CN104926536A - Production method of discoloring anti-counterfeit water-soluble microelement fertilizer - Google Patents
Production method of discoloring anti-counterfeit water-soluble microelement fertilizer Download PDFInfo
- Publication number
- CN104926536A CN104926536A CN201510381407.8A CN201510381407A CN104926536A CN 104926536 A CN104926536 A CN 104926536A CN 201510381407 A CN201510381407 A CN 201510381407A CN 104926536 A CN104926536 A CN 104926536A
- Authority
- CN
- China
- Prior art keywords
- acid
- water
- fertilizer
- counterfeit
- trace element
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003337 fertilizer Substances 0.000 title claims abstract description 18
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 7
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 10
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- 239000011573 trace mineral Substances 0.000 claims description 9
- 235000013619 trace mineral Nutrition 0.000 claims description 9
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 8
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 8
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 8
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- UBLOJEHIINPTTG-UHFFFAOYSA-J disodium;zinc;2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate Chemical compound [Na+].[Na+].[Zn+2].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O UBLOJEHIINPTTG-UHFFFAOYSA-J 0.000 claims description 6
- KJFMBFZCATUALV-UHFFFAOYSA-N phenolphthalein Chemical compound C1=CC(O)=CC=C1C1(C=2C=CC(O)=CC=2)C2=CC=CC=C2C(=O)O1 KJFMBFZCATUALV-UHFFFAOYSA-N 0.000 claims description 6
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims description 5
- 229910000368 zinc sulfate Inorganic materials 0.000 claims description 5
- 229960001763 zinc sulfate Drugs 0.000 claims description 5
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 4
- 239000004327 boric acid Substances 0.000 claims description 4
- 240000007124 Brassica oleracea Species 0.000 claims description 3
- 235000003899 Brassica oleracea var acephala Nutrition 0.000 claims description 3
- 235000011301 Brassica oleracea var capitata Nutrition 0.000 claims description 3
- 235000001169 Brassica oleracea var oleracea Nutrition 0.000 claims description 3
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 claims description 3
- 229910021538 borax Inorganic materials 0.000 claims description 3
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims description 3
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 claims description 3
- 239000004328 sodium tetraborate Substances 0.000 claims description 3
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- 229910000365 copper sulfate Inorganic materials 0.000 claims description 2
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 2
- 239000003607 modifier Substances 0.000 claims description 2
- 235000006408 oxalic acid Nutrition 0.000 claims description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 2
- 235000015320 potassium carbonate Nutrition 0.000 claims description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 2
- 241000282941 Rangifer tarandus Species 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 10
- 238000005562 fading Methods 0.000 abstract description 2
- 239000003002 pH adjusting agent Substances 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 5
- 241000283011 Rangifer Species 0.000 description 3
- 239000000975 dye Substances 0.000 description 3
- 238000004043 dyeing Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000003086 colorant Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000013401 experimental design Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 239000010871 livestock manure Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
The invention relates to a production method of a discoloring anti-counterfeit water-soluble microelement fertilizer. The fertilizer is obtained by mixing microelements, a pH adjuster, a discoloring agent and the like in a closed environment. Under the condition that the natural color of the fertilizer is not influenced, according to the theory that the discoloring agent is discolored by regulating the pH value, the fertilizer dissolves and discolors after being thrown in water, so that the purpose of preventing counterfeits is achieved, and the problem of fading is solved.
Description
Technical field
The present invention relates to a kind of preparation method with the trace element water-soluble fertilizer of color-changing anti-counterfeit effect.
Background technology
In order to make fertilizer have false proof effect, fertilizer is made to have become the Main of Production of manure industry with particular color.Current macroelement Water soluble fertilizer mainly dyes by adding dyestuff, because dyestuff add-on is subject to strict restriction, is difficult to accomplish even dyeing, situation about fading after also having a lot of dyeing, and it is all color that hand one grabs full hand, allows people feel dislike.
Summary of the invention
Technical problem to be solved by this invention is, provides a kind of color-changing anti-counterfeit trace element water-soluble fertilizer production method, utilizes
Soda acid makes the principle of colour-changing agent variable color, drops into variable color after dissolving in water.
In order to solve the problems of the technologies described above, present invention employs following technical scheme:
A kind of color-changing anti-counterfeit trace element water-soluble fertilizer production method, is characterized in that being prepared from according to following steps:
Using as one or several in the zinc sulfate of trace element fertilizer, ethylenediamine tetraacetic acid disodium zinc salt, disodium ethylene diamine tetraacetate ferrous iron, copper sulfate, disodium ethylene diamine tetraacetate copper, manganous sulfate, disodium ethylene diamine tetraacetate manganese, boric acid and borax, mixing in airtight dry environment as one or more in the citric acid of acid-base modifier, oxalic acid, oxysuccinic acid, salt of wormwood, sodium carbonate and as one or more in the phenolphthalein of colour-changing agent, purple cabbage and reindeer moss; The mass ratio of the adjustment agent of described trace element fertilizer, soda acid and colour-changing agent is 0.25 ~ 0.9999:0 ~ 0.1:0.0001 ~ 0.05.
The present invention has following Advantageous Effects: the present invention, when not affecting product true qualities, utilizes soda acid to make the principle of colour-changing agent variable color, drops into variable color after dissolving in water, to reach false proof object, there is not the problem faded.There is not the uneven problem of dyeing in product of the present invention yet.
Embodiment
The present invention is further illustrated below in conjunction with specific examples.
embodiment one
By zinc sulfate, ethylenediamine tetraacetic acid disodium zinc salt, disodium ethylene diamine tetraacetate ferrous iron, boric acid, phenolphthalein according to mass ratio 0.5:0.3:0.1:0.0992:0.0008, mix in closed environment, obtain product of the present invention.
embodiment two
By zinc sulfate, ethylenediamine tetraacetic acid disodium zinc salt, purple cabbage according to mass ratio 0.5:0.4993:0.0007, mix in closed environment, obtain product of the present invention.
embodiment three
By zinc sulfate, ethylenediamine tetraacetic acid disodium zinc salt, manganous sulfate, boric acid, reindeer moss according to mass ratio 0.3:0.4:0.2:0.099:0.001, mix in closed environment, obtain product of the present invention.
embodiment four
By ethylenediamine tetraacetic acid disodium zinc salt, disodium ethylene diamine tetraacetate manganese, borax, citric acid, reindeer moss according to the mass ratio of 0.3:0.4:0.2:0.099:0.001, mix in closed environment, obtain product of the present invention.
Closed environment described in above-described embodiment refers to dry environment, to avoid the material moisture absorption.
Beneficial effect of the present invention is further illustrated below in conjunction with experimental data:
1, experimental water: get use for laboratory tap water.
2, experiment is for examination material
Product of the present invention 1 kilogram, 1500 kilograms, water.
3, experimental design
Setup Experiments divides 2 process, is respectively: 800 kg of water dilute product of the present invention, 1500 kg of water dilute product of the present invention.
4, experiment is implemented
First use eye observation product of the present invention, then grab product of the present invention with hand, then dilute 1 kilogram of product of the present invention by 800 kg of water, then add remaining 700 kg of water in the product of dilution.
5, results and analysis
| Outward appearance | Uniform color, non-variegation |
| Hand is grabbed | There are not the phenomenons such as decolouring |
| Dilute 800 times of colour-change | Within latter 5 minutes of whole dissolving, product becomes pink or other colors from colourless |
| Dilute 1500 times of colour-change | Mix product within latter 5 minutes and become bluish voilet or other colors from pink |
As can be seen from the above results, product color of the present invention is even, and without decolouring phenomenon, variable color exists change along with the difference of extension rate, and mainly along with extension rate varying ph is also along with change, therefore color also exists change.
6, discuss: because the colour developing of this product is relevant with pH, the multiple that may dilute because user is different and color is slightly different, belongs to normal phenomenon, does not affect fertilizer efficiency.
Claims (1)
1. a color-changing anti-counterfeit trace element water-soluble fertilizer production method, is characterized in that being prepared from according to following steps:
Using as one or several in the zinc sulfate of trace element fertilizer, ethylenediamine tetraacetic acid disodium zinc salt, disodium ethylene diamine tetraacetate ferrous iron, copper sulfate, disodium ethylene diamine tetraacetate copper, manganous sulfate, disodium ethylene diamine tetraacetate manganese, boric acid and borax, mixing in airtight dry environment as one or more in the citric acid of acid-base modifier, oxalic acid, oxysuccinic acid, salt of wormwood, sodium carbonate and as one or more in the phenolphthalein of colour-changing agent, purple cabbage and reindeer moss; The mass ratio of the adjustment agent of described trace element fertilizer, soda acid and colour-changing agent is 0.25 ~ 0.9999:0 ~ 0.1:0.0001 ~ 0.05.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510381407.8A CN104926536B (en) | 2015-07-03 | 2015-07-03 | A kind of color-changing anti-counterfeit trace element water-soluble fertilizer production method |
| CN201710652107.8A CN107488061A (en) | 2015-07-03 | 2015-07-03 | A kind of color-changing anti-counterfeit trace element water-soluble fertilizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510381407.8A CN104926536B (en) | 2015-07-03 | 2015-07-03 | A kind of color-changing anti-counterfeit trace element water-soluble fertilizer production method |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710652107.8A Division CN107488061A (en) | 2015-07-03 | 2015-07-03 | A kind of color-changing anti-counterfeit trace element water-soluble fertilizer |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104926536A true CN104926536A (en) | 2015-09-23 |
| CN104926536B CN104926536B (en) | 2018-01-12 |
Family
ID=54113996
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510381407.8A Active CN104926536B (en) | 2015-07-03 | 2015-07-03 | A kind of color-changing anti-counterfeit trace element water-soluble fertilizer production method |
| CN201710652107.8A Withdrawn CN107488061A (en) | 2015-07-03 | 2015-07-03 | A kind of color-changing anti-counterfeit trace element water-soluble fertilizer |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710652107.8A Withdrawn CN107488061A (en) | 2015-07-03 | 2015-07-03 | A kind of color-changing anti-counterfeit trace element water-soluble fertilizer |
Country Status (1)
| Country | Link |
|---|---|
| CN (2) | CN104926536B (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105777389A (en) * | 2016-04-25 | 2016-07-20 | 纪新强 | Water-soluble color-changing fertilizer containing amino acids and trace elements and dilution control method of fertilizer |
| CN105777392A (en) * | 2016-04-25 | 2016-07-20 | 纪新强 | Macroelement-microelement type water-soluble color-changing fertilizer and dilution control method of same |
| CN105801273A (en) * | 2016-04-25 | 2016-07-27 | 纪新强 | Trace element liquid water soluble color change fertilizer and dilution control method thereof |
| CN105884532A (en) * | 2016-04-25 | 2016-08-24 | 纪新强 | Macro and trace elements type liquid water-soluble discoloring fertilizer and dilution control method thereof |
| CN105884531A (en) * | 2016-04-25 | 2016-08-24 | 纪新强 | Trace element water-soluble color-changing fertilizer and dilution control method thereof |
| CN105906429A (en) * | 2016-04-25 | 2016-08-31 | 纪新强 | Liquid water-soluble color-changing fertilizer containing amino acid and trace element and dilution control method of fertilizer |
| CN106380298A (en) * | 2016-08-30 | 2017-02-08 | 安徽辉隆集团五禾生态肥业有限公司 | Water soluble fertilizer with color self-change anti-counterfeiting function |
| CN110105107A (en) * | 2018-03-27 | 2019-08-09 | 湖北格林凯尔农业科技有限公司 | A kind of heartsease water-soluble fertilizer and application |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1690019A (en) * | 2004-04-28 | 2005-11-02 | 黄云祥 | Golden potassium fertilizer and its producing method |
| CN102093136A (en) * | 2010-12-27 | 2011-06-15 | 湖北富邦科技股份有限公司 | Inner fertilizer additive adopting edible bright cyanine and preparation method thereof |
| CN102173937A (en) * | 2011-01-27 | 2011-09-07 | 中盐安徽红四方股份有限公司 | Composite nitrogen fertilizer and production method thereof |
| CN102925135A (en) * | 2012-10-18 | 2013-02-13 | 金红叶纸业集团有限公司 | Color-change powder and color-change liquid applying same |
| CN103467159A (en) * | 2013-09-18 | 2013-12-25 | 张伟良 | Chelated compound trace element fertilizer and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104725101A (en) * | 2013-12-20 | 2015-06-24 | 刘玲 | Potted flower granular fertilizer and preparation method thereof |
-
2015
- 2015-07-03 CN CN201510381407.8A patent/CN104926536B/en active Active
- 2015-07-03 CN CN201710652107.8A patent/CN107488061A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1690019A (en) * | 2004-04-28 | 2005-11-02 | 黄云祥 | Golden potassium fertilizer and its producing method |
| CN102093136A (en) * | 2010-12-27 | 2011-06-15 | 湖北富邦科技股份有限公司 | Inner fertilizer additive adopting edible bright cyanine and preparation method thereof |
| CN102173937A (en) * | 2011-01-27 | 2011-09-07 | 中盐安徽红四方股份有限公司 | Composite nitrogen fertilizer and production method thereof |
| CN102925135A (en) * | 2012-10-18 | 2013-02-13 | 金红叶纸业集团有限公司 | Color-change powder and color-change liquid applying same |
| CN103467159A (en) * | 2013-09-18 | 2013-12-25 | 张伟良 | Chelated compound trace element fertilizer and preparation method thereof |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105777389A (en) * | 2016-04-25 | 2016-07-20 | 纪新强 | Water-soluble color-changing fertilizer containing amino acids and trace elements and dilution control method of fertilizer |
| CN105777392A (en) * | 2016-04-25 | 2016-07-20 | 纪新强 | Macroelement-microelement type water-soluble color-changing fertilizer and dilution control method of same |
| CN105801273A (en) * | 2016-04-25 | 2016-07-27 | 纪新强 | Trace element liquid water soluble color change fertilizer and dilution control method thereof |
| CN105884532A (en) * | 2016-04-25 | 2016-08-24 | 纪新强 | Macro and trace elements type liquid water-soluble discoloring fertilizer and dilution control method thereof |
| CN105884531A (en) * | 2016-04-25 | 2016-08-24 | 纪新强 | Trace element water-soluble color-changing fertilizer and dilution control method thereof |
| CN105906429A (en) * | 2016-04-25 | 2016-08-31 | 纪新强 | Liquid water-soluble color-changing fertilizer containing amino acid and trace element and dilution control method of fertilizer |
| CN106380298A (en) * | 2016-08-30 | 2017-02-08 | 安徽辉隆集团五禾生态肥业有限公司 | Water soluble fertilizer with color self-change anti-counterfeiting function |
| CN106380298B (en) * | 2016-08-30 | 2021-09-03 | 安徽辉隆集团五禾生态肥业有限公司 | Water-soluble fertilizer with self-color-changing anti-counterfeiting function |
| CN110105107A (en) * | 2018-03-27 | 2019-08-09 | 湖北格林凯尔农业科技有限公司 | A kind of heartsease water-soluble fertilizer and application |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104926536B (en) | 2018-01-12 |
| CN107488061A (en) | 2017-12-19 |
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Inventor after: Ma Yonglin Inventor before: Liu Bin |
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Effective date of registration: 20170801 Address after: 510665 Guangdong city of Guangzhou province Tianhe District Software Park Building No. 59 Middle East block, Grand Building Room 501 Applicant after: Ma Yonglin Address before: 264000, No. 17-6, West Ding Feng West Road, Zhifu District, Shandong, Yantai 211 Applicant before: Liu Bin |
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Effective date of registration: 20171213 Address after: 430040 Hubei province Dongxihu District of Wuhan City Road 1 road Wanan International seven Innovation Building 16 floor Applicant after: Hubei Green Kell agricultural science and Technology Co., Ltd. Address before: 510665 Guangdong city of Guangzhou province Tianhe District Software Park Building No. 59 Middle East block, Grand Building Room 501 Applicant before: Ma Yonglin |
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