CN104910750A - Anticorrosive amino resin paint and preparation method thereof - Google Patents
Anticorrosive amino resin paint and preparation method thereof Download PDFInfo
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- CN104910750A CN104910750A CN201510410946.XA CN201510410946A CN104910750A CN 104910750 A CN104910750 A CN 104910750A CN 201510410946 A CN201510410946 A CN 201510410946A CN 104910750 A CN104910750 A CN 104910750A
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- amino resin
- anticorrosive
- cyclohexylthiophthalimide
- aminoresin
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Abstract
The invention discloses anticorrosive amino resin paint and a preparation method thereof. The anticorrosive amino resin paint is prepared from the following raw materials in parts by weight: 100 to 120 parts of amino resin, 45 to 53 parts of phenolic resin, 10 to 15 parts of aluminium triphosphate, 10 to 15 parts of zinc phosphate, 10 to 15 parts of zinc oxide, 10 to 15 parts of sodium dehydroacetate, 1 to 5 parts of isopropanol, 1 to 5 parts of ethylate trimethylolpropane triacrylate, 1 to 5 parts of tetrabutylphosphonium chloride, 1 to 5 parts of naphthenic dicarboxylic acid monoester, 1 to 5 parts of styrene, 5 to 10 parts of N-cyclohexylthiophthalimide, 5 to 10 parts of glycidyl acrylate, 5 to 10 parts of butyl acetate, 5 to 10 parts of trimellitic anhydride, 5 to 10 parts of maleic anhydride, 5 to 10 parts of sodium hexametaphosphate, 3 to 8 parts of m-xylylenediamine, 3 to 8 parts of activated calcium carbonate, 3 to 8 parts of cresol, 3 to 8 parts of bi-tetradecanol polycarbonate, 1 to 3 parts of methyl acrylate, 1 to 3 parts of 2-malic acid, 1 to 3 parts of wollastonite in powder, and 1 to 3 parts of carbon black. The preparation method is simple; the cost is small; a paint film is high in attaching performance, resistant to corrosion, resistant to ageing, and long in service life.
Description
Technical field
The present invention relates to paint field, specifically a kind of anticorrosive amino resin coatings and preparation method thereof.
Background technology
Paint and be seen everywhere in schedule life; it mainly plays protection and decoration, and according to different environments for use, the kind of paint is also varied; traditional paint ubiquity smell weighs, easily come off, perishable; the problems such as inadequate environmental protection, can not meet the service requirements of human consumer to paint, therefore; need the formula improving original paint; increase practicality and the weather resistance of paint, reduce its harm to environment and human body, and various environment for use condition can be adapted to.
Summary of the invention
The object of the present invention is to provide a kind of rust resistance and corrosion resistance, gloss is full, fast in colour, anticorrosive amino resin coatings of weatherable and preparation method thereof, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the invention provides following technical scheme:
A kind of anticorrosive amino resin coatings, comprise according to the raw material of weight part: aminoresin 100-120 part, resol 45-53 part, aluminium triphosphate 10-15 part, zinc phosphate 10-15 part, zinc oxide 10-15 part, sodium dehydroacetate 10-15 part, Virahol 1-5 part, ethoxyquin Viscoat 295 1-5 part, tetrabutylphosphonium chloride 1-5 part, Cycloalkane dicarboxylic acid monoesters 1-5 part, vinylbenzene 1-5 part, N-cyclohexylthiophthalimide 5-10 part, glycidyl acrylate 5-10 part, butylacetate 5-10 part, trimellitic acid 1,2-anhydride 5-10 part, MALEIC ANHYDRIDE 5-10 part, Sodium hexametaphosphate 99 5-10 part, m-xylene diamine 3-8 part, activated Calcium carbonate 3-8 part, M-and P-cresols 3-8 part, two ten four carbon alcohols ester 3-8 parts, methyl acrylate 1-3 part, 2-hydroxy-butanedioic acid 1-3 part, wollastonite powder 1-3 part, carbon black 1-3 part.
As the further scheme of the present invention: described anticorrosive amino resin coatings, comprise according to the raw material of weight part: aminoresin 105-115 part, resol 48-52 part, aluminium triphosphate 12-14 part, zinc phosphate 12-14 part, zinc oxide 12-14 part, sodium dehydroacetate 12-14 part, Virahol 2-4 part, ethoxyquin Viscoat 295 2-4 part, tetrabutylphosphonium chloride 2-4 part, Cycloalkane dicarboxylic acid monoesters 2-4 part, vinylbenzene 2-4 part, N-cyclohexylthiophthalimide 7-9 part, glycidyl acrylate 7-9 part, butylacetate 7-9 part, trimellitic acid 1,2-anhydride 7-9 part, MALEIC ANHYDRIDE 7-9 part, Sodium hexametaphosphate 99 7-9 part, m-xylene diamine 5-6 part, activated Calcium carbonate 5-6 part, M-and P-cresols 5-6 part, two ten four carbon alcohols ester 5-6 parts, methyl acrylate 1-2 part, 2-hydroxy-butanedioic acid 1-2 part, wollastonite powder 1-2 part, carbon black 1-2 part.
As the further scheme of the present invention: described anticorrosive amino resin coatings, comprise according to the raw material of weight part: 110 parts, aminoresin, 50 parts, resol, aluminium triphosphate 13 parts, zinc phosphate 13 parts, 13 parts, zinc oxide, sodium dehydroacetate 13 parts, Virahol 3 parts, ethoxyquin Viscoat 295 3 parts, tetrabutylphosphonium chloride 3 parts, Cycloalkane dicarboxylic acid monoesters 3 parts, vinylbenzene 3 parts, N-cyclohexylthiophthalimide 8 parts, glycidyl acrylate 8 parts, butylacetate 8 parts, trimellitic acid 1,2-anhydride 8 parts, MALEIC ANHYDRIDE 8 parts, Sodium hexametaphosphate 99 8 parts, m-xylene diamine 5 parts, activated Calcium carbonate 5 parts, M-and P-cresols 5 parts, two ten four carbon alcohols ester 5 parts, methyl acrylate 2 parts, 2-hydroxy-butanedioic acid 2 parts, wollastonite powder 2 parts, carbon black 2 parts.
The preparation method of described anticorrosive amino resin coatings, comprises the steps:
(1) by sodium dehydroacetate, Virahol, ethoxyquin Viscoat 295, tetrabutylphosphonium chloride, the mixing of Cycloalkane dicarboxylic acid monoesters, join in the mixing solutions of aminoresin, resol, vinylbenzene, m-xylene diamine, be heated to 115-125 DEG C, reaction 3-6 hour;
(2) material of step (1) is cooled to 65-75 DEG C, adds aluminium triphosphate, zinc phosphate, zinc oxide, N-cyclohexylthiophthalimide, glycidyl acrylate, stirring reaction 3-6 hour;
(3) material of step (2) is cooled to 45-55 DEG C, adds other leftover materials, after stirring reaction 40-60 minute, be cooled to room temperature, grind to form 20-60 μm of slurry, to obtain final product.
Compared with prior art, the invention has the beneficial effects as follows:
Making method of the present invention is simple, and cost is low, and paint film adhesion is strong, difficult drop-off, safety and environmental protection, rust resistance and corrosion resistance, and gloss is full, fast in colour, weatherable, long service life, resistance to water resistance tide, safe and reliable, can be used for article decoration protection in multiple environment and use.
Embodiment
Below in conjunction with the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of anticorrosive amino resin coatings, comprise according to the raw material of weight part: 100 parts, aminoresin, 45 parts, resol, aluminium triphosphate 10 parts, zinc phosphate 10 parts, 10 parts, zinc oxide, sodium dehydroacetate 10 parts, Virahol 1 part, ethoxyquin Viscoat 295 1 part, tetrabutylphosphonium chloride 1 part, Cycloalkane dicarboxylic acid monoesters 1 part, vinylbenzene 1 part, N-cyclohexylthiophthalimide 5 parts, glycidyl acrylate 5 parts, butylacetate 5 parts, trimellitic acid 1,2-anhydride 5 parts, MALEIC ANHYDRIDE 5 parts, Sodium hexametaphosphate 99 5 parts, m-xylene diamine 3 parts, activated Calcium carbonate 3 parts, M-and P-cresols 3 parts, two ten four carbon alcohols ester 3 parts, methyl acrylate 1 part, 2-hydroxy-butanedioic acid 1 part, wollastonite powder 1 part, carbon black 1 part.
Preparation process, comprise the steps: that (1) is by sodium dehydroacetate, Virahol, ethoxyquin Viscoat 295, tetrabutylphosphonium chloride, the mixing of Cycloalkane dicarboxylic acid monoesters, join in the mixing solutions of aminoresin, resol, vinylbenzene, m-xylene diamine, be heated to 115 DEG C, react 6 hours.(2) material of step (1) is cooled to 65 DEG C, adds aluminium triphosphate, zinc phosphate, zinc oxide, N-cyclohexylthiophthalimide, glycidyl acrylate, stirring reaction 6 hours.(3) material of step (2) is cooled to 45 DEG C, adds other leftover materials, stirring reaction, after 60 minutes, is cooled to room temperature, grinds to form 20-60 μm of slurry, to obtain final product.
Embodiment 2
In the embodiment of the present invention, a kind of anticorrosive amino resin coatings, comprise according to the raw material of weight part: 120 parts, aminoresin, 53 parts, resol, aluminium triphosphate 15 parts, zinc phosphate 15 parts, 15 parts, zinc oxide, sodium dehydroacetate 15 parts, Virahol 5 parts, ethoxyquin Viscoat 295 5 parts, tetrabutylphosphonium chloride 5 parts, Cycloalkane dicarboxylic acid monoesters 5 parts, vinylbenzene 5 parts, N-cyclohexylthiophthalimide 10 parts, glycidyl acrylate 10 parts, butylacetate 10 parts, trimellitic acid 1,2-anhydride 10 parts, MALEIC ANHYDRIDE 10 parts, Sodium hexametaphosphate 99 10 parts, m-xylene diamine 8 parts, activated Calcium carbonate 8 parts, M-and P-cresols 8 parts, two ten four carbon alcohols ester 8 parts, methyl acrylate 3 parts, 2-hydroxy-butanedioic acid 3 parts, wollastonite powder 3 parts, carbon black 3 parts.
Preparation process, comprise the steps: that (1) is by sodium dehydroacetate, Virahol, ethoxyquin Viscoat 295, tetrabutylphosphonium chloride, the mixing of Cycloalkane dicarboxylic acid monoesters, join in the mixing solutions of aminoresin, resol, vinylbenzene, m-xylene diamine, be heated to 125 DEG C, react 3 hours.(2) material of step (1) is cooled to 75 DEG C, adds aluminium triphosphate, zinc phosphate, zinc oxide, N-cyclohexylthiophthalimide, glycidyl acrylate, stirring reaction 3 hours.(3) material of step (2) is cooled to 55 DEG C, adds other leftover materials, stirring reaction, after 40 minutes, is cooled to room temperature, grinds to form 20-60 μm of slurry, to obtain final product.
Embodiment 3
In the embodiment of the present invention, a kind of anticorrosive amino resin coatings, comprise according to the raw material of weight part: 105 parts, aminoresin, 48 parts, resol, aluminium triphosphate 12 parts, zinc phosphate 12 parts, 12 parts, zinc oxide, sodium dehydroacetate 12 parts, Virahol 2 parts, ethoxyquin Viscoat 295 2 parts, tetrabutylphosphonium chloride 2 parts, Cycloalkane dicarboxylic acid monoesters 2 parts, vinylbenzene 2 parts, N-cyclohexylthiophthalimide 7 parts, glycidyl acrylate 7 parts, butylacetate 7 parts, trimellitic acid 1,2-anhydride 7 parts, MALEIC ANHYDRIDE 7 parts, Sodium hexametaphosphate 99 7 parts, m-xylene diamine 5 parts, activated Calcium carbonate 5 parts, M-and P-cresols 5 parts, two ten four carbon alcohols ester 5 parts, methyl acrylate 1 part, 2-hydroxy-butanedioic acid 1 part, wollastonite powder 1 part, carbon black 1 part.
Preparation process, comprise the steps: that (1) is by sodium dehydroacetate, Virahol, ethoxyquin Viscoat 295, tetrabutylphosphonium chloride, the mixing of Cycloalkane dicarboxylic acid monoesters, join in the mixing solutions of aminoresin, resol, vinylbenzene, m-xylene diamine, be heated to 118 DEG C, react 4 hours.(2) material of step (1) is cooled to 68 DEG C, adds aluminium triphosphate, zinc phosphate, zinc oxide, N-cyclohexylthiophthalimide, glycidyl acrylate, stirring reaction 4 hours.(3) material of step (2) is cooled to 45-55 DEG C, adds other leftover materials, stirring reaction, after 45 minutes, is cooled to room temperature, grinds to form 20-60 μm of slurry, to obtain final product.
Embodiment 4
In the embodiment of the present invention, a kind of anticorrosive amino resin coatings, comprise according to the raw material of weight part: 115 parts, aminoresin, 52 parts, resol, aluminium triphosphate 14 parts, zinc phosphate 14 parts, 14 parts, zinc oxide, sodium dehydroacetate 14 parts, Virahol 4 parts, ethoxyquin Viscoat 295 4 parts, tetrabutylphosphonium chloride 4 parts, Cycloalkane dicarboxylic acid monoesters 4 parts, vinylbenzene 4 parts, N-cyclohexylthiophthalimide 9 parts, glycidyl acrylate 9 parts, butylacetate 9 parts, trimellitic acid 1,2-anhydride 9 parts, MALEIC ANHYDRIDE 9 parts, Sodium hexametaphosphate 99 9 parts, m-xylene diamine 6 parts, activated Calcium carbonate 6 parts, M-and P-cresols 6 parts, two ten four carbon alcohols ester 6 parts, methyl acrylate 2 parts, 2-hydroxy-butanedioic acid 2 parts, wollastonite powder 2 parts, carbon black 2 parts.
Preparation process, comprise the steps: that (1) is by sodium dehydroacetate, Virahol, ethoxyquin Viscoat 295, tetrabutylphosphonium chloride, the mixing of Cycloalkane dicarboxylic acid monoesters, join in the mixing solutions of aminoresin, resol, vinylbenzene, m-xylene diamine, be heated to 122 DEG C, react 5 hours.(2) material of step (1) is cooled to 72 DEG C, adds aluminium triphosphate, zinc phosphate, zinc oxide, N-cyclohexylthiophthalimide, glycidyl acrylate, stirring reaction 5 hours.(3) material of step (2) is cooled to 52 DEG C, adds other leftover materials, stirring reaction, after 55 minutes, is cooled to room temperature, grinds to form 20-60 μm of slurry, to obtain final product.
Embodiment 5
In the embodiment of the present invention, a kind of anticorrosive amino resin coatings, comprise according to the raw material of weight part: 110 parts, aminoresin, 50 parts, resol, aluminium triphosphate 13 parts, zinc phosphate 13 parts, 13 parts, zinc oxide, sodium dehydroacetate 13 parts, Virahol 3 parts, ethoxyquin Viscoat 295 3 parts, tetrabutylphosphonium chloride 3 parts, Cycloalkane dicarboxylic acid monoesters 3 parts, vinylbenzene 3 parts, N-cyclohexylthiophthalimide 8 parts, glycidyl acrylate 8 parts, butylacetate 8 parts, trimellitic acid 1,2-anhydride 8 parts, MALEIC ANHYDRIDE 8 parts, Sodium hexametaphosphate 99 8 parts, m-xylene diamine 5 parts, activated Calcium carbonate 5 parts, M-and P-cresols 5 parts, two ten four carbon alcohols ester 5 parts, methyl acrylate 2 parts, 2-hydroxy-butanedioic acid 2 parts, wollastonite powder 2 parts, carbon black 2 parts.
Preparation process, comprise the steps: that (1) is by sodium dehydroacetate, Virahol, ethoxyquin Viscoat 295, tetrabutylphosphonium chloride, the mixing of Cycloalkane dicarboxylic acid monoesters, join in the mixing solutions of aminoresin, resol, vinylbenzene, m-xylene diamine, be heated to 120 DEG C, react 4.5 hours.(2) material of step (1) is cooled to 70 DEG C, adds aluminium triphosphate, zinc phosphate, zinc oxide, N-cyclohexylthiophthalimide, glycidyl acrylate, stirring reaction 4.5 hours.(3) material of step (2) is cooled to 50 DEG C, adds other leftover materials, stirring reaction, after 50 minutes, is cooled to room temperature, grinds to form 20-60 μm of slurry, to obtain final product.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this specification sheets is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of specification sheets is only for clarity sake, those skilled in the art should by specification sheets integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (4)
1. an anticorrosive amino resin coatings, it is characterized in that, comprise according to the raw material of weight part: aminoresin 100-120 part, resol 45-53 part, aluminium triphosphate 10-15 part, zinc phosphate 10-15 part, zinc oxide 10-15 part, sodium dehydroacetate 10-15 part, Virahol 1-5 part, ethoxyquin Viscoat 295 1-5 part, tetrabutylphosphonium chloride 1-5 part, Cycloalkane dicarboxylic acid monoesters 1-5 part, vinylbenzene 1-5 part, N-cyclohexylthiophthalimide 5-10 part, glycidyl acrylate 5-10 part, butylacetate 5-10 part, trimellitic acid 1,2-anhydride 5-10 part, MALEIC ANHYDRIDE 5-10 part, Sodium hexametaphosphate 99 5-10 part, m-xylene diamine 3-8 part, activated Calcium carbonate 3-8 part, M-and P-cresols 3-8 part, two ten four carbon alcohols ester 3-8 parts, methyl acrylate 1-3 part, 2-hydroxy-butanedioic acid 1-3 part, wollastonite powder 1-3 part, carbon black 1-3 part.
2. anticorrosive amino resin coatings according to claim 1, it is characterized in that, comprise according to the raw material of weight part: aminoresin 105-115 part, resol 48-52 part, aluminium triphosphate 12-14 part, zinc phosphate 12-14 part, zinc oxide 12-14 part, sodium dehydroacetate 12-14 part, Virahol 2-4 part, ethoxyquin Viscoat 295 2-4 part, tetrabutylphosphonium chloride 2-4 part, Cycloalkane dicarboxylic acid monoesters 2-4 part, vinylbenzene 2-4 part, N-cyclohexylthiophthalimide 7-9 part, glycidyl acrylate 7-9 part, butylacetate 7-9 part, trimellitic acid 1,2-anhydride 7-9 part, MALEIC ANHYDRIDE 7-9 part, Sodium hexametaphosphate 99 7-9 part, m-xylene diamine 5-6 part, activated Calcium carbonate 5-6 part, M-and P-cresols 5-6 part, two ten four carbon alcohols ester 5-6 parts, methyl acrylate 1-2 part, 2-hydroxy-butanedioic acid 1-2 part, wollastonite powder 1-2 part, carbon black 1-2 part.
3. anticorrosive amino resin coatings according to claim 2, it is characterized in that, comprise according to the raw material of weight part: 110 parts, aminoresin, 50 parts, resol, aluminium triphosphate 13 parts, zinc phosphate 13 parts, 13 parts, zinc oxide, sodium dehydroacetate 13 parts, Virahol 3 parts, ethoxyquin Viscoat 295 3 parts, tetrabutylphosphonium chloride 3 parts, Cycloalkane dicarboxylic acid monoesters 3 parts, vinylbenzene 3 parts, N-cyclohexylthiophthalimide 8 parts, glycidyl acrylate 8 parts, butylacetate 8 parts, trimellitic acid 1,2-anhydride 8 parts, MALEIC ANHYDRIDE 8 parts, Sodium hexametaphosphate 99 8 parts, m-xylene diamine 5 parts, activated Calcium carbonate 5 parts, M-and P-cresols 5 parts, two ten four carbon alcohols ester 5 parts, methyl acrylate 2 parts, 2-hydroxy-butanedioic acid 2 parts, wollastonite powder 2 parts, carbon black 2 parts.
4. a preparation method for the anticorrosive amino resin coatings as described in as arbitrary in claim 1-3, is characterized in that, comprise the steps:
(1) by sodium dehydroacetate, Virahol, ethoxyquin Viscoat 295, tetrabutylphosphonium chloride, the mixing of Cycloalkane dicarboxylic acid monoesters, join in the mixing solutions of aminoresin, resol, vinylbenzene, m-xylene diamine, be heated to 115-125 DEG C, reaction 3-6 hour;
(2) material of step (1) is cooled to 65-75 DEG C, adds aluminium triphosphate, zinc phosphate, zinc oxide, N-cyclohexylthiophthalimide, glycidyl acrylate, stirring reaction 3-6 hour;
(3) material of step (2) is cooled to 45-55 DEG C, adds other leftover materials, after stirring reaction 40-60 minute, be cooled to room temperature, grind to form 20-60 μm of slurry, to obtain final product.
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| CN201510410946.XA CN104910750A (en) | 2015-07-14 | 2015-07-14 | Anticorrosive amino resin paint and preparation method thereof |
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| CN201510410946.XA CN104910750A (en) | 2015-07-14 | 2015-07-14 | Anticorrosive amino resin paint and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103709889A (en) * | 2013-12-07 | 2014-04-09 | 铜陵新九鼎铜文化产业有限公司 | Toughened amino resin paint for copper sculptures |
| CN103725054A (en) * | 2013-11-25 | 2014-04-16 | 铜陵天河特种电磁线有限公司 | Amino resin wire enamel and preparation method thereof |
| CN103788810A (en) * | 2014-01-26 | 2014-05-14 | 南通苏通分离工程科技有限公司 | High temperature resistant anticorrosive paint and preparation process thereof |
| CN103881443A (en) * | 2014-02-25 | 2014-06-25 | 蚌埠凯盛工程技术有限公司 | Environment-friendly antiseptic and anti-yellowing amino resin coating |
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2015
- 2015-07-14 CN CN201510410946.XA patent/CN104910750A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103725054A (en) * | 2013-11-25 | 2014-04-16 | 铜陵天河特种电磁线有限公司 | Amino resin wire enamel and preparation method thereof |
| CN103709889A (en) * | 2013-12-07 | 2014-04-09 | 铜陵新九鼎铜文化产业有限公司 | Toughened amino resin paint for copper sculptures |
| CN103788810A (en) * | 2014-01-26 | 2014-05-14 | 南通苏通分离工程科技有限公司 | High temperature resistant anticorrosive paint and preparation process thereof |
| CN103881443A (en) * | 2014-02-25 | 2014-06-25 | 蚌埠凯盛工程技术有限公司 | Environment-friendly antiseptic and anti-yellowing amino resin coating |
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Application publication date: 20150916 |