CN104928021A - Freezing-melting tank special for freezing-melting demulsification release - Google Patents
Freezing-melting tank special for freezing-melting demulsification release Download PDFInfo
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- CN104928021A CN104928021A CN201510370364.3A CN201510370364A CN104928021A CN 104928021 A CN104928021 A CN 104928021A CN 201510370364 A CN201510370364 A CN 201510370364A CN 104928021 A CN104928021 A CN 104928021A
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- freeze
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- release
- melting
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Abstract
The invention discloses a freezing-melting tank special for freezing-melting demulsification release. The freezing-melting tank comprises a cavity, a conveying device, a temperature control device, a control panel and a material carrying tank, the cavity is provided with a feeding port and a discharging port, the conveying device is mounted at the bottom in the cavity and penetrates the inside of the cavity, the temperature control device is mounted on the side wall of the cavity, the control panel is mounted outside the cavity, the material carrying tank is disposed on an article carrying face of the conveying device, the control panel is connected with the conveying device and the temperature control device respectively, the cavity is partitioned into a crystallizing chamber, a freezing chamber and a melting chamber which are arranged sequentially by flashboards, the crystallizing chamber is communicated with the feeding port, a temperature measuring end of the temperature control device is positioned inside a wall, the temperature control device comprises a first temperature control unit disposed in the crystallizing chamber, a second temperature control unit disposed in the freezing chamber, and a third temperature control unit disposed in the melting chamber, and the first temperature control unit, the second temperature control unit and the third temperature control unit are connected with the control panel respectively. The freezing-melting tank meets processing requirements on freezing-melting demulsification release of camphor tree seeds and is compact in structure and small in occupied area.
Description
Technical field
The present invention relates to the production unit field of biofuel, specifically refer to a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot.
Background technology
Biofuel refers to the waterplant greases such as oil crops, Wild oil plant and engineering microalgae and animal grease, food garbage wet goods to be the reproducibility diesel oil fuel of the replaced petrifaction diesel that stock oil is made by ester exchange process.Biofuel is the one of biomass energy, and it is the mono alkyl ester of a kind of longer chain fatty acid that the technology such as biomass economy thermo-cracking obtain.Biofuel is the mixture of the high complicated organic composition of oxygen level, and these mixtures organism that mainly number molecular weight is large, almost comprises the oxygen-bearing organic matter of all kinds, as: ether, ester, aldehyde, ketone, phenol, organic acid, alcohol etc.
Camphor Tree Seeds prepare in the novel process of biofuel need to use freeze fusion pot to Camphor Tree Seeds freeze molten deemulsification release a processing, but what do not meet production requirement at present freezes molten machine.
Summary of the invention
The object of the present invention is to provide a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot, meet in novel process to Camphor Tree Seeds freeze molten deemulsification release processing request, compact construction, floor space are little.
The present invention is achieved through the following technical solutions: a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot, comprise be provided with opening for feed and discharge port cavity, be arranged on cavity inner bottom part and the transport unit of through cavities inside, the temperature control unit being arranged on cavity wall, the control panel being arranged on containment portion and the material containing tank be placed on transport unit loading surface, control panel respectively at transport unit, temperature control unit connect; Described cavity is cut off into crystallisation chamber, refrigeration chamber, the melting chamber of arranging successively by flashboard, crystallisation chamber is communicated with opening for feed; The thermometric end of described temperature control unit is positioned at body of wall inside, comprise the first temperature conditioning unit being placed in crystallisation chamber, the second temperature conditioning unit being placed in refrigeration chamber and be placed in the 3rd temperature conditioning unit of melting chamber, the first temperature conditioning unit, the second temperature conditioning unit, the 3rd temperature conditioning unit connect respectively at control panel.
A kind of Camphor Tree Seeds prepare in the novel process of biofuel need to use freeze fusion pot to Camphor Tree Seeds freeze molten deemulsification release, the optimised process of its concrete course of processing the liquid phase that former process is processed is added to freeze fusion pot, first be cooled to 0 DEG C and carry out freezing and crystallizing, the completely laggard step of crystallization is cooled to-15 DEG C and carries out the freezing of 1.5h, then is warming up to the melting that 40 DEG C are carried out 1.5h.The present invention is in order to meet the actual demand of production, by flashboard, the inner chamber freezing fusion pot is cut off into crystallisation chamber, refrigeration chamber, melting chamber, liquid phase loads material containing tank from opening for feed, liquid phase is loaded into crystallisation chamber, refrigeration chamber, melting chamber successively by the material containing tank be placed on its loading surface of transport unit under the drive of transport unit, and progressively completes the course of processing under the processing condition of setting.The present invention meets the processing request in novel process, Camphor Tree Seeds being frozen to the release of molten deemulsification, and compact construction, floor space are little.
Further, described transport unit by flashboard cut off into be positioned at crystallisation chamber crystallized region, be positioned at freezing section of refrigeration chamber, be positioned at the melting section of melting chamber, crystallized region, freezing section, melt intersegmental connection breaking.
Further, described first temperature conditioning unit comprises the first thermometer and the first heat exchanger tube contacting low-temperature receiver; Described second temperature conditioning unit comprises the second thermometer and the second heat exchanger tube contacting low-temperature receiver; Described 3rd temperature conditioning unit comprises the 3rd thermometer and the 3rd heat exchanger tube contacting thermal source.
Further, circulate in described first heat exchanger tube, the second heat exchanger tube cold medium respectively, and circulate in the 3rd heat exchanger tube thermal medium.
Further, described cold medium is refrigerating fulid or refrigeration gas, and preferably the cold medium of circulation in the first heat exchanger tube is frozen water or icy salt solution, and preferably the cold medium of circulation in the second heat exchanger tube is liquefied ammonia or dry ice or liquid nitrogen; Described thermal medium is high-temperature liquid or High Temperature Gas, and preferably the thermal medium of circulation in the 3rd heat exchanger tube is the hot water of 45-60 DEG C.
The refrigeration of described frozen water is 0 DEG C; The refrigeration of described icy salt solution is at about-5 DEG C; The refrigeration of described liquefied ammonia is at about-18 DEG C; The refrigeration of described dry ice is at about-78 DEG C; The refrigeration of described liquid nitrogen is at about-200 DEG C; The heating effect of described 45-60 DEG C hot water is a little less than water temperature.According to processing request, the first heat exchanger tube needs the temperature of crystallisation chamber to control at about 0 DEG C, and therefore preferably frozen water or icy salt solution are as the cold medium of circulation in the first heat exchanger tube, and consider heat waste, icy salt solution becomes optimal selection; Second heat exchanger tube needs the temperature of refrigeration chamber to control at about-15 DEG C, therefore preferably liquefied ammonia or dry ice or liquid nitrogen as the cold medium of circulation in the second heat exchanger tube, if consider from the complexity of heat waste and control, liquefied ammonia is optimal selection, if consider from environment protection, dry ice or liquid nitrogen are optimal selections; Described 3rd heat exchanger tube needs the temperature of melting chamber to control at about 40 DEG C, and the temperature that therefore hot water of 45-60 DEG C can be easy to control melting chamber as thermal medium keeps about 40 DEG C.
Further, described flashboard comprise the first flashboard between opening for feed and crystallized region, the second flashboard between crystallized region and freezing section, at freezing section and the 3rd flashboard that melts between section with melting the 4th flashboard between section and discharge port.
When described flashboard is opened, crystallized region, freezing section, the connection of melting spacer segment, material containing tank can cross over interval, and the loading surface of transport unit steadily moves ahead successively; When flashboard cuts out, flashboard rises and embeds the inwall of cavity from interval, makes crystallisation chamber or refrigeration chamber or melting chamber close isolation, controls with the temperature realized in each chamber.When described first flashboard and the second flashboard are closed simultaneously, crystallisation chamber is closed; When second flashboard and the 3rd flashboard are closed simultaneously, refrigeration chamber is closed; When 3rd flashboard and the 4th flashboard are closed simultaneously, melting chamber is closed; First flashboard, the second flashboard, the 3rd flashboard, the 4th flashboard control all separately.
Under working order, all flashboards cut out:
The first step: open the first flashboard, introduces the material containing tank being arranged in crystallized region, closes the first flashboard by liquid phase, close crystallisation chamber, liquid phase is freezing and crystallizing 0.5-1h under the processing condition of 0 DEG C;
Second step: open the second flashboard, the material containing tank that crystallization phases is housed enters freezing section by crystallized region under transport unit effect, closes the second flashboard, and close refrigeration chamber, crystallization phases is freezing 1.5h under the processing condition of-15 DEG C;
3rd step: open the 3rd flashboard, the material containing tank that solid phase is housed enters melting section by freezing section under transport unit effect, closes the 3rd flashboard, and close melting chamber, solid phase melts 1.5h under the processing condition of 40 DEG C;
4th step: open the 4th flashboard, derives the oil phase material containing tank from discharge port, treats further process, closes the 4th flashboard.
Further, described gate panel surface coating heat-insulating layer.
Further, described cavity inner wall or outer wall coating heat-insulating layer.
Described heat-insulating layer strengthens heat insulation effect.
Further, the connection of described temperature control unit and cavity adopts welding by both sides.
Further, the sidewall of described cavity is also provided with peep window, the connection of peep window and cavity adopts welding by both sides.
Described welding by both sides closing mainly in order to internal space, strengthens heat insulation effect further.
The present invention compared with prior art, has the following advantages and beneficial effect:
(1) the present invention meets the processing request in novel process, Camphor Tree Seeds being frozen to the release of molten deemulsification.
(2) compact construction of the present invention, floor space are little.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
Fig. 2 is sectional view of the present invention.
Wherein: 1-cavity, 11-crystallisation chamber, 12-refrigeration chamber, 13-melting chamber, 101-opening for feed, 102-discharge port, 103-the first flashboard, the 104-the second flashboard, the 105-the three flashboard, 106-the four flashboard, 21-crystallized region, 22-freezing section, 23-melt section, the 31-the first temperature conditioning unit, the 32-the second temperature conditioning unit, 33-the three temperature conditioning unit, 4-control panel, 5-material containing tank.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
Embodiment 1:
The present embodiment a kind of be exclusively used in freeze the release of molten deemulsification freeze fusion pot, as shown in Figure 1 and Figure 2, comprise be provided with opening for feed 101 and discharge port 102 cavity 1, be arranged on cavity 1 inner bottom part and the transport unit of through cavities 1 inside, the temperature control unit being arranged on cavity 1 sidewall, the control panel 4 being arranged on cavity 1 outside and the material containing tank 5 be placed on transport unit loading surface, control panel 4 respectively at transport unit, temperature control unit connect; Described cavity 1 is cut off into crystallisation chamber 11, refrigeration chamber 12, the melting chamber 13 of arranging successively by flashboard, crystallisation chamber 11 is communicated with opening for feed 101; The thermometric end of described temperature control unit is positioned at body of wall inside, comprise the first temperature conditioning unit 31 being placed in crystallisation chamber 11, the second temperature conditioning unit 32 being placed in refrigeration chamber 12 and be placed in the 3rd temperature conditioning unit 33, first temperature conditioning unit 31, second temperature conditioning unit 32 of melting chamber 13, the 3rd temperature conditioning unit 33 connects respectively at control panel 4.
Embodiment 2:
The present embodiment does further optimization on the basis of above-described embodiment, as shown in Figure 2, further, described transport unit by flashboard cut off into be positioned at crystallisation chamber 11 crystallized region 21, be positioned at freezing section 22 of refrigeration chamber 12, be positioned at the melting section 23 of melting chamber 13, crystallized region 21, freezing section 22, melt section 23 connection breakings.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
Embodiment 3:
The present embodiment does further optimization on the basis of above-described embodiment, and further, described first temperature conditioning unit 31 comprises the first thermometer and the first heat exchanger tube contacting low-temperature receiver; Described second temperature conditioning unit 32 comprises the second thermometer and the second heat exchanger tube contacting low-temperature receiver; Described 3rd temperature conditioning unit 33 comprises the 3rd thermometer and the 3rd heat exchanger tube contacting thermal source.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
Embodiment 4:
The present embodiment does further optimization on the basis of above-described embodiment, and further, circulate in described first heat exchanger tube, the second heat exchanger tube cold medium respectively, and circulate in the 3rd heat exchanger tube thermal medium.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
Embodiment 5:
The present embodiment does further optimization on the basis of above-described embodiment, further, described cold medium is refrigerating fulid or refrigeration gas, and preferably the cold medium of circulation in the first heat exchanger tube is frozen water or icy salt solution, and preferably the cold medium of circulation in the second heat exchanger tube is liquefied ammonia or dry ice or liquid nitrogen; Described thermal medium is high-temperature liquid or High Temperature Gas, and preferably the thermal medium of circulation in the 3rd heat exchanger tube is the hot water of 45-60 DEG C.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
Embodiment 6:
The present embodiment does further optimization on the basis of above-described embodiment, further, described flashboard comprise the first flashboard 103 between opening for feed 101 and crystallized region 21, the second flashboard 104 between crystallized region 21 and freezing section 22, at freezing section 22 and the 3rd flashboard 105 that melts between section 23 with melting the 4th flashboard 106 between section 23 and discharge port 102.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
Embodiment 7:
The present embodiment does further optimization on the basis of above-described embodiment, further, and described gate panel surface coating heat-insulating layer.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
Embodiment 8:
The present embodiment does further optimization on the basis of above-described embodiment, further, and described cavity 1 inwall or outer wall coating heat-insulating layer.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
Embodiment 9:
The present embodiment does further optimization on the basis of above-described embodiment, and further, the connection of described temperature control unit and cavity 1 adopts welding by both sides.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
Embodiment 10:
The present embodiment does further optimization on the basis of above-described embodiment, and further, the sidewall of described cavity 1 is also provided with peep window, the connection of peep window and cavity 1 adopts welding by both sides.Other parts of the present embodiment are same as the previously described embodiments, therefore repeat no more.
The above is only preferred embodiment of the present invention, and not do any pro forma restriction to the present invention, every any simple modification, equivalent variations done above embodiment according to technical spirit of the present invention, all falls within protection scope of the present invention.
Claims (10)
1. one kind be exclusively used in freeze molten deemulsification release freeze fusion pot, it is characterized in that: comprise be provided with opening for feed (101) and discharge port (102) cavity (1), be arranged on cavity (1) inner bottom part and the inner transport unit of through cavities (1), the temperature control unit being arranged on cavity (1) sidewall, the material containing tank (5) that is arranged on the outside control panel (4) of cavity (1) and is placed on transport unit loading surface, control panel (4) is respectively at transport unit, temperature control unit connection; Described cavity (1) is cut off into crystallisation chamber (11), refrigeration chamber (12), the melting chamber (13) of arranging successively by flashboard, crystallisation chamber (11) is communicated with opening for feed (101); The thermometric end of described temperature control unit is positioned at body of wall inside, comprise the first temperature conditioning unit (31) being placed in crystallisation chamber (11), the second temperature conditioning unit (32) being placed in refrigeration chamber (12) and be placed in the 3rd temperature conditioning unit (33) of melting chamber (13), the first temperature conditioning unit (31), the second temperature conditioning unit (32), the 3rd temperature conditioning unit (33) connect respectively at control panel (4).
2. according to claim 1 a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot, it is characterized in that: described transport unit by flashboard cut off into be positioned at crystallisation chamber (11) crystallized region (21), be positioned at freezing section (22) of refrigeration chamber (12), be positioned at the melting section (23) of melting chamber (13), crystallized region (21), freezing section (22), melt connection breaking between section (23).
3. according to claim 2 a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot, it is characterized in that: described first temperature conditioning unit (31) comprises the first thermometer and the first heat exchanger tube contacting low-temperature receiver; Described second temperature conditioning unit (32) comprises the second thermometer and the second heat exchanger tube contacting low-temperature receiver; Described 3rd temperature conditioning unit (33) comprises the 3rd thermometer and the 3rd heat exchanger tube contacting thermal source.
4. according to claim 3 a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot, it is characterized in that: circulate in described first heat exchanger tube, the second heat exchanger tube cold medium respectively, circulate in the 3rd heat exchanger tube thermal medium.
5. according to claim 4 a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot, it is characterized in that: described cold medium is refrigerating fulid or refrigeration gas, the cold medium of preferred circulation in the first heat exchanger tube is frozen water or icy salt solution, and preferably the cold medium of circulation in the second heat exchanger tube is liquefied ammonia or dry ice or liquid nitrogen; Described thermal medium is high-temperature liquid or High Temperature Gas, and preferably the thermal medium of circulation in the 3rd heat exchanger tube is the hot water of 45-60 DEG C.
6. according to claim 2 a kind of be exclusively used in freeze the release of molten deemulsification freeze fusion pot, it is characterized in that: described flashboard comprises and is positioned at the first flashboard (103) between opening for feed (101) and crystallized region (21), is positioned at the second flashboard (104) between crystallized region (21) and freezing section (22), is positioned at the 3rd flashboard (105) between freezing section (22) and melting section (23) and is positioned at the 4th flashboard (106) melted between section (23) and discharge port (102).
7. according to claim 6 a kind of be exclusively used in freeze the release of molten deemulsification freeze fusion pot, it is characterized in that: described gate panel surface coating heat-insulating layer.
8. a kind of according to claim 1-7 any one be exclusively used in freeze the release of molten deemulsification freeze fusion pot, it is characterized in that: described cavity (1) inwall or outer wall coating heat-insulating layer.
9. according to claim 8 a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot, it is characterized in that: the connection of described temperature control unit and cavity (1) adopts welding by both sides.
10. according to claim 8 a kind of be exclusively used in freeze molten deemulsification release freeze fusion pot, it is characterized in that: the sidewall of described cavity (1) is also provided with peep window, the connection of peep window and cavity (1) adopts welding by both sides.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510370364.3A CN104928021B (en) | 2015-06-30 | 2015-06-30 | A kind of jelly fusion pot for being exclusively used in freezing molten demulsification release |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510370364.3A CN104928021B (en) | 2015-06-30 | 2015-06-30 | A kind of jelly fusion pot for being exclusively used in freezing molten demulsification release |
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| CN104928021A true CN104928021A (en) | 2015-09-23 |
| CN104928021B CN104928021B (en) | 2018-10-09 |
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| CN201510370364.3A Active CN104928021B (en) | 2015-06-30 | 2015-06-30 | A kind of jelly fusion pot for being exclusively used in freezing molten demulsification release |
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Cited By (1)
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| CN108251296A (en) * | 2016-12-29 | 2018-07-06 | 国家开发投资公司 | A kind of cell multigelation rupture of membranes extraction element |
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Effective date of registration: 20230904 Address after: 257000 Building 3, No. 1, Nanzhong Road, Hekou District, Dongying City, Shandong Province Patentee after: Dongying Xutong Can-making Co.,Ltd. Address before: 230000 B-1512, west of Ganquan Road, Shushan District, Hefei, Anhui. Patentee before: ANHUI YINGLONG INDUSTRIAL DESIGN Co.,Ltd. |