CN104928021B - A kind of jelly fusion pot for being exclusively used in freezing molten demulsification release - Google Patents
A kind of jelly fusion pot for being exclusively used in freezing molten demulsification release Download PDFInfo
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- CN104928021B CN104928021B CN201510370364.3A CN201510370364A CN104928021B CN 104928021 B CN104928021 B CN 104928021B CN 201510370364 A CN201510370364 A CN 201510370364A CN 104928021 B CN104928021 B CN 104928021B
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Abstract
The invention discloses a kind of jelly fusion pots for being exclusively used in freezing molten demulsification release, including being provided with the cavity of inlet port and outlet port, installing transmission device, the temperature control device mounted on cavity wall, the control panel mounted on containment portion and the material containing tank being placed on transmission device loading surface inside bottom in the cavity and through cavities, control panel is connected respectively at transmission device, temperature control device；The cavity by flashboard separate at arrange successively crystallisation chamber, freezing chamber, melting chamber, crystallisation chamber is connected to feed inlet；The thermometric end of the temperature control device is located inside wall, including being placed in the first temperature conditioning unit of crystallisation chamber, being placed in the second temperature conditioning unit of freezing chamber and being placed in the third temperature conditioning unit of melting chamber, the first temperature conditioning unit, the second temperature conditioning unit, third temperature conditioning unit are connected respectively at control panel.The present invention meets the processing request that in new process Camphor Tree Seeds freeze with molten demulsification release, compact-sized, floor space is small.
Description
Technical field
The present invention relates to the production equipment field of biodiesel, in particular to a kind of jellies for being exclusively used in freezing molten demulsification release
Fusion pot.
Background technology
Biodiesel refers to the water plants such as oil crops, Wild oil plant and engineering microalgae grease and animal oil
Fat, food garbage oil etc. can be replaced the reproducibility diesel fuel of petrifaction diesel by feedstock oil made of ester exchange process.It is raw
Object diesel oil is one kind of biomass energy, it is a kind of monoalkyl for long chain fatty acids that the technologies such as biomass economy thermal cracking obtain
Ester.Biodiesel is the mixture of the high complicated organic principle of oxygen content, these mixtures are mainly that number molecular weight is big
Organic matter almost includes the oxygen-bearing organic matter of all kinds, such as：Ether, ester, aldehyde, ketone, phenol, organic acid, alcohol etc..
A kind of Camphor Tree Seeds, which prepare to need to use in the new process of biodiesel, to be frozen fusion pot and carries out freezing molten demulsification to Camphor Tree Seeds
The processing of release still melts machine currently without the jelly for meeting production requirement.
Invention content
The purpose of the present invention is to provide a kind of jelly fusion pots for being exclusively used in freezing molten demulsification release, meet in new process to camphor tree
The seeds of trees freeze the processing request of molten demulsification release, compact-sized, floor space is small.
The present invention is achieved through the following technical solutions：A kind of jelly fusion pot for being exclusively used in freezing molten demulsification release, including setting
There is transmission device in the cavity inside bottom and through cavities of the cavitys of inlet port and outlet port, installation, be mounted on cavity side
The temperature control device of wall, the control panel mounted on containment portion and the material containing tank that is placed on transmission device loading surface, control panel
It is connected respectively at transmission device, temperature control device；The cavity by flashboard separate at arrange successively crystallisation chamber, freezing chamber, melting
Room, crystallisation chamber are connected to feed inlet；The thermometric end of the temperature control device is located inside wall, including is placed in the first temperature of crystallisation chamber
Control unit is placed in the second temperature conditioning unit of freezing chamber and is placed in the third temperature conditioning unit of melting chamber, the first temperature conditioning unit, the second temperature
Control unit, third temperature conditioning unit is connected respectively at control panel.
A kind of Camphor Tree Seeds, which prepare to need to use in the new process of biodiesel, to be frozen fusion pot and carries out freezing molten demulsification to Camphor Tree Seeds
Release, the optimised process of specific process are that jelly fusion pot is added in the liquid phase for process preceding working procedure, be first cooled to 0 DEG C into
Row freezing and crystallizing, is further cooled to the freezing of -15 DEG C of progress 1.5h after crystallization completely, then is warming up to 40 DEG C and carries out the molten of 1.5h
Solution.The inner cavity for freezing fusion pot is separated into crystallisation chamber in order to meet the actual demand of production, by flashboard, freezing chamber, is melted by the present invention
Room is solved, liquid phase is fitted into from feed inlet in material containing tank, is placed in drive of the material containing tank on transmission device its loading surface in transmission device
It is lower that liquid phase is loaded into crystallisation chamber, freezing chamber, melting chamber successively, and it is gradually completing process under the process conditions of setting.This
Invention meets the processing request that in new process Camphor Tree Seeds freeze with molten demulsification release, compact-sized, floor space is small.
Further, the transmission device is separated by flashboard into the crystallized region positioned at crystallisation chamber, the freezing positioned at freezing chamber
Section, positioned at the melting section of melting chamber, crystallized region, melts intersegmental connection breaking at freezing section.
Further, first temperature conditioning unit includes the first heat-exchange tube of the first thermometer and contact low-temperature receiver；It is described
Second temperature conditioning unit includes the second heat-exchange tube of second temperature meter and contact low-temperature receiver；The third temperature conditioning unit includes third temperature
The third heat-exchange tube of degree meter and contact heat source.
Further, circulate cold medium respectively in first heat-exchange tube, the second heat-exchange tube, in third heat-exchange tube
Circulate thermal medium.
Further, the cold medium is freezing liquid or refrigeration gas, the cold medium preferably to circulate in the first heat-exchange tube
For ice water or brine ice, the cold medium preferably to circulate in the second heat-exchange tube is liquefied ammonia or dry ice or liquid nitrogen；The thermal medium
For high-temperature liquid or High Temperature Gas, the thermal medium preferably to circulate in third heat-exchange tube is 45-60 DEG C of hot water.
The refrigeration effect of the ice water is 0 DEG C；The refrigeration effect of the brine ice is at -5 DEG C or so；The refrigeration of the liquefied ammonia
Effect is at -18 DEG C or so；The refrigeration effect of the dry ice is at -78 DEG C or so；The refrigeration effect of the liquid nitrogen is at -200 DEG C or so；
The heating effect of the 45-60 DEG C of hot water is slightly below water temperature.According to processing request, the first heat-exchange tube is needed the temperature of crystallisation chamber
Degree control is at 0 DEG C or so, therefore the preferably cold medium of ice water or brine ice as circulation in the first heat-exchange tube, it is contemplated that heat
Damage, brine ice become optimal selection；Second heat-exchange tube needs to control the temperature of freezing chamber at -15 DEG C or so, therefore preferably
The cold medium of liquefied ammonia or dry ice or liquid nitrogen as circulation in the second heat-exchange tube, if considering from heat waste and the complexity of control
Then liquefied ammonia is optimal selection, and dry ice or liquid nitrogen are optimal selections if considering from environmental protection；The third heat-exchange tube needs
The temperature of melting chamber is controlled at 40 DEG C or so, therefore 45-60 DEG C of hot water can be easily controlled melting chamber as thermal medium
Temperature keep 40 DEG C or so.
Further, the flashboard include the first flashboard between feed inlet and crystallized region, be located at crystallized region with it is cold
Freeze the second flashboard between section, the third flashboard between freezing section and melting section and between melting section and discharge port
4th flashboard.
When the flashboard is opened, crystallized region, freezing section, melting are intersegmental every connection, and material containing tank may span across interval, are filled in transmission
It is steady successively on the loading surface set to move ahead；When flashboard is closed, flashboard is risen from interval and the inner wall of embedded cavity so that crystallization
Room or the closing isolation of freezing chamber or melting chamber, to realize that the indoor temperature of each chamber controls.First flashboard and the second flashboard
When simultaneously closing off, crystallisation chamber closing；When second flashboard is simultaneously closed off with third flashboard, freezing chamber closing；Third flashboard and the 4th
When flashboard simultaneously closes off, melting chamber closing；First flashboard, the second flashboard, third flashboard, the 4th flashboard individually control.
All flashboards are closed under working condition：
The first step：The first flashboard is opened, liquid phase is introduced into the material containing tank of crystallized region, closes the first flashboard, closing
Crystallisation chamber, liquid phase freezing and crystallizing 0.5-1h under 0 DEG C of process conditions；
Second step：The second flashboard is opened, the material containing tank equipped with crystalline phase is entered under transmission device effect by crystallized region cold
Freeze section, close the second flashboard, close freezing chamber, crystalline phase freezes 1.5h under -15 DEG C of process conditions；
Third walks：Third flashboard is opened, the material containing tank equipped with solid phase enters melting under transmission device effect by freezing section
Section closes third flashboard, closes melting chamber, and solid phase melts 1.5h under 40 DEG C of process conditions；
4th step：The 4th flashboard is opened, is exported from discharge port by the oil phase in material containing tank, waits being further processed, close the
Four flashboards.
Further, the gate panel surface coats insulating layer.
Further, the cavity inner wall or outer wall coat insulating layer.
The insulating layer is to reinforce heat insulation effect.
Further, the connection of the temperature control device and cavity uses welding by both sides.
Further, inspection window is additionally provided on the side wall of the cavity, the connection of inspection window and cavity uses welding by both sides.
The welding by both sides primarily to inner space closing, further strengthen heat insulation effect.
Compared with prior art, the present invention haing the following advantages and advantageous effect：
（1）The present invention meets the processing request that in new process Camphor Tree Seeds freeze with molten demulsification release.
（2）Structure of the invention is compact, floor space is small.
Description of the drawings
Fig. 1 is schematic structural view of the invention.
Fig. 2 is the sectional view of the present invention.
Wherein：1-cavity, 11-crystallisation chambers, 12-freezing chambers, 13-melting chambers, 101-feed inlets, 102-dischargings
Mouthful, the 103-the first flashboard, the 104-the second flashboard, 105-third flashboards, the 106-the four flashboard, 21-crystallized regions, 22-is cold
Freeze section, 23-melt section, the 31-the first temperature conditioning unit, the 32-the second temperature conditioning unit, 33-third temperature conditioning units, 4-control planes
Plate, 5-material containing tanks.
Specific implementation mode
The present invention is described in further detail with reference to embodiment, embodiments of the present invention are not limited thereto.
Embodiment 1：
A kind of jelly fusion pot being exclusively used in freezing molten demulsification release of the present embodiment, as shown in Figure 1 and Figure 2, including be provided with into
The cavity 1 of material mouth 101 and discharge port 102, is mounted on chamber at the transmission device inside bottom in cavity 1 and through cavities 1
The temperature control device of 1 side wall of body, the control panel 4 outside cavity 1 and the material containing tank 5 being placed on transmission device loading surface,
Control panel 4 is connected respectively at transmission device, temperature control device；The cavity 1 by flashboard separate at the crystallisation chamber 11 arranged successively,
Freezing chamber 12, melting chamber 13, crystallisation chamber 11 are connected to feed inlet 101；The thermometric end of the temperature control device is located inside wall, packet
It includes and is placed in the first temperature conditioning unit 31 of crystallisation chamber 11, be placed in the second temperature conditioning unit 32 of freezing chamber 12 and be placed in the of melting chamber 13
Three temperature conditioning units 33, the first temperature conditioning unit 31, the second temperature conditioning unit 32, third temperature conditioning unit 33 are connected respectively at control panel 4.
Embodiment 2：
The present embodiment advanced optimizes on the basis of the above embodiments, as shown in Fig. 2, further, the transmission
Device is separated by flashboard at the crystallized region 21 positioned at crystallisation chamber 11, the freezing section 22 positioned at freezing chamber 12, positioned at melting chamber 13
Section 23 is melted, crystallized region 21, melts 23 connection breakings of section at freezing section 22.The other parts of the present embodiment and above-described embodiment phase
Together, so it will not be repeated.
Embodiment 3：
The present embodiment advanced optimizes on the basis of the above embodiments, further, first temperature conditioning unit 31
The first heat-exchange tube including the first thermometer and contact low-temperature receiver；Second temperature conditioning unit 32 includes second temperature meter and contact
Second heat-exchange tube of low-temperature receiver；The third temperature conditioning unit 33 includes third thermometer and contacts the third heat-exchange tube of heat source.
The other parts of the present embodiment are same as the previously described embodiments, and so it will not be repeated.
Embodiment 4：
The present embodiment advanced optimizes on the basis of the above embodiments, further, first heat-exchange tube,
Circulate cold medium respectively in two heat-exchange tubes, and circulate thermal medium in third heat-exchange tube.The other parts of the present embodiment with it is above-mentioned
Embodiment is identical, and so it will not be repeated.
Embodiment 5：
The present embodiment advanced optimizes on the basis of the above embodiments, and further, the cold medium is freezing liquid
Or refrigeration gas, the cold medium preferably to circulate in the first heat-exchange tube are ice water or brine ice, are preferably circulated in the second heat exchange
Cold medium in pipe is liquefied ammonia or dry ice or liquid nitrogen；The thermal medium is high-temperature liquid or High Temperature Gas, preferably circulates and is handed in third heat
The hot water that the thermal medium changed in pipe is 45-60 DEG C.The other parts of the present embodiment are same as the previously described embodiments, and so it will not be repeated.
Embodiment 6：
The present embodiment advanced optimizes on the basis of the above embodiments, further, the flashboard include be located at into
The first flashboard 103 between material mouth 101 and crystallized region 21, the second flashboard 104 between crystallized region 21 and freezing section 22, position
In freezing section 22 and melt the third flashboard 105 between section 23 and the 4th flashboard between melting section 23 and discharge port 102
106.The other parts of the present embodiment are same as the previously described embodiments, and so it will not be repeated.
Embodiment 7：
The present embodiment advanced optimizes on the basis of the above embodiments, further, gate panel surface coating every
Warm layer.The other parts of the present embodiment are same as the previously described embodiments, and so it will not be repeated.
Embodiment 8：
The present embodiment advanced optimizes on the basis of the above embodiments, further, 1 inner wall of the cavity or outer wall
Coat insulating layer.The other parts of the present embodiment are same as the previously described embodiments, and so it will not be repeated.
Embodiment 9：
The present embodiment advanced optimizes on the basis of the above embodiments, further, the temperature control device and cavity 1
Connection use welding by both sides.The other parts of the present embodiment are same as the previously described embodiments, and so it will not be repeated.
Embodiment 10：
The present embodiment advanced optimizes on the basis of the above embodiments, further, on the side wall of the cavity 1 also
It is provided with inspection window, the connection of inspection window and cavity 1 uses welding by both sides.The other parts of the present embodiment and above-described embodiment phase
Together, so it will not be repeated.
The above is only presently preferred embodiments of the present invention, not does limitation in any form to the present invention, it is every according to
According to the technical spirit of the present invention to any simple modification, equivalent variations made by above example, the protection of the present invention is each fallen within
Within the scope of.
Claims (7)
1. a kind of jelly fusion pot for being exclusively used in freezing molten demulsification release, it is characterised in that：Including being provided with feed inlet（101）And discharging
Mouthful（102）Cavity（1）, be mounted on cavity（1）Interior bottom and through cavities（1）The transmission device of inside is mounted on cavity（1）
The temperature control device of side wall is mounted on cavity（1）External control panel（4）With the material containing tank being placed on transmission device loading surface
（5）, control panel（4）It is connect respectively with transmission device, temperature control device；The cavity（1）By flashboard partition at successively arranging
Crystallisation chamber（11）, freezing chamber（12）, melting chamber（13）, crystallisation chamber（11）With feed inlet（101）Connection；The survey of the temperature control device
Wen Duan is located inside wall, including is placed in crystallisation chamber（11）The first temperature conditioning unit（31）, be placed in freezing chamber（12）Second temperature
Control unit（32）Be placed in melting chamber（13）Third temperature conditioning unit（33）, the first temperature conditioning unit（31）, the second temperature conditioning unit
（32）, third temperature conditioning unit（33）Respectively with control panel（4）Connection；
The transmission device is separated by flashboard at positioned at crystallisation chamber（11）Crystallized region（21）, be located at freezing chamber（12）Freezing section
（22）, be located at melting chamber（13）Melting section（23）, crystallized region（21）, freezing section（22）, melt section（23）Between connection breaking；
First temperature conditioning unit（31）The first heat-exchange tube including the first thermometer and contact low-temperature receiver；The second temperature control list
Member（32）The second heat-exchange tube including second temperature meter and contact low-temperature receiver；The third temperature conditioning unit（33）Including third temperature
The third heat-exchange tube of meter and contact heat source；
The flashboard includes being located at feed inlet（101）With crystallized region（21）Between the first flashboard（103）, be located at crystallized region（21）
With freezing section（22）Between the second flashboard（104）, be located at freezing section（22）With melting section（23）Between third flashboard（105）
With positioned at melt section（23）With discharge port（102）Between the 4th flashboard（106）.
2. a kind of jelly fusion pot for being exclusively used in freezing molten demulsification release according to claim 1, it is characterised in that：Described first
Circulate cold medium respectively in heat-exchange tube, the second heat-exchange tube, and circulate thermal medium in third heat-exchange tube.
3. a kind of jelly fusion pot for being exclusively used in freezing molten demulsification release according to claim 2, it is characterised in that：Circulation is the
Cold medium in one heat-exchange tube is ice water or brine ice, the cold medium to circulate in the second heat-exchange tube be liquefied ammonia or dry ice or
Liquid nitrogen；The hot water that the thermal medium to circulate in third heat-exchange tube is 45-60 DEG C.
4. a kind of jelly fusion pot for being exclusively used in freezing molten demulsification release according to claim 1, it is characterised in that：The flashboard
Surface coats insulating layer.
5. a kind of jelly fusion pot for being exclusively used in freezing molten demulsification release, feature exist according to any one of claims 1-4
In：The cavity（1）Inner wall or outer wall coat insulating layer.
6. a kind of jelly fusion pot for being exclusively used in freezing molten demulsification release according to claim 5, it is characterised in that：The temperature control
Device and cavity（1）Connection use welding by both sides.
7. a kind of jelly fusion pot for being exclusively used in freezing molten demulsification release according to claim 5, it is characterised in that：The cavity
（1）Side wall on be additionally provided with inspection window, inspection window and cavity（1）Connection use welding by both sides.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510370364.3A CN104928021B (en) | 2015-06-30 | 2015-06-30 | A kind of jelly fusion pot for being exclusively used in freezing molten demulsification release |
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| CN201510370364.3A CN104928021B (en) | 2015-06-30 | 2015-06-30 | A kind of jelly fusion pot for being exclusively used in freezing molten demulsification release |
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| CN104928021A CN104928021A (en) | 2015-09-23 |
| CN104928021B true CN104928021B (en) | 2018-10-09 |
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| CN108251296A (en) * | 2016-12-29 | 2018-07-06 | 国家开发投资公司 | A kind of cell multigelation rupture of membranes extraction element |
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| CN104232296A (en) * | 2014-09-28 | 2014-12-24 | 南昌大学 | Method for extracting camphor tree seed oil through water emulsion extraction and freeze-thaw demulsification release method |
| CN104342283A (en) * | 2013-07-26 | 2015-02-11 | 北京中天金谷科技股份有限公司 | Camellia oil dewaxing degreasing process |
| CN204848806U (en) * | 2015-06-30 | 2015-12-09 | 成都易胜科生物科技有限公司 | Be exclusively used in and freeze fusion pot that freezes that melts demulsification release |
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2015
- 2015-06-30 CN CN201510370364.3A patent/CN104928021B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202124608U (en) * | 2011-05-22 | 2012-01-25 | 湖南大三湘油茶科技有限公司 | Cooling device of grease winterization system |
| CN103540401A (en) * | 2012-07-13 | 2014-01-29 | 李宁 | Fool type automatic control system for edible oil winterization procedure |
| CN103252450A (en) * | 2013-05-11 | 2013-08-21 | 东裕(桐柏)精密金属有限公司 | Framework dewaxing and wax-melting purifying device and framework dewaxing and wax-melting purifying method |
| CN104342283A (en) * | 2013-07-26 | 2015-02-11 | 北京中天金谷科技股份有限公司 | Camellia oil dewaxing degreasing process |
| CN104232296A (en) * | 2014-09-28 | 2014-12-24 | 南昌大学 | Method for extracting camphor tree seed oil through water emulsion extraction and freeze-thaw demulsification release method |
| CN204848806U (en) * | 2015-06-30 | 2015-12-09 | 成都易胜科生物科技有限公司 | Be exclusively used in and freeze fusion pot that freezes that melts demulsification release |
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Effective date of registration: 20191211 Address after: Ganquan road Shushan District of Hefei City, Anhui Province, 230000 West hillock road to the South Wild Garden commercial office building room B-1512 Patentee after: ANHUI YINGLONG INDUSTRIAL DESIGN Co.,Ltd. Address before: 610000, No. 1, No. 304, building 1, 1, No. 1, Tianfu Road, Chengdu hi tech Zone, Sichuan Patentee before: CHENGDU YISHENGKE BIOTECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20230904 Address after: 257000 Building 3, No. 1, Nanzhong Road, Hekou District, Dongying City, Shandong Province Patentee after: Dongying Xutong Can-making Co.,Ltd. Address before: 230000 B-1512, west of Ganquan Road, Shushan District, Hefei, Anhui. Patentee before: ANHUI YINGLONG INDUSTRIAL DESIGN Co.,Ltd. |