a production method for dry-joint sticking clay of Nixing pottery. The production method for the dry-joint sticking clay of the Nixing pottery comprises the following steps that 1 raw materials of, by weight, 3 to 4 parts of east clay, 3 to 4 parts of west clay, 1 to 2 parts of cordierite, 1 to 2 parts of mineral powders and 0.5 to 1 part of feldspar are weighted; 2 the east clay and the west clay are mixed and are ground into mud through a ball mill, filtering is conducted, clay laths are formed in a suppressed mode, vacuum pugging is conducted, decaying is conducted, and A clay material is obtained; 3 the cordierite, the mineral powders and the feldspar are mixed and are mixed into mud through the ball mill, filtering is conducted, the clay laths are formed in a suppressed mode, vacuum pugging is conducted, decaying is conducted, and B clay material is obtained; 4 the A clay material and the B clay material are mixed to the dry-joint sticking clay, and the water content of the dry-joint sticking clay is 10 to 15 percents. According to the production method for the dry-joint sticking clay of the Nixing pottery, the dry-joint sticking clay still has comparatively good liquidity under the condition that the water content is comparatively low, the adhesive strength is strong, the figurability is comparatively good, and moulding body drying and burning crazing can be reduced greatly.
Description
Technical field
The present invention relates to the making method of pottery, be specifically related to the making method of Nixing pottery stem grafting sticking clay.
Background technology
Some Nixing pottery product can not once shaped, needs base substrate main body and annex to make shaping respectively, then main body is become a complete base substrate with accessory adhering with sticking clay.Modal have the main body such as kettle, tank and mouth, bonding, the annex such as ear, Gai Bing.Bondingly be divided into wet connecing and stem grafting, it is bonding that stem grafting refers to that the water ratio of base substrate main body and annex carries out about 2% time, and the water ratio of sticking clay is 25 ~ 27%, because base substrate parches, differ huge with the water ratio of sticking clay, both dry shrinkage are inconsistent, will produce string stress, cause the cracking of annex.On the other hand, the base substrate of overdrying and the moisture gradient of sticking clay are too large, and moisture is increased by the velocity of diffusion of sticking clay to base substrate, causes the violent contraction of mud, produce stress, meanwhile, the current that excessive velocity of diffusion is formed may drive a part of subparticle to embed the gluing of surfaces of base substrate, blocking pore, stop the continuation diffusion of moisture, also cause the layering of adhesive linkage large or fine granule, also can affect macrobead and embed base substrate, thus cause coming off of annex.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of Nixing pottery and wets the making method of dry joint mud, the stem grafting sticking clay that the method is made is when water ratio is relatively low, and still have good good fluidity, bonding force is strong, and plasticity-is better, can reduce season cracking.
Technical scheme provided by the invention is a kind of making method improving Nixing pottery stem grafting sticking clay, comprises the following steps:
1) raw material of following weight part is taken: 3 ~ 4 parts, eastern mud, 3 ~ 4 parts, western mud, trichroite 1 ~ 2 part, breeze 1 ~ 2 part, feldspar 0.5 ~ 1 part;
2) by eastern mud, the mixing of western mud, wear into mud through ball mill, filter, compacting mud bar, vacuum pugging, old, obtain A pug;
3) trichroite, breeze and feldspar are mixed, wear into mud through ball mill, filter, compacting mud bar, vacuum pugging, old, obtain B pug;
4) by A pug and the mixing of B pug, stem grafting sticking clay is; The water ratio of described stem grafting sticking clay is 10 ~ 15%.
The stem grafting technique of complete Nixing pottery is as follows:
1) preparing blank: by eastern mud and western mud by weight being 6:4 mixing, through ball milling 8h, then crossing 40 orders successively and 100 order twice are sieved, filtrate is suppressed mud bar, vacuum pugging, old 15 days, be blank.
2) blank forming: main body and the annex of blank being made respectively Nixing pottery base substrate, control subject and annex water ratio, 2% time, are that the stem grafting sticking clay of 10 ~ 15% is by its bonding one-tenth base substrate completed with water ratio.
3) body drying: base substrate is dried in the shade naturally.
4) fire: send kiln-firing by base substrate, kiln discharge, be Nixing pottery.
For Nixing pottery blank, wherein SiO
2content is 64 ~ 65%, Al
2o
3content is 16 ~ 17%, Fe
2o
3content is 5.1 ~ 6.8%, and the particle diameter of Nixing pottery blank is about 4 μm.
The theory of trichroite consists of: MgO:13.78%, Al
2o
3: 34.86%, SiO
2: 51.36%.SiO in trichroite
2content lower than Nixing pottery blank, and MgO, Al
2o
3for higher than Nixing pottery blank to the content of high-temperature liquid-phase contributive eutectic oxide compound, therefore, the sintering temperature that trichroite can reduce sticking clay is added in sticking clay formula, make in sintering process, sticking clay is more Zao than Nixing pottery base substrate (comprising main body and annex) there is liquid phase, these liquid phase substances can to not yet occur liquid phase Nixing pottery base substrate diffusion, on Nixing pottery base substrate formed a transition layer, thus more effectively by main body together with accessory adhering.
The main component of breeze is SiO
2: 33.76%, Al
2o
3: 11.37%, Fe
2o
3: 1.14%, CaO:40.34%, MgO:11.21%, TiO
2: 0.39%.Similarly, Al in breeze
2o
3, Fe
2o
3, CaO and MgO be to the contributive eutectic oxide compound of high-temperature liquid-phase, its total amount is higher than Nixing pottery blank, therefore, the sintering temperature that breeze can reduce sticking clay is added in sticking clay formula, be in sintering process, sticking clay is more Zao than Nixing pottery base substrate (comprising main body and annex) there is liquid phase, these liquid phase substances can to the Nixing pottery base substrate diffusion not yet occurring liquid phase, on Nixing pottery base substrate formed a transition layer, thus more effectively by main body together with accessory adhering.
Feldspar is conventional non-plastic raw material, can reduce the contraction of sticking clay in drying and sintering process.In addition, feldspar crystal is en plaque or sheet-pile shape, cordierite crystal is short cylinder, and the specific surface area of the particle of above-mentioned shape is larger than the spherical particle of Nixing pottery blank, and the contacting of en plaque, sheet-pile shape and the easy forming surface of short cylinder particle and face, the capillary radius formed reduces, enhance the mobility of stem grafting sticking clay, enhance adhesive effect, adding again due to breeze, its corner angle are many, symmetry is poor, large to the resistance of particle generation relative displacement, and then greatly strengthen the plasticity-of sticking clay.
Therefore, the firing temperature that trichroite, feldspar and breeze can reduce sticking clay is mixed in sticking clay, make it in sintering procedure, a large amount of high-temperature liquid-phase is produced prior to Nixing pottery base substrate, these high-temperature liquids are met towards the main body of Nixing pottery base substrate and annex diffusion, thus main body and annex are firmly clung, make annex difficult drop-off.By feldspar, interaction between trichroite and breeze, not only increase the adhesive power of sticking clay, also enhance the plasticity-of sticking clay, avoid base substrate in dry and sintering process to occur ftractureing and coming off.
Step 2) in, mud is crossed 100 ~ 150 orders and 200 ~ 250 mesh sieves successively, and get filtrate compacting mud bar, vacuum pugging, old 5 ~ 7 weeks, obtains the A pug that particle diameter is 1 ~ 2 μm.
Step 3) in, mud is crossed 200 ~ 250 orders and 300 ~ 350 mesh sieves successively, and get filtrate compacting mud bar, vacuum pugging, old 6 ~ 8 weeks, obtains the B pug that particle diameter is 0.5 ~ 1 μm.
The particle diameter of the A pug in sticking clay is 1 ~ 2 μm, B pug particle diameter is 0.5 ~ 1 μm, and the particle diameter of Nixing pottery blank is 4 μm, namely the grain diameter of sticking clay is less, specific surface area is comparatively large, and the capillary radius of piling up thus is less, and the capillary force of generation is larger, make sticking clay also have good mobility when water ratio is not significantly higher than base substrate, enhance the adhesive effect of sticking clay.Moreover, particle diameter and the B pug particle diameter of A pug differ, and the interface that size particles contacts exists wall effect, and porosity is higher, defines larger-size diffusion admittance, enhances the mobility of sticking clay, thus strengthen adhesive effect.
Therefore, reduce the grain diameter of sticking clay, make it to be less than Nixing pottery blank particle diameter, the mobility of sticking clay can be strengthened, be convenient to each component particles and mutually shift near and draw close, strengthen cohesive force; And A pug and B pug grain diameter differ in sticking clay, contribute to forming larger diffusion admittance in sticking clay inside, strengthen the mobility of sticking clay further, thus strengthen adhesive effect.
The present invention has following beneficial effect:
1) the stem grafting sticking clay water ratio that the present invention makes is only 10 ~ 15%, well below the water ratio of conventional stem grafting sticking clay, can ensure that in and sintering process dry at sticking clay, moisture shrinks less like this, string stress is less, thus greatly reduces annex cracking probability.Meanwhile, the moisture gradient of sticking clay and base substrate is less, can avoid the layering of adhesive linkage large or fine granule, and then greatly reduces annex and to come off probability.
2) stem grafting sticking clay of the present invention is when water ratio is only 10 ~ 15%, and still can ensure good mobility, accessory adhering is effective, difficult drop-off.
3) adopt stem grafting sticking clay of the present invention to carry out stem grafting to Nixing pottery base substrate, for the small-sized vessel of Nixing pottery, the stem grafting rate of burning till can reach more than 85%.
Embodiment
The present invention is further elaborated for following specific embodiment, but not as a limitation of the invention.
Embodiment 1
1) raw material of following weight part is taken: 3 parts, eastern mud, 3 parts, western mud, trichroite 1 part, breeze 1 part, feldspar 0.5 part;
2) by eastern mud, the mixing of western mud, obtain mud through ball milling 8h, then mud is crossed successively 40 orders and 100 order twice sieve, get filtrate compacting mud bar, vacuum pugging, old 15 days, obtains A pug;
3) trichroite, breeze and feldspar are mixed, obtain mud through ball milling 8h, then mud is crossed successively 40 orders and 100 order twice sieve, get filtrate compacting mud bar, vacuum pugging, old 15 days, obtains B pug;
4) by A pug and the mixing of B pug, stem grafting sticking clay is; The water ratio of described stem grafting sticking clay is 10%.
Embodiment 2
1) raw material of following weight part is taken: 4 parts, eastern mud, 4 parts, western mud, trichroite 2 parts, breeze 2 parts, feldspar 1 part;
2) by eastern mud, the mixing of western mud, obtain mud through ball milling 8h, then mud is crossed successively 40 orders and 100 order twice sieve, get filtrate compacting mud bar, vacuum pugging, old 15 days, obtains A pug;
3) trichroite, breeze and feldspar are mixed, obtain mud through ball milling 8h, then mud is crossed successively 40 orders and 100 order twice sieve, get filtrate compacting mud bar, vacuum pugging, old 15 days, obtains B pug;
4) by A pug and the mixing of B pug, stem grafting sticking clay is; The water ratio of described stem grafting sticking clay is 15%.
Embodiment 3
1) raw material of following weight part is taken: 3 parts, eastern mud, 4 parts, western mud, trichroite 1 part, breeze 2 parts, feldspar 0.5 part;
2) by eastern mud, the mixing of western mud, mud is crossed 100 orders and 200 mesh sieves successively, get filtrate compacting mud bar, vacuum pugging, old 5 weeks, obtains the A pug that particle diameter is 2 μm;
3) mixing of trichroite, breeze and feldspar is obtained mud through ball milling 8h, then mud is crossed successively 40 orders and 100 order twice sieve, get filtrate compacting mud bar, vacuum pugging, old 15 days, obtains B pug;
4) by A pug and the mixing of B pug, stem grafting sticking clay is; The water ratio of described stem grafting sticking clay is 12%.
Embodiment 4
1) raw material of following weight part is taken: 4 parts, eastern mud, 3 parts, western mud, trichroite 1 part, breeze 2 parts, feldspar 0.5 part;
2) by eastern mud, the mixing of western mud, obtain mud through ball milling 8h, then mud is crossed successively 40 orders and 100 order twice sieve, get filtrate compacting mud bar, vacuum pugging, old 15 days, obtains A pug;
3) trichroite, breeze and feldspar are mixed, wear into mud through ball mill, mud is crossed 250 orders and 350 mesh sieves successively, get filtrate compacting mud bar, vacuum pugging, old 8 weeks, obtains the B pug that particle diameter is 0.5 μm;
4) by A pug and the mixing of B pug, stem grafting sticking clay is; The water ratio of described stem grafting sticking clay is 15%.
Embodiment 5
1) raw material of following weight part is taken: 3.5 parts, eastern mud, 3.6 parts, western mud, trichroite 1.3 parts, breeze 1.6 parts, feldspar 0.6 part;
2) by eastern mud, the mixing of western mud, mud is crossed 150 orders and 250 mesh sieves successively, get filtrate compacting mud bar, vacuum pugging, old 7 weeks, obtains the A pug that particle diameter is 1 μm;
3) trichroite, breeze and feldspar are mixed, wear into mud through ball mill, mud is crossed 200 orders and 300 mesh sieves successively, get filtrate compacting mud bar, vacuum pugging, old 6 weeks, obtains the B pug that particle diameter is 1 μm;
4) by A pug and the mixing of B pug, stem grafting sticking clay is; The water ratio of described stem grafting sticking clay is 13%.
Prepare 500 covers Nixing pottery teapot base substrate (comprising kettle body and Hu Zui) according to a conventional method, the water ratio of kettle body and Hu Zui is 2%, and it is divided into 5 groups at random, often organizes 100 covers, is respectively experimental group 1,2,3,4,5.The stem grafting sticking clay of Example 1 ~ 5 carries out stem grafting to the 100 cover base substrates often organized respectively, bonding complete after, carry out conventional drying and sintering, the rate of burning till sees the following form:
| Group | Sum (individual) | Hardening crack, come off number (individual) | Burn till rate (%) |
| Experimental group 1 | 100 | 13 | 87 |
| Experimental group 2 | 100 | 12 | 88 |
| Experimental group 3 | 100 | 7 | 93 |
| Experimental group 4 | 100 | 8 | 92 |
| Experimental group 5 | 100 | 3 | 97 |
Claims (3)
1. the making method of Nixing pottery stem grafting sticking clay, is characterized in that: comprise the following steps:
1) raw material of following weight part is taken: 3 ~ 4 parts, eastern mud, 3 ~ 4 parts, western mud, trichroite 1 ~ 2 part, breeze 1 ~ 2 part, feldspar 0.5 ~ 1 part;
2) by eastern mud, the mixing of western mud, wear into mud through ball mill, filter, compacting mud bar, vacuum pugging, old, obtain A pug;
3) trichroite, breeze and feldspar are mixed, wear into mud through ball mill, filter, compacting mud bar, vacuum pugging, old, obtain B pug;
4) by A pug and the mixing of B pug, stem grafting sticking clay is; The water ratio of described stem grafting sticking clay is 10 ~ 15%.
2. the making method of Nixing pottery stem grafting sticking clay according to claim 1, is characterized in that: step 2) in, mud is crossed 100 ~ 150 orders and 200 ~ 250 mesh sieves successively, get filtrate compacting mud bar, vacuum pugging, old 5 ~ 7 weeks, obtains the A pug that particle diameter is 1 ~ 2 μm.
3. the making method of Nixing pottery stem grafting sticking clay according to claim 1 and 2, is characterized in that: step 3) in, mud is crossed 200 ~ 250 orders and 300 ~ 350 mesh sieves successively, get filtrate compacting mud bar, vacuum pugging, old 6 ~ 8 weeks, obtains the B pug that particle diameter is 0.5 ~ 1 μm.
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|---|---|---|---|
| CN201510413223.5A CN104944913B (en) | 2015-07-14 | 2015-07-14 | The manufacture method of Nixing pottery stem grafting sticking clay |
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| CN104944913B CN104944913B (en) | 2017-01-04 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105294088A (en) * | 2015-12-09 | 2016-02-03 | 钦州市华夏太极泉坭兴陶艺有限责任公司 | Process for preparing Nixing Jun pottery |
| CN108002808A (en) * | 2017-12-05 | 2018-05-08 | 西安理工大学 | A kind of dry and wet sticking clay for mud of making pottery and preparation method thereof |
| CN112679196A (en) * | 2021-01-30 | 2021-04-20 | 广东顺祥陶瓷有限公司 | Bonding process of handle and device body of medium-high temperature ceramic device |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103387377A (en) * | 2013-07-17 | 2013-11-13 | 彭红 | Splicing mud for splice of very large ceramic honeycomb carrier |
| CN104446347A (en) * | 2014-11-10 | 2015-03-25 | 钦州学院 | Method for reducing deformation rate of finished Nixing pottery product |
-
2015
- 2015-07-14 CN CN201510413223.5A patent/CN104944913B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103387377A (en) * | 2013-07-17 | 2013-11-13 | 彭红 | Splicing mud for splice of very large ceramic honeycomb carrier |
| CN104446347A (en) * | 2014-11-10 | 2015-03-25 | 钦州学院 | Method for reducing deformation rate of finished Nixing pottery product |
Non-Patent Citations (4)
| Title |
|---|
| 李家驹: "《陶瓷工艺学（上册）》", 31 January 2001 * |
| 李来胜等: "《陶瓷工业节能减排技术》", 31 May 2008 * |
| 肖汉宁等: "《高性能结构陶瓷及其应用》", 28 February 2006 * |
| 赵国堂等: "《高速铁路高性能混凝土应用管理技术》", 30 June 2009 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105294088A (en) * | 2015-12-09 | 2016-02-03 | 钦州市华夏太极泉坭兴陶艺有限责任公司 | Process for preparing Nixing Jun pottery |
| CN108002808A (en) * | 2017-12-05 | 2018-05-08 | 西安理工大学 | A kind of dry and wet sticking clay for mud of making pottery and preparation method thereof |
| CN112679196A (en) * | 2021-01-30 | 2021-04-20 | 广东顺祥陶瓷有限公司 | Bonding process of handle and device body of medium-high temperature ceramic device |
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| CN104944913B (en) | 2017-01-04 |
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Granted publication date: 20170104 Termination date: 20180714 |